Engineering Management Support, Inc.: West Lake OU-1

ENGINEERING MANAGEMENT SUPPORT, INC.
West Lake OU-1
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-07098-0R
August 9, 2013
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY
OAK RIDGE, TN
illti! ill 1
TABLE OF CONTENTS
SECTION
DESCRIPTION
PAGE
Chain of Custody & pH Check Sheet
0003
II
Sample Acknowledgement
0012
III
Case Narrative
0015
IV
Analytical Results Summary
0019
Analytical Standards
0026
VI
Quality Control Sample Results Summary
0050
VII
Laboratory Technician's Notes
0061
VIII
Analytical Data (Isotopic Uranium)
0095
IX
Analytical Data (Isotopic Thorium)
0249
Analytical Data (Radium-226)
0368
XI
Analytical Data (Radium-228)
0482
XII
Barium-133 Analytical Tracer Data
0498
Last Page Number
0578
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STANDARD OPERATING PROCEDURE
MP-001, Rev. 12
Effective: 10131112
SERVICES
Sample Receiving
Page 14 of14
Eberline Services - Oak Ridge Laboratory
LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
Eberline Services Work Order
#_~1~3~--0_7~0~9_..8~-----
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Initials
Date
1 /H..o/1,3
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Checklist Items
Data Compilation
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First Technical Data Review

Second Technical Data Review
.,4
Data Entry/Electronic Deliverable
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Case Narrative
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Samplel 8-nalyzed within Holding Time
Yes? 1 Y
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Client in Possession of Data
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Invoiced by Laboratory
Date/Initials
Technical/Clerical Corrections, Signatures Needed, Problems, Etc
Date package approved by: :

Laboratory
CopyNo. _ _ __
Date
Radiochemistry Services
CPJ2A
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
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Chain of Custody Record

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Chain of
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SERVICES
Oak Ridge Laboratory
Work Order#
13-07098
Lab Deadline
8/6/2013
UUISO - Level 4
Analysis
Water
Sample Matrix
Fraction
ll Detector
HP 210 / 270 I
Activity ]
Location
04
36
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Sample
Comments
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45
08
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Printed: 7/1712013 8:11 AM
m--mms
Internal
El?ER~R~C~
Chain of
Custody
13-07098
Lab Deadline
See Comments
UUISO - Level 4
Analysis
WA
Sample Matrix
Comments
Re-Analysis: 2Fxns 04,06,08,09,11,13,15,17 & 19 are TOTAL
Work Order#
Sample
Fraction
HP 2101270
Detector Activity
04
05
06
07
36
36
45
45
43
41
41
44
44
48
46
43
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39
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Original Lab Deadline: 08/13/13

Rerun Lab Deadline: 08/13/13MUST USE Fxn 11 as DUP
09
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12
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Printed: 7126/2013 10:10 AM

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Internal
EBERLINE
8/6/2013
Lab Deadline
Chain of
Custody
SERVICES
13-07098
Work Order
ThlSO Level 4
Analysis
Water
Sample Matrix
Sample
Comments
Fraction
HP 210
I 270
36
36
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45
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43
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45
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05
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Printed: 1111t2013 a:11AM
:fi)flf!r7
.
EBERLINE
SERVICES
Internal
Work Order#
Chain of
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Lab Deadline
11
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Storage
Location
HP 210 / 270
Detector Activity
04
-------
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Sample Matrix
Sample
Fraction
Comments
Ra226 - Level 4
Analysis
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Printed: 7/17/2013 8:11 AM
:tJtJ:-f!!S
Internal
EBERLINE
Chain of
Custody
SERVICES
13-07098
Work Order#
--------
8/6/2013
Lab Deadline
Ra228 - Level 4
Analysis
Water
Sample Matrix
Sample
Fraction
Comments
HP 210 I 270
Storage
Detector Activity
Location
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36
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Printed: 7/17/2013 8:11 AM
mmms
Page 1of2
Printed: 7/16/2013 2:09 PM
Internal Work Order
13-07098
Sample Receiving Report

(Volumes, pH, & CPM)
Received By
KCOULSTON
FR
ClientID
Matrix
Storage
Tl.2
Tl.2
WA
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MP-001. Rev 5
Effective: 11 /22/02
Page 2 of 2
Printed: 7/16/2013 2:09 PM

~EB.ERLINE
~
FRI
Received By
(Volumes, pH, & CPM)
SERVICES
KCOULSTON
ClientID
20 I PZ-112-AS DIS
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Received by:
~ ~Jaf"'--
Date:
7/(lb({'j
Matrix
Storaoe
<2
<2
WA
Tl.2
nH Oriel'.\'
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4.0000
0.00
40
45
.nH Final - - -.Volum&-flt .. "CPM
45
40
MP-001, Rev 5
Effective: 11/22/02
SECTION II
SAMPLE ACKNOWLEDGEMENT
Client
Na~e
.-~ontractfPO
PrlJ~~-l)'_Ee
West Lake OU-1

Internal to
Client ID
07/15/2013
.~_rT_l__ple Dis~_
Lab Deadline
-----
; West Lake OU-1 i
Sample Date
I Matrix
Storage
01
LCS
07/16/13
WA
Tl.2
02
BLANK
07/16/13
WA
Tl.2
03
DUP
04
07/16/13
WA
Tl.2
PZ-111-SD TOT
07/09/1310:42
WA
Tl.2
05
PZ-111-SD DIS
07/09/13 10:42
WA
Tl.2
06
S-5 TOT
07/09/1310:50
WA
Tl.2
07
S-5 DIS
07/09/1310:50
WA
Tl.2
08
FB@ PZ-110-SS TOT
07/09/1311:40
WA
Tl.2
09
PZ-110-SS TOT
07/09/1312:13
WA
Tl.2
10
PZ-110-SS DIS
07/09/1312:13
WA
Tl.2
11
1-4 TOT
07/09/1312:25
WA
Tl.2
12
I-4 DIS
07/09/1312:25
WA
Tl.2
13
PZ-100-SS TOT
07/09/1313:36
WA
T1.2
14
PZ-100-SS DIS
07/09/1313:36
WA
Tl.2
15
D-3 TOT
07/09/1313:42
WA
Tl.2
16
D-3 DIS
07/09/1313:42
WA
T1.2
17
PZ-100-SD TOT
07109/1314:32
WA
Tl.2
18
PZ-100-SD DIS
07/09/1314:32
WA
Tl.2
19
PZ-112-AS TOT
07/09/1314:46
WA
Tl.2
20
PZ-112-AS DIS
07/09/1314:46
WA
Tl.2
Totals Per Analysis (non QA samples)
.'
~
l...J
N E:::
SERVICES
Sample Log In Report
l':
00
~
x
x
x
x
~lTo"'
28
13-07098
mm
Internal Deadline
08/12/2013
08/13/2013
~ i"'"' "'5=>
i"
x x
x x x
x
x
x
x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
x x x x
11
11

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: (865) 481-0683
(865) 483-4621
Fax:
_~~~l_l-~~-~~:!"~narou~~.l?_a_:~--
- ----
08/06/2013
Invoice
E: 13 E::: R
-------
Client WO
:::
Name
Date Received
---------.
Environmental
Engineering Management Support, Inc. 1: West Lake OU-1

_P~~j_ect
--
t7
11
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
4
o I o
Report Data
Paul V. Rosasco, P.E
Er;;iineer1ng Management Suppor1, Inc
7220 W~s\ Jellerson Avenue.
7220 West Jefferson Ave. Sutte 406
Su~e 400
Lakewood, CO 80235
303-640-3426
Contact
'"
Lyn Fitzgerald
Voice
1303-601-4255
Paul V. Rosasco, P.E.
Englrieerirm Management Support, Inc_
Voice
Lakewood, CO 80235
Voic:e
303-940-3426
'"'
...
~,
l>I
Printed: 7/17/2013 8:12AM
STANDARD OPERATING PROCEDURE
MP001, Rev.12
Effective: 10131112
Sample Receiving
Page 13of14
Eberline Services - Oak Ridge Laboratory

SAMPLE RECEIPT CHECKLIST
MP-001-2
WORK ORDER
#_1_3_-_0_7_0_9_8_
SAMPLE MATRIX/MATRICES:
(CIRCLE ONE OR BOTH)
~QUEoU"S)
NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR N/A)

WERE SAMPLES
Received in good condition?
CD
If aqueous, properly preserved
Present on outside of package?
Unbroken on outside of package?
Present on samples?
(Y)
Unbroken on samples?
5)
Was chain of custody present upon sample receipt?
N/A
WERE CHAIN OF CUSTODY SEALS
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS:~-------------------------~
SIGNATURE:
Copy No. _ _ __
4;'n1W#. CruQ.dc,.._.
DATE:
1 It (g In
Radiochemistry Services
SECTION III
CASE NARRATIVE
EBERLINE ANALYTICAL CORPORATION

601 SCARBORO ROAD
OAK RIDGE, TENNESSEE 37830
PHONE (865) 481-0683
FAX (865) 483-4621
EBERLINE
SERVICES
EBS-OR-35923
August 9, 2013
Paul V. Rosasco, P .E.
Engineering Management Support, Inc.
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
CASE NARRATIVE
Work Order# 13-07098-0R
SAMPLE RECEIPT
This work order contains nine water samples received 07/15/2013. Eight samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228. One sample was analyzed
as total for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENT ID
LAB ID
CLIENT ID
LAB ID
PZ-111-SD TOT
PZ-111-SD DIS
S-5 TOT
S-5 DIS
FB @ PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
I-4 TOT
I-4 DIS
13-07098-04
13-07098-05
13-07098-06
13-07098-07
13-07098-08
13-07098-09
13-07098-10
13-07098-11
13-07098-12
PZ-100-SS TOT
PZ-100-SS DIS
D-3 TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
13-07098-13
13-07098-14
13-07098-15
13-07098-16
13-07098-17
13-07098-18
13-07098-19
13-07098-20
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using Method EPA 903.0. Radium-228 was analyzed using Method EPA 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page 1 of3
ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were prepared by removing representative aliquots followed by mixed acid digestions as
appropriate. Uranium was selectively extracted by ion exchange. Uranium was eluted, micro
precipitated and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238.
Chemical recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232
tracer was determined by alpha spectroscopy using an energy specific region of interest.
I'' Analytical Attempt

Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was low for
sample numbers S-5 TOT, I-4 TOT and I-4 DIS. These samples appear to have an elemental interference
present. Chemical recovery was acceptable for all other samples. The Uranium-234, Uranium-235 and
Uranium-238 method blank demonstrated acceptable results. Results for the Uranium-234, Uranium-235
and Uranium-238 duplicate demonstrated a high relative percent difference; however, normalized
difference is within acceptable limits for the analytical technique. Results for the Uranium-234 and
Uranium-238 laboratory control sample demonstrated an acceptable percent recovery.
2nd Analytical Attempt
Sample numbers S-5 TOT, I-4 TOT and I-4 DIS were reanalyzed due to low chemical recoveries in the
first analytical attempt. Samples demonstrated acceptable results for all Uranium analyses. Chemical
recovery was still low for sample numbers S-5 TOT, I-4 TOT and I-4 DIS. In this case, low chemical
recoveries are related to apparent elemental interferences. Due to limited sample volume a third
analytical attempt was not possible. Chemical recovery was acceptable for the laboratory control sample
and method blank. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated
acceptable results. Results for the Uranium-234 and Uranium-238 duplicate demonstrated a high relative
percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Uranium-235 duplicate demonstrated an acceptable relative percent difference
and normalized difference. Results for the Uranium-234 and Uranium-238 laboratory control sample
demonstrated an acceptable percent recovery.
ISOTOPIC THORIUM
appropriate. Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated
and mounted on micro-porous filter media. Sample activities were then determined by alpha
spectroscopy using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232.
Chemical recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229
tracer was determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228, Thorium-230 and Thorium-232 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample
demonstrated an acceptable percent recovery.
Page2of3
ANALYTICAL RESULTS CONTINUED

RADIUM-226
appropriate. This was followed by selective sulfate precipitations of the Radium. Samples were then
mounted by semi-micro-precipitations onto micro-porous filters. Samples were counted by alpha
spectroscopy using an energy specific region of interest for Radium-226. Chemical recovery was
calculated by the use of a Barium-133 tracer, which was determined by HPGe gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium
226 duplicate demonstrated an acceptable relative percent difference and normalized difference. Results
for the Radium-226 laboratory control sample demonstrated an acceptable percent recovery.
RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium
228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium
133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated results greater than the detection limit.
Results for the Radium-228 duplicate demonstrated a high relative percent difference; however,
normalized difference is within acceptable limits for the analytical technique. Results for the Radium-228
laboratory control sample demonstrated an acceptable percent recovery.
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.
\\
______,
M.R. McDougall
Laboratory Manage
Date: 8/9/2013
Eberline Analytical \vants and encourages your feedback regarding our perfonnance providing radioanalytical services. Please
visit http://www.eberlineservices.com/client.htm to provide us with feedback on our services.
Page 3 of3
SECTION IV
ANALYTICAL RESULTS SUMMARY
Project: West Lake OU-1

SDG: 1307098
Received: 07/15/2013
Matrix: Water

Lakewood, CO 80235
Client Samele ID
l~l;l!i
Analvsis Date/Time
Analvte
Method
LCS13-07098-01
LCS13-07098-01
LCS13-07098-01
LCS13-07098-01
LCS 13-07098-01
LCS 13-07098-01
LCS13-07098-01
LCS13-07098-01
LCS13-07098-01
LCS13-07098-01
LCS 13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
13-07098-01
07/24/2013 12:43:34
07/31/2013 08:18:29
07/25/201313:26:17
07/25/2013 13:26:17
07/25/2013 13:26:17
07/25/2013 10:13:39
08/01/2013 09:15:55
07/25/201310:13:39
08/01/2013 09:15:55
07/25/2013 10:13:39
08/01/2013 09:15:55
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
BLANK13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
13-07098-02
07/24/2013 12:43:29
07/31/2013 08:18:30
07/25/201313:26:19
07/25/2013 13:26:19
07/25/2013 13:26:19
07/25/201310:13:40
08/01/2013 09:15:56
07/25/201310:13:40
08/01/2013 09:15:56
07/25/2013 10:13:40
08/01/2013 09:15:56
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-234
Uranium-235
Uranium-235
Uranium-238
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-07098-03
13-07098-03
13-07098-03
13-07098-03
13-07098-03
13-07098-03
13-07098-03
13-07098-03
07/24/2013 12:43:30
07/31/2013 08:18:30
07/25/2013 13:26:13
07/25/201313:26:13
07/25/201313:26:13
08/01/2013 09:15:51
08/01/2013 09:15:51
08/01/2013 09:15:51
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
!ill
tl!ll
M
Lab Samele ID
DUP
DUP
DUP
DUP
DUP
DUP
DUP
DUP
-r-J,EBERLINE
Jl!J
SERVICES
Final Report of Analysis

Date: 8/9/2013
Page 1 of6
Result
Error
CSU
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
10.65
10.57
5.26
5.12
5.35
7.89
8.36
0.49
0.74
7.96
7.38
1.25
0.83
0.82
0.80
0.83
1.13
1.46
0.20
0.31
1.14
1.31
2.57
2.53
0.96
1.02
0.96
1.26
1.57
0.20
0.31
1.27
1.42
0.27
0.10
0.09
0.08
0.06
0.11
0.12
0.09
0.15
0.06
0.12
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.13
2.43
0.08
0.16
0.01
0.13
0.13
0.04
0.06
0.06
0.08
0.18
0.42
0.07
0.09
0.03
0.08
0.09
0.05
0.07
0.06
0.07
0.18
0.70
0.07
0.10
0.03
0.08
0.09
0.05
0.07
0.06
0.07
0.29
0.11
0.06
0.06
0.06
0.06
0.10
0.07
0.10
0.07
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.08
3.00
0.00
0.08
0.03
0.20
0.27
-0.09
0.39
0.44
0.07
0.10
0.07
0.30
0.37
0.16
0.45
0.81
0.07
0.10
0.07
0.30
0.37
0.16
0.23
0.10
0.15
0.15
0.14
0.51
0.58
0.49

601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683
FAX 865/483-4621
Qualifier
Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
u
u
u
u
u
u
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
u
J
J
u
u
u

Lakewood, CO 80235
Client Sample ID
!lill
!:~
l'l
~~

SDG: 1307098
Matrix: Water
Lab Sample ID
Analvsis Date/Time
AnaMe

Date: 8/9/2013
Page 2 of6
Method
Result
Error
CSU
MDA
0.37
0.51
0.05
0.07
0.05
0.14
0.07
0.12
0.43
0.98
0.05
0.07
0.05
0.14
0.07
0.12
0.16
0.11
0.09
0.10
0.08
0.09
0.10
0.07
PZ-111-SD TOT_07_09_2013
PZ-111-SD TOT_07 _09_2013
PZ-111-SD TOT_07_09_2013
PZ-111-SD TOT_07_09_2013
PZ-111-SD TOT_07_09_2013
PZ-111-SD TOT_07_09_2013
PZ-111-SD TOT_07_09_2013
PZ-111-SD TOT_07 _09_2013
13-07098-04
13-07098-04
13-07098-04
13-07098-04
13-07098-04
13-07098-04
13-07098-04
13-07098-04
07/24/201312:43:31
07/31/2013 08:18:31
07/25/201313:26:15
07/25/201313:26:15
07/25/2013 13:26:15
07/25/2013 10:13:42
07/25/2013 10:13:42
07/25/201310:13:42
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.05
3.72
0.02
0.07
0.02
0.35
0.06
0.26
PZ-111-SD
PZ-111-SD
PZ-111-SD
PZ-111-SD
PZ-111-SD
PZ-111-SD
PZ-111-SD
PZ-111-SD
13-07098-05
13-07098-05
13-07098-05
13-07098-05
13-07098-05
13-07098-05
13-07098-05
13-07098-05
07/24/201312:43:32
07/31/2013 08:18:35
07/25/2013 16:25:50
07/25/2013 16:25:50
07/25/2013 16:25:50
07/25/201310:13:43
07/25/201310:13:43
07/25/201310:13:43
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
HASL 300, 4.5.2
1.53
4.77
0.01
0.11
-0.01
0.30
0.05
0.18
0.47
0.58
0.05
0.08
0.03
0.13
0.06
0.10
0.57
1.22
0.05
0.08
0.03
0.13
0.06
0.10
0.24
0.11
0.11
0.06
0.08
0.06
0.08
0.08
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
S-5 TOT_07_09_2013
13-07098-06
13-07098-06
13-07098-06
13-07098-06
13-07098-06
13-07098-06
13-07098-06
13-07098-06
07/24/2013 12:43:32
07/31/2013 08:18:35
07/25/201316:25:51
07/25/201316:25:51
07/25/201316:25:51
08/01/2013 09:15:52
08/01/2013 09:15:52
08/01/2013 09:15:52
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.98
5.52
0.15
0.10
0.18
1.10
0.17
-0.06
0.67
0.80
0.13
0.11
0.13
0.91
0.41
0.33
0.70
1.48
0.13
0.11
0.13
0.91
0.41
0.33
0.80
0.17
0.17
0.15
0.12
0.79
0.85
0.79
S-5
S-5
S-5
S-5
S-5
S-5
S-5
S-5
13-07098-07
13-07098-07
13-07098-07
13-07098-07
13-07098-07
13-07098-07
13-07098-07
13-07098-07
07/24/201312:43:33
07/31/2013 08:18:35
07/25/201316:25:44
07/25/2013 16:25:44
07/25/2013 16:25:44
07/25/2013 13:24:25
07/25/2013 13:24:25
07/25/2013 13:24:25
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.83
4.01
0.07
0.01
-0.01
0.17
0.16
0.29
0.62
0.62
0.09
0.05
0.04
0.19
0.20
0.25
0.64
1.10
0.09
0.05
0.04
0.19
0.20
0.25
0.66
0.15
0.15
0.11
0.11
0.22
0.24
0.28
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
~.EBERLINE
JeJ
SERVICES

865/481-0683
FAX 865/483-4621
Qualifier
u
u
u
u
u
J
u
u
J
J
u
J
J
u
u
J
u
u
u
u
u
J
Units
pCi/I
pCiil
pCi/I
pCi/I
pCi/I
pCiil
pCi/I
pCiil
pCiil
pCi/I
pCi/I
pCi/I
pCi/I
pCi/1
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Lakewood, CO 80235
Client Sample ID
~~I
ll"'lJI
~JI
Lab Sample ID
Analysis Date/Time
Analvte
13-07098-08
13-07098-08
13-07098-08
13-07098-08
13-07098-08
13-07098-08
13-07098-08
13-07098-08
07124/201312:44:02
07/31/2013 08:18:36
07/25/2013 16:25:45
07/25/2013 16:25:45
07/25/2013 16:25:45
07/25/201313:24:26
07/25/201313:24:26
07/25/2013 13:24:26
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
PZ-110-SS TOT_07_09_2013
13-07098-09
13-07098-09
13-07098-09
13-07098-09
13-07098-09
13-07098-09
13-07098-09
13-07098-09
07/2412013 12:44:03
07/31/2013 08:18:28
07/25/201316:25:46
07/25/201316:25:46
07/25/201316:25:46
07/251201313:24:19
07/25/2013 13:24:19
07/25/2013 13:24:19
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
PZ-110-SS
13-07098-10
13-07098-10
13-07098-10
13-07098-10
13-07098-10
13-07098-10
13-07098-10
13-07098-10
07/24/2013 12:44:05
07131/2013 08:18:28
07/25/2013 16:25:47
07/2512013 16:25:47
07/25/2013 16:25:47
07/25/201313:24:20
07125/201313:24:20
07/25/201313:24:20
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-07098-11
13-07098-11
13-07098-11
13-07098-11
13-07098-11
13-07098-11
13-07098-11
13-07098-11
07/24/2013 12:44:06
07/31/2013 08:18:28
07/25/201316:25:48
07125/201316:25:48
07125/2013 16:25:48
08/01/2013 09:15:53
08/01/2013 09:15:53
08/01/2013 09:15:53
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
~.EBERLINE
J.l!J
SERVICES

Date: 8/9/2013
Page 3 of6
Method
FB@PZ-110-SS TOT_07_09_2013
FB@ PZ-110-SS TOT_07_09_2013
FB@ PZ-110-SS TOT_07_09_2013
FB@ PZ-110-SS TOT_07_09_2013
FB@PZ-110-SS TOT_07_09_2013
FB@PZ-110-SS TOT_07_09_2013
FB@ PZ-110-SS TOT_07_09_2013
FB@ PZ-110-SS TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07 _09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
1-4 TOT_07_09_2013
I<!

SDG: 1307098
Matrix: Water
Result
Error
CSU
MDA
Qualifier
Units
0.10
0.47
0.04
0.07
0.04
0.07
0.06
0.09
0.10
0.80
0.04
0.07
0.04
0.07
0.06
0.09
0.22
0.12
0.10
0.07
0.06
0.11
0.10
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.03
2.86
0.00
0.09
0.03
0.05
0.04
0.13
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.12
4.11
0.05
0.20
0.02
0.10
0.11
0.02
0.79
0.56
0.06
0.13
0.05
0.09
0.09
0.04
1.18
1.08
0.07
0.13
0.05
0.09
0.09
0.04
0.23
0.12
0.09
0.08
0.11
0.11
0.10
0.10
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.43
5.20
-0.01
0.10
0.06
0.08
0.01
0.06
0.70
0.60
0.04
0.07
0.06
0.08
0.05
0.07
1.01
1.32
0.04
0.08
0.06
0.08
0.05
0.07
0.21
0.11
0.11
0.07
0.07
0.10
0.12
0.10
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.37
5.20
0.01
0.06
0.01
0.60
0.32
0.17
0.52
0.59
0.07
0.07
0.03
0.51
0.44
0.29
0.60
1.32
0.07
0.07
0.03
0.51
0.44
0.29
0.28
0.11
0.14
0.11
0.07
0.43
0.67
0.49

865/481-0683
FAX 8651483-4621
u
J
u
u
u
J
u
J
u
J
J
u
J
u
u
u
u
u
u
u
J
u
u
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Lakewood, CO 80235
Client Sample ID
~~
ti-.:!t
WI
I,
Lab Sample ID
Analvsis Date/Time
Analvte
13-07098-12
13-07098-12
13-07098-12
13-07098-12
13-07098-12
13-07098-12
13-07098-12
13-07098-12
07/24/2013 12:44:08
07/31/2013 08:18:29
07/25/201316:25:49
07/25/201316:25:49
07/25/201316:25:49
08/01/2013 09:15:54
08/01/2013 09:15:54
08/01/2013 09:15:54
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
PZ-100-SS TOT_07_09_2013
13-07098-13
13-07098-13
13-07098-13
13-07098-13
13-07098-13
13-07098-13
13-07098-13
13-07098-13
07/24/2013 12:44:09
07/31/2013 08:17:08
07/25/2013 16:27:29
07/25/2013 16:27:29
07/25/201316:27:29
07/25/201313:24:23
07/25/201313:24:23
07/25/201313:24:23
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-100-SS
PZ-100-SS
PZ-100-SS
PZ-100-SS
PZ-100-SS
PZ-100-SS
PZ-100-SS
PZ-100-SS
13-07098-14
13-07098-14
13-07098-14
13-07098-14
13-07098-14
13-07098-14
13-07098-14
13-07098-14
07/24/2013 12:44:11
07/31/2013 08:17:09
07/25/2013 16:27:31
07/25/2013 16:27:31
07/25/2013 16:27:31
07/25/2013 13:24:24
07/25/201313:24:24
07/25/201313:24:24
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-07098-15
13-07098-15
13-07098-15
13-07098-15
13-07098-15
13-07098-15
13-07098-15
13-07098-15
07/24/201312:44:13
07/31/2013 08:17:09
07/25/201316:27:24
07/25/201316:27:24
07/25/2013 16:27:24
07/25/201313:24:44
07/25/2013 13:24:44
07/25/2013 13:24:44
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
18
EBERLINE
SERVICES

Date: 8/9/2013
Page 4 of6
Error
CSU
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.96
5.89
0.06
0.11
0.04
1.47
0.67
0.18
0.50
0.68
0.06
0.08
0.05
0.84
0.63
0.36
0.54
1.49
0.06
0.08
0.05
0.84
0.63
0.36
0.31
0.13
0.09
0.08
0.06
0.58
0.71
0.67
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.04
1.99
0.04
0.17
0.03
4.99
0.40
2.22
0.80
0.84
0.06
0.11
0.05
0.79
0.18
0.44
1.17
0.96
0.06
0.11
0.05
0.87
0.18
0.47
0.23
1.60
0.09
0.07
0.09
0.12
0.11
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.19
0.74
0.05
0.02
0.05
4.82
0.26
1.86
0.64
0.66
0.07
0.05
0.06
0.82
0.15
0.42
0.93
0.68
0.07
0.05
0.06
0.89
0.16
0.44
0.20
1.33
0.10
0.10
0.07
0.11
0.13
O.D7
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.53
4.81
0.15
0.15
0.00
0.18
0.10
0.09
0.94
0.96
0.13
0.12
0.04
0.19
0.15
0.17
1.20
1.45
0.13
0.12
0.04
0.19
0.15
0.17
0.30
1.60
0.13
0.13
0.09
0.24
0.22
0.32
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Qualifier
Result
Method
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
1-4 DIS_07_09_2013
0-3 TOT_07_09_2013
0-3 TOT_07_09_2013
D-3 TOT_07_09_2013
0-3 TOT_07_09_2013
D-3 TOT_07_09_2013
0-3 TOT_07_09_2013
0-3 TOT_07_09_2013
D-3 TOT_07_09_2013
lii.1

SDG: 1307098
Matrix: Water
865/481-0683
FAX 865/483-4621
u
J
u
J
u
J
u
J
u
u
u
J
u
u
u
u
Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I

Lakewood, CO 80235
Client Samele ID
D-3
D-3
D-3
D-3
D-3
D-3
D-3
D-3
~~
tl)~_I
f-,~1
I>

SDG: 1307098
Matrix: Water
Lab Samele ID
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
Analvsis Date/Time
Analyte
Method
13-07098-16
13-07098-16
13-07098-16
13-07098-16
13-07098-16
13-07098-16
13-07098-16
13-07098-16
07/24/201312:44:15
07/31/2013 08:17:10
07/25/201316:27:26
07/25/2013 16:27:26
07/25/2013 16:27:26
07/25/2013 13:24:44
07/25/201313:24:44
07/25/201313:24:44
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E.903.0
E.904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-100-SD TOT_07 _09_2013

PZ-100-SD TOT_07_09_2013
PZ-100-SD TOT_07_09_2013
PZ-100-SD TOT_07_09_2013
PZ-100-SD TOT_07_09_2013
PZ-100-SD TOT_07_09_2013
PZ-100-SD TOT_07_09_2013
PZ-100-SD TOT_07 _09_2013
13-07098-17
13-07098-17
13-07098-17
13-07098-17
13-07098-17
13-07098-17
13-07098-17
13-07098-17
07/24/201312:44:17
07/31/2013 08:17:12
07/25/2013 16:27:27
07/25/2013 16:27:27
07/25/2013 16:27:27
07/25/201313:24:45
07/25/201313:24:45
07/25/201313:24:45
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E.903.0
E.904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-100-SD
PZ-100-SD
PZ-100-SD
PZ-100-SD
PZ-100-SD
PZ-100-SD
PZ-100-SD
PZ-100-SD
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
13-07098-18
13-07098-18
13-07098-18
13-07098-18
13-07098-18
13-07098-18
13-07098-18
13-07098-18
07/24/2013 12:44:19
07/31/2013 08:17:12
07/25/201316:27:34
07/25/2013 16:27:34
07/25/201316:27:34
07/25/2013 13:24:46
07/25/2013 13:24:46
07/25/2013 13:24:46
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E.903.0
E.904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
PZ-112-AS TOT_07_09_2013
13-07098-19
13-07098-19
13-07098-19
13-07098-19
13-07098-19
13-07098-19
13-07098-19
13-07098-19
07/24/201312:44:21
07/31/2013 08:17:13
07/25/201316:27:36
07/251201316:27:36
071251201316:27:36
0712512013 13:24:47
0712512013 13:24:47
0712512013 13:24:47
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E.903.0
E.904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,

Date: 8/9/2013
Page 5 of6
EBERLINE
SERVICES
Result
Error
CSU
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
3.72
6.18
0.18
0.09
0.03
0.19
0.14
0.04
0.99
1.03
0.11
0.07
0.05
0.18
0.17
0.11
1.27
1.74
0.11
0.07
0.05
0.18
0.17
0.11
0.49
1.60
0.09
0.06
0.08
0.19
0.21
0.24
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.87
1.35
0.02
0.10
0.01
0.42
0.05
0.34
0.51
0.67
0.04
0.07
0.02
0.16
0.06
0.14
0.64
0.73
0.04
0.07
0.02
0.16
0.06
0.15
0.18
1.27
0.08
0.06
0.05
0.07
0.07
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.85
0.67
0.03
0.09
0.02
0.44
0.03
0.34
0.47
0.62
0.06
0.08
0.05
0.20
0.07
0.18
0.61
0.64
0.06
0.08
0.05
0.20
0.07
0.18
0.12
1.25
0.11
0.08
0.08
0.14
0.15
0.11
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
2.27
3.39
0.06
0.16
0.02
0.19
0.05
0.09
0.74
0.69
0.07
0.11
0.05
0.15
0.08
0.09
0.88
1.03
0.07
0.11
0.05
0.15
0.08
0.09
0.26
1.09
0.07
0.10
0.10
0.16
0.14
0.10

865/481-0683
FAX 865/483-4621
Qualifier
J
J
u
J
u
u
J
u
J
u
u
u
J
u
u
u
J
u
J
u
u
Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCill

SDG: 1307098
Matrix: Water

Lakewood, CO 80235
Client Sample ID
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
PZ-112-AS
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
DIS_07_09_2013
Lab Sample ID
Analvsis Date/Time
13-07098-20
13-07098-20
13-07098-20
13-07098-20
13-07098-20
13-07098-20
13-07098-20
13-07098-20
07/24/201312:44:24
07/31/2013 08:17:13
07/25/2013 16:27:32
07/25/2013 16:27:32
07/25/201316:27:32
07/25/201313:24:48
07/25/201313:24:48
07/25/201313:24:48
Analvte
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238

Date: 8/9/2013
Page 6 of 6
Method
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
Result
Error
CSU
MDA
1.19
1.96
0.07
0.13
-0.04
0.25
0.15
-0.03
0.52
0.75
0.07
0.10
0.05
0.18
0.16
0.07
0.58
0.87
0.08
0.10
0.05
0.19
0.16
0.07
0.38
1.40
0.09
0.10
0.17
0.15
0.19
0.19
I.fr~
Iii!
"~
!.J'l
EBERLINE
SERVICES

865/481-0683
FAX 865/483-4621
Qualifier
u
J
u
J
u
u
Units
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
pCi/I
SECTIONV
ANALYTICAL STANDARDS
()..-8
QA/QC REVIEWED CERTIFICATE OF CAI JBRATION

(? q(lnitials J ALPHA STANDARD SOLUTION
. Date
Radionuclide:
Half Life:
(4.468
Catalog No.:
Source No.:
U-238NAT
0.005) x 10-9 years
7338
479-50
Description of Solution
a. Mass of solution:
b. Chemical form:
TMA EBERLINE
Customer:
P.O.No.:
OR2778
...,.
12:00 PST.
Reference Date:
January l 1995
Contained Radioactivity: (Total U) 8.016 Ci
Contained Radioactivity: (Total U) 297 kBq
..;., --.
c. Carrier content:
65.2896 g in a 50 ml flame sealed ampoule

Uranyl Nitrate in H20
None
d. Density:
Approximately 1.3202
Radioimpurities
g/ml @20c.
'
....
Refer to attached technical data sheet
. ~
Radioactive Daughters
Refer to attached technical data sheet
Radionuclide Concentration
(Total U) 0.1228
Ci/g.
Method of Cahbration
Activity calculations are based upon known specific activity and mass.
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):

d. Total uncertainty at the 99% confidence level:
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear da'W were taken from "Table of Radioactive lsoto~, edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to ei.tablish and maintain implicit tcaceability for a ti.umber of nuclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide-4.15).
efl-tv AuA:2
QU
Y/\
l~
I. \
. ,
T 0
P E
PRODUCTS
l.AHO!(ATO:llES
YCONTROL
Date Signed
. JV
l S 0
''.
ISOTOPE PRODUCTS LABORATORIES

3017 N. SAN FERNANDO BLVD.
BURBANK, CAL!FORN!A 91504
8!88437000
FAX
8!88436!68
.,-.
1'.~ii;B.2 7.
QUALITY CONTROL PROGRAM

MP-009
Rev.8; 11/01103
Title:
Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES - OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION

MP 009
Half Life, Yeais
I 4.4sae+o91
Reference Date!
1.632E+12I
11111'995
O:ool
Ampoule /Solution Gross . . 97:6400 Weight, Grams

Empty Ampoule
32:.5020 Weight, Grams
Solution Net
65.1380 Weight, Grams
Total Activity in Ampoule
8.0160 Ci
Chemical Com ositlon of Standard Solution
Dilution Instructions:
Dilute to a volume otl . 1000:00
Certified Total Activity ofl
Dilution Solvent Used
8;0160JCI
Imilliliters
Which Eauals
1.780E+07ldpm atthe date listed above

This activity concentration Is based on the original
And after dilution the activity of this solution isl 1.77955E+D4ldpm/mh.terence date listed above. All actlVlties are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date: September 6, 2013
Date: _ _.;;.;9/=-26"'"/""20""1=-2-"0"":0...;..0
Date:
_.......,'l/~u--+-1/c_"2-__
~EBE~-~~~.Fi I QUALITY CONTROL PROGRAM

MP.009
Rev.6; 11101103
Title: Radioactive Reference Standards Solutlons & Records
EBERLINE SERVICES OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DIL.UTION RECERTIFICATION
Date I
916/2012 O:OO I
Solution #1 , U"lla '. " 'J
Half Llfe1 Da:i:s
1.e32E+12I
MP-009
Solution Reference #llPL479~50 . ;::..- .:_:.. :----.--:I
PrinciDal Radionuclide
Half Life, Years
~
I
4AeaE+mi
..,:i<!"'u
Radionuclide of lnteresd :.. 2;31..2~~. "''Ui

Parent Solution Cone. . 1:7796E+04 .'I dpm/ml
Reference Date
Chemical Coml!ositlon of Standard Solution
IUi'anlfNitiat~ ir 1~ HNO .
-111i1e9so:oo I
I
.I
l1M HN03'.
SECONDARY VOL.UMETRIC Dlt.UTION

Vol. Parent Solution: ,; .> 4.0000 ml
Total Activity: 7.1182E+04 dpm
Final Volume: . . . . 1000~00. ml
Final Activity Concentration:!
7.1182E+01 jdpm/ml
This activity concentration is based on the orlglnal

reference date listed above. All activities are
corrected to the date and time of analysis by the
-~--- tory data processing software.
NOTES:
Isotopic Distribution as:

U-238 Atom % =48.239 U-236 71.182 dpm/ml X 0.4ll249 = 34.345 dpm/ml
U235 Atom 0/o = 2.25
U-235 = 71.162 dpm/ml X 0.0225 = 1.602 dpm/ml
U234 Atom o/o =49.601 U-236 =71.162 dpm/ml X 0.49501 35.236 dpmlml
All values +/ 3.6%
Isotopic ratios from manufacturer's data sheet
\,
Verified & Approved By
QC Approval
"~
~~
~Jl4A
Expiration Date:! September 6, 2013
hll
Date:
9/26/2012 0:00
Date:
~iUPlrz
..
i
RECORD COPY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
Product Description & Measurement Certificate
Description
Principal radionuclide:
Daughter Nuclide:
uranium 232 (U-232)

Th-228
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
Volume of solution
Total activity ofU-232
which is equivalent to
Accuracy
Radionuclidic
Purity
Product code: UDPl0050

Batch Number: 9'21232/67
01 March 2000
6.739E+o3 becquerels per gram ofsolution
l.821E-01 microcuries per gram of solution
5.35 gn1;;1s
5.035 millilitres
3.61E+o4 becquerels
9.76E-01 microcuries
Method ofmeasurement (see reverse ofthis certificate)

Random uncertainty is: 0.7%
Systematic uncertainty: 0.5%
Overall uncertainty in the radioactive ci>ncentration quoted above: 1.7%
Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages
ofthe activity ofthe principle radionuclide at the reference date .
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00
Isotopic
Purity
~he
isotopic composition, exprossed as atom per cent at the reference date .
i>lot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Physical
Data
Recommended halflifo of uranium 232: 6.980E+ol yeill'S

Principle energies of alpha emissions (MeV): 5.263 31.7%, 5.320 68.0%
Branching ratio for alpha emission: 100%
Calculated specific activity ofuranium 232: 8.167E+o5 Bq per microgram U-232.
Remarks
For safety information and notes to ensure correct usage by all persons handling this radio'!Ctive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 900 I.
Approved
Signatory
Project Ref. AE231S
Roger Wiltshire
Prepared and characteried in the UK, for world wide distnllution by Isotrak, AEA Technology, QSA.
Trkcert.wps 10103100
AEA TechnrJ!ogy is the trading name of AEA Technology plcfi.
-B J !

