B T NHN Semen Platycladi orientalis L ht trong "nn ci" gi (cn gi l "qu") c phi hay sy kh ca cy Trc b ( Platycladus orientalis (L.

) Franco), h Hong n (Cupressaceae). M t Ht hnh trng di hoc bu dc hp, di 4 -7 mm, ng knh 1,5 - 3 mm. Mt ngoi mu trng vng nht hoc mu vng nu nht, c ph mt v la dng mng, nh hi nhn, c mt im nh mu nu thm, y trn t. Cht mm, nhiu du. Mi thm nh, v nht. m Khng qu 7% (Ph lc 12.13). Ch s acid Khng qu 40,0 (Ph lc 7.2). Tn thnh bt th 50 g mu th, cho vo bnh Soxhlet, thm 100 ml hexan (TT), chit hi lu trong 2 gi, ngui, lc qua phu lc thy tinh xp s 3, ct thu hi dung mi di p lc gim, ly mt phn du thu c xc nh ch s acid theo Ph lc 7.2. Phn cn li xc nh ch s carbonyl v ch s peroxyd. Ch s carbonyl Khng qu 30,0. Xc nh theo phng php sau: Cn chnh xc 0,02 g du vo bnh nh mc 25,0 ml, thm benzen (TT) ho tan v pha long n vch vi cng dung mi. Ly chnh xc 5,0 ml dung dch ny vo bnh nn 25 ml c nt mi , thm 3 ml dung dch acid tricloroacetic 4,3% trong benzen (TT) v 5 ml dung dch 2,4dinitrophenylhydrazin 0,05% trong benzen (TT), trn u, un 30 pht trong cch thu 60 oC, ngui, thm t t dc theo thnh ng nghim 10 ml dung dch kali hydroxyd 4% trong ethanol (TT), y nt bnh nn, lc k trong 1 pht, yn 10 pht. Tin hnh o hp th ca dung dch thu c (Ph lc 4.1) ti bc sng 453 nm, tnh ch s carbonyl theo cng thc sau: A Ch s carbonyl = ----------------------- x 1000 854 x G x V2/V1 Trong : A l hp thu ca cht kim tra G l khi lng ca mu th V1 l tng th tch pha long ca dung dch cht th V2 l th tch dung dch cht th dng pha dung dch o hp th 854 l gi tr trung bnh ca h s hp th phn t ca aldehyd. Ch s peroxyd Khng qu 0,26. Xc nh theo phng php sau: Ly 3 g du vo mt bnh nn 250 ml, thm 30 ml hn hp cloroform (TT) : acid acetic bng (TT) (1 : 1), lc cho tan hon ton. Thm chnh xc 1 ml dung dch kali iodid bo ho (TT) mi pha, y kn, lc nh trong 30 giy, yn ch ti 3 pht, thm 100 ml nc. Chun bng dung dch natri thiosulfat 0,005 M (C) n khi c mu vng nht, thm 1 ml h tinh bt (CT), tip tc chun n mt mu xanh. Song song tin hnh 1 mu trng. Tnh ch s peroxyd theo cng thc sau: (A B) x 0,005 x 0,1269 Ch s peroxyd = ------------------------------- x 100 G

Trong : A l th tch dung dch natri thiosulfat 0,005 M (C) dng vi mu th (ml) B l th tch dung dch natri thiosulfat 0,005 M (C) dng vi mu trng (ml) G l khi lng cht kim tra (g). 0,1296 l lng iod (g) tng ng vi 1 ml dung dch natri thiosulfat 1 M. Tp cht Khng qu 1% (Ph lc 12.11). Ch bin Thu hoch vo ma thu v ma ng. Khi ht chn, thu hi "qu", ly ht phi kh. Bo ch B t nhn: Loi b tp cht v v "qu" cn st li. B t sng: Ly B t nhn sch, gi nt, gi vo giy thm, sy cho hi kh, p b ht du, gi nh. Bo qun ni kh, mt, trnh nng v mc, mt. Tnh v, quy kinh Cam, bnh. Vo cc kinh tm, thn, i trng. Cng nng, ch tr Dng tm, an thn, ch hn, nhun trng. Ch tr: H phin mt ng, hi hp nh trng ngc, m h, ra m hi trm, to bn. Cch dng, liu lng Ngy ung 3 - 12 g.