MP-009
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records

PRIMARY DILUTION RECERTIFICAT/ON
MP 009
CURRENT DATE
12/13/2012 O;OO
SOLUTION REFERENCE #r.Af?.A/.=:':'A"""m-ers.,-;h-a"""m"::9:::21:::23::::2-:::/6::-7.-:,.,
SOLUTION #r--~-:.-rurc1"or..-'""'"1
Principal Radionuclide
Half Life, Days

2.630E+04I
Half Life, Years
u .
I... .
I .1.2o(JE+o1 I
Ce~~=~o:~:~::1.~.~=~E~Q1 lCi
Certified Concentration " : : . : Ci per gram
....
-'s...11...12_0""0.._.0""0"":0"'"'0I
Reference Datel._.'"'-_.
~-M
>1WOight
Empty Ampoule
. . . > Weight, Gnmo
Grams
GI.....
Solution Net
. . Weight, Grams
0.9760 Cl
Chemical Composition of Standard Solution
l2MHNO
. . . . . 3 :
Diiution Solvent Used
Diiute to a volume ofl 1000.00 ".!milliliters
Certified Total Activity of I
0.9760jCI
Which Eauals
i . 2.167E+06ldpm at the date listed above

Thfs activity concentration is based on the original
And after dllutlon the activity of this solution Is 2.167E+03ldpmlml reference date listed above. All activities are corrected
Expiration Date:/ December 7, 2013
Date:
Date:
12113/2012 0:00
1f.3d'
"::l
/
~EeJ::RLIJ..iE I QUALITY CONTROL PROGRAM

MP-1109
Se:Av1c:;; ....
Rev.6; 11/01/03
Title: Radioactive Raferenr;e Standards Solution' & Records
EBERLINE SERVICES- OAK RIDGE LABORATORY

SECONDARYDILUTION RECERT/FICATION
MP-009
Solution Reference #IAEA/Amershan1'92/232167 I
Princioal Radionuclide
Half Life, Years
I
7 .200E+01
.,,,u. .
Date I
Solution#!
....232.
Radionuclide of lnteresj
u
Parent Solution Cone. . 2.167E+03 ldpmlml
121712012 0:001
U'10a . . 1
Half Llfe 1 Dal!
2.630E+041
Reference Date!
31112000 o:oo
Chemical ComPOsition of Standard Solution
r~U(NO.Je;in2MHNO,
!2MHNOa :::;;--:
SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: 1
10.0000 ml
Total Activity:
2.1670E+04 dpm
Final Volume: I . .. 1000.00 ml
2.1670E+o1 dpmlml
This activity concentratlon is based on the original

laboratory data processing software.
NOTES:
Expiration Date:! December7, 2013
~-~
Date:
QCApproval
~ rdlJ J< ~\
Date:
12113/2012 0:00
12142=
i-:...
RID1CATE OF CALIBRATI
-LPHA STANDARD SOLUTIO
1.2!\!=;e:Radi=t;:"oi;!nu...!cli~.de~:::::.J
Th-230
TMA
Customer:
Half Life:
(7.54 0.03) x 10"4 years
Catalog No.:
7230
Source No.:
388-116
b. Chemical fonn:
c. Carner content:
d. Density:
at
,
99
c;;c'\ '
~~~\\~\\
EBE~i~~'t \,'?i
P.O.No.:
TI4944
''""
Reference Date:
November 1 1991
12:00 PST.
Coutained Radioactivity:
1.036
Ci.
5.0042
Th(N03)4 in O.lN HN03
None added
1.0016
grams.
gram1m1 @
2oc.
Radioimpurities
See attached technical dala sheet
See attached technical dala sheet
Radiouuclide Concentration
0.207
JLCi/gram.
Method of Calibration
Weighed aliquots of the solution were assayed using a liquid scintillation
counter.
of
Uncertainty
Measurement
a. Systematic uncertainty in instmment calibration:
d. Total uncertainty at the 99 % confidence level:
2.0%
0.5%
0.2%
2.7%
NIST Traceability
Notes
1. Nuclear data were taken from "Table of Isotopes", Seventh Edition, edited by Vllginia S. Shirley.
2. IPL participates in an NIST measuremenl assunmce prog111111 to establish and maintain implicit.
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatozy Guide 4.15)

1800 No. Keystone Street.,
Burbank, California 91504
818 843 7000
Rev.8; 11/01103
Title: Radioac;tive Reference Standards Solutions & Records

SECONDARY DILUTION RECERTIFICATION
314/2013 0:00
Date
Solution# . <:2Th,1b:. '
Half Life, Days
MP-009
Solution Reference# IPL 388416 i: "
Princi I Radionuclide
Half Life, Years
:.. 2'l!lTt( .::
7.MOE:f.Oill
Radionuclide of lnteres :~ 3HI'ho~i.im.:

Parent Solution Cone. '".2:30E+o3.. dpm/ml
Reference Date
2.754E;,07 I
F :1 '11i11sa1:o:ool

Vol. Parent Solution: \:/,:Ao,oooo ml

Total Activity: 2.2999E+04 dpm
Final Volume: ..... \''.''10.00.00 ml
NOTES:
2.2999E+01 ldpmlml

Expiration Date:!
March 4, 2014
Date: --'31"'2"'1""/2'"'0..;.13""-"'0;"'0"'-0
Date:
3.:?.l '~
Date:
--';S"i'"';i,'-l--+("""'---
<(Iii= Br;::" h~~.-fi I

MP--009
Rev.8; 11/01/03

PRIMARY DILUTION RECERTIFICAT/ON
MP009
SOLUTION REFERENCE # IPL 3.88416 .
Principal Radionuclide
Half Life, Years
...
1-' ,____ -.;.ffl. .
7:540E+041
<> i
'.'<:.
IJ:
.-;i
. 3/4/2013 0:001
CURRENT DATE!
I
SOLUTION #r ' >
.-.:d
Half Life, Dale
2.754E+o1j
Reference Date j
Radionuclide 7"1 lioriuirl'

Certified Activity f:036Ef00. Cl
Certified Concentration I.:.:.
>: Ci per gram
,, . . . ':111111 il01;ci:oo I
Ampoule /Solution Gross <s;2660 Weight, Grams

Empty Ampoule +4:521a Weight, Grams
Solution Net . 4.6442 Weight, Grams
Total Activity In Ampoule . . 1.0360 Ci
,.
...
...... . . ..... . ... ...... }\..::.~:-:>';\:".''' .
:.. _,--;; . ... 9s)~io:O:lN !'11\fPs:

122~ti(N
.~
>"
..:I
loc1NHNO
._. - -- . ..3 ...<
Dilution lnstruction.s:
-, ..
.,
,:-
. . ...,_,,
Dilute to a volume ofl Y. 1.000:00 ' jmillillters
1.0360jCI
Which Eauals
2:300E+06 j dpm at the date listed above
And after dilution the activity of this solution Is 2.300E+Q3jdpm/ml

reference date IJsted above. All activlttes are corrected
to the da~ and time of analysis by the laboratory data
Expiration Date: l
Recertified By
~-1\
QC Approval
C~Aj 1,J"Ji J
-
""'
Date:
Date:
March 4, 2014
3/21/2013 0:00
"f~L
l
1
1'1-8
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radionuclide:
Th-232
Half Life:
(1.405 0.006) x 10'10 years
Catalog No.:
7232
Source No.:
435-104-2
b. Chemical form:
c. Carrier content:
d. Density:
TMAEBERLINE
Customer:
P.O.No.:
VH1632
12:00 PST.
Reference Date:
November 11993
Ci.
Contained Radioactivity:
(Th-232) 0.0933
(Th-232) 3.4:5
kBq.
11.9712 g (in a 10 ml flame sealed ampoule)
Th(N03)4 in water
None added
APPfoX. 1.21
g/ml@ 20C.
Nolle detected(other than daugbters).
Radioimpurities
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212, Po-212, Tl-208
Radionuclide Concentration
(Th-232) 0.00779
Ci/g.
Activity calculations are based upon known specific activity and mass.
c. Random uncertainty in weigbing(s):
3.0%
0.0%
2.0%
3.6%
NIST Traceability
Leak Test(s)
Notes
i.. Nuclear data ."!\'.ere iaken from "Ta~Je of Radioactive Isotopes". edited by Virgi"nia S. ShirtCy, -.1986.
2. IPL participates in an NIST measurement assurance program lo establish and maintain implicit traceability for a number of nuclid~s,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
QUALITY CONTROL
Date Signed
1800 North Keystone Street
818 843 - 7000

MP-409
Rev.a; 1110103
Trtfe:

MP009
CURRENT DATE
SOLUTION REFERENCE #r::IP""J:f"'<ll"'3""'5"""JO"'j!""}2...,:."";:"':.:"':"";;"";<"'"fc=:\i
SOLUTION# ~~~~=-=======I
Half Life, Years
Half Life, Days
Ri't:'.!fa)ld5!$'t~OI
:5.132E+12l
I : .
Radionuclide ~~>: l:fr.;:

certified Activity W:.a:aaoJE\:02 Ci
Certified Concentration
Ci per gram
.:{c'>11111N9\lai:6io61
Reference Datel
Ampoule /Solution Gross >.D '1B:i$.4t5 Weight, Grams

Empty Ampoule ;g;;:;a:9296 Weight, Grams
Solution Net .:.: A1!9t1.9 Weight, Grams
Total Activity in Ampoule . : Q'.0033 Ci
Diiute to a volume oflO::::YlOOO."Ooi>lmllllllters
Certified Total Activity otl > 0:09.33 Ci
Which Eauals
r: "'2.071E+oSldpm at the date listed above
And after dilution the 11r;tivity ofthi'> solution h11 2;071E+02ldpmlml
This activity concentration is based on the original

reference date listed above. All actiVlties are corrected
Expiration Date:!
Date:
0to~r9,"2013
101912012 0:00
-------
Date: _
_,,__,_.,"1--.L'---
~EBE:Rht!':'c~ I QUALITY CONTROL PROGRAM

MP-009
Rev.8; 1/10/03
T\Ue: Radioactive Reference standards Solution& & Records

SECONDARY DILUTION RECERTIF/CAnoN
MP-009
Solution Reference# IPL 435'1042
PrinciDal Radionuclide
Half Life, Years
1'4o5E"'10!
. us" '2tti I
Datel . 111912012 0:00 I

. 1
Solutlon#I . .Th:{ib
Half Life, Dais
5.132E,.12!
I.
I .-::,:.
Radionuclide of lnteresd'C:'t2~""'1Th .
Parent Solution Conc.r 2:07E+o2 ldpmlml
Reference Date ,
Chemical ComDosltlon of Standard Solution

ITh(N0,}4 in 1% HNQ3 .. .-, .:': ... ' ' -. : . _. .
'
'
'
111111 ee:i o:oo I
. ..I
j1%N~rieAcid

Vol. Parent Solution: . soo;oooo ml
Total Activity: 1.0355!0+06 dpm
Final Volume: 1 . 1000.00 ml
1.0356E+o2 !dpm/ml

NOTES:
Expiration Date:
Verified & Approved
B~ \'i
QC Approval
~I lr 1 ..,,~ ~~
Date:
Date:
I . October 9, 2013 I
11/9/2012 0:00
h ,.., I1-t...
I
-~mJa
Isotope Products
Laboratories
An Eckert & Ziegler Company
lh-18
24937 Avenue Tibbitts

Valencia, California 91355
Tel 6613091010
Fax 6612578303
ALPHA STANDARD SOLUTION
Th-229
7340 160 years
7229
867-54
Radionuclide:
Half-life:
Catalog No.:
Source No.:
Customer:
P.O. No.:
Reference Date:
(Tb-229 only)
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST
1.013
Ci
37.48
kBq
Physical Description:
A.
B.
C.
D.
Mass of solution:
Chemical form:
Carrier content:
Density:
5.0147 gin 5 ml fiame-sealed ampoule

Th(N0 3 ) 4 in 0.1 M HN0 3
10g Th/ml
1.0016 g/ml @ 20'C.
Radioimpurities:
None detected (daughters in equilibrium)
Radionuclide Concentration:
0.2020 Ci/g,
kBq/g
7.474
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in Ci/g was determined
using gamma ray spectrometry.
Peak energy used for integration:

193.5 keV
Branching ratio used:
0.0441 gammas per decay
Uncertainty of Measurement:
A. Type A (random) uncertainty:
B. Type B (systematic) uncertainty:
C. Uncertainty in aliquot weighing:
D. Total uncertainty at the 99% confidence level:
0.7
3.0
0.0
3.1
%
%
%
%
Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
QualityTuntrol
Date Signed
IPL Ref. No.:
867-54
- - - - - - - - - - - - - - - - - - IS09001CERTIFIED - - - - - - - - - - - - - - - - -
Medical Imaging Laboratory
24937 Avenue Tibbitts
Valencia, California 91355
Industrial Gauging Laboratory
1800 North Keystone Street Burbank, California 91504

MP..009
Rev.8; 1/10103

MP009
CURRENT DATE .
11/9/2012 0:00
SOLUTION REFERENCE #'"'IP"'L-.s"'s7"'.;s"'"4'""..-._
__,,______.,..,
SOLUTION #r_.--.,,,,......T;;"h"'",.-;1s"_..:-.,-:."'"'-;
Half Life, Days
2.ea1 E+oel
Half Life, Years

1 7.34oe+o31
Radionuclide1 ~29fil"/I
Certified Activity " 1.013E+OO Ci
Certified Concentration .. > : " Ci per gram
Ampoule /Solution Gross
Empty Ampoule
Solution Net
1f15/200:2o:bol
Reference Datel
..

1.0130 Ci
Chemical Com osltlon of Standard Solution
Dilute to a volume of!
Certified Total Activity of
1000.00 milliliters
1.0130lCi
Which Eauals
2c249E+06ldpm atthe date listed above

This activity concentrlltlon Is based on the original
And after dilution the activity of this solution is 12.249E+o3ldpmlml reference date listed above. All activities are corrected
Expiration Date:
October 9, 2013
Date: --"'-11;.;./9""/2""0;...;1.;;;;2..;;0.;.;;:0.;;..0
Date:
11/rz/,z_
--"'+1'-"'-11=---
~E!O!.ERL,J_NE I QUALITY CONTROL PROGRAM

MP-009
Sl!Rv1ci;:s
Rev.7; 9/29/99
Title: Radioactive Reference Standards SOluUons & ReoordS

SECONDARY DILUTION RECERTIFICATION
MP..009
Solution Reference# IPLB6.7;;;i4 .
Princinal Radionuclide
Half Life, Years
' 229Th 71
7,34oE+o3
I .
Date I
11/9/2012 0:00 I
Solution llL :
Th..1Ba : ..:. -. I
Half Life, Dal'.:s
2.es1E+osl
. I
Radionucllde of lnteres1 ~
Parent Solution Cone. 2,25E+03 ;ldpmlml
Reference Date
Chemical Comnosition of Standard Solution

cc ... .. :..- .. >.._.: -:- .. '..'
ITH(N0,)41no.. 1MHN00 .. .
--. _,
1115/20020:001
'l
!0.1MHN03
....... ,
Vol. Parent Solution: . .. 10.0000 mt

Total Activity: . 2.2490E+04 dpm
Final Volume: .. 1000.00 ml
.
Flnal Activity Concentration:!
2.2490E+01 tdpmtml

NOTES:
Expiration Date:!

QC Approval
s:
,h;liJ"-; I t . L
~.
~
' J
October 9, 2013
Date:
11/912012 0:00
Date:
ul1~fr-2. . .
i r
Jlattonal 1Jnstttutc of
~tanl:Jarbs
&
~ttbnologp
<terttftcati
--...
Standard Reference Material 4251C

J3arium-13~ Radioactivity Standard
This Standard Reference Material.(SRM) consists of radioactive barium-133. cJ;i.l01:ide,..non-!adioactive barium

chloride, and hydrochloric acid dissolved iu 5 mL of distilled water. The solution is containedin a flame
sealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization' chambers and
solid-state gamma-ray,spectrometry.sy~tems.
Radiological Hazard
The SrovI ~mpoule contains barium-133 with 'a.total activity of approximately 2.5 MBq. Barium-133 decays
by electron capture and during .\lie decay process X-rays, and ganna;rays with energies from 4 to 400 ke V are
emitted. Most of these photons escape from the SRM ampoule and can represent a raiiiati<:m hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be used to minimize. personnel exposure.. :.The .SRM should be
~sed, only by persons qualified to han'!le radioactivtmaterial.

II
'
I
I
I
Chemil:lll Ha;.;rd
The SRM amp011le c_ontain.s hydr~chloric acid (HCi) with a concentration of l mole per liter ,of .water. The
solution is corrosive and represents a health hazard if it comes in contact with.eyes or skin,, If the ampoule
is to be opened to transfer the solution, the recommended procedureis given on page 2. The ampoule should
be opened only by persons qualified.to hanclle both radioactive material and strong acid solution.
Storage and Handling
The SRM should be stored and used at a temperature between 5 and 65 C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by L.L. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.

The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standard Reference Materials Program by N.M. Tralley.
Gaithersburg, Maryland 20899
October 1994
Thomas E. Gills, Chief

Standard Reference Materials Program
Ii
I
i .
iI
i
I
I
I
SRM. 4251C,wge.1of6
*Notes and references. are. on pages.~ and 6.
'
I'
l'
i.
I
I

QCP.009
Rev.B; 11/10/03
rrtte: Radioactive Reference standards Solutions & Records


QCP 009-1
CURRENT DATE
611612013 0:00
SOLUTION REFERENCE #"'N"'.1s==r"'$"'R"".M"'.4"'25""J"'c""":.(""':;.,. ,:.:"".::"":\""'"
SOLUTION # \:'\:::>:Wii\Bl!i$/i:. , hi .
Princi al Radionuclide
Half Life, Days
Half Life, Years
I
:
$.82$E+O$I
1~eari6mi
1'1 1:d46Ef011
Reference DateV/Y'"f.
91fN!laa>oiool
Ampoule /Solution Gross \\i$::6Pl3t Weight, Grams

Empty Ampoule '''<Cif2582 Weight, Grams
Solution Net .5.04$9 Weight, Grams
Total Activity in Ampoule .:.: 66.557'.7 Cl
1MH e1
': .:. :.....: :.,.,.

:t ..,..:.,:. .. : .. :.,.)
Dilute to a volume ofh\ f1ooo;oo<:<Ulmilliliters
66.55771 Ci
Which Eauals l
1A76E+08Jdpm at the date listed above

And after dilution the activity of this solution isl 1.478E+05ldpm/m1 reference date listed above. All activities are corrected
proce5sing software.
Expiration Date:I : June 16, 2014
Date: ---'7"-/1.;,;./.;.;13;;..___
Date: _ _ _'J.yl-"'~"'1,_:3.___
I .
I!.
mmil:!
Rev.8; 11110103
T'rtle:
Radioactive Reference standards Solutions & Records

SECONDARY DILUTION RECERTIFICAnON
QCP--009-1-A
Solution Reference #INISJYSRM4251C'<'c??\ ''I
Princioal Radionuclide
Half Life, Years
Dater 6118113.. .. J
Solution #l;;;;e.,;;,,..:,ea'6a/''\''.'\;,.d
Half Life, Days
r :/1!o41iE:ii'1i'1J
i.!c1~Ba\{J
ll
Radionuclide of Interest !,\ji:'.A.~EiaA\'i.{f

Parent Solution Conc.F.';1\1A6Ef0$'C}ldpmlml

Vol. Parent Solution: 'Y{'.\\25JOllilP ml
Total Activity: '.3.695QE+06 dpm
Final Volume: :,'''}'!\'51llMillP ml
Final Activity Concentration: J' ' , 3J39?QE,..03Jdpm/ml

NOTES:
Expiration Date:J
June 18, 2014
Date; ---'-7"'11"-11'-'3'"--
QC Approval
Ii
Date:
'1}:L-l I~
--+-,
-~---
CERTIFICATE OF CALIBRATI
ALPHA STANDARD SOLUTIO
Radionuclide:
Half Life:
Catalog No.:
Source No.:
Ra-226
1600 7 years
7'126.
453-26
Description of. Solution

b. Chemical form:
c. Carrier content:
d. Density:
Initials-
Customer:
TMA EBERLINE
VH1888
P,O.No.:
Reference Date:
February 1 1994
12,QOPST.
Contained Radioactivity: (Ra-226) 1.001 !'Ci.
37.0 kBq.
Contained Radioactivity: (Ra-226)
5.1864 g (in a 5 ml Flame Sealed Ampoule)
Ra(N03)2 in 1 N HN03
None added
l.0318
Radioimpurities
glml @2oc.
None detected(other thah daughters)
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Ph-210, Bi-210, Po-210 and Tl-206.
Radionuelide Concentration
(Ra-226) . 0.1929
.,... .Cilg.
Weighed aliquots of the solution were assayed using ganuna spectrometry:
Energy peak(s) integrated under: 186 keV.
Branching ratio(s) used:

0.0351
gamma rays per decay.
3.4%
3.1%
0.2%
4.6%
NIST Trnceability
This calibration is implicitly traceable to the Natinnal Institnte of Standards anli Technology.
Leak Test(s)
Notes
1. Nuclear data were takCn "ftom "Table of Radioactive Isotopes", edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement 8ssurance program to eStablish and maintain implicit traceability for a num~r of nuclides,
" .-based on-the'blirl.(1""8.SS'ilY(aDd"litef NIST-"CemfiCis:tiODJ "OfStiDdafd "'llefeioii)ilC<fMiiterialS\AS"ill 'NRC "RCgiilitOfy""Gliide-4; r5) ~ .. ... -
QUALITY CONTROL
fi,I,. ~I 199 !f
Date Signed
1800 North Keystone Street
818 843 - 7000
~EEIERLINI;;; I

MP009
Se':RVIC1':S
Rev.8; 11/01/03
Tiiie: Radioactfve Reference Standards Solutions & Records
.

MP009
SOLUTION REFERENCE #llPL 453;25 . ...
Prlncioal Radionuclide
Half Life, Years
~~Radium I
. 1.60llE+o31
..
CURRENT DATE!
1119/2012 0:001
SOLUTION #I \ .. .. 'Ra-5 . . . I
I
Half Life, Daxs
I ... 5.B44E+osl
Reference Datel . ... .. ..211i1!i94 o:ooj
Radionuclide ...?'Radium :
Certified Activity
1'.0.0.1 E+oo Ci
.... : Ci per gram
...
.,, ,.,. ,..,.,.. .
~~~~r
. .
Empty Ampoule . . : : Weight, Grams

Solution Net
Weight, Grams
1.0010 Cl
Chemical Comeosition of Standard Solution
.,:.::.:;:'
,~~~Ra(N03J2 in 1M}INO~ ...
I
.
Dilute to a volume of! 1000.00.
Certified Total Activity of!
1.0010lCI
j1M'HN03
Imilliliters
Which Eauals \
. 2.222E+06\dpm at the date listed above
And after dilution the activity of this solution isl 2.222E+03ldpmlml

reference date Usted above. All activities are corrected
Expiration Date:! November 9, 2013

QC Approval
~:W:\
Date:
Date:
11/912012
If 1i-l1?
Rev.6; 11/01/03

SECONDARY DILUflON RECERTIFICATION
Date!. . 11/912012 0:001

Solution #10'.\'.k:,:,;,:.a.~o5.t\\i.%"i\(d
Half Life, Days
MP009
PrinclPal Radionuclide
Half Life, Years
lk'"Weooec?o.31
~Radium' I
I. < 5:a44e+osl
Radionuclide of Interest :.:~ftiiaiilmJ

Parent Solution Cone. .7:'.2;22E'!'0.3.' !' dpm/ml
Dilution Solve.nt Used

' '<i'}:2o:ooocr
Vol. Parent Solution:

ml
Total Activity: I : '4.4440E+04 dpm
Final Volume:. '>:>!<looa'.00, ml
I :.'
'4.4440E+01 Jdpm/ml
Final Activity Concentration:
reference date listed above. Ali activities are
NOTES:
Expiration Date:f November 9, 2013
~__,...-,.-..,..;:1---lh~l>1~r-----
Verified & Approved By _ _
QC Approva1 _--<,<.,,L.LJi,,!!.!1Ull!IJI':it:lulr...y.U_"-.:::0....,\._ __
Date:
Date:
11/9/2012 O:OO
''
/iz. f Z-
Rfi.-\\
ANALYTICS
1380 Seaboard Industrial Blvd.

Atlanta, Georgia 30318 U.S.A.
Phone (404) 352-8677
Fax (404) 352-2837
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
Ra-228
ACTIVITY (dps) :
2.585 E3
HALF-LIFE:
5.75 years
CALIBRATION DATE:
November 7, 2001 12:00 EST
TOTAL UNCERTAINTY*:
4.0%
SYSTEMATIC:
3.0%
RANDOM:
1. 0%
*99% Confidence Level
Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams O.lM HCl solution with 50 g/g Ba carrier.
P 0 NUMBER
9508, Item 1 (Part #4339A)
SOURCE PREPARED BY:
Q A APPROVED:
M,/(f,i~mi<

MP-009
Rev.8; 1110103
Title:

RECERTIFICAT/ON
MP009
CURRENT DATE
SOLUTION REFERENCE #""Ari"":"'"'ai""Y!""i"":s:"':e2"'.68""
. "'o"4""'.."'. l$=-.""'r""';,;,...,,..,.,,"(
SOLUTION #
Half Life, Years
$11.112013.0:00
J>S'i's:7stiE't061
Radionuclide . 8,~e~~i@\/i
Certified Activity ?;)9XS8$t:;oz Ci
Ci per gram
Reference Dateh
...
iIOQEfo3J
\:'.~'1/ti~ood1oltiol
Ampoule /Solution Gross !\VS''!lc;4S~2 Weight, Grams

Empty Ampoule <<:J;::4;ila9$ Weight, Grams
Solution Net , . >.5:0087 Weight, Grams
Total Activity In Ampoule
0.0699 Ci
Chemical Com ositlon of Standard Solution
. Dilution Instructions:
Dilute to a volume ofJ\'fjQO.O::OO'i' ;!milliliters
Certified Total Activity of!
Of0699J Ci
Which Equals
I<' > '1551.Etli5ldpm at the date listed above
And after dilution the activity of this solution isl1;551E+02ldpm/ml
This activity ccncemration is based on tho original

reference date listed above. All activities are corrected
Expiration Date:!
Date:
March26; 2014 1
__
5/30/13
...;.;"""'----'--
SECTION VI
QUALITY CONTROL SAMPLE RESUL TS SUMMARY
Eberline Services
Analysis Control Chart
Printed: 7/26/2013 9:48 AM

Page 1 of 2
WO
A-na1ysis
Run
13-07098
UUISO
Activil:t Units
_Aliguot Units
<?.!!~nt Name
pCi
Laboratory Control Sample

Analyte
Normalized
Difference
LCS
Measured
CSU
Measured
0.45
96.39o/o
15.001o
Uncert.
Expected
Known
Known
Em>
Result
CSU
Standard
ID
100.00%
3.60%
8.18E+OO
2.95E.01
7.89E+OO
1.26E+OO
U-Sa
3.52E+01
3.60E+OO
5.16E-01
100.00%
3.60%
7.98E+OO
2.87E-01
7.96E+OO
1.27E+OO
U-8a
3.44E+01
3.60E+OO
5.16E-01
Sample
Result
Sample
CSU
Sample
Aliquot
Standard
Standard
Error%
Standard
Added(g)
Rep RPO
Rep ND
OK
OK
NA
OK
NA
OK
LCS
Expected
Standard
ACT(dpm)
Standard
Error
Standard
Added (g)
U-234
U-238
99.85%
0.02
15.96/o
Matrix Spike
Normalized
Difference
Analyte
MS Actual
%Rec
Expected
MS Result
Expected
MSUncert
Actual
MS CSU
Actual
MS Result
U-234
U-238
Normalized
Difference
RPD
Original
Result
'
Original
CSU
I
I
Replicate
Result
Replicate
CSU
LCS Relative
Bias
LCS%R
0.25
200.00
I O.OOE+OO
4.37E-01
5.96E-02
1.63E-01
0.96
OK
1.12
118.49
4.44E-01
5.58E-01
1.14E-01
1.59E-01
1.00
OK
'
LCSND
tt~I
a!!i
t,11
~-.4.
Version
1.09
272.04
-3.31E-02
3.87E-01
2.17E-01
2.27E-01
OK
MS%R
MSND
OK
OK
I
U-235
Standard
ACT(dpm)
QC Summary
Replicate Sample
Analyte
ID
OK
Eberline Services
Printed: 7/26/2013 9:48 AM

Page 2 of 2
WO
Analysis
Run
Activity Units
13-07098
UUISO
pCi
Aliquot Units
Client Name
Replicate Sample RPO
LCS % Recovery
130.00
--------.--
120.00
40.00
35.00
110.00
3000
100.00
2.5.00
20.00
90.00
15.00
ao.oo
10.00
U-234
76.79
115.99
96.39
80
100
120
Lower Error
Uooer Error
%R
-LCL
---Mean
1-
-UCL
5.00
U-238
80.29
119.40
99.85
80
100
120
-CL
1-
U-L.)'I
u-~38
1207.24
-807.24
200.00
35
194.65
42.34
118.49
35
..
Normalized Difference
No Matrix Spike
3.50
3.00
2.50
2.00
1.50
1.00
0.50
000
1!!!!!!!!!!!11! U-234
~U-238
-,
UCL
t:l1
t;l~I
Ll1
r~,~
Version
LCS NO
0.45
0.02
0.00
3
REP NO
0.25
1.12
MSND
0.00
0.00
o.oo
0.00
U-235
726.73
-182.64
272.04
35
Eberline Services
Printed: 811120131:47 PM
Page 1 of 2
WO
Ari81ysis
Run
13-07098
UUISO
Activ~ Units
Ali_guot U_o_l_t,_ _ __,____
pCi
Client Name

Normalized
Difference
LCS
Measured
CSU
Measured
LCS
Expected
Uncert.
Expected
U-234
0.41
104.16/o
1s.a21o
100.00/o
3.60%
U-238
0.60
3.60%
Analyte
94.39%
19.18%
100.003
Known
8.02E+OO
7.82E+OO
Known
E=r
Result
- f
'
Standard
""'~ I ...,,~
~.38E+OO
2.82E-01
CSU
1.42E+OO
Standard
ACT(dpm)
ID
3.52E+01
U-8a
U-8a
Standard
E=r
3.44E+01
3.60E+OO
Standard
Added(g)
I 5.05E-01
I 3.60E+OO I 5.05E-01
'
Matrix Spike
Analyte
Normalized
Difference
I
,
MS Actual
% Rec
I
j
Exp0<td
MS Result
+--
---t-
I,
Expected
MS Uncett
Actual
MS CSU
Actual
MS Result
'
.
Sample
Result
Sample
CSU
=t=
U-234
U-238
U-235
j~~I
~jl
lJ1
1:.~
Version
RPD
Original
Result
1.33
100.96
5.99E-01
1.53
635.14
Normalized
Difference
0.14
13.93
Standard
ID
Standard
ACT(dpm)
Standard
Error%
Standard
Added {g)
RepRPD
Rep ND
. -+
QC Summary
Replicate Sample
Analyte
Sample
Aliquot
Original
Replicate
CSU
Replicate
Result
5.11 E-01
1.97E-01
I
i 3.03E-01
-8.85E-02
1.70E-01
2.90E-01
3.16E-01
4.42E-01
2.75E-01
LCS % R
LCS Relative
Bias
CSU
LCS ND
1.04~+0K
1.61E-01
3.73E-01
0.94
OK
~-~
I
'
MS%R
MSND
NA
NA
OK
-OK
NA
OK
OK
OK
Eberline Services
Printed: 8/1/20131:47 PM
Page 2 of2
WO
Analysis
13-07098
UUISO
Run
Activit~-~nits
pCi
__________ g~~!!1._cN~a~m~e~_ _ _ _ _ _ _ _ _ _
Aliquot Units
LCS % Recovery
130,00
40.00
120.00
35.00
\t0.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
70.00
Lower Error
=---.__!deeerError
~-
I - -LCL
fy'lean
1 - -UCL
U-234
U-238
81.74
126.58
71.61
117.1~,------
104.16
80
100
120
94.39
80
100
120
5.00
o.oo t-----~~-c------,-----ccc=----U-L;:!4
Lower Error
Uooer Error
1-
RPD
-CL
152.58
49.34
100.96
~-
u-238
2394.28
- -1124.01
635.14
35
No Matrix Spike
3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00
0.41
c:::::J U-238
0.60
0.00
3
UCL
i;1j1
Si!
Ul
11~,
Version
MS ND
LC:-; N
~U-234
1.33
1.53
0.00
0.00
o.oo
3
0.00
U-235
23.54
4.32
13.93
35
Eberline Services
Printed: 712612013 9:33 AM
Page 1 of 2
WO
Analysis
Ron
Activity Unit~
13-07098
Th ISO
pCi
Cli~f'!! Name
Aliquot Units
----I

Nonnalized
Difference
LCS
Measured
CSU
Measured
LCS
Expected
Uncert.
Expected
Known
Known
Error
TH-228
0.77
107.78%
18.25%
100.00%
3.60%
4.88E+OO
1.76E-01
TH-230
0.67
93.56o/o
20.00/o
100.00%
2.70%
5.47E+OO
109.61%
17.89%
100.00/o
4.88E+OO
Analyte
TH-232
0.95
3.60o/o
CSU
Standard
ID
5.26E+OO
9.60E-01
Th-8b
1.48E-01
5.12E+OO
1.02E+OO
1.76E-01
I 5.35E+OO I
9.57E-01
Sample
Result
Sample
CSU
Sample
Aliquot
Result
'
Standard
ACT(dpm)
Standard
Error
Standard
Added (g)
1.04E+02
3.60E+OO
1.05E-01
Th-1b
2.35E+01
2.70E+OO
5.16E-01
Th-8b
1.04E+02 ; 3.60E+OO
I 1.05E-01
Matrix Spike
Nonnalized
Difference
Analyte
MSActual
%Rec
--!-
Expected
MS Result
Exp<ted
A<luI
Actual
MS CSU
Nonnalized
Difference
RPD
Original
Result
Standard
Standard
ACT(dpm)
ID
Standard
Error%
Standard
Added (g)
QC Summary
Replicate Sample
Analyte
Original
CSU
Replicate
Result
LCS Relative
Bias
Replicate
CSU
LCS%R
LCSND
MSND
MS%R
RepRPD
Rep ND
TH-228
0.25
200.00
TH-230
0.34
31.35
TH-232
IJi!I
~I
IJ11
Version
0.56
104.08
1.21E-02
5.65E-02
1.02E-02
6.59E-02
7.05E-02
3.13E-02
O.OOE+OO
6.92E-02
1.08
OK
OK
7.74E-02
9.99E-02
0.94
3.24E-02
7.03E-02
1.10
OK
OK
OK
OK
OK
NA
OK
NA
OK
+OK
Eberline Services
Printed: 7/26/2013 9:33 AM
Page 2 of 2
WO
Anal~~
13-07098
Th ISO
"""
Activity Units
Aliauot Units
Client Name
pCi
LCS % Recovery
130.00
40.00
-------------..iUCL
120.00
35 00
110.00
30.00
100.00
25.00
20.00
9{),00
15.00
-------LCL
60.00
10.00
~
10.00
Lower Error
_!dp_P._er Error
1
-
%R
-LCL
---Mean
1-
-UCL
TH-228
85.94
129.63
107.78
80
100
120
-
--
on-..:..:>u
TH-232
70.86
116.26
93.56
80
100
120
68.12
131.09
109.61
80
100
120
5.00
0,00t------------~----~~~-----~----~cc------~
Lower Error
Uooer Error
+ RPD
-CL
TH-221:1
1313.82
-913.82
200.00
3s
IH-230
51.30
11.40
31.35
35
No Matrix Spike
3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00
li!!!!!!!!!!!!!!TH-226
ic::=:lTH-230
UCL
l!ll
ft~I
Ul
I))
Version
LCSND
REP ND
MS ND
0.77
0.25
0.34
0.00
0.67
3
0.00
3
TH-232
228.19
-20.02
104.08
35
Eberline Services
WO
Printed: 7/25/2013 8:13 AM
Page 1 of 2
/-----
Analysis
Ra226
13-07098
Run
Activlty_Units
pCi
Aliquot Units
Client Name

Nonna1ized
Difference
Analyte
LCS
Measured
' = ' mm
CSU
Measured
'
LCS
Expected
Uncert.
Expected
~ ' '"""~ '
Known
r~~"'
Known
Error
Result
CSU
4.74E-01
1.07E+01
2.57E+OO
Standard
Standard
ACT(dpm)
ID
Ra-5b
Standard
Error
4.41E+01
Standard
Added (g)
4.60E+OO
5.19E-01
---f----f------1
_ _ ___,
Matrix Spike
Normalized
Analyte
Difference
MSAr:tual
%Rec
Exper:ted
MS Result
Exper:ted
MS Uncert
Actual
MS Result
Ar:tua/
MS CSU
Sample
Result
Sample
CSU
RA-226
lfi.il
~~
t..l'l
1,~.JI
Version
Normalized
Difference
0.76
RPD
23.69
Sample
Aliquot
Standard
ID
-+-~
Standard
Error%
II
Standard
Added(g)
QC Summary
Original
Result
1.37E+OO
Standard
ACT(dpm)
1--t
Replicate Sample
Analyte
Original
CSU
Replir:ate
Result
5.97E-01
I 1.0SE+OO
Replir:ate
CSU
I 4.53E-01
LCS Relative
Bias
1.03
LCS%R
OK
LCSND
OK
i
I
MS%R
MSND
RepRPD
Rep ND
NA
OK
Eberline Services
Printed: 712512013 8:13 AM
Page 2 of 2
WO
Analysis
Ruo
Activity Units
13-07098
Ra226
pCi
A!i.9.~-~~.l:J..r:!~ts
Client._t~am"e~------------1
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
100.00
25.00
20.00
90.00
15.00
80.00
1000
70.00+-----------------------------------~
"""
RA-226
74.66
132.17
103.42
80
100
120
Lower Error
Uooer Error
%R
r - -LCL
---Mean
-UCL
o.oo
RA-226
Lower Error
Uooer Error
28.77
18.61
RPO
23.69
,_-CL
35
3.50 - - - - - - - - - - - - - - - - - - - - - - - - - -
3.00
2.50r-----
2.00+----
1.50
-!--------------
1.00
+-----
0.50 + - - - - - - - - - -
0.00
!!!!!!!!!!!!!!! RA-226
UCL
llElJ
tl:E.ll
I.JU
!;)(Ji
Version
LCS ND
REP ND
MSND
0.27
0.76
3
0.00
No Matrix Spike
Eberline Services
Printed: 815/2013 10:19 AM
Page 1 of 2
WO
Anal}/sis
13-07098
Ra228
R~o
A9;~~o;ts
Aliqi.Jiif Units .
Client N~!!'~.--------

Normalized
Difference
Analyte
'
LCS
Measured
LCS
Expected
CSU
Measured
Un cert.
Expected
Known
Known
Result
"'""
Standard
CSU
'~ I "'~ I '~,;,_, ''~- ~~oo I " " " I 'M~"' I =~o I ~"
'
Standard
ACT(dpm)
ID
'''".'"'
Standard
Error
Standard
Added (g)
''"~"'
5.1BE01
Standard
Error%
Standard
Added (g)
'
Matrix Spike
Normalized
Difference
Analyte
MS Actual
%Rec
+- '
Expected
MS Result
Expected
MSUncert
Actual
MS Result
Actual
MS CSU
Sample
Result
Sample
CSU
Sample
Aliquot
_l + +
Standard
Standard
ACT(dpm)
ID
.i_:_T-1
+--
QC Summary
Replicate Sample
Anatyte
~228
Normalized
Difference
RPD
+2~5.3.52
----t1--1
i
Ci~~
~i~
IJ1
l~ll
Version
Original
Original
Result
CSU
Replicate
Result
5.20E+OO
1.32E+OO
3.00E+OO
Replicate
CSU
LCS Relative
Bias
LC5%R
8.11E01
1.20
OK
-t -
LCSND
OK
MSND
M5%R
-+
RepRPD
Rep ND
+~H
1..
'
NA
OK
Eberline Services
Printed: 8151201310:19 AM
Page 2 of 2
______cAcncacl<y,_;_,__
WO
13-07098
Ra228
Run
Activity Units
pCi
.--
Aliquot Units .
Client Name
LCS % Recovery
130.00
40.00
120.00
35.00
110.00
30.00
25.00
100.00
20.00
90.00
15.00
80.00
10.00
10_00
Lower Error
Upper Error
,_oo
RA-228
90.45
-~1'48'.~5~6------
%R
RA-228
119.50
-LCL
---Mean
1-
0.00
-UCL
60.47
Lower Error
- 46.58
U""er Error
RPO
CL
53.52
35
No Matrix Spike
3.50
3.00
2.50
2.00
1.50
1.00
0.50
0.00
-RA-2281
UCL
,~
i
t~
I!:!
m
~~
Version
LCSND
REP ND
MS ND
1.33
2.78
0.00
SECTION VII
LABORATORY TECHNICIAN'S NOTES
ISOUNOTES
Run 1
Printed: 7/1912013 8:47 AM
Page 1 of 1
~EBER~~~c~
Work Order Analysis Notes
#
1
Date
07/19/13 08:47
Dept
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com
Internal Work OrQer

Analysis Code
13-07098
UUISO
1
Run Number
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES DOWN-ADDED HN03 TO
PRESERVE SAMPLES EXCEPT FOR FRACTIONS 5, 8, 13, 14, 17 AND 18- THESE FRACTIONS WERE
ALREADY PRESERVED
,l. J,I ~
qiiY
Printed: 7124/2013 5:46 PM
Page 1 of 1
~EBERl._.INE
SERVICES
Date
Dept
07/19/13 08:47
PREP
JWOLFE
07/24/13 17:46
CHEM
JDEMELAS
User

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
UUISO
1
Notes
PRESERVE SAMPLES EXCEPT FOR FRACTIONS 5, 8, 13, 14, 17 AND 18-THESE FRACTIONS WERE
ALREADY PRESERVED
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml 8N HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml 8N
HCl, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI - 0.1 N NH41, 35 ml
of 6.SN HCl - 0.04N HF, and 10 ml of 6.SN HCI; Eluted Uranium with 50 ml of a.SN HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with DI H20. Set samples aside for later precipitation and filtering.
Printed: 7/25/2013 6:06 AM
~
#
1
~--
Page 1 of 1
E:: !;;!_I:: R-~.-t!:':'le~

Date
07/19/13 08:47
Dept
PREP
" 6712471317:46 -------CHEM
07/25/13 06:06
CHEM
User
JWOLFE
--JDEMELAs____
RMARTZ
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
--....
----
Analysis Code
Run Number
13-07098
UUISO
1
Notes
PRESERVE SAMPLES EXCEPT FOR FRACTIONS 5, 8, 13, 14, 17 AND 18- THESE FRACTIONS WERE
ALR_~.QY ~~ESERVED
__
-
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml SN HCL to samples and
transferred to new, labeled C-Tubes, rinsing with SN HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml SN HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml SN
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml SN HCI- 0.1N NH41, 35 ml
of 6.5N HCI - 0.04N HF, and 10 ml of 6.5N HC!; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES
FROM C- TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
Printed: 7/25/2013 6:07 AM
Eberline Analytical
Page 1 of 1
.:::.. a
Reagent
Name
014109P
Nitric Acid
014076P
Anion Exchange Resin

-
HCI - HF
014101S
Analysis Code
Hydrochloric Acid
--
-
1
Analyst
ID
Reagent
.. Concentration
-
Run
UUISO
Reagents Used in an Analysis
ID
014127S
13-07098
i:;:: ~ ~!ii~c:Fi
Reagent
.
Internal Work Order

---
-
--~~---
Date
Recorded
Reagent Grade
JWOLFE
7/19/2013
Reagent Grade
JDEMELAS
7/24/2013
6.5N - 0.04N
-
0.5N
JDEMELA5
7(24/20131
JDEMELAS
7/24/2013
JDEMELA5
7/24/2013
JDEMELA5
7/24/2013
JDEMELAS
7/24/2013
0139S5S
Hydrochloric Acid
6.5N
0141605
SN
013S96P
Hydrochloric Acid
--
Hydrochloric Acid
0141755
HCI - NH41
Reagent Grade
- ' --M
SN - O.lM
JDEMELA5
7/24/2013
0140425
----
Carbon substrate
Solution
RMARTZ
7/25/2013
013221P
Hydrofluoric Acid
Reagent Grade
RM ARTZ
7/25/2013
013191S
Neodymium Carrier
1 mg/ml
RMARTZ
7/25/2013
013574P
Reagent Alcohol
Reagent Grade
RMARTZ
7/25/2013
013434P
Titanous Chloride
Reagent Grade
RM ARTZ
7/25/2013
r--:~
..~ "
l.AA"\.1
ti:)/)~
-,
'
I -
.
I,.,..,
I I I -'
1"J.n -J Hf-A. { /-1.r

,
'
t:~,.; . fV! O.""-;?i <.,,
ffl.::
I(
fl :in;~
Ur._..
1~oc.
'IL...-._.......
, ..,., \I
2- h_.,-'S,l) --.:
~~
.
(l
,.
'11 "l '01 ., f '1. ,,-,. "(atH 1-'.J}

.:j/l.6)1'J l3o-:k:A \,)A- C1-1"')
,/
./
~txU_.,., 1. J'"/... I
..-l.
'
45
'
. .
Arvt-l-41
..
'
rfG~.l
~
(_,
.. _
.
u....v-.. \U7
A
'
'
.
'
.
'
..
'
'
'
..
..
.
--o.-e,,
-'"
"''"''
I'
_.~--0~~--'
,.-_,.,_,._--
...ii1
.
""
'
...
"1';.-.il'i...,,,,.,..
~~~I
ISOUNOTES
Run2
Printed: 7/29/201312:24 PM
Page 1 of 1
~E;. .
B ERLINE
SERVICES
Date
07/29/13 12:24
Dept
PREP
User
JWOLFE
601 Scarboro Rd.

Oak Ridge, TN 3 7830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
UUISO
2
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS-ADDED HNQ3 TO PRESERVE SAMPLES- DRIED
SAMPLES DOWN
_d~~),,
I
I
I
I!
I
!
Page 1 of 1
Printed: 7/31/2013 4:41 PM
~
E
~
E3E::RLI NI;;
SERVICES
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
UUISO
2
#
1
Date
Dept
07/29/13 12:24
PREP
JWOLFE
ALIOUOTED AND ADDED SPIKES AND TRACERS- ADDED HN03 TO PRESERVE SAMPLES- DRIED
SAMPLES DOWN
07/31/13 16:41
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to dryness; Added 20 ml SN HCL to samples and
transferred to new, labeled C-Tubes, rinsing with SN HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml SN HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml SN
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml SN HCl- 0.1N NH41, 35 ml
of 6.5N HCI 0.04N HF, and 10 ml of 6.5N HC!; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HC1; Transferred to
User
Notes
7(31//3
Printed: 8/1/2013 6:14AM
~
#
1
!;
Page 1of1
e::e~R.h~~'~
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Date
Dept
07129113 12;24
PREP
- 2 . ---------07131113 16:41
~----
CHEM
User
JWOLFE
---------""-------
JDEMELAS
'
Internal Work Order

............
--"'""
--
Analysis Code
Run Number
- .. ----"""'
13-07098
--------""'"
UUISO
- -
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- ADDED HN03 TO PRESERVE SAMPLES- DRIED
SAMPLES DOWN
---Add9d concentrate-Ci"HC! to sampiebeai<ersan-r.rheated
todrYnSSS; Added 2om1-SN"'"HC-ctosamp1esand-----
transferred to new, labeled C-Tubes, rinsing with SN HCI to bring volume to -35 ml; Preconditioned resin
columns with 35 ml SN HCl; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 ml SN
HC!, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml SN HCI - 0.1 N NH41, 35 ml
of 6.5N HCl - 0.04N HF, and 10 ml of 6.SN HCI; Eluted Uranium with 50 ml of 0.5N HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCl; Transferred to
3
08101113 06:14
CHEM
RMARTZ
ADDED 0.1 ML NEODYMIUM CARRIER, 0.3 ML TITANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET
SIT IN ICE BATH FOR ONE HOUR SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM.
<la"'
Eberline Analytical
I
Ii
I
1--
I
!
--
Printed: 8/1/2013 6:14 AM
Page 1 of 1
Internal Work Order
13-07098
E:J? I;; R h 1R~C~
Analysis Code
UUISO
Run
----~-
Reagent
ID
Reagent
Name
Reagent
Concentration
Analyst
ID
-w
014076P
014142P
Hydrochloric Acid
0141965
Hydrochloric Acid
--
Reagent Grade
JDEMELAS
Reagent Grade
SN
JD EMEL.AS
-
JD EMEL.AS
f-----
0142065
HCI - NH41
SN - 0.1M
JD EMEL.AS
0142045
HCI - HF
6.SN - 0.04N
JD EMEL.AS
0141995
Hydrochloric Acid
6.SN
JDEMELAS
014142001
Hydrochloric Acid
O.SN
JD EMEL.AS
0140425
Carbon substrate
Solution
RMARTZ
..
1----------------
'
:---
..
--
7/31/2013
- - - - -
7/31/2013
-
7/31/2013
7/31/2013
7/31/2013
-- ----
~013._
S/1/2013
Hydrofluoric Acid
0131915
Neodymium Carrier
1 mg/ml
RM ARTZ_.,_.,_.,.,._,_________ . S/1/2013
RMARTZ
S/1/2013
013574P
Reagent Alcohol
Reagent Grade
RMARTZ
Tita nous Chloride
Reagent Grade
013221P
:;;-.i ~ Grade
r---~----------
7/31/2013
'
Date
Recorded
-----~-~-------
tc;13;;34f>
w------w
~-----
w----
-~--------
RMARTZ
---
S/ 1/~~-1-~__j
S/1/2013
J-
'4J
'~--
Q,~
(\
9:/1//:...
<bl ff/'\
'
"
,::... VY\
~~H-t
~
J
I'? O
r~
~/Lt~,,,,_.,\
f'1.\) "zt.11
Al
I~,-
" ...,,,i":." .
O'J1.r
091&.
L.. . . !
I...,...._
'
47
'
0-r' ~
\I
' ,J;;,,.,/
'
- 1~L-"I ? I::i...h..-~mln~
ri / - , ; (
l (,..
n ru<;
-iL..
/ "1, ..-z_" 'i 'le' >'l , I"
@> ({/1"1
"
/j_'L<- 0.
~
.n.p.~
~'7 II 1"\. 1 '"1..'~a. \I.'._./\ ( 1-'l.J

<1J //(;;.,
x._ .
\cf,
.., r ..-,
}?4"
<
I '!.,_....,_
....__
L.u,_.,..
...., LV-
c:._.
...
.,
'
-_
.,
'
..
..
..
'..
"'i\,
_.,
-----''
--.-
'
. -_-.
'-"
....
.
'.
.. l
ISO TH NOTES
Printed: 7/19/2013 8:47 AM
~I;: B
Page 1 of 1
i:;::_F:;!J.....
lN..i:::::
SERVICES
Date
Dept
07/19/13 08:47
PREP
User
JWOLFE
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Werle Order
Analysis Code
Run Number
13-07098
Th ISO
1
Notes
PRESERVE SAMPLES EXCEPT FOR FRACTIONS 5, 8, 13, 14, 17 AND 18-THESE FRACTIONS WERE
ALREADY PRESERVED
Printed: 7124/201311:26 AM
~
#
1
--
Page 1 of 1
E;J3 ER ~R!';'IC~
Date
Dept
07/19/13 OS:47
PREP
User
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
-
Analysis Code
Run Number
13-07098
----
Thi SO
1
Notes
JWOLFE
PRESERVE SAMPLES EXCEPT FOR FRACTIONS 5, S, 13, 14, 17AND1S-THESE FRACTIONS WERE
ALREADY PRESERVED
----- ---CHEM --- --------- ----------
-
. --PRECONDITIONED RESlNCDLUMN-WITH 50 ML BN HN03 &CENTRIFUGED SAMPLES; ADDED
07/24/1311:26
RMARTZ
SAMPLES TO COLUMNS; AFTER SAMPLES RAN THROUGH THE COLUMNS, ADDED 40 ML SN HN03 &
LET RUN THROUGH, & ELUTED SAMPLES WITH 50 ML SN HCL INTO CLEAN 1DO ML BEAKERS. TOOK
SAMPLES TO DRYNESS ON HOTPLATE & ADDED 10 ML CONCENTRATED HCL TO SAMPLES;
TRANSFERRED SAMPLES INTO C-TUBES WITH DJ. H20.
~-ti77
Page 1 of 1
Printed: 7125/2013 6:05 AM
E _ _ a _ l:;;._R'"b-~~c-~
601 Scarboro Rd.

Oak Ridae1 TN 37830
Voice: 865.481.0683

I
Date
'
'
Dept
User
PREP
JWOLFE
07/24/1311:26
CHEM
RMARTZ
07/25/13 06:05
CHEM
RMARTZ
07/19/13 OS:47
Internal Work Order
13-07098
.... -------- ----- .. ------- - .. -Analysis Code
Run Number
-----
------
Th ISO
1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- DRIED SAMPLES OOWN- ADDED HN03 TO
PRESERVE SAMPLES EXCEPT FOR FRACTIONS 5, S, 13, 14, 17 AND 1S- THESE FRACTIONS WERE
ALREADY PRESERVED
PRECONDITIONED RESIN COLUMN WITH 50 ML SN HN03 & CENTRIFUGED SAMPLES; ADDED
SAMPLES TO COLUMNS; AFTER SAMPLES RAN THROUGH THE COLUMNS, ADDED 40 ML SN HN03 &
LET RUN THROUGH, & ELUTED SAMPLES WITH 50 ML SN HCL INTO CLEAN 100 ML BEAKERS. TOOK
SAMPLES TO DRYNESS ON HOTPLATE & ADDED 10 ML CONCENTRATED HCL TO SAMPLES;
TRANSFERRED SAMPLES INTO C-TUBES WITH D.I. H20.
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML DI H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
--
Printed: 7/25/2013 6:07 AM
Page 1 of 1
Eberline Analytical
Internal .Work Order_
13-07098
e:: eJ;::: .Rc.. ~IR~C~
Analysis Code
Th ISO
Reagent
Reagent
Name
ID
Run
1
Analyst
Reagent
Concentration
ID
Date
Recorded
014109P
Nitric Acid
Reagent Grade
JWOLFE
7/19/2013
014160S
Hydrochloric Acid
SN
RMARTZ
7/24/2013
01416SS
Nitric Acid
SN
RM ARTZ
7/24/2013
014076P
Reagent Grade
RMARTZ
7/24/2013
014042S
Carbon substrate
Solution
RM ARTZ
7/25/2013
O.lmg/ml
RMARTZ
7/25/2013
RMARTZ
7/25/2013
RMARTZ
7/25/2013
014040S
~------.~~-~---
013221P
Cerrium Carrier
-- ----------
---~~~---
Hydrofluoric Acid
----------
Reagent Grade
---~~-------------~-----"---
013574P
Reagent Alcohol
Reagent Grade
--
~'
_ :._ :_ ,. _]~~g!.~~~-t->.:::ha;-~~-~:'l.!:~~~--,~(l:.::!'!:J:~.!:!~2:~=--_,;...::~
-~~:l!Jn;~ r'.:i:1'1.f1.J!:. ._: : :. .~'c.J.:>i:Jd:.':j:.2i-~4.5~-.
~ ,_. .
::J-=t...,-.1:.
_...o
-1f"L.J7'- ,_ f-~.'-.P
1'1.n 7111..A.
f/-i..1.
I 1 I-'
'""St'
/{_.J,,_y-,__ ~l..'-t/ <-...
__;_+-J.--.ll-"L!..:::i==--...
.~O!'!Z:.!J'..:.':llll:IJ--.1.&_!.;~='--t-.f-J."-"'..l>--+--""~~=4-'====-J-'.'=---.,,.,. . ,~
. '71'1.ab /'1. - - ... A'-'"
I ,,
1-oc.
..., L ,,.-...,_.. "-- _,__ .
~4-Jq;L__Jq...i;q.L1.'.l,.ftl!4}1--\.U.ot.<>=--f--,-l.a2'4___1.d~~~~,:;J.._~~-_,._.,.;
i.:/ IM/1?1 I~()~ A- (~-1..l) "'- ~. Mo."4-~. <..
Z-h-r'Sl>~
, ..,, "
Vb
t.uA-
~==-1:~~~t.1<\. =-:f~.-~,~::~-.~;~:Ei~~,,~t;-~.-~~~~-c-~-.~.,,.~-~~n.~~-~~~l
. ~,..lz.,~,"~"'~~~~~~~~~'t-ir-.~i~~~~~-~:::'.:
.--\ -. .:. .
=
--'-1:---.--+-----t-------i------t----t-----"----t--f;:
"'""".A / _ '.
'""~~l-:..
"-ir "T
'lL/7
.I.\..<:
:
q-h.~~ 1'3o'l....,"'~~ r~-\'2') r......tl\G.~-.Se.t..u,
t 1.,,1,l.
::>I.,,.~
"11--V-i'J ,,
__;1.-'-~t-=i.+='-l.1-L'J-l-"""M'.J<Y.UL!l~O!::.!.!'.:~-J""'~-""'""'~""'""'--lf--'...-""-''.:..>1'--f'"'1ll.l<""'--'"-""--+-lL!-=--+-''-'-"4o~...'.:. .' ).
---"+---l-----+--~-~----+-1----------jt-------;-------;-------t----if/~
--'--l-----t-+--------,.--t--------1--------r-------r------t---J;~~/~
~Yt~
!f,_
~~--1-----+----------1---~----1-+-----.------.------r----iM~:::'-~
K"
~-+-~-1-----1-----------1--------1------;------;------i---;r:J
I;
_ ___;-1-----t-----------t--------t----~-t-+-----1------t--+-'i;,-ef,~-:-~
.
',
. ...
..
"
...
"
. .-:
..
.
.
..
.
.
__ , __
.. _., ...
"""
,,-._;_
,_,,_-.
.....
;":
.._,
',":':;__--,_,
-~~,#~t;H;*it:W;WWttflFift~iff"ilfWft&fi*i;-,;~-
- - - + - - - - + - - - - - - - - t - - - - - - t - - - - - t - - - - - t - - - - - + - - - - r '.
~------+--~-----t------t-----t-----t-----+------J"''
il ~
----t----+---------t------t-----t-----t-----+------J
----t----+---------t------1-----1-----1-----1------j~;,,_
'---'---l----+-----------1------+-----+-----1-~'------l---if.:
r,
---r----+--<~---1---~~-+-----t----.__,_,__--1-----;'1:
' r
.. ,:
----1----+-----~--1------+-----t----~-+----+--.-"~,:'.:
----!----+----------li--------t------t----~-t----1---it.'li
---l----.,.--l--~-----t-----+---~1-----1---.,.--1--____,I :
:.1
f..'.
- - - - 1 - - - - + - - - - - - - - i i - - - - - - - - - r - - - - - - r - - - - - t - - - - r - - , i
-----1----+----------ii--------+-----+------t----+---:t~
-
-----1----+----------il---------+-------+-------1----1---__,,)
I'
i>
----tr-----1---------1r--~----t-----+~----1----t---f"'(;
4:i:
-----1r-----+----------i1--~------+-------+-----1i------t-----r
- - - - f - - - - - - + - - - - - - - - + - - - - t - - - - - + - - - - - - 1 - - - + - - - i [:
~.~- -.~~---.--.~
- - - 1 - - - - + - - - - - - - - - - , - 1 - - - - - - - r - - - - - + - - - _ .__._.--_--..-.......
---- __-_
..
-~-~~-
- ........--.- ...
......._..___
~==
"
...
_--J---ijJ
. ...r-..
.._.-
RA-226 NOTES
Printed: 7/19/2013 8:45 AM
Page 1 of 1
jfJ E;: E3..~ ~ Lt....... !;;:

~
SERVICES
#
1
Date
Dept
07/19/13 08:45
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
Ra226
1
Notes
ALI QUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
CARRIERS AND AMMONIUM SULFATE- DECANTED SAMPLES AND CENTRIFUGED- SUBMITTED
RADIUM PRECIP TO SEPARATIONS
Printed: 7/23/2013 6:24 PM
j!J E;J:;l E
~
Page 1 of 1
~J,,,J_N E
SERVICES
Date
Dept
07119/13 08:45
PREP
JWOLFE
User
07/19/13 19:27
PREP
LWALKER
07/23/1318:23
PREP
LWALKER

601 Scarboro Rd.
Oak Ridge1 TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
Ra226
1
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BAAND PB
ADDED EDTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.8 IN AP-006 REV 12 FOR RA 226 ANALYSIS-(SYRINGE FILTERED
PRECIP-FILTERED-DRIED-OBTAIN FINAL WEIGHT}-SUBMIT TO COUNT ROOM.
Printed: 7/24/2013 12:27 PM
Page 1 of 1
Eberline Analytical
>
.:
....
,:-_:::::;:internal Wor1<?6h:i~i:;/_: >
13-07098
E_.E:IE:::~R_L,,J_l""-I_ E
- An~lysis Code - -'
SERVICES
..
Reagent
- --:N~iiie
....
---'. -
..
..
Ra226
Reagent
ID
: _Rea_gent
C()J]cen_tration
.).
P.u11y.
1 .
Analyst
ID
-i
Date
013376P
Ammonium Hydroxide
Reagent Grade
JWOLFE
: Re_corded
7/19/2013
013930001
Ammonium Sulfate
200 mg/ml
JWOLFE
7/19/2013
014007001
Barium Carrier
1 mg/ml
JWOLFE
7/19/2013
014008002
Lead Carrier
166 mg/ml
JWOLFE
7/19/2013
014109P
Nitric Acid
Reagent Grade
JWOLFE
7/19/2013
014140S
EDTA
0.25M
LWALKER
7/19/2013
011383P
Acetic Acid
Reagent Grade
LWALKER
7/23/2013
013575005
Ammonium Sulfate
200 mg/ml
LWALKER
7/23/2013
.:.
>
43
........, ,:
',
.;,\.
-~~_,
:...--
:_
lll-til87
RA-228 NOTES
Printed: 7/19/2013 8:45 AM
Page 1 of 1
~~-El
EB..b l NI;;
~
SERVICES
Date
Dept
07/19/13 08:45
PREP
User
JWOLFE

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
Ra228
1
Notes
i::>AQIUM PRECIP TO SEPARATIONS
Printed: 7/30/2013 7:28 PM
Page 1 of 1
j!!JEBERLINE
~
- --- _____________.. _... s-ER_V_1_C_E_S
Date
Dept
1
.
07/19/13 08:45
PREP
JWOLFE
07/24113 18:18
PREP
LWALKER
07/30/1319:28
PREP
LWALKER
User
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-07098
Ra228
1
Notes
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTA AND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1TO12.7 IN AP-007REV18 (CHEMICAL CLEANUP FOR RA 228)
Printed: 7131/2013 6:31 AM
Page 1 of 1
~--a_-~_R__~JR~-~
Internal Work Order
Analysis Code
Run Number
13-07098
Ra228
1
Date
Dept
07119/13 08:45
PREP
JWOLFE
07124/1318:18
PREP
LWALKER
07/30113 19:28
PREP
LWALKER
FOLLOWED STEPS 12.1TO12.7 IN AP-007 REV 18 {CHEMICAL CLEANUP FOR RA 228)
07/31/13 06:31
CHEM
TSMITH
Followed steps 12.7 to 12.15 in AP-007 rev. 17. (Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discarded
supemate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil and took to count room l
User
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Notes
ALIQUOTED AND ADDED SPIKES AND TRACERS- PH'D SAMPLES- PRECIPITATED WITH BA AND PB
RECEIVED FILTERS BACK FROM COUNT ROOM-PUT BACK INTO C-TUBES-ADDED EDTAAND
SWIRLED-LET SIT OVERNIGHT TO DIGEST.
Eberline Analytical
Printed: 8/5/2013 10:17 AM
Page 1 of 1
Internal Work Order
(EBER~~~"!',;
13-07098
Analysis Code
Ra228

Reagent
Reagent
Name
ID
Run
Reagent
Concentration
1
Date
Recorded
Analyst
ID
013376P
Ammonium Hydroxide
Reagent Grade
JWOLFE
7/19/2013
013930001
Ammonium Sulfate
200 mg/ml
JWOLFE
7/19/2013
014007001
Barium Carrier
1 mg/ml
JWOLFE
7/19/2013
014008002
Lead Carrier
166 mg/ml
JWOLFE
7/19/2013
014109P
Nitric Acid
Reagent Grade
JWOLFE
7/19/2013
011504031
Ammonium Sulfide
2%
LWALKER
7/30/2013
014008001
Lead Carrier
1.5 mg/ml
LWALKER
7/30/2013
014109P
Nitric Acid
Reagent Grade
LWALKER
7/30/2013
014060S
Yttrium Carrier
9 mg/ml
LWALKER
7/30/2013
013065006
Sodium Hydroxide
lOM
LWALKER
7/30/2013
014116S
Ammonium Oxalate
5%
TSMITH
7/31/2013
013910007
Nitric Acid
lN
TSMITH
7/31/2013
013910008
Nitric Acid
6N
TS MITH
7/31/2013
013065006
Sodium Hydroxide
10 M
TSMITH
7/31/2013
013065007
Sodium Hydroxide
18M
TSMITH
7/31/2013
f--~~~~~~-i--~~~~~~~~~~~~~+--~~~~~~~~~+-~~~~~~-+-
-. /\ -:, CL '3 b \Ct:!

'\ V'~
o._'3 lo '{./,
~--'--'--~~-j-~'fJJJ~~~~-f:JJ~W.O~~~~,~~+-~-f,4:"'.L~-+--&'F.J~----c~1'&?-l----At'9---+-
qo 7c17kllf{~l-&~-='l~'..,g2>"'#1~'"=1
23
SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
,...,..
RUNl
Eberline Services
Analysis Sheet
Printed: 7/25/2013 6:07 AM

Page 1 of3
13-07098
UUISO
Run 1
Work Order
Analysis Code
Internal
Fraction
Sample
Desc
Client
Login
ID
CPM
01
LCS
LCS
Sample
Date
Sample
Aliquot
07/16/13 00:00
1.0000E+OO
Run
02
MBL
BLANK
07/16/13 00:00
1.0000E+OO
-
Date Received
03
8/6/2013
04
1-4 TOT
44
07/09/13 12:25
1.0000E+OO
TRG
PZ-111-SDTOT
36
07/09/13 10:42
1.0000E+OO
05
TRG
PZ-111-SD DIS
36
07/09/13 10:42
1.0000E+OO
West Lake OU-1
06
TRG
S-5 TOT
45
07/09/13 10:50
1.0000E+OO
Report Level
07
TRG
S-5 DIS
45
07/09/13 10:50
1.0000E+OO
Activity Units
pCi
08
TRG
FB@ PZ-110-SS TOT
43
07/09/13 11 :40
1.0000E+OO
Aliquot Units
09
TRG
PZ-110-SS TOT
41
07/09/1312:13
1.0000E+OO
WA
10
TRG
PZ-110-SS DIS
41
07/09/13 12:13
1.0000E+OO
HASL 300, 4.5.2
11
DO
1-4 TOT
44
07/09/13 12:25
1.0000E+OO
Alpha Spectroscopy
12
TRG
1-4 DIS
44
07/09/13 12:25
1.0000E+OO
Radiometric Tracer
U-232
13
TRG
PZ-100-SS TOT
46
07/09/13 13:36
1.0000E+OO
Radiometric Sol#
U-10a
14
TRG
PZ-100-SS DIS
46
07/09/1313:36
1.0000E+OO
Tracer Act {dpm/g)
19.051
15
TRG
D-3 TOT
43
07/09/13 13:42
1.0000E+OO
Carrier
16
TRG
D-3 DIS
43
07/09/13 13:42
1.0000E+OO
Carrier Cone {mg/ml)
17
TRG
PZ-100-SD TOT
39
07/09/13 14:32
1.0000E+OO
18
TRG
PZ-100-SD DIS
39
07/09/13 14:32
1.0000E+OO
19
TRG
PZ-112-AS TOT
45
07/09/13 14:46
1.0000E+OO
20
TRG
PZ-112-AS DIS
45
07/09/1314:46
1.0000E+OO
Lab Deadline
Client
Project
Matrix
Method
Instrument Type
7/15/2013
DUP
t'~~I
~~
~,D
'"-'JI
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
*"Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 7/25/2013 6:07 AM

Page 2 of 3
13-07098
UUISO
Run 1
Internal
Fraction
Sample
Desc
Tracer
Aliquot(g)
Tracer Total
ACT(dpm)
01
LCS
0.6105
11.6
02
MBL
0.6056
11.5
0.00
03
DUP
0.6051
11.5
0.00
04
TRG
0.6040
11.5
0.00
05
TRG
0.6032
11.5 I
0.00
06
TRG
0.6032
11.5
0.00
07
TRG
0.6031
11.5
0.00
08
TRG
0.6013
11.5
0.00
09
TRG
0.6013
11.5
0.00
10
TRG
0.6008
11.4
0.00
11
DO
0.6022
11.5
0.00
12
TRG
0.6016
11.5
0.00
13
TRG
0.5993
11.4
0.00
0.00
Radiometric
Tracer (pCi)
Radiometric Grav Carrier

%Rec
Added(ml)
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net(g)
Grav
%Rec
Mean
%Rec
SAF
SAF
0.00
-- f-"
II
~-
14
TRG
0.6035
11.5
15
TRG
0.6015
11.5
0.00
16
TRG
0.5993
11.4
0.00
17
TRG
0.5997
11.4
0.00
18
TRG
0.6004
11.4
0.00
19
TRG
0.6025
11.5
0.00
20
TRG
0.6055
11.5
0.00
''
-
...
!><ii
e1
t!ll
(1)1
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 7/25/2013 6:07 AM

Page 3 of 3
13-07098
UUISO
Run 1
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
By
Internal
Fraction
Sample
Desc
01
LCS
07/19/13 09:00
JWOLFE
02
MBL
07/19/13 09:00
JWOLFE
SeptO
Date/Time
SeptO
By
Sept1
Date/Time
Sep t1
By
-
----
-~
03
DUP
07/19/13 09:00
JWOLFE
04
TRG
07/19/13 09:00
JWOLFE
05
TRG
07/19/13 09:00
JWOLFE
06
TRG
07/19/13 09:00
JWOLFE
07
TRG
07/19/13 09:00
JWOLFE
08
TRG
07/19/13 09:00
JWOLFE
09
TRG
07/19/13 09:00
JWOLFE
10
TRG
07/19/13 09:00
JWOLFE
11
DO
07/19/13 09:00
JWOLFE
12
TRG
07/19/13 09:00
JWOLFE
13
TRG
07/19/13 09:00
JWOLFE
14
TRG
07/19/13 09:00
JWOLFE
15
TRG
07/19/13 09:00
JWOLFE
16
TRG
07/19/13 09:00
JWOLFE
17
TRG
07/19/13 09:00
JWOLFE
18
TRG
07/19/13 09:00
JWOLFE
19
TRG
07/19/13 09:00
JWOLFE
20
TRG
07/19/13 09:00
JWOLFE
~l,,
I</)
~.O
l.J~I
Eberline Services
;:
~
.g
8
.~
Printed: 7/26/2013 9:48 AM

Page 1 of 3
Preliminary Data Report & Analytical Calculations
Work Order: 13-07098-UUIS0-1
LCS
LCS
LCS
Known
%R
Flag
96.39
OK
RPO
Flag
MOA
Blank
Flag
Flag
Lb
Fraction
Nuclide
Sample
Desc
Client
Activity
Identification
Units
01
U-234
LCS
LCS
pCi/I
7.89E+OO
1.13E+OO
1.07E01
02
U-234
MBL
BLANK
pCi/I
1.29E-01
7.98E..02
5.77E..02
03
U-234
DUP
14TOT
pCi/I
5.96E..02
1.63E..01
3.37E..01
04
U-234
TRG
PZ-111.SD TOT
pCi/I
3.49E..01
1.40E..01
8.56E..02
OK
05
U-234
TRG
P:Z..111SD DIS
pCill
3.01E.01
1.26E01
6.08E02
OK
06
U-234
TRG
S-5 TOT
pCi/I
2.15E..01
3.84E01
6.84E..01
OK
07
U234
TRG
S5 DIS
pCill
1.72E-01
1.SSE..01
2.24E01
OK
08
U-234
TRG
FB@ PZ110SS TOT
pCi/I
5.43E..02
6.BOE02
1.07E..01
OK
09
U-234
TRG
PZ-110.SS TOT
pCill
1.03E..01
8.82E02
1.07E..01
OK
10
U-234
TRG
PZ-110-SS DIS
pCi/I
8.28E..02
8.21E..02
9.67E02
OK
11
U234
DO
14TOT
pCill
O.OOE+OO
4.37E01
9.45E..01
OK
12
U-234
TRG
14DIS
pCl/I
3.07E..02
1.99E01
5.41E..01
OK
,,;
.5
13
U234
TRG
pz.100.ss TOT
pCi/I
4.99E+OO
7.92E..01
1.24E..01
'!:!"
14
U-234
TRG
PZ-100.SS DIS
pCi/I
4.82E+OO
8,19E01
1.09E..01
OK
15
U-234
TRG
D3 TOT
pCi/I
1.83E01
1.91E..01
2.39E01
OK
16
U234
TRG
D3 DIS
pCl/I
1.87E..01
1.BOE..01
1.92E.01
OK
..
17
U-234
TRG
PZ-100.SD TOT
pCUI
4.19E-01
1.59E..01
6.76E..02
OK
Cl
c:
18
U-234
TRG
PZ-100.SD DIS
pCi/I
4.36E-01
2.02E..01
1.38E..01
OK
c:
19
U234
TRG
PZ-112AS TOT
pCill
1.95E-01
1.47E01
1.63E..01
OK
20
U-234
TRG
PZ112AS DIS
pCi/I
2.48E01
1.85E..01
1.55E..01
OK
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Error Estimate
MDA
8.18E+OO
OK
OK
OK
OK
OK
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Radiometric
%Rec
Mean
%Rec
Sample
Date
01
U-234
LCS
07116/13 00:00
1.00E+OO
103.24
0.00
0.00
02
U-234
MBL
07/16/13 00:00
1.00E+OO
128.59
0.00
0.00
03
U-234
DUP
07/09/1312:25
1.00E+OO
33.37
0.00
0.00
04
U-234
TRG
07/09/13 10:42
1.00E+OO
118.22
0.00
0.00
05
U-234
TRG
07/09/1310:42
1.00E+OO
107.28
0.00
0.00
06
U-234
TRG
07/09/13 10:50
1.00E+OO
17.24
0.00
0.00
07
U-234
JRG
07/09/1310:50
1.00E+OO
32.43
0.00
0.00
08
U-234
TRG
07/09/13 11:40
1.00E+OO
99.74
0.00
0.00
09
U-234
TRG
07/09/1312:13
1.00E+OO
86.82
0.00
o.oo
10
U-234
TRG
07/09/1312:13
1.00E+OO
70.23
0.00
0.00
11
U-234
DO
07/09/13 12:25
1.00E+OO
8.47
o.oo
0.00
12
U-234
TRG
07/09/13 12:25
1.00E+OO
14.82
0.00
0.00
13
U-234
TRG
07/09/13 13:36
1.00E+OO
94.81
0.00
0.00
t:
14
U-234
TRG
07/09/1313:36
1.00E+OO
103.57
0.00
0.00
15
U-234
TRG
07/09/13 13:42
1.00E+OO
35.21
0.00
0.00
16
U-234
TRG
07/09/13 13:42
1.00E+OO
39.87
0.00
0.00
17
U-234
TRG
07/09/13 14:32
1.00E+OO
116.47
0.00
0.00
18
U-234
TRG
07/09/13 14:32
1.00E+OO
82.79
0.00
0.00
U-234
TRG
07/09/13 14:46
1.00E+OO
67.52
0.00
0.00
U-234
TRG
07/09/13 14:46
1.00E+OO
47.93
0.00
0.00
Gra
%Rec
SAF
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Nuclide
Lab
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Printed: 7/26/2013 9:48 AM
Page 3 of 3
Eberline Services
Counting
Lb
Fraction
Nuclide
Sample
Desc
Datemme
01
U-234
LCS
02
U-234
03
Halflife
(days)
Count
Counts
Bkg
CPM
Detect
Carrier
07125113 10:13
A_Spec
Alpha_023
170 5.24 E+02
9.00 E-03
17.1
MBL
07125113 10:13
A_Spec
Alpha_024
170 1.07 E+01
2.00 E-03
17.1
U-234
OUP
07125113 10:13
A_Spec
Alpha_025
170 1.30 E+OO
1.00 E-02
17.4
04
U-234
TRG
07/25113 10:13
A_Spec
Alpha_027
170 2.68 E+01
7.00 E-03
17.3
05
U-234
TRG
07125113 10:13
A_Spec
Alpha_029
170 2.37 E+01
2.00 E-03
19.5
06
U-234
TRG
07125113 10:13
A_Spec
Alpha_031
170 1.98 E+OO
6.00 E-03
14.2
07
U-234
TRG
07125113 13:24
A_Spec
Alpha_003
170.02 3.66 E+OO
2.00 E-03
17.5
08
U-234
TRG
07/25/13 13:24
A_Spec
Alpha_004
170 3.96 E+OO
1.20 E-02
19.4
09
U-234
TRG
0712511313:24
A_Spec
Alpha_010
170 6.64 E+OO
8.00 E-03
19.7
10
U-234
TRG
07125113 13:24
A_Spec
Alpha_011
170.02 4.49 E+OO
3.00 E-03
20.5
11
U-234
DO
07125113 13:24
A_Spec
Alpha_012
170.02 1.00 E+OO
0.00 E+OO
19.9
12
U-234
TRG
0712511313:24
A_Spec
Alpha_013
170.02 3.20 E-01
4.00 E-03
18.7
<.i
13
U-234
TRG
0712511313:24
A_Spec
Alpha_014
170 3.29 E+02
1.40 E-02
18.5
t'
0
14
U-234
TRG
07125113 13:24
A_Spec
Alpha_015
170.02 2.78 E+02
6.00 E-03
14.8
-"
15
U-234
TRG
07125113 13:24
A_Spec
Alpha_018
170.02 4.32 E+OO
4.00 E-03
17.8
16
U-234
TRG
07/2511313:24
A_Spec
Alpha_019
170.02 4.66 E+OO
2.00 E-03
16.6
17
U-234
TRG
07125/13 13:24
A_Spec
Alpha_020
170.02 2.97 E+01
2.00 E-03
16.1
18
U-234
TRG
0712511313:24
A_Spec
Alpha_022
170.02 2.08 E+01
7.00 E-03
15.3
"
19
U-234
TRG
0712511313:24
A_Spec
Alpha_023
170.02 8.47 E+OO
9.00 E-03
17.1
0712511313:24
A_Spec
Alpha_024
170.02 7.66 E+OO
2.00 E-03
17.1
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Printed: 7/26/2013 9:48 AM
Page 1 of 3
Sample
Client
Oesc
Identification
Activity
Units
Results
Error Estimate
LCS
Known
MDA
LCS
%R
LCS
RPO
MDA
Flag
Flag
Flag
99.85
OK
OK
01
U-238
LCS
LCS
pCi/I
7.96E+OO
1.14E+OO
6.25E-02
02
U-238
MBL
BLANK
pCi/I
6.19E-02
5.88E-02
7.20E-02
03 '
U-238
DUP
1-4 TOT
pCill
1.14E-01
1.59E-01
2.40E-01
04
U-238
TRG
PZ-111-SD TOT
pCi/I
2.63E-01
1.20E-01
7.30E-02
OK
05
U-238
TRG
PZ-111-SD DIS
pCUI
1.77E-01
9.80E-02
7.59E-02
OK
06
U-238
TRG
S-5 TOT
pCi/I
2.99E-01
5.49E-01
9.84E-01
OK
07
U-238
TRG
S-5 DIS
pCi/I
2.87E-01
2.51E-01
2.79E-01
OK
08
U-238
TRG
FB@ PZ-110-SS TOT
pCi/I
1.32E-01
8.62E-02
6.53E-02
OK
U-238
TRG
PZ-110-SS TOT
pCl/I
1.52E-02
4.48E-02
9.75E-02
OK
U-238
TRG
PZ-110-SS DIS
pCi/I
6.40E-02
7.32E-02
9.63E-02
OK
U-238
DO
1-4 TOT
pCUI
4.44E-01
5.57E-01
6.55E-01
OK
12
U-238
TRG
1-4 DIS
pCi/I
-6.49E-02
1.98E-01
5.38E-01
OK
13
U-238
TRG
PZ-100-SS TOT
pCill
2.22E+OO
4.43E-01
9.04E-02
OK
U-238
TRG
PZ-100-SS DIS
pCi/I
1.86E+OO
4.19E-01
7.21E-02
OK
U-238
TRG
D-3 TOT
pCi/I
9.00E-02
1.73E-01
3.20E-01
OK
16
U-238
TRG
D-3 DIS
pCill
4.00E-02
1.11E-01
2.40E-01
OK
17
U-238
TRG
PZ-100-SD TOT
pCi/I
3.45E-01
1.44E-01
7.39E-02
OK
18
U-238
TRG
PZ-100-SD DIS
pCi/I
3.44E-01
1.75E-01
1.09E-01
OK
19
U-238
TRG
PZ-112-AS TOT
pCi/I
8.77E-02
9.09E-02
9.55E-02
OK
20
U-238
TRG
PZ-112-AS DIS
pCi/I
-2.74E-02
6.78E-02
1.93E-01
OK
7.98E+OO
OK
NA
OK
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Lob
Fraction
Nuclide
Sample
Desc
Sample
Sample
Radiometric
Date
Aliquot
%Rec
01
U-238
LCS
07/16/13 00:00
1.00E+OO
103.24
o.oo
0.00
02
U-238
MBL
07/16/13 00:00
1.00E+OO
128.59
0.00
0.00
--
Grav
%Rec
Mean
%Rec
SAF
03
U-238
DUP
07/09/13 12:25
1.00E+OO
33.37
o.oo
0.00
04
U-238
TRG
07/09/13 10:42
1.00E+OO
118.22
o.oo
0.00
05
U-238
TRG
07/09/13 10:42
1.00E+OO
107.28
o.oo
0.00
06
U-238
TRG
07/09/13 10:50
1.00E+OO
17.24
o.oo
0.00
07
U-238
TRG
07/09/13 10:50
1.00E+OO
32.43
o.oo
0.00
08
U-238
TRG
07 /09/13 11 :40
1.00E+OO
99.74
0.00
0.00
09
U-238
TRG
07/09/13 12:13
1.00E+OO
86.82
0.00
o.oo
10
U-238
TRG
07/09/13 12:13
1.00E+OO
70.23
0.00
o.oo
11
U-238
DO
07/09/1312:25
1.00E+OO
8.47
0.00
o.oo
12
U-238
TRG
07/09/13 12:25
1.00E+OO
14.82
0.00
0.00
07/09/13 13:36
1.00E+OO
94.81
0.00
o.oo
TRG
07/09/1313:36
1.00E+OO
103.57
0.00
0.00
U-238
TRG
07/09/13 13:42
1.00E+OO
35.21
0.00
0.00
16
U-238
TRG
07/09/1313:42
1.00E+OO
39.87
0.00
0.00
17
U-238
TRG
07/09/13 14:32
1.00E+OO
116.47
0.00
0.00
"'
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c,
18
U-238
TRG
07/09/1314:32
1.00E+OO
82.79
0.00
0.00
19
U-238
I TRG
07/09/13 14:46
1.00E+OO
67.52
0.00
0.00
20
U-238
TRG
07/09/1314:46
1.00E+OO
47.93
0.00
0.00
.;
13
U-238
14
U-238
15
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Page 2 of 3
SeptO
Date/Time
Sep t1
Datemme
Eberline Services
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..
Lob
Fraction
Printed: 7/26/2013 9:48 AM

Page 3 of 3
Sample
Counting
Halflife
Desc
Daternme
(days)
Detect
Carrier
Count
Time
Counts
Bkg
CPM
Eff
.
01
U-238
LCS
07/25/13 10:13
A_Spec
Alpha_023
170 5.32 E+02
1.00 E-03
17,1
02
U-238
MBL
07/25/1310:13
A_Spec
Alpha_024
170 5.15 E+OO
5.00 E-03
17.1
03
U-238
DUP
07/25/13 10:13
A_Spec
Alpha_o25
170 2.49 E+OO
3.00 E-03
17.4
04
U-238
TRG
07/25/13 10:13
A_Spec
Alpha_027
170 2.03 E+01
4.00 E-03
17.3
05
U-238
TRG
07/25/1310:13
A_ Spec
Alpha_029
170 1.40.E+01
0.00 E+OO
19.5
06
U-238
TRG
07/25/1310:13
A_Spec
Alpha_031
170 2.77 E+OO
1.90 E-02
14.2
07
U-238
TRG
07/25/1313:24
A_Spec
Alpha_003
170.02 6.15E+OO
5.00 E-03
17.5
08
U-238
TRG
07/25/1313:24
A_Spec
Alpha_004
170 9.66 E+OO
2.00 E-03
19.4
09
U-238
TRG
07/25/13 13:24
A_Spec
Alpha_010
170 9.80 E-01
6.00 E-03
19.7
10
U-238
TRG
07/25/1313:24
A_Spec
Alpha_o11
170.02 3.49.E+OO
3.00 E-03
20.5
11
U-238
DO
07/25/13 13:24
A_Spec
Alpha_012
170.02 2.83 E+OO
1.00 E-03
19.9
12
U-238
TRG
07/25/13 13:24
A_Spec
Alpha_013
170.02 -6.80 E-01
4.00 E-03
18.7
13
U-238
TRG
07/25/1313:24
A_Spec
Alpha_014
170 1.47 E+02
5.00 E-03
18.5
14
U-238
TRG
07/25/13 13:24
A_Spec
Alpha_015
170.02 1.08 E+02
1.00 E-03
14.8
15
U-238
TRG
07/25/1313:24
A_Spec
Alpha_018
170.02 2.13 E+OO
1.10 E-02
17.8
16
U-238
TRG
07/25/1313:24
A_Spec
Alpha_019
170.02 1.00 E+OO
0.00 E+OO
16.6
..
17
U-238
TRG
07/25113 13:24
A_Spec
Alpha_020
170.02 2.45 E+01
3.00 E-03
16.1
"'
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a,
18
U-238
TRG
07/25/13 13:24
A_Spec
Alpha_022
170.02 1.65 E+01
3.00 E-03
.15.3
19
U-238
TRG
07/25/1313:24
A_Spec
Alpha_023
170.02 3.83 E+OO
1.00 E-03
17.1
20
U-238
TRG
07/25/13 13:24
A_Spec
Alpha_024
170.02 -8.50 E-01
5.00 E-03
17.1
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Sample
Oesc
Client
Identification
Activity
01
U235
LCS
LCS
pCi/I
4.95E-01
1.97E-01
8.87E-02
OK
02
U-235
MBL
BLANK
pCi/I
3.96E-02
5.12E-02
7.12E-02
OK
03
U-235
DUP
14TOT
pCl/I
2.17E-01
2.26E-01
2.36E-01
U-235
TRG
PZ-111-SD TOT
pCi/I
6.38E-02
7.18E-02
1.01E-01
OK
05
U-235
TRG
PZ-111-SD DIS
pCi/I
5.48E-02
6.25E-02
8.23E-02
OK
06
U-235
TRG
S-5 TOT
pCi/I
1.11E-01
2.68E01
5.59E-01
OK
07
U-235
TRG
S-5 DIS
pCi/I
1.64E-01
2.00E-01
2.41E01
OK
08
U-235
TRG
FB@ PZ-110-SS TOT
pCi/I
3.64E-02
5.90E-02
1.01E-01
OK
09
U-235
TRG
PZ-110-SS TOT
pCi/I
1.05E-01
9.35E02
1.01E-01
OK
10
U-235
TRG
PZ-110-SS DIS
pCi/I
1.11E-02
4.65E-02
1.19E-01
OK
11
U-235
DO
14TOT
pCi/I
-3.31E-02
3.87E-01
8.11E-01
OK
12
U-235
TRG
14DIS
pCill
O.OOE+OO
3.28E-01
7.09E-01
OK
13
U235
TRG
PZ-100-SS TOT
pCl/I
3.99E-01
1.79E-01
1.0GE-01
OK
14
U-235
TRG
PZ-100-SS DIS
pCi/I
2.57E-01
1.54E-01
1.28E-01
OK
15
U-235
TRG
D-3 TOT
pCi/I
9.58E-02
1.47E01
2.18E-01
OK
16
U-235
TRG
D-3 DIS
pCi/I
1.40E-01
1.71E-D1
2.07E01
OK
""'
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17
U-235
TRG
PZ100-SD TOT
pCi/I
4.94E-02
5.98E02
7.28E-02
OK
U-235
TRG
PZ100-SD DIS
pCill
3.41E-02
7.38E-02
1.46E-01
OK
U235
TRG
PZ-112AS TOT
pCi/I
4.71E-02
8.00E-02
1.36E-01
OK
U-235
TRG
PZ-112-AS DIS
pCi/I
1.46E-01
1.SOE-01
1.91 E-01
OK
{l
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Nuclide
.~
Printed: 7/26/2013 9:48 AM

Page 1 of 3
Lob
Fraction
T""
04
en
----
-:::>
:::>
Units
Results
Error Estimate
MDA
LCS
Known
LCS
%R
LCS
Flag
RPO
Flag
NA
MDA
Flag
OK
~--
1-
.5
Q.
Q.
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"'c:
1------
~-
18
"c:
--
UJ
20
c:
~~I
ll=Ji
tt~~!
tn
19
"
;;,
---
Blank
Flag
OK
Eberline Services
(
&
"I:""
.g
8
.~
"
-::::>
ti)
::::>
Printed: 7/26/2013 9:48 AM

Page 2 of 3
Sample
Aliquot
Radiometric
Lb
Fraction
Nuclide
Sample
Desc
Sample
Date
01
U-235
LCS
07/16/13 00:00
1.00E+OO
103.24
0.00
0.00
02
U-235
MBL
07/16/13 00:00
1.00E+OO
128.59
o.oo
0.00
03
U-235
DUP
07/09/1312:25
1.00E+OO
33.37
o.oo
0.00
04
U-235
TRG
07/09/1310:42
1.00E+OO
118.22
o.oo
0.00
05
U-235
TRG
07/09/1310:42
1.00E+OO
107.28
0.00
0.00
06
U-235
TRG
07/09/13 10:50
1.00E+OO
17.24
o.oo
0.00
07
U-235
TRG
07/09/13 10:50
1.00E+OO
32.43
0.00
0.00
08
U-235
TRG
07/09/13 11:40
1.00E+OO
99.74
0.00
0.00
09
U-235
TRG
07/09/13 12:13
1.00E+OO
86.82
0.00
o.oo
10
U-235
TRG
07/09/1312:13
1.00E+OO
70.23
0.00
0.00
11
U-235
DO
07/09/1312:25
1.QOE+OO
8.47
0.00
o.oo
12
U-235
TRG
07/09/13 12:25
1.00E+OO
14.82
0.00
0.00
%Rec
Grav
%Rec
Mean
%Rec
Sep to
SAF
DatefTime
J
.E
13
U-235
TRG
07/09/13 13:36
1.00E+OO
94.81
0.00
0.00
'!:'.
14
U-235
TRG
07/09/1313:36
1.00E+OO
103.57
0.00
0.00
15
U-235
TRG
07/09/13 13:42
1.00E+OO
35.21
0.00
0.00
16
U-235
TRG
07/09/1313:42
1.00E+OO
39.87
0.00
0.00
17
U-235
TRG
07/09/13 14:32
1.00E+OO
116.47
0.00
o.oo
18
U-235
TRG
07/09/13 14:32
1.00E+OO
82.79
0.00
0.00
"c
19
U-235
TRG
07/09/1314:46
1.00E+OO
67.52
0.00
0.00
c
\U
20
U-235
TRG
07/09/13 14:46
1.00E+OO
47.93
0.00
o.oo
Q,
Q,
CJ)
~
E
"01
"'c
::l!
01
;::
"
c,
~lll
~"'~
1!!1
'-l
'
Sept1
Date/Time
Eberline Services
~
&
.g
8
-~
t
"
Counting
Desc
Oatemme
U-235
LCS
02
U-235
03
en
~
~
Halflife
{days)
Count
Time
Bkg
CPM
Detect
Carrier
07/25/1310:13
A_Spec
Alpha_023
170 2.67 E+01
2.00 E-03
17.1
MBL
07/25/13 10:13
A_Spec
Alpha_024
170 2.66 E+OO
2.00 E-03
17.1
U-235
DUP
07/25/1310:13
A_Spec
Alpha_025
170 3.83 E+OO
1.00 E-03
17.4
04
U-235
TRG
07/25/13 10:13
A_Spec
Alpha_027
170 3.98 E+OO
6.00 E-03
17.3
05
U-235
TRG
07/25/13 10:13
A_Spec
Alpha_029
170 3.49 E+OO
3.00 E-03
19.5
06
U-235
TRG
07/25/13 10:13
A_Spec
Alpha_031
170 8.30 E-01
1.00 E-03
14.2
07
U-235
TRG
07/25/13 13:24
A_Spec
Alpha_003
170.02 2.83 E+OO
1.00 E-03
17.5
08
U-235
TRG
07/25/13 13:24
A_Spec
A1pha_oo4
170 2.15E+OO
5.00 E-03
19.4
U-235
TRG
07/25/1313:24
A_Spec
Alpha_010
170 5.49 E+OO
3.00 E-03
19.7
Nuclide
01
"('""
Sample
Lb
Fraction
Printed: 7/26/2013 9:48 AM
Page 3 of 3
Counts
Eff
..
- - -e
09
10
U-235
TRG
07/25/1313:24
A_Spec
Alpha_o11
170.02 4.90 E-01
3.00 E-03
20.5
11
U-235
DO
07/25/13 13:24
A_Spec
Alpha_012
170.02 -1.70 E-01
1.00 E-03
19.9
12
U-235
TRG
07/25/13 13:24
A_Spec
Alpha_013
170.02 1.00 E+OO
0.00 E+OO
18.7
..;
.5
t
o
13
U-235
TRG
07125/13 13:24
A_Spec
Alpha_014
170 2.13E+01
4.00 E-03
18.5
14
U-235
TRG
07/25/13 13:24
A_Spec
Alpha_015
170.02 1.20 E+01
0.00 E+OO
14.8
-"'"
15
U-235
TRG
07/25/1313:24
A_Spec
Alpha_018
170.02 1.83 E+OO
1.00 E-03
17.8
16
U-235
TRG
07/25/13 13:24
A_Spec
Alpha_019
170.02 2.83 E+OO
1.00 E-03
16.6
c:
17
U-235
TRG
07/25/13 13:24
A_Spec
Alpha_020
170.02 2.83 E+OO
1.00 E-03
16.1
Cl
18
U-235
TRG
07/25/1313:24
A_Spec
Alpha_022
170.02 1.32 E+OO
4.00 E-03
15.3
U-235
TRG
07/25/1313:24
A_Spec
Alpha_023
170.02 1.66 E+OO
2.00 E-03
17.1
U-235
TRG
07/25/13 13:24
A_Spec
Alpha_024
170.02 3.66 E+OO
2.00 E-03
17.1
c.
c.
c:
~QI
..
Cl
:';!
c:
;:
QI
QI
c:
;;,
c:
w
~~
1..1.,
~~
(ll)I
19
-
20
Count Room Report

Client: Engineering Management Su
13-07098-UUIS0-1 (pCi/I) in WA
Tracer ID: U-1 Oa
Printed: 7/25/2013 6:07 AM

Page 1of1
/1\~
Internal
Fraction
01 (
l1
Sample
Desc
{f LCS
02
MBL
03
DUP
04
TRG
05
Sample
Aliquot
LCS
07/16/13 00:00
1.0000
0.6105
11.6306
0.00
BLANK
07/16/13 00:00
1.0000
0.6056
11.5373
0.00
1-4 TOT
07/09/13 12:25
1.0000
0.6051
11.5278
0.00
PZ-111-SD TOT
07/09/13 10:42
1.0000
0.6040
11.5068
0.00
I
I
PZ-111-SD DIS
07/09/13 10:42
1.0000
0.6032
S-5 TOT
07/09/1310:50
1.0000
0.6032
11.4916
0.00 I
01109113 10:50
1.0000
0.6031
11.4897
0.00
FB @ PZ-110-SS TOT
07/09/13 11 :40
1.0000
0.6013
11.4554
0.00
PZ-110-SS TOT
07/09/13 12:13
1.0000
0.6013
11.4554
0.00
,-.
i
TRG
06::/ ( TRG
07
Sample
Date
...
TRG
~
/
\!~~
l:iil:
!.O
Radiometric
Tracer (pCI)
Radiometric
%Rec
S-5 DIS
11.4916
0.00
iI
!
TRG
10
TRG
PZ-110-SS DIS
07/09/1312:13
1.0000
0.6008
11.4458
0.00
' I~ ~1
DO
1-4 TOT
07/09/13 12:25
1.0000
0.6022
11.4725
0.00
/12
TRG
07/09/1312:25
1.0000
0.6016
11.4611
0.00
13
TRG
PZ-100-SS TOT
07/09/1313:36
1.0000
0.5993
11.4173
0.00
14
TRG
PZ-100-SS DIS
07/09/1313:36
1.0000
0.6035
11.4973
o.oo I
15
TRG
D-3TOT
07/09/13 13:42
1.0000
0.6015
11.4592
0.00
16
TRG
D-3 DIS
07/09/1313:42
1.0000
0.5993
11.4173
0.00
\J\17
TRG
PZ-100-SD TOT
07/09/1314:32
1.0000
0.5997
11.4249
0.00
18
TRG
PZ-100-SD DIS
07/09/13 14:32
1.0000
0.6004
11.4382
0.00
19
TRG
PZ-112-AS TOT
07/09/13 14:46
1.0000
0.6025
11.4782
0.00
20
TRG
PZ-112-AS DIS
07/09/13 14:46
1.0000
0.6055
11.5354
1-4 DIS
...
SAF
1*
09
r\ v
....
Tracer
ACT(dpm)
TRG
I.
Tracer
Aliquot(g)
08
..
..
Client
ID
0.00
SAF
2*
Eberline Services
Isotope
Sol#
U-234
U-Ba
U-238
U-Ba
Activity
dpmlg
35.240
'
Page 1 of 1
Printed: 7/1912013 9:00 AM
Spike and Tracer Worksheet
34.350
Solution
Date
7/19/2013
7/19/2013
Approx
Addition
Analysis Code
l:Jate
Technician
UUISO
7/19/2013 8:59
JWOLFE
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used{g)
Known
pCi
o.500
Error
Estimate
8.18
0.500 I.. . 0.5155
7.98i
0.5155
Isotope
So/#
01
U-232
U-10a
02
U-232
U-10a
Activity
dpmlg
19.051
Volume
Used(g)
7/19/2013
19.051
7/19/2013
Approx
Addition
0.6300
0.6051
0.6300
0.6040
0.6300
-0~
-o" 1:,~r:.2
04
U-232
U-10a
19.051
7/19/2013
05
U-232
U-10a
19.051
7/19/2013
0.6032
0.6300
7/19/2013
0.6032
0.6300
06
U-232
U-10a
19.051
07
U-232
U-10a
19.051
7/19/2013
_o.~_931
08
U-232
U-10a
19.051
7/19/2013
M013
""'0~
i~~
0.6300
09
U-232
U-10a
19.051
7/19/2013
0.6013
0.6300
10
U-232
U-10a
19.051
7/19/2013
0.6008
0.6300
11
U-232
U-10a
19.051
7/19/2013
,,0.6022
0.6300
12
U-232
U-10a
19.051
7/19/2013
0.6016
0.6300
13
U-232
U-10a
19.051
7/19/2013
0.5993
0.6300
14
U-232
U-10a
19.051
7/19/2013
0.6035
0.6300
15
U-232
U-10a
19.051
7/19/2013
0.6015
0.6300
16
U-232
U-10a
19.051
7/19/2013
0.5993
0.6300
17
U-232
U-10a
19.051
7/19/2013 I
. o.5991
0.6300
18
U-232
U-10a
19.051
7/19/2013
!!:I
Version 2.0 08/99
0.00
0.000
0.00
0.0001
0.00
0.000
0.00
0.000
0.00
o.oool
6El3i ::;
6013 ::i
-0~ 612'13 ':;\
-o,, 1:.uoc:
' .1
-0" 6022
"'!
:0:59'~)3
0.6004
0.6300
U-10a
19.051
7/19/2013
0.6025
0.6300
U-10a
19.051
7/19/2013
0.6055
0.6300
-0. lf:l.016
-i~1. ~s::19::;;
<Cl
:i
.... ~3. '.5':)9-;:' '3
-0" 60\?.14 ::i
-0. i;g2::.i ~j
--0. E.li55 9
----~
&<~~'
0.000
6132 '3
:i
-0~
0.6300
Erro'
Estimate
0.00
~i~
-G. G.03E, .;i
~I!
Added
pCi
~J
M056
7/19/2013
O.E.J.i:'.j5
1:'..056 '3
-a. i:.0'.::i1 '3
--~j. f,040 '3
19.051
U-232
Error
Estimate
LCS
0.6300
U-10a
20
Known
pCi
~-
Tracer
0.6105
U-232
U-232
Error
Estimate
Balance Printer Tapes

Solution
Date
03
19
Wftness Initials
Leso - ---- MSD
MS
Added
pCi
0.295
-0.287
Tracers
fraction
LCS
Technician Initials
lj.,;J1.55 :;
Matrix Spike
Eberline Analytical
Lab
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
Client ID
Type
LCS
BLANK
1-4 TOT
PZ-111-SD TOT
PZ-111-SD DIS
S-STOT
S-5 DIS
FB@PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
1-4 TOT
l-4DIS
PZ-100-SS TOT
PZ-100-SS DIS
D-3 TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
Comments
l;C~I
I-'
t>~
~~
Technician
Page 1 of 1
Analysis Code
Rpt Units
Lab Deadline
Technician
UUISO
liters
8/6/2013
JWOLFE
Dilution Data
Muffle Data
Ratio
Sample
Fraction
01
02
03
04
05
Printed: 7/19/2013 8:49 AM
Aliquot Worksheet
Aliquot Data
Post/Pie
No of Dils
R8tio
_-
----
Oil Factor_
Aliquot
__
.
.
..
.
..
..
.
....
..
.
.
..
..
.
- _,,__
.. .
.
..
.
..
H-3 Solids Only
..
.
..
MS Aliquot Data
Net Equiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.llOOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO . 1.0000E+OO
1.0000E+OO
1.-0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
Aliquot
>Net Equiv
1 __
..
Water Added
H3 Dist
(ml)
Aliq
.
.
I
I.
'
'
..
I
.,Jy)>\~
_Date
+-iP
~~Apex-Alpha
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
SPIKE
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000639
1307098A-UU
01
Shelf 2
u iso
Detector Name:
Alpha_023
Chamber Serial Number:
Detector Serial Number:

23
Env. Background:
System Bkgd 62759

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
1. OOOE+OOO +/- O.OOOE+OOO liter

7 /25/2013
9:15:58 AM
7/25/2013 10:13:39 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chem. Recovery Factor:
U232 UU-lOA
0.610 mL
0.1765 +/- 0.0103
0.1710 +/- 0.0030 on 7/20/2013

1.0324 +/
0.0631
Control Certificate Name: NatU U-8A

Chem. Recov. of Control:
U-238
Peak Match Tolerance:
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.285
4.743
4.382
4.168
T
Net
Pk Area
347.00
524.47
26.66
531.83
0.973290 +/
AREA
6:18:25 PM
0.076642
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
10.54
8.57
38.24
8.50
0.00
1.53
0.34
0.17
0.00E+OOO
0.00E+OOO
O.OOE+OOO
O.OOE+OOO
8.9
46.0
6.2
62.8
Tracer Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.998
1. 000
0.998
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.22E+OOO
7.89E+OOO
4.95E-00l
7.96E+OOO
+/+/+/+/-
5.98E-001
l.13E+OOO
1. 97E-001
l.14E+OOO
MDA
(pCi/liter
9.02E-002
l.07E-001
8.87E-002
6.25E-002
+/+/+/+/-
l.03E-002
1. 23E-002
1. 02E-002
7.16E-003
-lf-C.
'?(J!of!J
~112
0000063930.CNF
Live Time 10200.000 sec

Real Time 10200.000 sec
start:
1 3403.0(kev)
stop : 1024 6588.l(kev)
Acq. Start Thu Jul 25 10:13:39 2013
60
SS
so
4S
40
3S
V>
+-'
<:::
::s
8 30
2S
~j
~
11
iJ
20
~~
m11'
lS
I~
10
l.1 .1 ~
. '11
!j
''
r1
'
3SOO
,_.
L1o11
r:1,
\'
I,11
..'
~I
1il i
4SOO
t;l1
I-'
'
4000
ROI Type: 1
1~
,1r~ l
1.1.11
' ;
~~11
,"1\r111I
'IiI
!1,
1f 111
\r!I I
11 111
' ".111
11
iliJVll 1
sooo
Energy(kev)
1'
i,
\,
ssoo
6000
ROI Type: 3
6SOO
Channel Data Report
7/25/2013
Page
4:38:18 PM
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
Channell------l-------l-------1-------1-------1-------l-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
1
1
1
0
2
2
3
13
14
17
6
0
0
0
0
1
2
1
1
0
0
1
0
10200
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
1
3
0
0
0
2
2
6
14
17
22
5
0
0
0
0
1
1
1
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
1
0
0
1
0
1
2
1
0
0
0
0
0
0
0
1
1
5
12
21
18
16
3
0
0
1
1
0
0
0
0
0
0
0
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1
ll11tl
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0
Sample Title:
4:38:18 PM
1
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-~11,5
Channel Data Report

801:
7/25/2013
0
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01
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1009:
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B116
~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1307098A-UU
02
Shelf 2
u iso
Detector Name:
Alpha_024

24
Env. Background:
System Bkgd 62760

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1.000E+OOO +/- O.OOOE+OOO liter
7/25/2013
9:15:58 AM
7/25/2013 10:13:40 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.606 mL
0.2199 +/- 0.0118
0.1710 +/- 0.0032 on 12/15/2012
1. 2859 +/- 0.0730
0.150 MeV
PEAK
Nuclide
U-232
U-234
U-235
U-238
Energy
(MeV)
Net
Pk Area
5.252
4.694
4.404
4.171
428.81
10.66
2.66
5.15
AREA
REPORT
Pk Area
Error %
9.48
61.14
128.85
94.34
2:02:15 PM
Ambient
Backgnd
1.19
0.34
0.34
0.85
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
12.1
3.1
3.1
3.1
Nuclide
U-232
U-234
U-235
U-238
Id
Conf.
Energy
(keV)
0.982
5302.50*
4761.50*
4385.50*
4184.40*
0. 968
0.998
0.999
Activity
(pCi/liter )
5.18E+OOO
1.29E-001
3.96E-002
6.19E-002
+/- 5.43E-001
+/- 7.98E-002
+/- 5.12E-002
+/- 5.88E-002
kG
'7/~11~
MDA
(pCi/liter
7.95E-002
5.77E-002
7.12E-002
7.20E-002
+/- 8.35E-003
+/- 6.06E-003
+/- 7.48E-003
+/- 7.56E-003
0000063929.CNF
Live Time
Real Time
start:
I
stop : 1024
Acq. start
60
10200.000 sec
10200.000 sec
J411.6(kev)
6597 .O(kev)
Thu Jul 25 10:13:40 2013
55
50
45
40
35
....,
V>
c:
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25
20
15
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ROI Type: 1
11
1111
I,/I
1'iii
l\v1j
I,
5000
Energy(kev)
I
1
6000
5500
ROI Type: 3
6500
Channel Data Report
7/25/2013
Page
4:38:26 PM
*******************************************************
*****
S P E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
02
Elapsed Live time:

Elapsed Real Time:
10200
10200
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~'12S
Channel Data Report

801:
7/25/2013
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Sample Title:
4:38:26
0
PM
0
Page
0
02
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5121
Cf(A
Al
~--~-1'"\pex-
pha

TM
I-4 TOT-DUP
\\OR-AIPHAl\Canberra\ApexAlpha\Root\Data\00000639
1307098A-UU
03
Shelf 2
u iso
Detector Name:
Alpha_025
Sample Description:
Spectrum File:
Sample Geometry:

Env. Background:
25
System Bkgd 62761
Reagent Blank:
<not performed>
1.000E+OOO +/ O.OOOE+OOO liter

7/9/2013
9:15:58 AM
7/25/2013 10:13:41 AM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Chern. Recovery Factor:
U232 UU-lOA
0.605 mL
0.0579 +/ 0.0056
0.1736 +/ 0.0032 on 12/15/2012
0.3337 +/ 0.0330
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.284
4.780
4.385
4 .119
Net
Pk Area
112.83
1. 30
3.83
2.49
AREA
1:57:27 PM
REPORT
Pk Area
Ambient
Reagent
FWHM
Error %
Backgnd
Backgnd
(keV)
0.17
1. 70
0.17
0.51
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
18.47
273.42
102.72
138.29
4.6
3.1
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.998
1. 000
0.970
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.17E+OOO
5.96E-002
2.17E-001
1.14E-001
+/
+/
+/
+/
9.84E-001
1.63E-001
2.26E-001
l.59E-001
MDA
(pCi/liter
1. 91E-001
3.37E-001
2.36E-001
2.40E-001
+/ 3.64E-002
+/ 6.40E-002
+/ 4.49E-002
+/ 4.55E-002
'7/Jc.//'!J
~122
0000063928.CNF
Live Time :10200.000 sec

Real Time :10200.000 sec
start:
1:3405.9(kev)
stop : 1024:6615.B(kev)
Acq. Start :Thu Jul 25 10:13:41 2013
60
SS
so
4S
40
3S
....,
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=>
8 30
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20
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10
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4SOO
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M
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ROI Type: 1
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Energy(kev)
ssoo
6000
ROI Type: 3
6SOO
Channel Data Report
7/25/2013
4:38:33 PM
Page
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*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
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801:
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~126
~J\
~~-/"\pexSample Description:
Al pha
TM
Sample Geometry:
PZ-lll-SD TOT
l307098A-UU
04
Shelf 2
U iso
Detector Name:
Env. Background:
Alpha_027
Spectrum File:
27
System Bkgd 62762
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
l. OOOE+OOO +/ 0.000E+OOO liter

9:15:58 AM
7/9/2013
7/25/2013 10:13:42 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.604 mL
0.2042 +/ 0. 0113
0.1728 +/ 0.0032 on 12/15/2012
l.1822 +/ 0.0690
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.282
4.723
4.385
4.162
T
Net
Pk Area
397.15
26.81
3.98
20.32
AREA
2:27:41 PM
REPORT
Pk Area
Ambient
Error %
Backgnd
9.85
38.82
112.0l
44.32
0.85
l.19
l.02
0.68
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
27.6
4.0
3.2
6.4
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.989
l. 000
0. 996
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.17E+OOO
3.49E-001
6.38E-002
2.63E-00l
+/ 5.59E-00l
+/ l. 40E-001
+/ 7.18E-002
+/ l.20E-00l
Ac;
7/{)fofI!;
MDA
(pCi/liter
7.79E-002
8.56E-002
l. OlE-001
7.30E-002
+/ 8.43E-003
+/ 9.28E-003
+/ l. 09E-002
+/- 7. 91E-003
0000063976.CNF
Live Time
Real Time
start:
I
Stop : 1024
Acq. start
60
10200.000 sec
10200.000 sec
3402.4(kev)
6658.l(kev)
Thu Jul 25 10:13:42 2013
55
50
45
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ROI Type: 1
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6500
Channel Data Report
7/25/2013
4:39:00 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
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04
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369:
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1131
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801:
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..,,.,.
/"\pex-
Al pha
t!t(A
~--===~~
TM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-111-SD DIS
1307098A-UU
05
Shelf 2
u iso
Detector Name:
Alpha_029

29
Env. Background:
System Bkgd 62763
Reagent Blank:
<not performed>

l.OOOE+OOO +/- O.OOOE+OOO liter

9:15:58 AM
7/9/2013
7/25/2013 10:13:43 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.603 mL
0.2087 +/- 0.0114
0.1945 +/- 0.0036 on 12/15/2012
1.0728 +/- 0.0620
0.150 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.285
4.723
4.403
4.155
Net
Pk Area
AREA
REPORT
Pk Area
Error %
405. 32
23.66
3.49
14.00
2:30:02 PM
9.75
40.63
113. 53
54.22
Ambient
Backgnd
0.68
0.34
0.51
0.00
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
37.0
3.1
3.1
4.7
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.989
0.998
0.994
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.16E+OOO
3.0lE-001
5.48E-002
l.77E-001
+/
+/
+/
+/
5.54E-001
l.26E-001
6.25E-002
9.80E-002
MDA
(pCi/liter
7.18E-002
6.08E-002
8.23E-002
7.59E-002
+/- 7.71E-003
+/- 6.53E-003
+/- 8.84E-003
+/- 8.16E-003
I(;
1/;x,/13
0000063977.CNF

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~I
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1;\!!fl1I,\
'
3500
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t"'~
l 1/,
ROI Type: 1
11111
'\,I'
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4500
4000
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(~
::!: !
I ' !
'-'
i~ I
10
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' \
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6500
Channel Data Report
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p E C T R A L
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lll135
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t!f(A
Al pha
~~--/""\pex-
TM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
S-5 DIS
1307098A-UU
07
Shelf 2
u iso
Alpha_003
3
System Bkgd 62747
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/-
0.000E+OOO liter
7/9/2013
9:15:58 AM
1:24:25 PM
7/25/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.603 mL
0.0566 +/- 0.0056
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM

0.3243 +/- 0.0325
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.271
4.753
4.374
4.158
Net
Pk Area
AREA
REPORT
Pk Area
Error %
109.98
3.66
2.83
6.15
18.79
107.88
120. 54
85.19
Ambient
Backgnd
1. 02
0.34
0.17
0.85
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
4.4
3.0
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.993
0.999
0.999
0.995
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.l6E+OOO
l.72E-00l
1. 64E-00l
2.87E-00l
+/- 9.97E-00l
+/- 1. 88E-00l
+/- 2.00E-001
+/- 2.5lE-00l
MDA
(pCi/liter
2.95E-00l
2.24E-00l
2.4lE-00l
2.79E-00l
+/- 5.7lE-002
+/- 4.33E-002
+/- 4.66E-002
+/- 5.40E-002
It&
'1 (J(..(r.J
1!1137
0000063979.CNF

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Channel Data Report
7/25/2013
Page
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*****
SPECTRAL
DAT A
R E P 0 R T
*****
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Sample Title:
07
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Channel Data Report

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4:40:08
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~~~.Apex-Alpha
Sample Geometry:
FB @ PZ-110-SS TOT
1307098A-UU
08
Shelf 2
U iso
Detector Name:
Alpha_004
Env. Background:
Reagent Blank:
System Bkgd 62748
Sample Description:
Spectrum File:
<not performed>
Sample Size:
l.OOOE+OOO +/ 0.000E+OOO liter

7/9/2013
9:15:58 AM
1:24:26 PM
7/25/2013
170.0 minutes
Sample Date/Time:
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232_UU-10A
0.601 mL
0.1935 +/ 0.0110
0.1940 +/ 0.0036 on 12/15/2012 11:26:46 AM
0.9974 +/ 0.0593
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.273
4. 722
4.408
4.134
AREA
REPORT
Net
Pk Area
Ambient
Pk Area
Error %
Backgnd
374.66
3.96
2.15
9.66
10.13
124.69
161.66
64.35
0.34
2.04
0.85
0.34
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
35.7
2.9
2.9
5.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
0.994
0.989
0.996
5302.50*
4761.50*
4385.50*
U-238
0.982
4184.40*
Activity
(pCi/liter )
5.14E+OOO
5.43E-002
3.64E-002
1.32E-001
+/ 5.70E-001
+/ 6.80E-002
+/ 5.90E-002
+/ 8.62E-002
MDA
(pCi/liter
6.56E-002
l.07E-001
1. OlE-001
6.53E-002
+/
+/
+/
+/
7.28E-003
1.19E-002
l.12E-002
7.24E-003
0000063980.CNF

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4:40:29 PM
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9146
4tfl\
~~--/""\pex- Al pha
TM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-11-SS TOT
1307098A-UU
09
Shelf 2
u iso
Detector Name:
Alpha_OlO
10
System Bkgd 62749
Env. Background:
Reagent Blank:
<not performed>
1.000E+OOO +/ 0.000E+OOO liter

7/9/2013
9:15:58 AM
1:24:19 PM
7/25/2013
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
U232_UU-10A
0.601 mL
0.1708 +/ 0.0102
0.1967 +/ 0.0036 on 12/15/2012 11:26:40 AM
0.8682 +/ 0.0542
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.278
4.709
4.428
4.081
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
330.64
6.64
5.49
0.98
Ambient
Backgnd
10.80
84.69
88.08
294.84
1.36
1.36
0.51
1. 02
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
11.2
5.9
2.9
5.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0. 996
0.981
0.987
0.926
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+OOO
1.03E-001
1. 05E-001
l . 52E-002
+/- 6.02E-001
+/- 8.82E-002
+/- 9.35E-002
+/-
4.48E-002
MDA
(pCi/liter
1.07E-001 +/- 1.25E-002
1.07E-001 +/- 1. 25E-002
1. OlE-001 +/- 1.18E-002
9.75E-002 . ,/ _ 1.14E-002
~
/>G
1("((J
~147
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5000
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6000
5500
.~,
t~,
l~ll
--- ..
ii-
-----~
ROI Type: 1
ROI Type: 3
6500
Channel Data Report
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-m 1 s1~
Channel Data Report

801:
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6151
Ct(A
~~-1"\pex-
Al pha
TM
Sample Geometry:
PZ-llO-SS DIS
1307098A-UU
10
Shelf 2
Detector Name:
Env. Background:
Reagent Blank:
Alpha_Oll
Sample Description:
Spectrum File:
iso
ll
System Bkgd 62750
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/ 0.000E+OOO liter

7/9/2013
9:15:58 AM
7/25/2013
1:24:20 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.601 mL
0.1440 +/ 0.0093
0.2051 +/ 0.0035 on 7/20/2013
0.7023 +/ 0.0468
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
AREA
REPORT
Net
Pk Area
Ambient
Pk Area
Error %
Backgnd
5.275
4.719
4.320
4.163
278.64
4.49
0.49
3.49
11. 78
98.45
417.03
113.53
2:50:46 PM
1.36
0.51
0.51
0.51
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
6.6
2.6
2.6
2.6

Id
Conf.
Energy
Nuclide
U-232
U-234
U-235
U-238
0.995
0.987
0.970
0.997
5302.50*
4761.50*
4385.50*
4184.40*
(keV)
Activity
(pCi/liter )
5.14E+OOO
8.28E-002
l. llE-002
6.40E-002
+/ 6.48E-001
+/ 8.21E-002
+/ 4.65E-002
+/ 7.32E-002
MDA
(pCi/liter
l.26E-001
9.67E-002
l.19E-001
9.63E-002
+/ 1. 59E-002
+/ 1. 22E-002
+/ 1. 50E-002
+/ 1. 21E-002
AA
'1{Jt(1J
111152
0000063982.CNF
Live Time
Real Time
60
10201.000 sec
10201.000 sec
Start:
l 3640.l(kev)
stop : 1024 6315.3(kev)
Acq. start Thu Jul 25 13:24:20 2013
55
50
45
40
35
.....,
"'
s:::
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ROI Type: 1
ROI Type: 3
6000
Channel Data Report
7/25/2013
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~Apex-Alpha
Sample Geometry:
PZ-100-SS TOT
1307098A-UU
13
Shelf 2
u iso
Detector Name:
Env. Background:
Alpha_Ol4
Sample Description:
Spectrum File:
14
System Bkgd 62753
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/ O.OOOE+OOO liter

7/9/2013
9:15:58 AM
1:24:23 PM
7/25/2013
170.0 minutes
170.0 minutes
U232_UU-10A
0.599 mL
0.1750 +/ 0.0104
0.1846 +/ 0.0034 on 12/15/2012 11:26:44 AM
0.9481 +/ 0.0588
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.282
4.734
4.401
4.152
AREA
REPORT
FWHM
(keV)
Net
Pk Area
Error %
Ambient
Backgnd
Reagent
Pk Area
10.69
10.86
43.23
16.21
1. 36
2.38
0.68
0.85
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
337.64
328.62
21.32
147 .15
Backgnd
18.3
6.9
3.7
4.8
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.997
0.994
0.998
0.992
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+OOO
4.99E+OOO
3.99E-001
2.22E+OOO
+/ 5.95E-001
+/ 7.92E-001
+/ l.79E-001
+/ 4.43E-001
MDA
(pCi/liter
l.04E-001
1. 24E-001
1.06E-001
9.04E-002
+/
+/
+/
+/
1.21E-002
1.44E-002
1. 23E-002
1. 05E-002
A&
t7/~f3
l1157
0000063985.CNF

start:
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Acq. Start :Thu Jul 25 13:24:23 2013
60
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45
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Channel Data Report
7/25/2013
4:42:26 PM
Page
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Channel Data Report

369:
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l916l!J
Channel Data Report

801:
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~Apex-Alpha
Sample Geometry:
PZ-100-SS DIS
1307098A-UU
14
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_Ol5
Sample Description:
Spectrum File:
15
System Bkgd 62754
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/
O.OOOE+OOO liter
9:15:58 AM
7/9/2013
7/25/2013
1:24:24 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.604 mL
0.1530 +/
0.0096
0.1477 +/
0.0027 on 7/20/2013
1.0357 +/
0.0673
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.285
4.739
4.367
4.159
Net
Pk Area
297. 32
277.98
12.00
107.83
AREA
6:27:27 PM
REPORT
Pk Area
Ambient
Reagent
FWHM
Error %
Backgnd
Backgnd
(keV)
11.38
11. 78
58.89
18.89
0.68
1. 02
0.00
0.17
O.OOE+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
5.5
15.6
3.0
4.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.997
0.998
0.995
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.16E+OOO +/
4.82E+OOO +/
2.57E-001 +/
6.32E-001
8.19E-001
l.54E-001
+/
4.19E-00l
l.86E+OOO
MDA
(pCi/liter
9.79E-002
l.09E-001
l.28E-001
7.21E-002
+/
+/
+/
+/
l.20E-002
1. 34E-002
1. 57E-002
8.83E-003
I&
1/~(!3
_162
0000063986.CNF

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Acq. Start :Thu Jul 25 13:24:24 2013
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6500
Channel Data Report
7/25/2013
Page
4:42:48 PM
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*****
S P E C T R A L
DAT A
R E P 0 R T
*****
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Sample Title:
14
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8'16-5
Channel Data Report

801:
7/25/2013
0
Sample Title:
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1il 166
~J\
~~-1"\pex-
Al pha
TM
D-3 TOT
1307098A-UU
15
Shelf 2
u iso
Detector Name:
Alpha_018
Sample Description:
Spectrum File:
Sample Geometry:
18
Env. Background:
System Bkgd 62755
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

9:15:58 AM
7 /9/2013
1:24:44 PM
7/25/2013
170.0 minutes
170.0 minutes
U232 UU-lOA
0.601 mL
0.0626 +/ 0.0059
0.1776 +/ 0.0033 on 12/15/2012
0.3521 +/ 0.0338
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.255
4.705
4.441
4.151
Net
Pk Area
121.15
4.32
1. 83
2 .13
AREA
1:57:26 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
0.85
0.68
0.17
1.87
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
17.88
102.62
152.56
191. 23
FWHM
(keV)
4.4
3.1
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.984
0.978
0.978
0.992
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.14E+OOO
1. 83E-001
9.58E-002
9.00E-002
+/- 9.49E-001
+/- 1. 91E-001
+/- 1.47E-001
+/- 1. 73E-001
;\&
1/~lfJ
MDA
(pCi/liter
2.54E-001
2.39E-001
2.18E-001
3.20E-001
+/- 4.69E-002
+/- 4.41E-002
+/- 4.03E-002
+/- 5.90E-002
0000063987.CNF

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~~
8-"""'
t$l
001
11
ROI Type: 1
I.Ii
5000
Energy(kev)
5500
6000
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6500
Channel Data Report

369:
7/25/2013
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~m
1 7ij
""'~ ;;' -'loill'
Channel Data Report

801:
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Page
4:43:08 PM
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S171
~A
~~-1"\pexSample Description:
Spectrum File:
Sample Geometry:
Al pha
TM
D-3 DIS
l307098A-UU
16
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U iso
Detector Name:
Alpha_Ol9

19
Env. Background:
System Bkgd 62756

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

9:15:58 AM
7/9/2013
7/25/2013
1:24:44 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.599 mL
0.0662 +/- 0.0061
0.1659 +/- 0.0029 on 2/17/2013

0.3987 +/- 0.0372
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.261
4.738
4.380
4.179
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
127.66
4.66
2.83
1. 00
10:45:23 AM
Ambient
Backgnd
17.37
94.59
120. 54
277.19
0.34
0.34
0.17
0.00
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
6.5
3.3
3.3
3.3
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.988
0.996
1.000
1.000
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+OOO
1. 87E-001
l.40E-00l
4.00E-002
+/- 9.20E-001
+/- l.80E-001
+/- l.71E-001
+/- 1.llE-001
MDA
(pCi/liter
1. 92E-001
1. 92E-00l
2.07E-001
2.40E-001
+/+/+/+/-
3.45E-002
3.44E-002
3.71E-002
4.30E-002
A-G
7(u,{f)
117.2
0000063988.CNF

1:3279.3(kev)
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Acq. Start :Thu Jul 25 13:24:44 2013
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Channel Data Report
7/25/2013
4:43:33 PM
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*****
p E C T R A L
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1175
Channel Data Report

801:
7/25/2013
0
Sample Title:
4:43:33
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16
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Al pha

~-~..sv/'"\pexTM
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
PZ-100-SD TOT
1307098A-UU
17
Shelf 2
u iso
Alpha_020
20
System Bkgd 62757
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/ O.OOOE+OOO liter

7/9/2013
9:15:58 AM
7 /25/2013
1:24:45 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.600 mL
0.1877 +/ 0.0108
0.1612 +/ 0.0029 on 7/20/2013
1.1647 +/ 0.0701
0.150 Mev
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.286
4. 723
4.365
4.150
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
362.47
29.66
2.83
24.49
10.32
36.23
120.54
40.09
6:29:23 PM
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1.53
0.34
0.17
0.51
0.00E+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
12.6
4.9
3.3
4.4
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.989
0.997
0. 992
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+OOO
4.19E-001
4.94E-002
3.45E-001
+/- 5.78E-001
+/- l.59E-001
+/- 5.98E-002
+/- 1. 44E-001
A;G
<7~/0
MDA
(pCi/liter
1. OlE-001
6.76E-002
7.28E-002
7.39E-002
+/+/+/+/-
l.13E-002
7.62E-003
8.20E-003
8.32E-003
0000063989.CNF
Live Time
Real Time
60
10201.000 sec
10201.000 sec
start:
1 3371.4(kev)
stop : 1024 6724.l(kev)
55
50
45
40
35
"'
.....
c:
::>
8 30
25
20
!I
15
u1
I
10
rff.,
11r:r .
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j
~
~!,
di\
A ! I~ iW 111
3500
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00
111il
,,I
4000
4500
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jj.... ~.
111 1I
ROI Type: 1
5000
Energy(kev)
111'
1.1!1'
'
5500
6000
ROI Type: 3
6500
Channel Data Report
7/25/2013
Page
4:43:53 PM
*******************************************************
*****
S P E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
17
Elapsed Live time:

Elapsed Real Time:
10201
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369:
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,m_1snt
~-
Channel Data Report

801:
7/25/2013
0
Sample Title:
4:43:53
PM
0
Page
0
17
Channell------l-------l-------l-------1-------1-------1-------l-------I
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905:
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l':l18.1
~!lt'Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-SD DIS
1307098A-UU
18
Shelf 2
u iso
Detector Name:
Alpha_022

22
Env. Background:
System Bkgd 62758

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
7/9/2013
9:15:58 AM
1:24:46 PM
7/25/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.600 mL
0.1268 +/- 0.0086
0.1531 +/- 0.0029 on 12/15/2012
0.8279 +/- 0.0586
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5 .249
4.689
4.389
4.109
AREA
REPORT
Pk Area
Error %'
Net
Pk Area
245.13
20.81
1. 32
16 .49
1:57:26 PM
12.57
44.38
215.98
49.13
Ambient
Backgnd
1.87
1.19
0.68
0.51
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
34.3
4.7
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.980
0.964
1. 000
0 .960
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.13E+OOO
4.36E-001
3.41E-002
3.44E-001
+/
+/
+/
+/
6.86E-001
2.02E-001
7.38E-002
l.75E-001
'1/Jhf!3
MDA
(pCi/liter
1. 59E-001
1. 38E-001
1.46E-001
1.09E-001
+/+/+/+/-
2.12E-002
l.84E-002
1. 95E-002
1.46E-002
0000063990.CNF

start:
1 3421.S(kev)
stop : 1024 6608.B(kev)
60
55
50
45
40
35
..,r::
Vl
:::>
8 30
25
20
15
10
1. 1in~ ~un
'
3500
4000
4500
~~I
jft..i.1
001
t.~
l,f\I;
i,
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
Channel Data Report
7/25/2013
4:44:14 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
18
Elapsed Live time:

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N184
"'1i'
Channel Data Report

369:
7/25/2013
0
Sample Title:
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0
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i.185
Channel Data Report

801:
7/25/2013
0
Sample Title:
4:44:14
0
PM
0
Page
0
18
Channell------l-------l-------l-------1-------1-------1-------l-------I
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937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
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~186
~~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-ll2-AS TOT
l307098A-UU
l9
Shelf 2
U iso
Alpha_023
23
System Bkgd 62759
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/ O.OOOE+OOO liter

7/9/20l3
9:l5:58 AM
7/25/20l3
l:24:47 PM
l70.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.603 mL
O.ll55 +/ 0.0082
O.l7l0 +/ 0.0030 on 7/20/20l3
0.6752 +/ 0.0493
O.l50 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.285
4.722
4.409
4.l56
Net
Pk Area
AREA
REPORT
Pk Area
Error %
224.00
8.47
l.66
3.83
l3.l3
74.l2
l69.38
l02.72
6:l8:25 PM
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.00
l.53
0.34
O.l7
O.OOE+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
5.3
3.l
3.l
3.l
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.989
0.996
0.994
5302.50*
476l.50*
4385.50*
4l84.40*
Activity
(pCi/liter )
5.l5E+OOO
l.95E-00l
4.7lE-002
8.77E-002
+/ 7.l5E-00l
+/ l.47E-00l
+/ 8.00E-002
+/ 9.09E-002
MDA
(pCi/liter
l.38E-00l
l. 63E-00l
l.36E-00l
9.55E-002
+/
+/
+/
+/
l.9lE-002
2.27E-002
l. 88E-002
l. 33E-002
K;
1(~()
~187
0000063991.CNF

Start:
1:3403.0(kev)
stop : 1024:6588.J(kev)
Acq. Start :Thu Jul 25 13:24:47 2013
60
55
50
45
40
35
...,"'c::
8 30
25
20
15
10
~n
'''II i
11\
5
~
Mir 1l! 1\
!'''
1111
J /,,\
3500
4000
4500
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(JI)
,l
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ROI Type: 1
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(\M,
11 1fli
INlil i
(/,!
5000
Energy(kev)
1''1111.
'
'
II
6000
5500
ROI Type: 3
6500
Channel Data Report
7/25/2013
4:44:36 PM
Page
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*****
p E C T R A L
DAT A
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*****
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!ii .19 ll!
,,
Channel Data Report

801:
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Page
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19
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~191
~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-112-AS DIS
1307098A-UU
20
Shelf 2
U iso
Detector Name:
Env. Background:
Alpha_024
24
System Bkgd 62760
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/9/2013
9:15:58 AM
7/25/2013
1:24:48 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.605 mL
0.0820 +/ 0.0068
0.1710 +/ 0.0032 on 12/15/2012
0.4793 +/ 0.0406
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.260
4.730
4.357
4.131
Net
Pk Area
159.81
7.66
3.66
-0.85
AREA
REPORT
Pk Area
Ambient
Error %'
Backgnd
15.57
72 .63
107.88
246.67
2:02:15 PM
1.19
0.34
0.34
0.85
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
3.5
3.1
0.0
0.0
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.987
0.993
0.994
0.980
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.18E+OOO
2 .48E-001
l.46E-001
-2.74E-002
+/ 8.39E-001
+/ l.85E-001
+/ 1. 60E-001
+/ 6.78E-002
MDA
(pCi/liter
2.13E-001
1. 55E-001
1. 91E-001
l.93E-001
+/ 3.46E-002
+/ 2.51E-002
+/ 3.lOE-002
+/ 3.13E-002
AG
lf{~f'}J
.m1s:2
0000063992.CNF
start:
1 3411.G(kev}
Stop : 1024 6597 .O(kev}
60+
E_
55
50
45
40
35
.._,
V)
c:
8 30
25
20
15
10
3500
~
4000
4500
1<11
l..JI,
rn1
t~1~
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
6500
Channel Data Report
7/25/2013
4:45:00 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
20
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801:
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0
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1
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'!ll1S6
Page 1 of 2
7/25/2013 5:32:50 AM
QA SUMMARY REPORT
Review Of QA Results - Pulser Check
Date
Time
: 7/25/2013
: 5:32:50 AM
CHAMBER
Aloha OOl
Alpha 002
Aloha 003
Alpha 004
Aloha 005
Aloha 006
Aloha 007
Aloha 008
Alpha 009
Aloha 010
Alpha Oil
Aloha 012
Alpha 013
Aloha 014
Aloha 015
Alpha 016
Aloha 017
Alpha 018
Aloha 019
Alpha 020
Aloha 021
Alpha 022
Alpha 023
Aloha 024
Aloha 025
Aloha 026
Alpha 027
Aloha 028
Alpha 029
Aloha 030
Alpha 03 l
Aloha 032
Alpha 033
Aloha 034
Alpha 035
Aloha 036
Alpha 037
Aloha 038
Alpha 039
Aloha 040
Alpha 041
Aloha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alnha AnalystlOODC
Aloha Analvstl OODC
Alpha Analyst!OODC
Aloha Analvstl OODC
Alpha Analvstl OODC
Aloha Analvstl OODC
Alpha Analyst! OODC
Aloha Analvstl OODC
Alpha Analyst l OODC
Aloha Analvst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
7/25/2013 5:16:27 AM
7/25/2013 5:16:28 AM
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
5:16:29 AM
5:16:29 AM
5:16:30 AM
5:16:31 AM
5:16:32 AM
5:16:33 AM
7/25/2013 5:16:34 AM
7/25/2013 5:16:34 AM
7/25/2013
7/25/2013
7/25/2013
712512013
5:16:35 AM
5:16:36 AM
5:16:37 AM
5:16:38 AM
7/25/2013 5:16:38 AM
7/25/2013 5:16:39 AM
7/25/2013 5:16:40 AM
7/25/2013 5:16:41 AM
7/25/2013 5:16:42 AM
7/25/2013 5:16:44 AM
7/25/2013 5:16:45 AM
7/25/2013 5: 16:46 AM
7/25/2013 5:16:48 AM
7/25/2013 5:16:49 AM
7/25/2013 5:16:51 AM
7/25/2013 5:16:52 AM
7/25/2013 5:16:54 AM
1 '
Page 2 of 2
Review of QA Results - Pulser Check

7/25/2013 53250 AM
CHAMBER
Alpha 043
Aloha 044
Alpha 045
Aloha 046
Alpha 047
Aloha 048
DEVICE
Aloha AnalvstlOODC
Alpha AnalystlOODC
Aloha AnalvstlOODC
Alpha AnalystlOODC
Aloha Analvstl OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed
DATE
7/25/2013
7/25/2013
7/25/2013
7/25/2013
5:16:56 AM
5:16:57 AM
5:16:59 AM
5:17:00 AM
APPROVED BY:
APPROVAL DATE:
Uli98
Library Listing Report
6/12/12
Page
12:17:04 PM
*************************************************************************
*****
L I B R A R Y
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:
Uranium
Nuclide Library Description:

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
U-232,-234,-235,-238
Energy
(keV )
Energy
Uncert. (keV )
0.000
0.000
0.000
0.000
5302.500*
4761.500*
4385.500*
4184.400*
Yield
( %)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs.+-)
0.0000
0.0000
0.0000
0.0000
* = key line
TOTALS:
Nuclides
Energy Lines
V11B9
RUN2
Eberline Services
Analysis Sheet
13-07098
Printed: 8/1/2013 6:14 AM

Page 1 of3
UUISO
Run 2
Internal
Fraction
Sample
Desc
Client
Analysis Code
01
LCS
LCS
Run
02
MBL
BLANK
03
DUP
1-4 TOT
Work Order
7/15/2013
Date Received
--Lab Deadline
Client
ID
Login
CPM
Sample
Date
Sample
Aliquot
I 07/16/13 00:00
I
1.0000E+OO
07/16/13 00:00
1.0000E+OO
07/09/13 12:25
5.0000E-01
07/09/13 10:50
5.0000E-01
07/09/13 12:25
5.0000E-01
07/09/13 12:25
5.0000E-01
44
-
8/6/2013
06
TRG
S-5 TOT
45
11
DO
1-4 TOT
44
12
TRG
1-4 DIS
44
Project
West Lake OU-1
--
Report Level
Activity Units
pCi
----
i
'
Aliquot Units
-
Matrix
I
WA
'
..
HASL 300, 4.5.2
Method
Instrument Type
I'
Alpha Spectroscopy
--
Radiometric Tracer
Radiometric Sol#
U-232
U-10a
...
Tracer Act (dpm/g)
19.045
Carrier
Carrier Cone (mg/ml)
--
'
li!lll
~~
~~;!l
,...,
Eberline Services
Analysis Sheet
Printed: 8/1/2013 6:14 AM

Page 2 of 3
13-07098
UUISO
Run 2
Internal
Fraction
Sample
Desc
01
LCS
Tracer
Aliquot (g)
0.6118
Tracer Total
ACT{dpm)
Radiometric
Tracer (pCi)

%Rec
Added(ml)
11.7
0.00
11.6
0.00
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net (g)
Grav
%Rec
Mean
%Rec
SAF
SAF
..
'
02
MBL
0.6109
03
DUP
0.6022
11.5
0.00
06
TRG
0.5848
11.1
0.00
11
DO
0.6073
11.6
0.00
12
TRG
0.6096
11.6
0.00
..
I
I
..
..
i
I
..
'
I
t~
r~~.:11
it?.1.51
1~~~
""Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 8/1/2013 6:14 AM

Page 3 of 3
13-07098
UUISO
Run 2
Internal
Fraction
Sample
Desc
01
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
By
LCS
07/29/13 12:18
JWOLFE
02
MBL
07/29/1312:18
JWOLFE
03
DUP
07/29/13 12:18
JWOLFE
06
TRG
07/29/13 12:18
JWOLFE
11
DO
' 07/29/13 12:18
JWOLFE
12
TRG
07/29/13 12:18
JWOLFE
to
Sep to
By
Sep
Date/Time
Sep t1
By
--- --"----..
---
Sep t1
Date/Time
I
I
'
I
I
I
~;:)
l"'J
@al
(.,,.JI
"'SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
"'"'Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline SeNices
0:
-
0
u
.~
~
~
""
en
-:>:>
Lab
Fraction
t"
0
c.
c.
"'"
~
~I
"E
~
CJ
"'"
"'
"
~
o,
"
w
"
:;:
CJ
~
!!l'l1
~~~I
ffl~I
,~!J,
Printed: 8/1/2013 1:47 PM
Page 1 of 3
Nuclide
Sample
Desc
Client
Activity
Identification
Units
LCS
LCS
pCi/I
8.36E+OO
1.46E+OO
1.24E-01
Results
Error Estimate
MDA
LCS
Known
LCS
%R
LCS
Flag
104.16
OK
RPO
MDA
Blank
Flag
Flag
Flag
OK
01
U-234
02
U-234
MBL
BLANK
pCUI
1.28E-01
8.82E-02
9.59E-02
03
U-234
DUP
1-4 TOT
pCi/I
1.97E-01
3.0JE-01
5.12E-01
06
U-234
TRG
S-5 TOT
pCill
1.10E+OO
9.0GE-01
7.90E-01
OK
11
U-234
DO
1-4 TOT
pCi/I
5.99E-01
5.09E-01
4.29E-01
OK
12
U-234
TRG
1-4 DIS
pCi/I
1.47E+OO
8.35E-01
5.78E-01
OK
.;
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8.02E+OO
OK
NA
OK
OK
~
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Lab
Nuclide
Fraction
Sample
Sample
Sample
Radiometric
Desc
Date
Aliquot
%Rec
Grav
%Rec
Mean
SAF
%Rec
01
U-234
LCS
07116113 00:00
1.00E+OO
64.50
0.00
0.00
02
U-234
MBL
07116113 00:00
1.00E+OO
108.06
0.00
0.00
03
U-234
DUP
0710911312:25
5.00E-01
36.14
0.00
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U-234
TRG
0710911310:50
5.00E-01
15.67
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0710911312:25
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25.97
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07109113 12:25
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27.71
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Page 3 of 3
lid
Sample
Desc
Counting
Date/Time
Halflife
(days)
0 etec t
.
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Count
Time
oun
ts
Bkg
CPM
E
ff
01
U-234
LCS
08/01/13 09:15
A_Spec
Alpha_003
170 3.54 E+02
3.00 E-03
17.5
02
U-234
MBL
08/01/13 09:15
A_Spec
Alpha_004
170 1.01 E+01
1.10 E-02
19.4
03
U-234
DUP
08/01/13 09:15
A_Spec
Alpha_010
170.02 2.64 E+OO
8.00 E-03
19.7
06
U-234
TRG
08/01/13 09:15
A_Spec
Alpha_011
170 6.66 E+OO
2.00 E-03
20.5
en
11
U-234
DO
08/01/13 09:15
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Alpha_012
170.02 5.83 E+OO
1.00 E-03
19.9
::::>
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TRG
08/01/13 09:15
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170.02 1.43 E+01
4.00 E-03
18.7
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94.39
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Sample
Desc
Client
Identification
Activity
U-238
LC5
LCS
pCi/I
7.38E+OO
1.31E+OO
1.23E-01
U-238
MBL
BLANK
pCi/I
8.18E-02
6.64E-02
6.62E-02
U-238
DUP
1-4 TOT
pCi/I
-8.85E-02
1.61E-01
4.90E-01
U-238
TRG
5-5 TOT
pCifl
-5.59E-02
3.32E-01
7.87E-01
OK
U-238
DO
1-4 TOT
pCi/I
1.70E-01
2.90E-01
4.89E-01
OK
U-238
TRG
1-4015
pCi/I
1.85E-01
3.GOE-01
6.73E-01
OK
Units
Results
Error Estimate
MDA
7.82E+OO
OK
OK
NA
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01
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LCS
07/16/13 00:00
1.00E+OO
64.50
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U-238
MBL
07/16/13 00:00
1.00E+OO
108.06
0.00
0.00
03
U-238
DUP
07/09/13 12:25
5.00E-01
36.14
0.00
0.00
06
U-238
TRG
07/09/13 10:50
5.00E-01
15.67
0.00
0.00
12
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TRG
07/09/1312:25
5.00E-01
27.71
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LCS
02
U-238
03
U-238
06
U-238
11
12
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Fraction
Printed: 8/1/20131:47 PM
Page 3 of 3
Halflife
(days)
Count
Bkg
CPM
Eff
Detect
Carrier
08101113 09:15
A_Spec
Alpha_003
170 3.14 E+02
3.00
E~03
17.5
MBL
08101113 09:15
A_Spec
Alpha_004
170 6.49 E+OO
3.00 E-03
19.4
DUP
08101113 09:15
A_Spec
Alpha_010
7.00 E-03
19.7
TRG
08101113 09:15
A_Spec
Alpha_011
170 -3.40 E-01
2.00 E-03
20.5
U-238
DO
08101113 09:15
A_Spec
Alpha_012
170.02 1.66 E+OO
2.00 E-03
U-238
TRG
08101113 09:15
A_Spec
Alpha_013
170.02 1.81 E+OO
7.00 E-03
-
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Time
Counts
170.02 1.19 E+OO
19.9
18.7
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Activity
Desc
U-235
LCS
LCS
pCi/I
7.41E-01
3.09E-01
1.53E-01
OK
02
U-235
MBL
BLANK
pCi/I
5.95E-02
7.01E-02
1.03E-01
OK
03
U-235
DUP
1-4 TOT
pCUI
2.75E-01
3.72E-01
5.81E-01
U-235
TRG
S-5 TOT
pCi/I
1.69E-01
4.0BE-01
8.51E-01
OK
U-235
DO
1-4 TOT
pCill
3.16E-01
4.41E-01
6.65E-01
OK
U-235
TRG
1-4 DIS
pCi/I
6.73E-01
6.28E-01
7.13E-01
OK
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Nuclide
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Flag
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Nuclide
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Desc
Sample
Date
01
U-235
LCS
07116113 00:00
1.00E+OO
64.50
0.00
0.00
02
U-235
MBL
07116113 00:00
1.00E+OO
108.06
0.00
0.00
03
U-235
DUP
07109113 12:25
5.00E-01
36.14
0.00
0.00
06
U-235
07109/13 10:50
5.00E-01
15.67
0.00
0.00
11
U-235
0710911312:25
5.00E-01
25.97
0.00
0.00
07109113 12:25
5.00E-01
27.71
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0.00
Lb
Fraction
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DatefTime
01
U-235
LCS
02
U-235
03
Halflife
(days)
Count
Time
Counts
Bkg
Eff
Detect
Carrier
08/01/13 09:15
A_Spec
Alpha_003
170 2.55 E+01
3.00 E-03
17.5
MBL
08/01/13 09:15
A_Spec
Alpha_004
170 3.81 E+OO
7.00 E-03
19.4
U-235
DUP
08/01/13 09:15
A_Spec
Alpha_010
170.02 2.98 E+OO
6.00 E-03
19.7
06
U-235
TRG
08/01/13 09:15
A_Spec
Alpha_011
1.00 E-03
20.5
11
U-235
DO
08/01/13 09:15
A_Spec
Alpha_012
170.02 2.49 E+OO
3.00 E-03
19.9
12
U-235
TRG
08/01/13 09:15
A_Spec
Alpha_013
170.02 5.32 E+OO
4.00 E-03
18.7
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Count Room Report

Internal
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Sample
Desc
13-07098-UUIS0-2 (pCi/I) in WA
Tracer ID: U-10a
Client
ID
01 ,,,, i LCS
LCS
Sample
Date
Sample
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07/16/13 00:00
1.0000
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MBL
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0.6118
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0.6109
11.6346
: 07/09/1312:25
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0.6022
11.4689
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0.5000
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07/09/13 12:25
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07/09/13 10:50
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11.6517
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0.5848
11.1375
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Page 1 of 1
Printed: 7/29/201312:18 PM
Activity
dpmlg
Solution
Date
Approx
Addition
Analysis Code
Date
UUISO
7/29/2013 12:17
Technician
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
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LCSD
MS
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Estimate
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U-8a
35.240
7129/2013
0.500
0.5054
8.02
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U-8a
34.350
7/2912013
0.500
0.5054
7.82
0.282
0.00
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-----
0.00
0.000
0.00
0.000
U-234
--
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Activity
dpmlg

Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
Sol#
01
U-232
U-10a
19.045 712912013
0.6118
0.6300
02
U-232
U-10a
19.045 712912013
0.6109
0.6300
03
U-232
U-10a
19.045 712912013
0.6022
0.6300
06
U-232
U-10a
19.045 7129/2013
0.5848
0.6300
11
U-232
U-10a
19.045 7129/2013
0.6073
0.6300
U-232
U-10a
19.045 712912013
0.6096
0.6300
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liters
8/6/2013
JWOLFE
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Ratio
Fraction
01
02
03
06
11
12
Printed: 7/29/201312:18 PM
Page 1 of 1
Aliquot Worksheet
Client ID
Type
LCS
BLANK
1-4 TOT
S-5 TOT
1-4 TOT
1-4015
LCS
MBL
OUP
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POst/Pre:>, - -
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1.0000E+OO
1.0000E+OO
5.0000E-01
5.0000E-01
5.0000E-01
5.0000E-01
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1.0000E+OO
1.0000E+OO
5.0000E-01
5.0000E-01
5.0000E-01
5.0000E-01
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Detector Name:
Env. Background:
Alpha_003
Sample Description:
Spectrum File:
System Bkgd 63304
Reagent Blank:
<not performed>

8/l/20l3
7:l8:50 AM
8/1/2013
9:l5:55 AM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
U232 UU-lOA
0.612 mL
O.l126 +/- 0.0080
0.1746 +/- 0.0033 on 12/15/20l2 11:26:47 AM
0.6450 +/- 0.0475
Tracer Certificate:
Tracer Quantity:
Control Certificate Name: NatU U-SA

Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.276
4.726
4.385
4.153
U-238
0.150 MeV
0.920150 +/-
PEAK
REPORT
Net
Pk Area
AREA
Pk Area
Error %
221.81
354.49
25.49
314.49
13.20
10.42
39.27
11. 06
0.088027
FWHM
(keV)
Ambient
Reagent
Backgnd
Backgnd
1.l9
0.51
0.5l
0.5l
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.6
24.9
4.5
l2.2
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.995
0.991
l.000
0.993
5302.50*
4761. 50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.23E+OOO
8.36E+OOO
7.41E-001
7.38E+OOO
+/+/+/+/-
7.29E-001
l.46E+OOO
3.09E-001
1. 31E+OOO
~{3
MDA
(pCi/liter
1.55E-001
1.24E-001
1.53E-001
1.23E-001
+/+/+/+/-
2.17E-002
1. 73E-002
2.13E-002
1. 72E-002
0000064789.CNF

Start:
l:l498.4(kev)
stop : 1024:6549.5(kev)
Acq. Start :Thu Aug 01 09:15:55 2013
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8/1/2013
12:24:26 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
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1:
9:
17:
25:
33:
41:
49:
57:
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105:
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161:
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177:
185:
193:
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209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
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337:
345:
353:
361:
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0
1
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5-9..if
]3~,i~
Channel Data Report

369:
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12 '19
Channel Data Report

801:
8/1/2013
0
Sample Title:
12:24:26
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PM
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0
01
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Ct(A
~~-/'"\pexSample Description:
Spectrum File:
Sample Geometry:
Al pha
TM
BLANK
1307098B-UU
02
Shelf 2
U iso
Detector Name:
Alpha_004

4
Env. Background:
System Bkgd 63305

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7:18:50 AM
8/1/2013
9:15:56 AM
8/1/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.611 mL
0.2097 +/- 0.0114
0.1940 +/- 0.0036 on 12/15/2012 11:26:46 AM

1.0806 +/- 0.0621
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.284
4.733
4.367
4.147
Net
Pk Area
AREA
REPORT
Pk Area
Error %
412.30
10.13
3.81
6.49
9.68
67.91
117.33
80.40
Ambient
Backgnd
1. 70
1.87
1.19
0.51
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
O.OOE+OOO
0.00E+OOO
25.0
2.9
5.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.994
0.998
0.990
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.22E+OOO +/- 5.57E-001

1. 28E-001 +/- 8.82E-002
5.95E-002 +/- 7.0lE-002

8.18E-002 +/- 6.64E-002
MDA
(pCi/liter
9.30E-002
9.59E-002
1. 03E-001
6.62E-002
+/- 9.93E-003
+/- 1. 02E-002
+/- l . lOE-002
+/- 7.06E-003
~, /(:?>
@_221
0000064792.CNF

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Acq. start :Thu Aug 01 09:15:56 2013
60
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ROI Type: 1
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5500
6000
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6500
Channel Data Report
8/1/2013
12:24:38 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
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801:
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02
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m.22s
'l)J,\,,
Al pha
Ct(J\
~~,_/"\pex-
Sample Description:
Spectrum File:
Sample Geometry:
!\\'
TM
I-4 TOT-DUP
13070988-UU
03
Shelf 2
u iso
Detector Name:
Alpha_OlO

10
Env. Background:
System Bkgd 63306

Reagent Blank:
<not performed>
5.000E-001 +/- O.OOOE+OOO liter

7/9/2013
7:18:50 AM
8/1/2013
9:15:51 AM
Sample Size:
Sample Date/Time:
;,
170.0 minutes
170.0 minutes
U232 UU-lOA
0.602 mL
0.0711 +/- 0.0063
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM

0.3614 +/- 0.0327
0.150 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
Nuclide
U-232
U-234
U-235
U-238
(MeV)
T
5.280
4. 713
4.423
4 .132
Net
Pk Area
137.81
2 .64
2.98
-1.19
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
16.78
152.72
134.37
180.58
1.19
1.36
1.02
1.19
FWHM
Reagent
Backgnd
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.9
2.9
2.9
0.0

Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.996
0.983
0.990
0.980
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
1.03E+001
1.97E-001
2.75E-001
-8.85E-002
+/
+/
+/
+/
1.79E+OOO
3.03E-001
3.72E-001
1.61E-001
MDA
(pCi/liter
4.92E-001
5.12E-001
5.81E-001
4.90E-001
+/+/+/+/-
8.56E-002
8.90E-002
1.0lE-001
8.51E-002
S-/f/t'?J
tit226
0000064790.CNF

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Ctr/\
~~-/"\pex-
Al pha
TM
Sample Description:
Spectrum File:
Sample Geometry:
S-5 TOT
1307098B-UU
06
Shelf 2
U iso
Detector Name:
Env. Background:
Alpha_Oll
11
System Bkgd 63307
Reagent Blank:
<not performed>
5.000E-001 +/ O.OOOE+OOO liter

7/9/2013
7:18:50 AM
8/1/2013
9:15:52 AM
Sample Size:
Sample Date/Time:
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.585 mL
0.0321 +/ 0.0042
0.2051 +/ 0.0035 on 7/20/2013
0.1567 +/ 0.0207
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
Net
Pk Area
5.281
4.743
4.323
4.132
T
60.49
6.66
0.83
-0.34
AREA
REPORT
Pk Area
Error %
25.32
78.18
239.53
592.91
2:50:46 PM
Ambient
Backgnd
0.51
0.34
0.17
0.34
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
7.8
2.6
2.6
0.0
Nuclide
U-232
U-234
U-235
U-238
Id
Conf.
Energy
(keV)
0.997
0.998
0 .972
5302.50*
4761.50*
4385.50*
0.980
4184,40*
Activity
(pCi/liter )
1. OOE+OOl
1. lOE+OOO
1.69E-001
-5.59E-002
MDA
(pCi/liter
+/ 2.57E+OOO
+/ 9.06E-001
+/ 4.08E-001
+/ 3.32E-001
8.68E-001
7.90E-001
8.51E-001
7.87E-001
+/ 2.23E-001
+/ 2.03E-001
+/ 2.19E-001
+/ 2.02E-001
fK.;.
&/t/1:,
;m.231
0000064820.CNF

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~234
Channel Data Report

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Env. Background:
Al pha
TM
I-4 TOT
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ll
Shelf 2
u iso
Alpha_Ol2
12
System Bkgd 63308
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
5.000E-OOl +/ O.OOOE+OOO liter

7:18:50 AM
7/9/20l3
9:l5:53 AM
8/1/2013
l70.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.607 mL
0.05l7 +/ 0.0053
0.1989 +/ 0.0034 on l2/ll/2011
0.2597 +/ 0.0270
O.l50 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.265
4.732
4.385
4.l86
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Pk Area
101.00
5.83
2.49
1. 66
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
19.60
82.55
138.30
169.38
2:21:56 PM
0.00
0.17
0.5l
0.34
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Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
6.7
3.0
3.0
3.0
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Energy
(keV)
U-232
U-234
U-235
U-238
0.990
0.994
1. 000
1. 000
5302.50*
4761.50*
4385.50*
4l84.40*
Activity
(pCi/liter )
1. 04E+001
5.99E-001
3.16E-00l
1. 70E-00l
+/ 2.09E+OOO
+/ 5.09E-001
+/ 4.41E-001
+/ 2.90E-00l
MDA
(pCi/liter
6.17E-00l
4.29E-001
6.65E-001
4.89E-001
+/ 1.24E-001
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+/ 1. 34E-001
+/ 9.84E-002
~
&/f{l?J
~236
0000064821.CNF

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~~~/"\pex-
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TM
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I-4 DIS
1307098B-UU
12
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Spectrum File:
iso
Detector Name:
Alpha_013

13
Env. Background:
System Bkgd 63309

Reagent Blank:
<not performed>
5.000E-001 +/- O.OOOE+OOO liter
7:18:50 AM
7/9/2013
8/1/2013
9:15:54 AM
170.0 minutes
170. O minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-lOA
0.610 mL
0.0518 +/- 0.0053
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
0.2771 +/- 0.0289
0.150 MeV
Sample Size:
Sample Date/Time:
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.279
4. 713
4.407
4.117
Net
AREA
REPORT
Pk Area
Error %
Pk Area
101.64
14.32
5.32
1.81
19.59
53.21
91.11
193.79
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Backgnd
1.36
0.68
0.68
1.19
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0.00E+OOO
0.00E+OOO
0.00E+OOO
4.4
4.9
2.8
2.8
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U-234
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0.996
0.983
0.997
5302.50*
4761.50*
4385.50*
4184.40*
0 .969
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1.04E+001
1.47E+OOO
6.73E-001
1.85E-001
+/
+/
+/
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8.35E-001
6.28E-001
3.60E-001
MDA
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5.78E-001
7.13E-001
6.73E-001
1.41E-001
1.16E-001
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Qll
!! !
1111
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11
11,
11
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4000
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AM
6000
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ROI Type: 3
!!
rai
11
Channel Data Report
8/1/2013
Page
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p E
TR AL
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R E P 0 R T
*****
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12
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
'2.~3
...
Channel Data Report

369:
8/1/2013
0
Sample Title:
12:25:48
0
PM
0
Page
0
12
Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
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681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
0
1
0
0
0
0
0
0
0
0
0
1
0
0
1
0
0
0
0
1
0
1
0
0
0
0
0
0
2
1
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
2
2
1
3
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
1
1
0
0
1
0
0
0
1
1
0
0
2
1
4
2
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
1
0
2
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
2
0
0
0
0
0
2
3
4
7
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
3
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
2
0
9
1
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
1
0
1
1
1
0
1
1
2
0
0
0
0
1
0
1
1
2
3
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
3
1
0
1
2
3
1
5
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
1
1
0
1
0
0
0
0
0
0
0
1
3
3
3
4
4
3
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
B'2A,tj
~
Channel Data Report

801:
8/1/2013
0
Sample Title:
12:25:48 PM
0
Page
0
12
Channell------l-------l-------l-------1-------1-------1-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
Page 1 of 2
8/1/2013
5:57:00 AM
~Apex-Alpha']
QA SUMMARY REPORT
Date
Time
: 8/1/2013
: 5:57:00 AM
CHAMBER
Alpha 001
Aloha 002
Alpha 003
Aloha 004
Alpha 005
Alpha 006
Aloha 007
Aloha 008
Aloha 009
Alpha 010
Aloha Oil
Alpha 012
Alpha 013
Aloha 014
Aloha 015
Aloha 016
Alpha 017
Aloha 018
Alpha 019
Aloha 020
Alpha 021
Aloha 022
Aloha 023
Alpha 024
Aloha 025
Alpha 026
Aloha 027
Alpha 028
Aloha 029
Alpha 030
Aloha 031
Alpha 032
Aloha 033
Alpha 034
Aloha 035
Alpha 036
Aloha 037
Alpha 038
Aloha 039
Alpha 040
Aloha 041
Alpha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
21f
2lf
2lf
2lf
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Aloha Analvstl OODC
Aloha Analvstl OODC
Aloha Analvst!OODC
Aloha AnalvstlOODC
Aloha AnalvstlOODC
Aloha Analvst!OODC
Aloha AnalvstlOODC
Aloha Analvstl OODC
Alpha Analyst! OODC
Aloha Analvstl OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
Peak Enerov
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
PeakFWHM
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Action
Not Done
Not Done
Passed
Passed
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Not Done
Action
Passed
Passed
Passed
Passed
DATE
8/1/2013 5:25:35 AM
8/1/2013 5:25:35 AM
8/1/2013
8/1/2013
8/1/2013
8/1/2013
8/1/2013
8/1/2013
5:25:36 AM
5:25:37 AM
5:25:38 AM
5:25:39 AM
5:25:40 AM
5:25:41 AM
8/1/2013 5:25:41 AM
8/1/2013 5:25:42 AM
8/1/2013 5:25:43 AM
8/l/201J 5:25:44 AM
8/1/2013 5:25:45 AM
8/1/2013 5:25:45 AM
8/1/2013 5:25:46 AM
8/1/2013 5:25:47 AM
8/1/2013 5:25:48 AM
8/1/2013 5:25:49 AM
8/1/2013
8/1/2013
8/1/2013
8/1/2013
5:25:50 AM
5:25:51 AM
5:25:53 AM
5:25:55 AM
8/1/2013
8/1/2013
8/1/2013
8/1/2013
8/1/2013
5:25:57 AM
5:25:59 AM
5:26:01 AM
5:26:02 AM
5:26:04 AM
Page 2 of 2
CHAMBER
043
044
045
046
047
048
Alpha
Aloha
Aloha
Alpha
Aloha
Aloha
DEVICE
PARAMETER
Aloha Analvstl OODC

Alpha Analyst! OODC
Aloha Analvstl OODC
Alpha AnalystlOODC
Aloha Analvstl OODC
Alpha Analyst! OODC
FLAG
ALL
ALL
ALL
ALL
ALL
ALL
Not Done
Not Done
Passed
Passed
Passed
Passed
c
APPROVED BY:
<;<{(((']
APPROVAL DATE: _ _ _
"-"
_ __
8/1/2013 5:57:00 AM
DATE
8/1/2013
8/1/2013
8/1/2013
8/1/2013
5:26:07 AM
5:26:09 AM
5:26:12 AM
5:26:14 AM
6/12/12
Page
12:17:04 PM
*************************************************************************
L I B R A R Y
*****
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Uranium

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1. 410E+017
U-232,-234,-235,-238
Energy
(keV )
Energy
Uncert. (keV )
0.000
0.000
0.000
0.000
5302.500*
4 761. 500*
4385.500*
4184.400*
* = key line
TOTALS:
Nuclides
Energy Lines
Yield
( %- )
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs.+-)
0.0000
0.0000
0.0000
0.0000
SECTION IX
ANALYTICAL DATA (ISOTOPIC THORIUM)
Eberline Services
Analysis Sheet
13-07098
Printed: 7/25/2013 6:07 AM

Page 1 of3
Th ISO
Run 1
Internal
Fraction
Work Order
Sample
Desc
Client
Login
CPM
ID
Sample
Date
Sample
Aliquot
Analysis Code
01
LCS
LCS
07/16/13 00:00
1.0000E+OO
Run
02
MBL
BLANK
07/16/13 00:00
1.0000E+OO
7/15/2013
03
DUP
1-4 TOT
44
07/09/13 12:25
1.0000E+OO
8/6/2013
04
TRG
PZ-111-SDTOT
36
07/09/13 10:42
1.0000E+OO
Date Received
-
Lab Deadline
-Client
05
TRG
PZ-111-SD DIS
36
07/09/13 10:42
1.0000E+OO
West Lake OU-1
06
TRG
S-5 TOT
45
07/09/13 10:50
1.0000E+OO
07
TRG
S-5 DIS
45
07/09/13 10:50
1.0000E+OO
Activity Units
pCi
08
TRG
FB@PZ-110-SS TOT
43
07/09/13 11 :40
1.0000E+OO
Aliquot Units
09
TRG
PZ-110-SS TOT
41
07/09/13 12:13
1.0000E+OO
WA
10
TRG
PZ-110-SS DIS
41
07/09/13 12:13
1.0000E+OO
HASL 300, 4.5.2
11
DO
1-4 TOT
44
07/09/13 12:25
1.0000E+OO
12
TRG
1-4 DIS
44
07/09/13 12:25
1.0000E+OO
Th-229
13
TRG
PZ-100-SS TOT
46
07/09/13 13:36
1.0000E+OO
Th-18a
14
TRG
PZ-100-SS DIS
46
07/09/1313:36
1.0000E+OO
15
TRG
D-3 TOT
43
07/09/1313:42
1.0000E+OO
Carrier
16
TRG
D-3 DIS
43
07/09/13 13:42
1.0000E+OO
17
TRG
PZ-100-SD TOT
39
07/09/13 14:32
1.0000E+OO
18
TRG
PZ-100-SD DIS
39
07/09/13 14:32
1.0000E+OO
19
TRG
PZ-112-AS TOT
45
07/09/13 14:46
1.0000E+OO
20
TRG
PZ-112-AS DIS
45
07/09/1314:46
1.0000E+OO
Project
Report Level
Matrix
-Method
Instrument Type
Radiometric Tracer
Radiometric Sol#
Tracer Act (dpm/g)
Alpha Spectroscopy
22.466
t~I
ui.J
U1i
Qjl
*"-Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
13-07098
Printed: 712512013 6:07 AM

Page 2 of 3
ThiSO
Run 1
Internal
Fraction
Sample
Desc
01
LCS
Tracer
Aliquot(g)
Tracer Total
ACT(dpm)
0.4763
Radiometric
Tracer (pCi)

1
% Rec
Added (ml)
10.7
0.00
5.4
0.001
Grav Filter
Tare (g)
Grav Filter
Final (g}
I
I
Grav Filter
Net(g)
Grav
%Rec
Mean
%Rec
SAF
SAF
02
MBL
03
DUP
0.2385
----~-
5.3
04
TRG
05
TRG
0.2345
06
TRG
0.2343
07
TRG
0.2335
08
TRG
09
0.2345
0.00
.
5.3
0.00
5.3
0.00
5.3
0.00
5.2
0.00
0.2338
5.3
0.00
TRG
0.2347
5.3
0.00
10
TRG
0.2331
5.2
0.00 I
11
DO
0.2330
5.2
0.00
12
TRG
0.2335
5.2
0.00
13
TRG
0.2335
5.2
0.00
'"'.: I
I
.
----~
~.
14
TRG
0.2345
15
TRG
16
'
--
~-
5.3
0.00
0.2324
5.2
0.00
TRG
0.2322 .
5.2
0.00
17
TRG
0.2321
5.2
0.00
18
TRG
0.2326 .
5.2
0.00
19
TRG
0.2320
5.2
0.00
20
TRG
0.2329
5.2
0.001
..
121
f1~~
(,j'j
"'~
Eberline Services
Analysis Sheet
Printed: 7/2512013 6:07 AM

Page3of3
13-07098
Th ISO
Run 1
Prep
Date
Prep
LCS
07/19/13 08:58
JWOLFE
02
MBL
07/19/13 08:58
JWOLFE
03
DUP
07/19/13 08:58
JWOLFE
04
TRG
07/19/13 08:58
JWOLFE
05
TRG
07/19/13 08:58
JWOLFE
06
TRG
07/19/13 08:58
JWOLFE
07
TRG
07/19/13 08:58
JWOLFE
08
TRG
07/19/13 08:58
JWOLFE
09
TRG
07/19/13 08:58
JWOLFE
10
TRG
07/19/13 08:58
JWOLFE
11
DO
07/19/13 08:58
JWOLFE
12
TRG
07/19/13 08:58
JWOLFE
13
TRG
07/19/13 08:58
JWOLFE
14
TRG
07/19/13 08:58
JWOLFE
15
TRG
07/19/13 08:58
JWOLFE
16
TRG
07/19/13 08:58
JWOLFE
17
TRG
07/19/13 08:58
JWOLFE
18
TRG
07/19/13 08:58
JWOLFE
19
TRG
07/19/13 08:58
JWOLFE
20
TRG
07/19/13 08:58
JWOLFE
Internal
Fraction
Sample
Desc
01
Rough Prep
Date
Rough Prep
By
By
SeptO
Date/Time
SepW
By
Sep t1
Date/Time
Sep 11
By
'~
''J
U'i
w.J1
_______ .
Eberline Services
~
~
~
.~
"'
-en
.c:
Printed: 7/26/2013 9:33 AM

Page 1 of 3
Work Order: 13-07098-ThlS0-1
RPO
Flag
Nuclide
Sample
Desc
Client
Identification
AcUvity
Units
01
TH-228
LCS
LCS
pCi/I
5.26E+OO
8.22E-01
8.54E-02
02
TH-228
MBL
BLANK
pCi/I
7.82E-02
6.58E-02
5.60E-02
03
TH-228
DUP
l-4TOT
pCi/I
O.OOE+OO
6.92E-02
1.50E-01
04
TH-228
TRG
PZ-111-SD TOT
pCill
2.14E-02
4.64E-02
9.16E-02
OK
05
TH-228
TRG
PZ-111-SD DIS
pCUI
5.83E-03
4.71E-02
1.09E-01
OK
TH-228
TRG
S-5 TOT
pCill
1.48E-01
1.34E-01
1.75E-01
OK
Lb
Fraction
""""
Results
Error Estimate
MDA
LCS
Known
4.BBE+OO
LCS
%R
Flag
LCS
107.78
OK
MDA
Flag
OK
OK
OK
OK
- - - f--
06
---
---
07
TH-228
TRG
S-5 DIS
pCi/I
7.26E-02
9.17E-02
1.45E-01
OK
08
Tll-228
TRG
FB@ PZ-110-SS TOT
pCill
-2.55E-03
3.67E-02
9.72E-02
OK
09
Hl-228
TRG
PZ-110-SS TOT
pCi/I
4.99E-02
6.49E-02
8.96E-02
OK
10
TH-228
TRG
PZ-110-SS DIS
pCi/I
-8.75E-03
4.42E-02
1.13E-01
OK
TH-228
DO
l-4TOT
pCi/I
1.21E-02
6.58E-02
1.43E-01
OK
TH-228
TRG
l-4DIS
pCi/I
5.51E-02
6.23E-02
8.72E-02
OK
TH-228
TRG
PZ-100-SS TOT
pCi/I
3.73E-02
5.60E-02
9.08E-02
OK
- - - -----
11
12
..;
.E
13
t:0
14
Tli-228
TRG
PZ-100-SS DIS
pCi/I
5.44E-02
6.96E-02
1.03E-01
OK
-"
15
TH-228
TRG
D-3 TOT
pCi/I
1.54E-01
1.25E-01
1.32E-01
OK
16
lli-228
TRG
D-3 DIS
pCi/I
1.79E-01
1.0GE-01
8.67E-02
OK
"'"'c
17
TH-228
TRG
PZ-100-SD TOT
pCi/I
2.00E-02
4.31E-02
8.37E-02
OK
"':;;
18
Tii-228
TRG
PZ-100-SD DIS
pCi/I
2.92E-02
5.69E-02
1.0GE-01
OK
19
Tii-228
TRG
PZ-112-AS TOT
pCl/I
6.36E-02
6.62E-02
6.93E-02
OK
20
TH-228
TRG
PZ-112-AS DIS
pCi/I
7.49E-02
7.49E-02
8.75E-02
OK
c.
c.
U)
...
Q)
Q)
:;;
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Q)
a,
c
w
I!~
~J11
[i.1~1
Blank
Flag
OK
Eberline Services
,:
0:
.g
0
"
.~
~
~
"'
Lb
Fraction
Nuclide
Sample
Sample
Sample
Radiometric
Oesc
Date
Aliquot
%Rec
Grav
%Rec
Mean
SAF
%Rec
01
TH-228
LCS
07/16/13 00:00
1.00E+OO
102.45
0.00
0.00
02
TH-228
MBL
07/16/13 00:00
1.00E+OO
110.44
0.00
0.00
03
TH-228
DUP
07/09/1312:25
1.00E+OO
59.27
0.00
0.00
04
Hl-228
TRG
07/09/13 10:42
1.00E+OO
98.80
0.00
0.00
(J)
05
TH-228
TRG
07/09/13 10:42
1.00E+OO
119.03
0.00
o.oo
J:
06
TH-228
TRG
07/09/1310:50
1.00E+OO
63.63
0.00
o.oo
07
TH-228
TRG
07/09/13 10:50
1.00E+OO
80.73
0.00
0.00
08
Tll-228
TRG
07/09/1311:40
1.00E+OO
108.10
0.00
o.oo
09
TH-228
TRG
07/09/1312:13
1.00E+OO
72.25
0.00
o.oo
10
Tll-228
TRG
07/09/1312:13
1.00E+OO
121.98
0.00
o.oo
11
TH-228
DO
07/09/13 12:25
1.00E+OO
92.73
0.00
o.oo
12
TH-228
TRG
07/09/13 12:25
1.00E+OO
131.81
0.00
o.oo
13
TH-228
TRG
07/09/1313:36
1.00E+OO
90.60
0.00
o.oo
14
TH-228
TRG
07/09/1313:36
1.00E+OO
84.04
0.00
o.oo
15
TH-228
TRG
07/09/13 13:42
1.00E+OO
67.26
0.00
o.oo
16
TH-228
TRG
07/09/13 13:42
1.00E+OO
102.54
0.00
o.oo
"'c:"'
17
TH-228
TRG
07/09/1314:32
1.00E+OO
128.21
0.00
0.00
"'c:
18
TH-228
TRG
07/09/13 14:32
1.00E+OO
84.87
0.00
o.oo
"
;;,
"c:
19
TH-228
TRG
07/09/13 14:46
1.00E+OO
85.44
0.00
o.oo
20
TH-228
TRG
07/09/13 14:46
1.00E+OO
81.64
0.00
0.00
.;
E
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Printed: 7/26/2013 9:33 AM
Page 2 of 3
SeptO
Sep t1
DatefTime
OatefTime
Eberline Services
<(
~
.~
Lb
Fraction
Sample
Counting
Halflife
Oesc
Date!Time
(days)
Detect
Canier
Count
Time
Counts
Bkg
CPM
Eff
01
TH-228
LCS
07/25/13 13:26
A_Spec
Alpha_045
170 3.88 E+02
6.00 E-03
19.1
02
TH-228
MBL
07/25/13 13:26
A_Spec
Alpha_046
170 5.83 E+OO
1.00 E-03
17.9
03
TH-228
DUP
07/25/1313:26
A_Spec
Alpha_047
170 1.00 E+OO
0.00 E+OO
18.2
04
TH-228
TRG
07/25/1313:26
A_Spec
Alpha_048
170 1.32 E+OO
4.00 E-03
16.8
05
TH-228
TRG
07/25/13 16:25
A_Spec
Alpha_003
170 4.50 E-01
1.50 E-02
17.5
06
TH-228
TRG
07/25/13 16:25
A_Spec
Alpha_004
170 6.79 E+OO
1.30 E-02
19.4
07
TH-228
TRG
07/25/13 16:25
A_Spec
Alpha_010
170 4.28 E+OO
1.60 E-02
19.7
08
TH-228
TRG
07/25/1316:25
A_Spec
Alpha_011
170.02 -2.10 E-01
1.30 E-02
20.5
09
TH-228
TRG
07/25/1316:25
A_Spec
Alpha_012
170 2.66 E+OO
2.00 E-03
19.9
10
n1-228
TRG
07/25/13 16:25
A_Spec
Alpha_013
170.02 -7.40 E-01
2.20 E-02
18.7
11
TH-228
DO
07/25/1316:25
A_Spec
Alpha_014
1.90 E-02
18.5
12
TH-228
TRG
07/25/1316:25
A_Spec
Alpha_015
170.02 3.98 E+OO
6.00 E-03
14.8
._;
.5
13
TH-228
TRG
07/25/13 16:27
A_Spec
Alpha_033
170 2.32 E+OO
4.00 E-03
18.5
14
TH-228
TRG
07/25/13 16:27
A_Spec
Alpha_034
170 3.15 E+OO
5.00 E-03
18.6
"'1:"w
15
TH-228
TRG
07/25/13 16:27
A_Spec
Alpha_035
170 7.00 E+OO
0.00 E+OO
18.3
E
w
....
"'
16
TH-228
TRG
07/25/1316:27
A_Spec
Alpha_036
170 1.30 E+01
6.00 E-03
19.1
c:
17
TH-228
TRG
07/25/1316:27
A_Spec
Alpha_038
170 1.64 E+OO
8.00 E-03
17.2
c:
"'
18
Tli-228
TRG
07/25/1316:27
A_ Spec
Alpha_039
170 1.81 E+OO
7.00 E-03
19.7
c:
19
Tli-228
TRG
07/25/1316:27
A_Spec
Alpha_040
170 3.83 E+OO
1.00 E-03
19
20
Tli-228
TRG
07/25/1316:27
A_Spec
Alpha_041
170 4.49 E+OO
3.00 E-03
19.8
en
-
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Printed: 7/26/2013 9:33 AM

Page 3 of 3
170 7.70 E-01
::;;
':wii
;;,
c:
w
~ll
r:'l'.11
Ul
tJI
Eberline Services
Lab
Client
Activity
Oesc
Identification
Units
Results
Error Estimate
MDA
LCS
Known
LCS
%R
Flag
93.56
OK
LCS
RPO
Flag
MDA
Flag
LCS
pCill
5.12E+OO
8.04E-01
8.14E-02
02
TH-230
MBL
BLANK
pCi/I
1.59E-01
9.47E-02
5.61E-02
03
TH-230
DUP
1-4 TOT
pCi/I
7.74E-02
9.94E-02
1.47E-01
04
TH-230
TRG
PZ-111-SD TOT
pCi/I
6.64E-02
7.20E-02
9.58E-02
OK
05
TH-230
TRG
PZ-111-SD DIS
pCi/I
1.11E-01
7.73E-02
6.11E-02
OK
.~
en
~
<(
..c:
I
06
TH-230
TRG
S-5TOT
pCi/I
9.61E-02
1.07E-01
1.53E-01
OK
Tll-230
TRG
S-5 DIS
pCi/I
1.07E-02
4.90E-02
1.15E-01
OK
08
Tll-230
TRG
FB@ PZ-110-SS TOT
pCi/l
8.76E-02
6.82E-02
6.75E-02
OK
09
Tll-230
TRG
PZ-110-SS TOT
pCi/I
2.00E-01
1.26E-01
7.71E-02
OK
10
Tfl-230
TRG
PZ-110-SS DIS
pCill
1.0SE-01
7.45E-02
7.33E-02
OK
11
Tfl-230
DO
1-4 TOT
pCi/I
5.65E-02
7.02E-02
1.0SE-01
OK
12
TH-230
TRG
1-4 DIS
pCill
1.13E-01
8.27E-02
7.69E-02
OK
13
Tli-230
TRG
PZ-100-SS TOT
pCUI
1.72E-01
1.07E-01
6.62E-02
OK
14
TH-230
TRG
PZ-100-SS DIS
pCi/I
1.70E-02
4.73E-02
1.02E-01
OK
15
TH-230
TRG
D-3 TOT
pCi/I
1.51E-01
1.24E-01
1.30E-01
OK
~m
16
TRG
D-3 DIS
pCi/I
9.03E-02
7.21E-02
6.48E-02
OK
c:
17
TH-230
----
TH-230
TRG
PZ-100-SD TOT
pCi/I
1.02E-01
7.27E-02
6.31E-02
OK
18
TH-230
TRG
PZ-100-SD DIS
pCi/I
9.01E-02
7.83E-02
7.61E-02
OK
TH-230
TRG
PZ-112-AS TOT
pCi/I
1.64E-01
1.10E-01
9.SOE-02
OK
TH-230
TRG
PZ-112-AS DIS
pCi/I
1.31E-01
1.00E-01
1.04E-01
OK
07
<.i
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Cl)
5.47E+OO
OK
NA
OK
c:
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20
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OK
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LCS
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TH-230
Printed: 7/26/2013 9:33 AM

Page 1of3
01
~~I
Nuclide
Fraction
--
OK
Eberline Services
0:
.g
0
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.~
"'c
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Lob
Sample
01
TH-230
LCS
07/16/13 00:00
02
TH-230
MBL
07/16/13 00:00
1.00E+OO
110.44
0.00
0.00
03
TH-230
DUP
07/09/1312:25
1.00E+OO
59.27
0.00
0.00
rn..230
TRG
07/09/13 10:42
1.00E+OO
98.80
0.00
0.00
04
05
rn..230
TRG
07/09/1310:42
1.00E+OO
119.03
0.00
0.00
..c:
06
TH-230
TRG
07/09/13 10:50
1.00E+OO
63.63
0.00
o.oo
07
TH-230
TRG
07/09/1310:50
1.00E+OO
80.73
0.00
0.00
08
TH-230
TRG
07/09/13 11:40
1.00E+OO
108.10
0.00
0.00
09
TH-230
TRG
07/09/1312:13
1.00E+OO
72.25
0.00
0.00
10
TH-230
TRG
07/09/1312:13
1.00E+OO
121.98
0.00
0.00
11
TH-230
DO
07/09/13 12:25
1.00E+OO
92.73
0.00
0.00
12
TH-230
TRG
07/09/13 12:25
1.00E+OO
131.81
0.00
0.00
13
TH-230
TRG
07/09/1313:36
1.00E+OO
90.60
0.00
0.00
t:0
14
TH-230
TRG
07/09/1313:36
1.00E+OO
84.04
0.00
0.00
15
TH-230
TRG
07/09/13 13:42
1.00E+OO
67.26
0.00
0.00
16
Hl-230
TRG
07/09/13 13:42
1.00E+OO
102.54
0.00
0.00
"'"'c:
17
Tfl-230
TRG
07/09/1314:32
1.00E+OO
128.21
0.00
0.00
"'c:
18
Tfl-230
TRG
07/09/13 14:32
1.00E+OO
84.87
0.00
0.00
c:
19
Tfl-230
TRG
07/09/1314:46
1.00E+OO
85.44
0.00
0.00
20
Tfl-230
TRG
07/09/1314:46
1.00E+OO
81.64
0.00
0.00
1.00E+OO
Radiometric
%Rec
Mean
Sample
Desc
Date
Sample
Aliquot
Grav
%Rec
Nucllde
Fraction
102.45
SAF
%Rec
0.00
0.00
'
en
-
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Printed: 7/26/2013 9:33 AM

Page 2 of 3
Sep to
Sep t1
Date/Time
DatefTime
Eberline Services
.g
8
~
c
<>:
Counting
Halflife
(days)
'
Count
Sample
Desc
Datefrime
LCS
0712511313:26
A_Spec
Alpha_045
170 3.77 E+02
0.00 E+OO
19.1
MBL
-
0712511313:26
A_Spec
Alpha_046
170 1.18 E+01
1.00 E-03
17.9
Detect
Carrier
Time
Counts
Bkg
CPM
Eff
TH-230
03
TH-230
DUP
0712511313:26
A_Spec
Alpha_047
170 3.15 E+OO
5.00 E-03
18.2
04
TH-230
TRG
0712511313:26
A_Spec
Alpha_048
170 4.15 E+OO
5.00 E-03
16.8
CJ)
05
rn..230
TRG
0712511316:25
A_Spec
Alpha_003
170 8.66 E+OO
2.00 E-03
17.5
.s:::
06
rn..230
TRG
0712511316:25
A_Spec
Alpha_004
170 4.47 E+OO
9.00 E-03
19.4
07
TH-230
TRG
07125113 16:25
A_Spec
Alpha_010
170 6.40 E-01
8.00 E-03
19.7
08
TH-230
TRG
07125113 16:25
A_Spec
Alpha_011
170.02 7.32 E+OO
4.00 E-03
20.5
09
TH-230
TRG
07125113 16:25
A_Spec
Alpha_012
170 1.08 E+01
1.00 E-03
19.9
10
TH-230
TRG
07125113 16:25
A_Spec
Alpha_013
170.02 8.98 E+DO
6.00 E-03
18.7
11
TH-230
DO
07125113 16:25
A_Spec
Alpha_014
170 3.64 E+OO
8.00 E-03
18.5
12
TH-230
TRG
07125113 16:25
A_Spec
Alpha_015
170.02 8.32 E+OO
4.00 E-03
14.8
13
TH-230
TRG
0712511316:27
A_Spec
Alpha_033
170 1.08 E+01
1.00 E-03
18.5
t:0
14
TH-230
TRG
0712511316:27
A_Spec
Alpha_034
170 1.00 E+OO
0.00 E+OO
18.6
"'
15
TH-230
TRG
07125113 16:27
A_Spec
Alpha_035
170 7.00 E+OO
0.00 E+OO
18.3
16
TH-230
TRG
07125113 16:27
A_Spec
Alpha_036
170 6.66 E+OO
2.00 E-03
19.1
17
TH-230
TRG
07125113 16:27
A_Spec
Alpha_038
170 8.49 E+OO
3.00 E-03
17.2
18
TH-230
TRG
0712511316:27
A_Spec
Alpha_039
170 5.66 E+OO
2.00 E-03
19.7
19
TH-230
TRG
07125113 16:27
A_Spec
Alpha_040
170 1.00 E+01
0.00 E+OO
19
20
TH-230
TRG
07125113 16:27
A_Spec
Alpha_041
170 7.98 E+OO
6.00 E-03
19.8
Nuclide
02
.~
TH-230
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Printed: 7/26/2013 9:33 AM
Page 3 of 3
01
Lab
Fraction
.;
c.
c.
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(/)
-
-
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8
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Identification
Activity
Units
01
TH-232
LCS
LCS
pCi/I
5.35E+OO
8.32E-01
5.65E-02
02
TH-232
MBL
BLANK
pCUI
1.11E-02
2.67E-02
5.GOE-02
03
TH-232
DUP
1-4 TOT
pCi/I
3.24E-02
7.03E-02
1.38E-01
04
TH-232
TRG
PZ-111-SD TOT
pCl/I
2.38E-02
4.54E-02
8.38E-02
OK
05
TH-232
TRG
PZ-111-SD DIS
pCi/I
-1.08E-02
2.68E-02
7.63E-02
OK
06
TH-232
TRG
S-5 TOT
pCill
1.79E-01
1.32E-01
1.21 E-01
OK
07
TH-232
TRG
S-5 DIS
pCi/I
-6.01E-03
3.63E-02
1.14E-01
OK
08
TH-232
TRG
FB @ PZ-110-SS TOT
pCi/I
3.18E-02
4.12E-02
5.71E-02
OK
09
TH-232
TRG
PZ-110-SS TOT
pCi/I
1.84E-02
5.12E-02
1.11E-01
OK
10
TH-232
TRG
PZ-110-SS DIS
pCl/I
6.18E-02
5.71E-02
6.56E-02
OK
11
TH-232
DO
1-4 TOT
pCi/I
1.02E-02
3.13E-02
7.40E-02
OK
12
TH-232
TRG
1-4 DIS
pCl/I
3.85E-02
4.68E-02
5.68E-02
OK
TH-232
TRG
PZ-100-SS TOT
pCi/I
3.16E-02
5.40E-02
9.49E-02
OK
14
TH-232
TRG
PZ-100-SS DIS
pCi/I
4.81E-02
5.86E-02
7.09E-02
OK
15
TH-232
TRG
D-3TOT
pCl/I
-3.67E-03
4.29E-02
9.00E-02
OK
16
TH-232
TRG
D-3 DIS
pCi/I
3.14E-02
4.71E-02
7.63E-02
OK
""'c
17
TH-232
TRG
PZ-100-SD TOT
pCi/i
9.96E-03
2.39E-02
5.01E-02
OK
"'c
18
TH-232
TRG
PZ-100-SD DIS
pCUI
2.37E-02
4.52E-02
8.34E-02
OK
c
c
19
TH-232
TRG
PZ-112-AS TOT
pCi/i
1.63E-02
4.53E-02
9.79E-02
OK
20
Tti-232
TRG
PZ-112-AS DIS
pCill
-3.97E-02
5.38E-02
1.67E-01
OK
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Printed: 7/26/2013 9:33 AM

Page 1 of 3
Nuclide
Lab
Fraction
.;
.E
13
Client
Results
Error Estimate
MDA
LCS
Known
4.88E+OO
LCS
%R
LCS
Flag
109.61
OK
RPO
MDA
Flag
Flag
Blank
Flag
OK
OK
NA
OK
OK
Eberline Services
Lob
a:
.g
0
.~
~
~
'<
Sample
Aliquot
Grav
Mean
%Rec
%Rec
Sample
Desc
Sample
Date
TH-232
LCS
07/16/13 00:00
1.00E+OO
102.45
0.00
0.00
02
TH-232
MBL
07/16/13 00:00
1.00E+OO
110.44
0.00
o.oo
03
TH-232
DUP
07/09/13 12:25
1.00E+OO
59.27
0.00
0.00
04
TH-232
TRG
07/09/13 10:42
1.00E+OO
98.80
0.00
0.00
05
TH-232
TRG
07/09/13 10:42
1.00E+OO
119.03
0.00
0.00
06
TH-232
TRG
07/09/1310:50
1.00E+OO
63.63
0.00
0.00
07
TH-232
TRG
07/09/1310:50
1.00E+OO
80.73
0.00
0.00
08
TH-232
TRG
07/09/13 11 :40
1.00E+OO
108.10
0.00
09
Tfl-232
TRG
07/09113 12:13
1.00E+OO
72.25
0.00
o.oo
10
TH-232
TRG
07/09/13 12:13
1.00E+OO
121.98
0.00
0.00
11
TH-232
DO
07/09/13 12:25
1.00E+OO
92.73
0.00
o.oo
12
TH-232
TRG
07/09/13 12:25
1.00E+OO
131.81
0.00
o.oo
13
TH-232
TRG
07/09/13 13:36
1.00E+OO
90.60
0.00
o.oo
14
TH-232
TRG
07/09/13 13:36
1.00E+OO
84.04
0.00
o.oo
01
___
Radiometric
%Rec
""""
"'.c
t:'
0
a.
,,,a.
~
0.00
----
15
TH-232
TRG
07/09/1313:42
1.00E+OO
67.26
0.00
o.oo
-----
16
TH-232
TRG
07/09/13 13:42
1.00E+OO
102.54
0.00
o.oo
17
TH-232
TRG
07/09/13 14:32
1.00E+OO
128.21
0.00
o.oo
:;;
-----
"'
18
TH-232
TRG
07/09/13 14:32
1.00E+OO
84.87
0.00
0.00
19
TH-232
TRG
07/09/13 14:46
1.00E+OO
85.44
0.00
o.oo
20
Tli-232
TRG
07/09/1314:46
1.00E+OO
81.64
0.00
o.oo
-~ ......
.."'
..
c;,
c
UJ
~tl..:n1
Sep t1
Date/Time
~-
Cll'.D
Sep to
Date/Time
---
.s
hll
SAF
,____________
!:iii
Printed: 7/26/2013 9:33 AM

Page 2 of 3
Nuclide
Fraction
Eberline Services
a:
.g
8
.~
..
<;
c
Lb
Fraction
Halflife
(days)
Detect
Carrier
Count
Time
Counts
Bkg
CPM
Eff
07/25/13 13:26
A_Spec
Alpha_045
170 3.95 E+02
1.00 E-03
19.1
02
TH-232
MBL
07/25/1313:26
A_Spec
Alpha_046
170 8.30 E-01
1.00 E-03
17.9
03
TH-232
DUP
07/25/13 13:26
A_Spec
Alpha_047
170 1.32 E+OO
4.00 E-03
18.2
04
TH-232
TRG
07/25/13 13:26
A_Spec
Alpha_048
170 1.49 E+OO
3.00 E-03
16.8
05
TH-232
TRG
07/25/13 16:25
A_Spec
Alpha_003
170 -8.50 E-01
5.00 E-03
17.5
06
TH-232
TRG
07/25/1316:25
A_Spec
Alpha_004
170 8.32 E+OO
4.00 E-03
19.4
07
TH-232
TRG
07/25/1316:25
A_ Spec
Alpha_010
170 -3.60 E-01
8.00 E-03
19.7
08
TH-232
TRG
07/25/1316:25
A_Spec
Alpha_011
170.02 2.66 E+OO
2.00 E-03
20.5
09
TH-232
TRG
07/25/13 16:25
A_Spec
Alpha_012
170 1.00 E+OO
0.00 E+OO
19.9
10
TH-232
TRG
07/25/1316:25
A_Spec
Alpha_013
170.02 5.32 E+OO
4.00 E-03
18.7
11
TH-232
DO
07/25/1316:25
A_Spec
Alpha_014
2.00 E-03
18.5
12
TH-232
TRG
07/25/13 16:25
A_Spec
Alpha_015
170.02 2.83 E+OO
1.00 E-03
14.8
.;
13
T>l-232
TRG
07/25/13 16:27
A_Spec
Alpha_033
170 2.00 E+OO
0.00 E+OO
18.5
t:
0
14
TH-232
TRG
07/25/1316:27
A_ Spec
Alpha_034
170 2.83 E+OO
1.00 E-03
18.6
"
15
TH-232
TRG
07/25/13 16:27
A_Spec
Alpha_035
170 -1.70 E-01
1.00 E-03
18.3
16
TH-232
TRG
07/25/13 16:27
A_Spec
Alpha_036
170 2.32 E+OO
4.00 E-03
19.1
17
TH-232
TRG
07/25/13 16:27
A_Spec
Alpha_038
170 8.30 E-01
1.00 E-03
17.2
18
TH-232
TRG
07/25/1316:27
A_Spec
Alpha_039
170 1.49 E+OO
3.00 E-03
19.7
19
TH-232
TRG
07/25/13 16:27
A_Spec
Alpha_040
170 1.00 E+OO
0.00 E+OO
19
20
TH-232
TRG
07/25/1316:27
A_Spec
Alpha_041
170 -2.42 E+OO
2.60 E-02
19.8
T""
-"'.s::
I
.""'
--
170 6.60 E-01
Cl
Cl
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w
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l:lli
Counting
Date/Time
LCS
j""~J
Sample
Desc
Nuclide
TH-232
(/)
t~
01
c.
c.
I\)
Printed: 7/26/2013 9:33 AM
Page 3 of 3
.s
Count Room Repo11

~
~
13-07098-ThlS0-1 (pCi/I) in WA
Tracer ID: Th-18a
Printed: 712512013 6:07 AM
~\(V
Internal
Fraction
Sample
Desc
Client
ID
Sample
Date
Sample
Aliquot
01
LCS
LCS
07/16/13 00:00
1.0000
0.4763
10.7006
' .JI 02
\("\
MBL
BLANK
07/16/13 00:00
1.0000
0.2385
5.3581
03
DUP
1-4 TOT
07/09/13 12:25
1.0000
0.2356
5.2930
04
TRG
PZ-111-SDTOT
07/09113 10:42
1.0000
0.2345
5.2683
::>
05
Tracer
Aliquot(g)
Page 1 of 1
Tracer
ACT{dpm)
Radiometric
Tracer (pCi)
Radiometric
SAF
%Rec
0.00
0.00
TRG
PZ-111-SD DIS
0.00
0.00
~-
07/09/1310:42
1.0000
0.2345
5.2683
0.00
---
06
(,,
"5'
TRG
S-5 TOT
07/09/1310:50
1.0000
0.2343
5.2638
0.00
...l
07
TRG
S-5 DIS
07/09/1310:50
1.0000
0.2335
5.2458
0.00
08
TRG
FB@PZ-110-SS TOT
07/09/13 11 :40
1.0000
0.2338
5.2526
0.00
09
TRG
PZ-110-SS TOT
07/09/13 12:13
1.0000
0.2347
5.2728
0.00
10
TRG
PZ-110-SS DIS
07/09/13 12:13
1.0000
0.2331
5.2368
0.00
11
DO
1-4 TOT
07/09/13 12:25
1.0000
0.2330
5.2346
0.00
12
TRG
1-4 DIS
07/09/13 12:25
1.0000
0.2335
5.2458
0.00
13
TRG
PZ-100-SS TOT
07/0911313:36
1.0000
0.2335
5.2458
14
TRG
PZ-100-SS DIS
07/0911313:36
1.0000
0.2345
5.2683
0.00
15
TRG
D-3TOT
07/09/13 13:42
1.0000
0.2324
5.2211
0.00
16
TRG
D-3 DIS
07/09/1313:42
1.0000
0.2322
5.2166
0.00
17
TRG
PZ-100-SD TOT
07109113 14:32
1.0000
0.2321
5.2144
0.00
18
TRG
PZ-100-SD DIS
07/09/13 14:32
1.0000
0.2326
5.2256
0.00
19
TRG
PZ-112-AS TOT
07/09/13 14:46
1.0000
0.2320
5.2121
20
TRG
PZ-112-AS DIS
07/09/13 14:46
1.0000
0.2329
5.2323
~
~,
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1:11
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-~-
I
I
0.00
0.00
0.00
SAF
2
Eberline Services
Page 1 of 1
Printed: 7/19/2013 8:58 AM
Activity
dpmlg
Solution
Approx
Addition
Analysis Code
b8te
T0Chnician
Th ISO
7/19/2013 8:57
JWOLFE
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Technician Initials
LCS
Known
pCi
MS
Error
Estimate
Added
pCi
- - ------ivrso
LCSD
Error
Estimate
Known
pCi
Witness Initials
Error
Estimate
Added
pCi
Error
Estimate
Isotope
So/#
Th-228
Th-Sb
103.560
7/19/2013
0.100
0.1046
4.88
0.176
0.00
0.000
0.00
0.000
0.00
0.000
Th-230
Th-1b
23.525
7/19/2013
0.500
0.5160
5.47
0.148
0.00
0.000
0.00
0.000
0.00
0.000
Th-232
Th-Bb
103.560
7/19/20131
0.100
0.1046
4.88
0.176
0.00
0.000
o.ool
0.000
0.00
0.000
Date
Tracers
Activity
dpmlg
Solution I
i
Date
Volume
Used(g)
Approx
Addition

Tracer
LCS
fraction
Isotope
Sol#
01
Th-229
Th-18a
22.466 7/19/2013
0.4763
0.2200
02
Th-229
Th-18a
22.466
7/19/2013
0.2385
0.2200
03
Th-229
Th-18a
22.466 7/19/2013
0.2356
0.2200
-0. 2345 :1
04
Th-229
Th-18a
22.466 7/1912013
0.2345
0.2200
-0.
234!:~
05
Th-229
Th-18a
22.466 7/19/2013
0.2345
0.2200
-0 n
23~55
'3
0 .::rf'63 g
o. z3;35 9
-0. z35r::;.
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-""' ,,.,,,. .... ,,,, .,.

~-8. 2::~3~:~ .;:i
06
Th-229
Th-18a
22.466 7/19/2013
0.2343
0.2200
07
Th-229
Th-18a
22.466 7/19/2013
0.2335
0.2200
08
Th-229
Th-18a
22.466 7/19/2013
0;2338
0.2200
--fl"
0.2347
0.2200
-0" 23~5 J. ,::1

{ir. 23~.(:i 3
'
:2~;4 7
Ci.~;it.i~l
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09
Th-229
Th-18a
22.466 7/19/2013
10
Th-229
Th-18a
22.466 7/19/2013
0.2331
0.2200
11
Th-229
Th-18a
22.466 7/19/2013
0.2330
0.2200
12
Th-229
Th-18a
22.466 7/19/2013
0.2335
0.2200
-[i.
2324 9
13
Th-229
Th-18a
22.466 7/19/2013
0.2335
0.2200
-~1.
2322 :1
14
Th-229
Th-18a
22.466
7/19/2013
0.2345
0.2200
--fi. '(''.':21
15
Th-229
Th-18a
22.466 7/19/2013
0.2324
0.2200
16
Th-229
Th-18a
22.466 7/19/2013
0.2322
0.2200
17
Th-229
Th-18a
22.466 7/19/2013
0.2321
0.2200
-Et . 2:;2(21
;~\
18
Th-229
Th-18a
22.466
0.2326
0.2200
19
Th-229
Th-18a
22.466 7/19/2013 ..
0.2320
0.2200
-0~2329
0.2329
0.2200
20
til!I
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m
1-i
Th-229
Version 2.0 08/99
Th-18a
22.466
7/19/2013
7/19/2013
:g:~35 ~
-0. 2345
O::J
.aaau
0. 1046 '3
Matrix Spike
Eberline Analytical
Lab
Analysis Code
Rpt Units
Lab Deadline
Technician
ThiSO
liters
8/6/2013
JWOLFE
Sample
Muffle Data
Type
Ratio
Post/Pre
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
Client ID
LCS
BLANK
1-4 TOT
PZ-111-SD TOT
PZ-111-SD DIS
S-5TOT
S-5 DIS
FB@PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
1-4 TOT
l-4DIS
PZ-100-SS TOT
PZ-100-SS DIS
D-3TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
Comments
1~~ll
,~,,
ir
Technician
Dilution Data
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
Aliquot Data
MS Aliquot Data
No of Dils
Oil Factor
Ratio
'
'
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Aliquot
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------
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Date
1JLI~
Water Added
(ml)
Net Equiv
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO I .1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO 1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO . .1.00POE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO ' 1.0000E+OO
1.0000E+OO I 1.0000E+OO
1.0000E+OO
1:0000E+OO
1.0000E+OO -1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO : : 1.0000E+OO
1.0000E+OO
.1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO I 1.0000E+OO
1.0000E+OO , 1.0000E+OO
H-3 Solids Only
'
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LCS
MBL
DUP
TRG
TRG
TRG
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TRG
TRG
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11!1
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Printed: 711912013 8:49 AM

Page 1 of 1
Aliquot Worksheet
'
H3 Dist
Aliq
'
'
... ..
'
,',,
,'
',
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''
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'
__
~JtApex-Alpha
Sample Geometry:
SPIKE
1307098A-TH
01
Shelf 2
Th iso
Detector Name:
Alpha_045
04026482A

Env. Background:
System Bkgd 62775
Sample Description:
Spectrum File:
91131
Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:

7/25/2013 10:21:48 A.M
7/25/2013
1:26:17 PM
170.0 minutes
170.0 minutes

Th229 TH-18A
0.476 mL
0.1956 +/- 0.0120
0.1909 +/- 0.0033 on 7/20/2013

1.0245 +/- 0.0654
Tracer Certificate:
Tracer Quantity:
Control Certificate Name: NatTh Th-8
TH-232
1.096062 +/Peak Match Tolerance:
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.805
5.368
4.866
4.634
3.963
Net
Pk Area
6.66
387.98
355.83
377.00
394.83
AREA
2:31:26 PM
0.093049
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
78.18
9.97
10.39
10.11
9.87
0.34
1. 02
0.17
0.00
0.17
O.OOE+OOO
0.00E+OOO
O.OOE+OOO
O.OOE+OOO
0.00E+OOO
FWHM
(keV)
3.0
27.4
12.7
23.1
8.8

Id
Energy
Activity
MDA
Nuclide
Conf.
(keV)
(pCi/liter )
(pCi/liter
____
J __________________________________________________________________________
_
TH-227
TH-228
TH-229
TH-230
TH-232
0.989
0.995
1.000
0.993
0.994
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
9.25E-002
5.26E+OOO
4.84E+OOO
5.12E+OOO
5.35E+OOO
+/- 7.32E-002
+/+/+/+/-
8.22E-001
5.83E-001
8.04E-001
8.32E-001
6.64E-002
8.54E-002
5.68E-002
8.14E-002
5.65E-002
+/- 8.00E-003
+/+/+/+/-
1.03E-002
6.84E-003
9.80E-003
6.81E-003
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7/26/2013
Page
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Sample Title:
01
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Elapsed Real Time:
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10200
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fi!2S7
Channel Data Report

369:
7/26/2013
1
Sample Title:
Page
5: :23 :l;:t l:)t
01
Channell------l-------l-------1-------1-------1-------l-------I-------[
377:
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393:
401:
409:
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lll.258
~
Channel Data Report

801:
7/26/2013
0
Sample Title:
5: 23 d.i.
0
Page
0
01
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. .J\
~/"\pex-
Al pha
TM
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1307098A-TH
02
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_046
04026482B
58762
System Bkgd 62776
<not performed>
Sample Size:
Sample Date/Time:

7/25/2013 10:21:48 AM
1:26:19 PM
7 /25/2013
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.238 mL
0.1976 +/- 0.0160
0.1789 +/- 0.0031 on 12/16/2012
1.1044 +/- 0.0914
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.855
5 .272
4.822
4.556
4.076
AREA
REPORT
Pk Area
Error %
Net
Pk Area
6.00
5.83
180.00
11. 83
0.83
86.43
82.55
14.65
57.46
239.53
5:49:23 PM
Ambient
Backgnd
0.00
0.17
0.00
0.17
0.17
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
3.0
6.0
3.6
3.0
3.0
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Id
Conf.
Energy
(keV)
1. 000
0.918
0.987
0.932
0.968
5850.00*
5400.00*
4872.00*
4672. 00*
3997.00*
MDA
(pCi/liter
Activity
(pCi/liter )
8.25E-002
7.82E-002
2.43E+OOO
1.59E-001
1. llE-002
+/- 7.25E-002
+/- 6.58E-002
+/- 3.85E-001
+/- 9.47E-002
+/- 2.67E-002
A-G
?/~(fJ
8.25E-002
5.60E-002
8.08E-002
5.61E-002
5.60E-002
+/- 1.31E-002
+/- 8.88E-003
+/- 1. 28E-002
+/- 8.89E-003
+/- 8.87E-003
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DAT A
R E P 0 R T
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Channel Data Report

369:
7/26/2013
1
Sample Title:
$;~it~
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Page
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B273
..,,
Channel Data Report

801:
7/26/2013
0
Sample Title:
~l~,A.~- . .
0
Page
0
02
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...JtApex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
I-4 TOT DUP

1307098A-TH
03
Shelf 2
Th iso
Alpha_047
02030596A
91086
System Bkgd 62777
Reagent Blank:
<not performed>

1. OOOE+OOO +/O.OOOE+OOO liter

7/9/2013
10:21:48 AM
7/25/2013
1:26:13 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.236 mL
0.1080 +/- 0.0115
0.1822 +/- 0.0032 on 12/16/2012
0.5927 +/- 0.0640
0.175 MeV
Sample Size:
Sample Date/Time:
PEAK
AREA
REPORT
Energy
Net
Pk Area
Nuclide
(MeV)
Pk Area
Error %
TH-227
TH-228
TH-229
TH-230
TH-232
5.794
5.300
4.874
4.678
3.983
2. 83
0.00
97.15
3.15
1. 32
120.53
1960. 0
19.99
126.67
215.97
5:49:21 PM
Ambient
Backgnd
0.17
0.00
0.85
0.85
0.68
FWHM
(keV)
Reagent
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0.00E+OOO
0.00E+OOO
O.OOE+OOO
0.00E+OOO
2.9
0.0
9.3
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.984
0.949
1. 000
1. 000
0.999
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
7.13E-002 +/ 8.73E-002
O.OOE+OOO +/ 6.92E-002
2.40E+OOO +/ 5.00E-001
7.74E-002 +/ 9.94E-002
3.24E-002 +/ 7.03E-002
7(2-Co{I)
MDA
(pCi/liter
1. 05E-001 +/ 2.20E-002
l.50E-001 +/ 3.13E-002
1. 48E-001 +/ 3.08E-002
1. 4 7E-001 +/ 3.07E-002
1. 38E-001 +/ 2.89E-002
0000063972.CNF
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5000
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5500
6000
ROI Type: 3
Channel Data Report
7/26/2013
Page
5:23:25 AM
*******************************************************
S P E C T R A L
DAT A
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
03
Elapsed Live time:

Elapsed Real Time:
10200
10200
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1:
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369:
7/26/2013
0
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Channel Data Report

801:
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~H-',...
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7/25/20l3
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Channel Data Report
7/26/2013
5 ;3314~
iW
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369:
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Channel Data Report

801:
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Sample Title:
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0
0
0
~-
0
0
0
0
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0
0
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0
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0
0
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0
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1
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0
0
~A
~--~-/"\pex-
Al pha

TM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-111-SD DIS
1307098A-TH
05
Shelf 2
Th iso
Detector Name:
Alpha_003

Env. Background:
Reagent Blank:
System Bkgd 62747

<not performed>
Sample Size:
Sample Date/Time:

7/9/2013
10:21:48 AM
7/25/2013
4:25:50 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-lBA
0.235 mL
0.2079 +/- 0.0166
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM

1.1903 +/- 0.0975
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.806
5.411
4.826
4. 537
3.949
Net
Pk Area
2.60
0.45
186.15
8.66
-0.85
AREA
REPORT
Pk Area
Error %
193.34
807.07
14.40
68.12
246.69
Ambient
Backgnd
3.40
2.55
0.85
0.34
0.85
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
3.0
3.0
5.4
3.0
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.990
0.999
0.989
0.909
0.988
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.40E-002
5.83E-003
2.38E+OOO
1.llE-001
-1. 08E-002
+/
+/
+/
+/
+/
6.60E-002
4.71E-002
3.73E-001
7.73E-002
2.68E-002
MDA
(pCi/liter
l.21E-001
1. 09E-001
7.67E-002
6.llE-002
7.63E-002
+/- 1.90E-002
+/- 1. 70E-002
+/- 1.20E-002
+/- 9.55E-003
+/- 1.19E-002
l'G
1()..'f)
~285
0000064057.CNF

start:
1 3498.4{kev)
stop : 1024 6549.S(kev)
60
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Channel Data Report
7/26/2tl13
5;il\t>i
Page
*******************************************************
*****
p E C T R A L
DAT A
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*****
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05
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v.o.
Channel Data Report

369:
7/26/2013
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-m2sa
.....
Channel Data Report

801:
7/26/2013
0
Sample Title:
Page
5:23:40 AN
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cft(A
Al pha

~/"\pexTM
Sample Description:
Spectrum File:
Sample Geometry:
S-5 TOT
1307098A-TH
06
Shelf 2
Th iso
Detector Name:
Alpha_004
Env. Background:
Reagent Blank:
System Bkgd 62748

<not performed>
1.000E+OOO +/
O.OOOE+OOO liter
7/9/2013
10:21:48 AM
7/25/2013
4:25:51 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
Th229 TH-18A
0.234 mL
0.1235 +/ 0.0124
0.1940 +/
0.0036 on 12/15/2012 11:26:46 AM
0.6363 +/
0.0652
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.747
5.310
4.866
4.604
3. 937
AREA
REPORT
FWHM
(keV)
Net
Pk AJCea
Ambient
Reagent
Pk Area
Error %
Backgnd
Backgnd
1.53
2.21
1. 53
1. 53
0.68
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
4.47
6.79
110.47
4.47
8.32
109. 71
88.39
18.80
109.71
71.13
2.9
5.9
4.9
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.946
0.959
1. 000
0.976
0.981
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/liteJC )
9.85E-002
1.48E-001
2.38E+OOO
9.61E-002
l.79E-001
+/
+/
+/
+/
+/
1. lOE-001
l.34E-001
4. 71E-001
1. 07E-001
l.32E-001
AG
7/8.{-f"J
MDA
(pCi/liter
l.57E-001
l.75E-001
l.53E-001
l.53E-001
l.21E-001
+/ 3.lOE-002
+/ 3.45E-002
+/ 3.03E-002
+/ 3.02E-002
+/ 2.39E-002
0000064058.CNF

60
start:
1:3493.l(kev)
stop: 1024:6486.9(kev)
Acq. Start :Thu Jul 25 16:25:51 2013
55
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5500
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6500
Channel Data Report
Page
7/26/2013
*******************************************************
S P E C T R A L
DAT A
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
06
Elapsed Live time:

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369:
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0
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0
~293
Channel Data Report

801:
7/26/2013
0
Sample Title:
5:23:49
0
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0
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0
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0
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0
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0
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1
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0
0
0
0
~~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
S-5 DIS
1307098A-TH
07
Shelf 2
Th iso
C---
H~
i .
Detector Name:
Alpha_OlO

10
Env. Background:
System Bkgd 62749
Reagent Blank:
<not performed>
Sample Size:
10:21:48 AM
7/9/2013
7/25/2013
4:25:44 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
Th229_TH-18A
0.234 mL
0.1588 +/- 0.0143
0.1967 +/- 0.0036 on 12/15/2012 11:26:40 AM
0.8073 +/- 0.0744
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.865
5.383
4.879
4.644
3.868
Net
Pk Area
1. 79
4.28
141.62
0.64
-0.36
AREA
REPORT
FWHM
(keV)
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
2.21
2.72
2.38
1.36
1. 36
0.00E+OOO
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
229. 04
125.10
16.63
457.43
604.15
2.9
2.9
4.3
2.9
2.9
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
Id
Conf.
Energy
(keV)
0.999
0.998
1.000
0. 996
0.917
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.07E-002
7.26E-002
2.37E+OOO
1. 07E-002
-6.0lE-003
+/
+/
+/
+/
+/
7.05E-002
9.17E-002
4.20E-001
4.90E-002
3.63E-002
MDA
(pCi/liter
1.37E-001
1.45E-001
l.37E-001
1.15E-001
l.14E-001
+/
+/
+/
+/
+/
2.43E-002
2.58E-002
2.43E-002
2.03E-002
2.03E-002
fJ.G
1(~('3
ti2~l5
0000063994.CNF

start:
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Acq. Start :Thu Jul 25 16:25:44 2013
55
50
45
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35
'-'
s=
::::s
8 30
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I I
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ROI Type: 1
5000
Energy(kev)
6000
5500
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6500
Channel Data Report
li!:~~lii
7/2?/:2013
!?age
*******************************************************
*****
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DAT A
RE P 0 R T
*****
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07
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Channel Data Report

369:
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'1Jl29S
~
Channel Data Report

801:
7/26/2013
0
Sample Title:
5:23:57
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1
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1
1
0
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0
0
0
4t{A
~~-5'/"'\pex-
Al pha
TM
Sample Description:
Spectrum File:
Sample Geometry:
FB@PZ-110-SS TOT
l307098A-TH
08
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_Oll
ll
System Bkgd 62750
<not performed>
Sample Size:
Sample Date/Time:

10:21:48 AM
7/9/2013
7/25/2013
4:25:45 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.2217 +/- 0.0172
0.2051 +/- 0.0035 on 7/20/2013
1.0810 +/- 0.0861
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.807
5.404
4.874
4.552
4.008
Net
Pk Area
l.64
-0.21
197.98
7.32
2.66
AREA
2:50:46 PM
REPORT
Pk Area
Error %
214.85
1437.1
13.97
76.28
128.85
Ambient
Backgnd
1. 36
2.21
1.02
0.68
0.34
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
2.6
2.6
5.6
2.6
5.2
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.990
1.000
1. 000
0.928
0.999
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.0lE-002
-2.55E-003
2.38E+OOO
8.76E-002
3.l8E-002
+/+/+/+/+/-
4. 34E-002
3.67E-002
3.62E-001
6.82E-002
4.12E-002
Ac
"1(Jro(r3
MDA
(pCi/liter
8.42E-002
9.72E-002
7.57E-002
6.75E-002
5.7lE-002
+/+/+/+/+/-
1.28E-002
l.48E-002
1.15E-002
l.03E-002
8.7lE-003
0000064059. CNF

60
start:
1:3640.l(kev)
Stop : 1024:6315.J(kev)
Acq. Start :Thu Jul 25 16:25:45 2013
55
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45
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6000
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Channel Data Report
7/26/2013
Page
!ii :~41a~.
*******************************************************
*****
p E CTR AL
DAT A
RE p 0 R T
*****
*******************************************************
Sample Title:
08
Elapsed Live time:

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m3m2
Channel Data Report

369:
7/26/2013
0
Sample Title:
5;jl#~4j
w
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Pa,ge
0
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J!l 31!l 3
Channel Data Report

801:
7/26/2013
0
Sample Title:
5; ;Ji 1.U
0
Page
~
0
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-110-SS TOT
1307098A-TH
09
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_Ol2
12
System Bkgd 62751
<not performed>
Sample Size:
Sample Date/Time:

10:21:48 AM
7/9/2013
7/25/2013
4:25:46 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.235 mL
0.1437 +/- 0.0134
0.1989 +/- 0.0034 on 12/11/2011
0.7225 +/- 0.0687
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.766
5.321
4.854
4.601
3.989
AREA
REPORT
Pk Area
Error %
Net
Pk Area
2.66
2.66
128.83
10.83
1. 00
2:21:56 PM
128.85
128.85
17.28
60.10
277.19
Ambient
Backgnd
0.34
0.34
0.17
0.17
0.00
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
3.6
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.963
0. 968
0.998
0.974
1.000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
5.04E-002
4.99E-002
2. 3 9E+OOO
2.00E-001
1. 84E-002
+/+/+/+/+/-
6.55E-002
6.49E-002
4.37E-001
l.26E-001
5.12E-002
/tG
'7 (;w,{(3
MDA
(pCi/liter
9.05E-002
8.96E-002
7.73E-002
7.71E-002
1. llE-001
+/+/+/+/+/-
l.66E-002
1. 64E-002
l.42E-002
1.41E-002
2.02E-002
0000063993.CNF

Start:
1 3502.l(kev)
Stop : 1024 6535. 3(kev)
60+
55
II
50
45
40
35
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25
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6000
ROI Type: 3
6500
Channel Data Report
7/26/2013
5:24:12
Page
*******************************************************
S P E C T R A L
DAT A
R E P 0 R T
*****
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
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Channel Data Report

369:
7/26/:2013
0
Sample Title:
$1Mll If
0
Page
0
09
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~311i-8
Channel Data Report

801:
7/26/2013
0
Sample Title:
Page
5:24::j,).
0
09
Channell------l-------l-------l-------l-------l-------1-------1-------1
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817:
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0
0
0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
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0
~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
PZ-110-SS DIS
1307098A-TH
10
Shelf 2
Th iso
Alpha_Ol3
13
System Bkgd 62752
Reagent Blank:
<not performed>

7/9/2013
10:21:48 AM
7/25/2013
4:25:47 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229_TH-18A
0.233 mL
0.2280 +/- 0.0175
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
1.2198 +/- 0. 0965
0.175 MeV
Sample Size:
Sample Date/Time:
PEAK
Nuclide
Energy
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
5.823
5.394
4.846
4.666
3.967
Net
Pk Area
1.43
-0.74
202.98
8.98
5.32
AREA
REPORT
Pk Area
Error %
324.62
504.84
13.80
69.62
91.11
Ambient
Backgnd
3.57
3.74
1.02
1. 02
0.68
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
2.8
2.8
5.1
2.8
2.8
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.996
1. 000
0.996
1. 000
0.995
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
l.71E-002
-8.75E-003
2.37E+OOO
l.05E-001
6.18E-002
+/
+/
+/
+/
+/
5.55E-002
4.42E-002
3.57E-001
7.45E-002
5.71E-002
J:16
l(J<o(f)
MDA
(pCi/liter
l.13E-001
l.13E-001
7.36E-002
7.33E-002
6.56E-002
+/
+/
+/
+/
+/
1. 70E-002
1. 71E-002
1. llE-002
1. llE-002
9.88E-003
0000063996.CNF

Start:
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Acq. Start :Thu Jul 25 16:25:47 2013
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Channel Data Report
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nf313
Channel Data Report

801:
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__stApex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
I-4 TOT
1307098A-TH
11
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_Ol4
14
System Bkgd 62753
<not performed>
Sample Size:
Sample Date/Time:

7/9/2013
10021:48 AM
7/25/2013
4:25:48 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.1712 +/- 0.0149
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
0.9273 +/- 0.0827
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.833
5.355
4.860
4.530
3.943
AREA
REPORT
Pk Area
Error %
Net
Pk Area
4.28
0.77
152.30
3.64
0.66
125.10
542.91
15.99
123.16
305.43
Ambient
Backgnd
2. 72
3.23
1. 70
1. 36
0.34
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
4.4
2.9
4.7
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.998
0.990
0.999
0.900
0.985
5850.00*
5400.00*
4872. 00*
4672. 00*
3997.00*
Activity
(pCi/liter )
6.81E-002 +/- 8.59E-002

1. 21E-002 +/- 6.58E-002
2.37E+OOO +/- 4.05E-001

5.65E-002 +/- 7.02E-002
1. 02E-002 +/- 3.13E-002
fJ.G
7{~0
MDA
(pCi/liter
l.36E-001
l.43E-001
l.14E-001
1. 06E-001
7.40E-002
+/+/+/+/+/-
2.33E-002
2 .45E-002
l.95E-002
l.82E-002
l.27E-002
0000064060 .CNF
live Time 10200.000 sec

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7/26/2013
Page
5:24:26 AM
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*****
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Sample Title:
11
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'n1318
Channel Data Report

801:
7/26/2013
0
Sample Title:
5;@.f1.fj
0
w
0
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0
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fJl.319
~~Apex-Alpha
I-4 DIS
1307098A-TH
12
Shelf 2
Th iso
Detector Name:
Alpha_Ol5
Sample Description:
Spectrum File:
Sample Geometry:
Numb~r:
Chamber Serial

Env. Background:
15
System Bkgd 62754
Reagent Blank:
<not performed>

10:21:48 AM
7/9/2013
7/25/2013
4:25:49 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Th229 TH-18A
0.234 mL
0.1947 +/- 0.0160
0.1477 +/- 0.0027 on 7/20/2013
1.3181 +/- 0.1107
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.802
5.336
4.869
4.695
3.883
AREA
6:27:27 PM
REPORT
Net
Pk Area
Ambient
Reagent
Pk Area
Error %
Backgnd
Backgnd
3.00
3.98
173.66
8.32
2.83
130.67
112. 01
14.89
71.13
120.54
0.00
1.02
0.34
0.68
0.17
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
4.5
12.5
4.5
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.988
0.979
1.000
0.997
0.934
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.19E-002
5.51E-002
2.37E+OOO
l.13E-001
3.85E-002
+/
+/
+/
+/
+/
5.52E-002
6.23E-002
3.82E-001
8.27E-002
4.68E-002
A:G
7 f.)<oi(>
MDA
(pCi/liter
8.38E-002
8. 72E-002
6.54E-002
7.69E-002
5.68E-002
+/
+/
+/
+/
+/
l.35E-002
l.40E-002
1. 05E-002
l.24E-002
9.13E-003
0000063998.CNF

start:
1:3490.S(kev)
stop : 1024:6558.S(kev)
Acq. Start :Thu Jul 25 16:25:49 2013
60
55
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4500
4000
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~.II
ROI Type: 1
5000
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5500
6000
ROI Type: 3
6500
Channel Data Report
7/26/2013
5:24:36 AW
Page
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*****
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DAT A
R E P 0 R T
*****
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Sample Title:
12
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B323
Channel Data Report

801:
7/26/2013
0
Sample Title:
Page
5:24:3G" M(
0
12
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1
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0
~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-SS TOT
1307098A-TH
13
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_033
04026479A
91132
System Bkgd 62765
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/0.000E+OOO liter

7/9/2013
10:21:48 AM
7/25/2013
4:27:29 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.0147
0.1674 +/0.1848 +/0.0032 on 7/20/2013
0.9060 +/- 0.0810
0.175 MeV
PEAK
Nuclide
Energy
(MeV)
TH-227
TH-228
TH-229
TH-230
TH-232
5.874
5.307
4.866
4.537
3.990
Net
Pk Area
-0.51
2.32
149.32
10.83
2.00
AREA
2:31:30 PM
REPORT
Pk Area
Error %"
Ambient
Backgnd
0.51
0.68
0.68
0.17
0.00
400.63
149 .12
16.08
60.10
169.74
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
0.0
3.0
3.3
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.956
1.000
0.909
1.000
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/liter )
-8.29E-003
3.73E-002
2.37E+OOO
1. 72E-001
3.16E-002
+/+/+/+/+/-
3.32E-002
5.60E-002
4.08E-001
1. 07E-001
5.40E-002
MDA
(pCi/liter
8.53E-002
9.08E-002
8.97E-002
6.62E-002
9.49E-002
+/+/+/+/+/-
l.47E-002
1. 56E-002
1. 54E-002
1.14E-002
1. 63E-002
..AG
7/~()
~325
0000064061. CNF

start:
1 3447 .3(kev)
stop : 1024 6496.6(kev)

Acq. Start Thu Jul 25 16:27:2g 2013
60
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1
11
I If II ..
_
i_
5000
Energy(keV)
5500
6000
ROI Type: 3
6500
Channel Data Report
Page
7/26/2013
*******************************************************
*****
S P E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
13
Elapsed Live time:

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!3.27
Channel Data Report

369:
7/26/2013
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5:24:11~
Page
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-''
Channel Data Report

801:
7/26/20'.l.3
0
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Page
5 :2~ , . , . ,
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Detector Name:
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PZ-lOO-SS DIS
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Reagent Blank:
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l. OOOE+OOO +/- O.OOOE+OOO liter

l0:2l:48 AM
7/9/20l3
7/25/20l3
4: 27: 3l PM
l70.0 minutes
l 70. 0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-l8A
0.235 mL
O.l559 +/- O.Ol4l
0.1856 +/- 0.0032 on 12/16/2012
0.8404 +/- 0.0772
0.175 MeV
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PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.859
5.357
4.858
4.560
3.994
AREA
REPORT
Net
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Ambient
Reagent
Pk Area
Error %
Backgnd
Backgnd
0.83
3.15
139. 66
l. 00
2.83
5:49:43 PM
239.53
l26.67
16.61
277.19
120.53
0.17
0.85
0.34
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0.00E+OOO
0.00E+OOO
0.00E+OOO
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7.1
3.0
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0.990
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1.000
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4872. 00*
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Channel Data Report
7/26/2013
5: ;#I tiif
Page
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*****
p E C T R A L
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Channel Data Report

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Ui333
Channel Data Report

801:
7/26/;2013
0
Sample Title:
5:~4l"
0
\'
Page
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D-3 TOT
1307098A-TH
15
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Detector Name:
Alpha_035
04026477A
58771
Env. Background:
System Bkgd 62767

Reagent Blank:
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7/9/2013
10:21:48 AM
7/25/2013
4:27:24 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
Th229 TH-18A
0.232 mL
0.1228 +/- 0.0124
0.1826 +/- 0.0032 on 12/16/2012

0.6726 +/- 0.0690
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.742
5.344
4.882
4.671
3.949
Net
Pk Area
2.00
7.00
109.00
7.00
-0.17
AREA
5:49:42 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
169.74
79.20
18.86
79.20
1169.4
0.00
0.00
0.00
0.00
0.17
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
5.9
2.9
3.7
2.9
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.941
0.984
1. 000
1. 000
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.43E-002
1.54E-001
2.36E+OOO
1. 51E-001
-3.67E-003
+/
+/
+/
+/
+/
7.57E-002
1.25E-001
4.68E-001
1. 24E-001
4.29E-002
MDA
(pCi/liter
1. 33E-001
1. 32E-001
1.30E-001
1.30E-001
9.00E-002
+/+/+/+/+/-
2.63E-002
2.61E-002
2.58E-002
2.57E-002
1. 78E-002
}4
1(:>..v(t3
ID33.5
0000064003.CNF
Live Time
Real Time
60
10200.000 sec
10200.100 sec
Start:
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Channel Data Report
7/26/2013
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RE P 0 R T
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'li338
Channel Data Report

801:
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15
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4ffA
~~~f"\pex- Al
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
pha

TM
D-3 DIS
1307098A-TH
16
Shelf 2
Th iso
Alpha_036
040264778
84167
System Bkgd 62768
<not performed>
Sample Size:

10:21:48 AM
7/9/2013
4:27:26 PM
7/25/2013
170.0 minutes
Sample Date/Time:
170.0 minutes
Th229 TH-18A
0.232 mL
0.1958 +/- 0.0161
0.1910 +/- 0.0033 on 7/20/2013
1.0254 +/- 0.0860
0.175 Mev
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.738
5.317
4.862
4.547
3.951
AREA
REPORT
Pk Area
Error %
Net
Pk Area
3.32
12.98
173.66
6.66
2.32
2:31:37 PM
119.77
56.85
14. 89
78.18
149 .12
FWHM
(keV)
Ambient
Reagent
Backgnd
Backgnd
0.68
1. 02
0.34
0.34
0.68
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
3.0
3.0
4.1
3.0
3.0

---------------------------------L---------------
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.937
0.965
0.999
0.922
0.989
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.61E-002
1. 79E-001
2.36E+OOO
9.03E-002
3.14E-002
+/+/+/+/+/-
5.58E-002
l.06E-001
3.80E-001
7.21E-002
4.71E-002
AG
7/413
MDA
(pCi/liter
7.84E-002
8.67E-002
6.50E-002
6.48E-002
7.63E-002
+/+/+/+/+/-
1.26E-002
1. 39E-002
l.OSE-002
1. 04E-002
1. 23E-002
0000064063.CNF

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5SOO
6000
ROI Type: 3
Channel Data Report
7/26/2013
Page
5:4:<84 ~
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p E C T R A L
DAT A
RE P 0 R T
*****
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16
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Channel Data Report

369:
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fi343
Channel Data Report

801:
7/26/2013
0
Sample Title:
5:251i~
Page
iH0
16
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4t(A
Al pha
~~..21"\pex-
Sample Description:
Spectrum File:
Sample Geometry:
Procedure Desc.ription:
TM
PZ-100-SD TOT
1307098A-TH
17
Shelf 2
Th iso
Detector Name:
Alpha_038
040264788
91134
Env. Background:
System Bkgd 62770

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:


10:21:48 AM
7/9/2013
7/25/2013
4:27:27 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.2207 +/- 0.0172
0.1722 +/- 0.0030 on 5/11/2013

1.2821 +/- 0.1025
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.852
5.290
4.890
4.634
3.958
AREA
REPORT
Pk Area
Error %
Net
Pk Area
3.32
1.64
195.66
8. 49
0.83
5:13:35 PM
119.77
214. 83
14.03
69.59
239.53
Ambient
Backgnd
0.68
1.36
0.34
0.51
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
4.7
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1. 000
0.938
0.998
0.993
0.992
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
4.09E-002
2.00E-002
2.36E+OOO
1. 02E-001
9.96E-003
+/
+/
+/
+/
+/
4.94E-002
4.31E-002
3.61E-001
7.27E-002
2.39E-002
MDA
(pCi/liter
6.95E-002
8.37E-002
5.77E-002
6.31E-002
5.0lE-002
+/+/+/+/+/-
l.06E-002
l.28E-002
8.82E-003
9.65E-003
7.66E-003
1!~(/1 I'!>
{;]345
0000064001.CNF
start:
1 3482.S(kev)
stop : 1024 6501.G(kev)
55
35
25
20
15
10
0
3500
!)
4000
4500
t~:~
t~.11
.it:;~.
l:lfll
l:[.i ! J,1
11~p,l11\1i1l
!) '~:{id
1
11111 ~(11\:J 1;11

11
1,tl , JJ!
i='
ROI Type: 1
11
'i! , 111 ,.;1W
11 , Jn,: ia1~
5000
Energy(kev)
,I,!
11,
6000
5500
ROI Type: 3
6500
Channel Data Report

369:
7/26/2013
0
Sample Title:
Page
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-fi:3A8
Channel Data Report

801:
7/26/2013
1
Sample Title:
Page
5:25:11 AM
0
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/"\pex- Al pha

tfttJ\
~____,~-=
TM
Sample Geometry:
PZ-100-SD DIS
1307098A-TH
18
Shelf 2
Th iso
Sample Description:
Spectrum File:
Detector Name:
Alpha_039
06027396A
83109
Env. Background:
System Bkgd 62771

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
7/9/2013
10:21:48 AM
7/25/2013
4:27:34 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.1668 +/- 0.0147
0.1965 +/- 0.0034 on 4/20/2013
0.8487 +/- 0.0762
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.757
5.282
4.875
4.498
4.042
AREA
REPORT
Pk Area
Error %
Net
Pk Area
3.00
1. 81
148.15
5.66
1.49
2:01:25 PM
FWHM
(keV)
Ambient
Reagent
Backgnd
Backgnd
0.00
1.19
0.85
0.34
0.51
0.00E+OOO
O.OOE+OOO
0.00E+OOO
0.00E+OOO
O.OOE+OOO
13 0. 67
193.78
16.16
85.23
190.02
3.0
3.0
14 .1
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.956
0. 929
1.000
0.853
0.989
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/ liter )
4.90E-002
2.92E-002
2.37E+OOO
9.0lE-002
2.37E-002
+/
+/
+/
+/
+/
6.45E-002
5.69E-002
4.08E-001
7.83E-002
4.52E-002
14
1(:xof0
MDA
(pCi/liter
9.78E-002
1. 06E-001
9.56E-002
7.61E-002
8.34E-002
+/+/+/+/+/-
1. 69E-002
1. 84E-002
1. 65E-002
1.31E-002
l.44E-002
0000064064.CNF
Live Time
Real Time
10200.000 sec
10200.100 sec
start:
1 3449.7(kev)
stop : 1024 6497.l(kev)
55
35
V>
+-'
<=
8 30
25
20
15
10
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'
3500
1"1
ll'I
~,,..,i,,
!l
,\ ,\
4500
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ROI Type: 1
5000
Energy(kev)
6000
5500
ROI Type: 3
6500
Channel Data Report
7/26/2013
5:2S,t
Page
*******************************************************
*****
p E C T R A L
DAT A
R E p 0 R T
*****
*******************************************************
Sample Title:
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m352
Channel Data Report

801:
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Sample Title:
5:25:'1~
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c!t(A
~~~/'"\pexSample Description:
Spectrum File:
Sample Geometry:
Al pha

TM
PZ-112-AS TOT
1307098A-TH
19
Shelf 2
Th iso
Detector Name:
Alpha_040
060273968
91135
Env. Background:
System Bkgd 62772

Reagent Blank:
<not performed>
Sample Size:
Sample Date/Time:
1. OOOE+OOO +/0.000E+OOO liter

10:21:48 AM
7/9/2013
7/25/2013
4:27:36 PM
170.0 minutes
Acquisiti~n
Real Time:
170.0 minutes
Th229_TH-18A
0.232 mL
0.1623 +/- 0.0144
0.1900 +/- 0.0033 on 12/16/2012

0.8544 +/- 0.0775
0.175 MeV
Tracer Certificate:
Tracer Quantity:
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.860
5.263
4.890
4.503
3.910
Net
Pk Area
3.49
3.83
143.83
10.00
1. 00
AREA
5:49:33 PM
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
113.53
1.(12. 72
16.35
65.01
277.19
0.51
0.17
0.17
0.00
0.00
FWHM
(keV)
O.OOE+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
3.0
3.0
7.4
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.999
0.907
0.998
0.861
0. 962
5850.00*
5400.00*
4872. 00*
4672.00*
3997.00*
Activity
(pCi/liter )
5.85E-002
6.36E-002
2.36E+OOO
l.64E-001
1. 63E-002
+/
+/
+/
+/
+/
6.72E-002
6.62E-002
4.12E-001
1. lOE-001
4.53E-002
MDA
(pCi/liter
8.80E-002
6.93E-002
6.84E-002
9.80E-002
9.79E-002
+/+/+/+/+/-
1. 53E-002
1. 21E-002
l.19E-002
1. 71E-002
1. 71E-002
?/~(()
i!!355
0000064065.CNF

Start:
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i:>..il
!Al
U1
1:111!
"'
/,1! I
11
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4000
ROI Type: 1
5000
Energy(keV)
5500
6000
ROI Type: 3
6500
Channel Data Report
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*****
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RE P 0 R T
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t!357
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0
-ID35:9
~..JtApex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-112-AS DIS
1307098A-TH
20
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 62773
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/O.OOOE+OOO liter

10:21:48 AM
7/9/2013
7/25/2013
4:27:32 PM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-l8A
0.233 mL
0.1615 +/- 0.0144
0.1978 +/- 0.0034 on 12/16/2012
0.8164 +/- 0.0741
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5. 849
5.303
4.855
4.551
3. 996
Net
Pk Area
2.15
4.49
143.66
7.98
-2.42
AREA
5:49:31 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
161. 66
98.45
16.38
74.39
134.34
0.85
0.51
0.34
1. 02
4.42
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
0.00E+OOO
3.0
3.0
4.0
4.5
3.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
1.000
0.952
0.998
0. 927
1.000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
3.62E-002
7.49E-002
2.37E+OOO
1.31E-001
-3.97E-002
+/+/+/+/+/-
5.89E-002
7.49E-002
4.14E-001
1. OOE-001
5.38E-002
Ac
7/~/r3
MDA
(pCi/liter
1. OlE-001
8.75E-002
7.88E-002
1. 04E-001
1. 67E-001
+/+/+/+/+/-
l.76E-002
1. 53E-002
l.38E-002
l.81E-002
2.92E-002
0000064066.CNF

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Channel Data Report
Page
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S P E C T R A L
DAT A
R E P 0 R T
*****
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=ID363
Channel Data Report

801:
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Page 1 of 2
7/25/2013 5:32:50 AM
Jt'Apex-Alpha'l
QA SUMMARY REPORT

Date
Time
: 7/25/2013
: 5:32:50 AM
CHAMBER
Alpha 001
Aloha 002
Alpha 003
Aloha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Aloha 009
Alpha 010
Aloha 011
Alpha 012
Aloha 013
Alpha 014
Alpha 015
Aloha 016
Alpha 017
Aloha 018
Alpha 019
Aloha 020
Alpha 021
Aloha 022
Alpha 023
Alpha 024
Aloha 025
Alpha 026
Aloha 027
Alpha 028
Aloha 029
Alpha 030
Aloha 031
Alpha 032
Aloha 033
Aloha 034
Aloha 035
Alpha 036
Aloha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2\f
2lf
2lf
21f
2\f
2\f
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Aloha Analvst IOODC
Alpha Analyst! OODC
Aloha Analvstl OODC
Alpha Analyst!OODC
Aloha Analvst 1OODC
Alpha Analyst!OODC
AIPha Analvstl OODC
Alpha Analyst 1OODC
AIPha Analvst!OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
7/25/2013 5:16:27 AM
7/25/2013 5:16:28 AM
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/2512013
5:16:29 AM
5:16:29 AM
5:16:30 AM
5:16:31 AM
5:16:32 AM
5:16:33 AM
7/25/2013 5:16:34 AM
7/25/2013 5:16:34 AM
7/25/2013
7/25/2013
7/25/2013
7/25/2013
5:16:35 AM
5:16:36 AM
5:16:37 AM
5:16:38 AM
7/25/2013 5:16:38 AM
7/25/2013 5:16:39 AM
7/25/2013 5:16:40 AM
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
7/25/2013
5:16:41 AM
5:16:42 AM
5:16:44 AM
5:16:45 AM
5:16:46 AM
5:16:48 AM
5:16:49 AM
5:16:51 AM
5:16:52 AM
5:16:54 AM
~365
Page 2 of 2

7/25/2013 5:32:50 AM
CHAMBER
Alpha 043
Aloha 044
Alpha 045
Aloha 046
Alpha 047
Aloha 048
DEVICE
Alpha Analyst! OODC
Aloha Analyst! OODC
Aloha Analyst! OODC
Aloha AnalystlOODC
Alpha Analyst! OODC
Aloha AnalvstlOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
APPROVED BY:
APPROVAL DATE:
FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed
DATE
7/25/2013
7/25/2013
7/25/2013
7/25/2013
5:16:56
5:16:57
5:16:59
5:17:00
AM
AM
AM
AM
6/12/12
Page
12:16:29 PM
*************************************************************************
L I B R A R Y
*****
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Thorium
Nuclide
Name
Half-Life
(Seconds)
TH-227
TH-228
TH-229
TH-230
TH-232
6.873E+008
6.034E+007
2.487E+Oll
2.379E+Ol2
4.434E+017
Th-227,-228,-229,-230,-232
Energy
(keV )
Energy
Uncert. (keV
5850.000*
5400.000*
4872.000*
4672.000*
3997.000*
0.000
0.000
0.000
0.000
0.000
Yield
( %)
97.5000
99.9400
99.5200
99.8200
100.0000
Yield
Uncert. (Abs.+-)
0.0000
0.0000
0.0000
0.0000
0.0000
key line
TOTALS:
Nuclides
Energy Lines
.fJ367
SECTIONX
ANALYTICAL DATA (RADIUM-226)
i368
Eberline Services
Analysis Sheet
13-07098
Printed: 7/24/201312:28 PM
Page 1 of3
Ra226
Run 1
Work Order
Analysis Code
Run
Date Received
Lab Deadline
13-07098
Internal
Fra'ction
Ra226
01
02
7/15/2013
8/6/2013
Client I Engineering Management Support, Inc.
Project I
Report Level
Activity Units
Sample
Desc
Client
ID
LCS
LCS
Login
CPM
Sample
Date
07/16/13 00:00
-
03
04
MBL
BLANK
DUP
TRG
1-4 TOT
II
44
PZ-111-SD TOT
36
Sample
Aliquot
I
I
1.0000E+OO
II
07/16/13 00:00
1.0000E+OO
07/09/13 12:25
1.0000E+OO
--,
07/09/13 10:42
1.0000E+OO
05
TRG
PZ-111-SD DIS
36
07/09/13 10:42
1.0000E+OO
06.
TRG
S-5 TOT
45
07/09/13 10:50
1.0000E+OO
07
TRG
S-5 DIS
45
07/09/13 10:50
pCi
08
TRG
FB@ PZ-110-SS TOT
43
07/09/13 11 :40
09
TRG
PZ-110-SS TOT
41
07/09/13 12:13
West Lake OU-1
t-~~~~~~~~1
'
1.0000E+OO
-
1.0000E+OO
'
Aliquot Units
1.0000E+OO
-
WA
07/09/13 12:13
1.0000E+OO
07/09/13 12:25
1.0000E+OO
10
TRG
PZ-110-SS DIS
41
11
DO
1-4 TOT
44
12
TRG
1-4 DIS
44
07/09/13 12:25
Ba-133
13
TRG
PZ-100-SS TOT
46
07/09/13 13:36
1.0000E+OO
Radiometric Sol#
Ba-Ga
14
TRG
PZ-100-SS DIS
46
07/09/13 13:36
1.0000E+OO
Tracer Act (dpm/g)
993.635
15
TRG
D-3 TOT
43
07/09/13 13:42
1.0000E+OO
Carrier
16
TRG
D-3 DIS
43
07/09/13 13:42
1.0000E+OO
17
TRG
PZ-100-SD TOT
39
07/09/13 14:32
1.0000E+OO
18
TRG
PZ-100-SD DIS
39
07/09/13 14:32
19
TRG
PZ-112-AS TOT
45
07/09/13 14:46
1.0000E+OO
20
TRG
PZ-112-AS DIS
07/09/13 14:46
1.0000E+OO
Matrix
Method
Instrument Type
Radiometric Tracer
E903.0
Alpha Spectroscopy
II
I
I
45
I
!
1.0000E+OO
1.0000E+OO
t':all1
IJ.ji
llll
K.l!lt
Eberline Services
Analysis Sheet
Printed: 7/24/201312:28 PM
Page 2 of 3
13-07098
Ra226
Run 1
IRadiometric IGrav Ca"ier

% Rec
I Added (ml)
Internal
Fraction
Sample
Desc
01
LCS
0.9214
915.5
397.0
96.26
0.0226
0.0293
0.0067
02
MBL
0.9118
906.0
351.3
86.08
0.0224
0.0287
03
DUP
0.9114
905.6
383.9
94.11
0.0224
04
TRG
0.9096
903.8
385.9
94.79
05
TRG
0.9105
904.7
386.0
06
TRG
0.9085
902.7
227.5
Tracer
Aliquot (g)
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
Grav Filter
Tare (g)
Grav Filter
Final (g)
Grav Filter
Net(g)
Grav
%Rec
Mean
%Rec
SAF
SAF
96.26
2.40
1.00
0.0063
86.08
2.27
1.00
0.0296
0.0072
94.11
2.55
1.00
0.0225
0.0291
0.0066
94.79
2.37
1.00
94.72
0.0227
0.0295
0.0068
94.72
2.44
1.00
55.95
0.0224
0.0331
0.0107
55.95
3.50
1.00
'
07
TRG
0.9086
08
TRG
0.8957
902.8
280.0
68.85
0.0227
0.0375
0.01481
68.85
6.24
1.00
890.0
339.1
84.58
0.0225
0.0283
0.0058
84.58
2.08
1.00
88.65
0.0224
0.0290
0.0066
88.65
2.37
1.00
2.37
1.00
'
09
TRG
0.9078
902.0
360.2
10
TRG
0.9090
903.2
391.6
96.25
0.0227
0.0293
0.0066
96.25
11
DO
0.9076
901.8
410.0
100.93
0.0224
0.0334
0.0110
100.93
3.61
1.00
12
TRG
0.9114
905.6
354.2
86.83
0.0224
0.0339
0.0115
86.83
3.82
1.00
13
TRG
0.9086
902.8
362.2 i
89.06
0.0225
0.0289
0.0064
89.06
2.31
1.00
14
TRG
0.9057
899.9
385.1
95.00
0.0225
0.0288
0.0063
95.00
2.27
1.00
15
TRG
0.9055
899.7
356.1
87.86
0.0225
0.0363
0.0138
87.86
5.26
1.00
16
TRG
0.9046
898.8
332.7
82.17
0.0226
0.0373
0.0147
82.17
6.13
1.00
97.47
2.37
1.00
'
17
t~
"''
~~~I
..
TRG
0.9066
900.8
18
TRG
0.9067
900.9
19
TRG
0.9063
20
TRG
0.9059
395.5
97.471
'
0.0291
0.00661
I
0.0226
0.0285
0.00591
98.37
2.12
1.00
96.04
0.0225
0.0361
0.01361
96.04
5.10
1.00
89.82
0.0225
0.0329
0.01041
89.82
3.40
1.00
399.2
98.37
900.5
389.6
900.1
364.2
0.0225
Eberline Services
Analysis Sheet
Printed: 7/24/2013 12:28 PM

Page 3 of 3
13-07098
Ra226
Run 1
Internal
Fraction
Sample
Desc
Rough Prep
Date
Rough Prep
By
I
Prep
Date
Prep
By
Sep to
Sep to
Sep t1
Sep t1
Date/Time
By
Date!Time
By
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
01
LCS
02
MBL
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
03
DUP
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
04
TRG
07/19/13 08:55
JWOLFE
07123113 12:55
LWALKER
05
TRG
07/19/13 08:55
07/23/13 12:55
LWALKER
JWOLFE
I
'
I
I
06
TRG
07119/13 08:55
07
TRG
08
JWOLFE
07/23/13 12:55
LWALKER
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
09
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
10
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
11
DO
07/19/13 08:55
JWOLFE
07/23/1312:55
LWALKER
12
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
13
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
14
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
'
15
TRG
16
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
17
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
18
TRG
07/19/13 08:55
JWOLFE
07/23/13 12:55
LWALKER
19
TRG
07119113 08:55
07/23/13 12:55
LWALKER
20
TRG
07119113 08:55
JWOLFE
JWOLFE
07/23/13 12:55
LWALKER
!:;Ji
i.i1
lll,
11<..
Eberline Services
~
c
RPO
"'"
Flag
Identification
Activity
Units
01
RA-226
LCS
LCS
pClll
1.07E+01
1.25E+OO
2.72E-01
02
RA-226
MBL
BLANK
pCill
1.29E-01
1.76E-01
2.91E-01
03
RA-226
DUP
1-4 TOT
pCi/I
1.0SE+OO
3.91E-01
2.31E-01
04
RA-226
TRG
PZ-111-SD TOT
pCl/I
1.0SE+OO
3.71E-01
1.59E-01
OK
05
RA-226
TRG
PZ-111-SD DIS
pCUI
1.53E+OO
4.74E-01
2.41E-01
OK
06
RA-226
TRG
S-STOT
pCill
9.83E-01
6.72E-01
8.02E-01
OK
07
RA-226
TRG
S-5 DIS
pCUI
8.31E-01
6.19E-01
6.56E-01
OK
08
RA-226
TRG
FB@ PZ-110-SS TOT
pCi/I
3.46E-02
1.02E-01
2.22E-01
OK
09
RA-226
TRG
PZ-110-SS TOT
pCi/I
4.12E+OO
7.94E-01
2.29E-01
OK
10
RA-226
TRG
PZ-110-SS DIS
pCi/I
3.43E+OO
7.00E-01
2.14E-01
OK
11
RA-226
DO
1-4 TOT
pCl/I
1.37E+OO
5.23E-01
2.83E-01
OK
12
RA-226
TRG
1-4 DIS
pCill
9.59E-01
4.99E-01
3.13E-01
OK
J
.E
13
RA-226
TRG
PZ-100-SS TOT
pCi/I
4.04E+OO
8.03E-01
2.25E-01
OK
t:"
14
RA-226
TRG
PZ-100-SS DIS
pCi/I
3.19E+OO
6.41E-01
2.03E-01
OK
15
RA-226
TRG
D-3 TOT
pCi/I
3.53E+OO
9.39E-01
3.04E-01
OK
16
RA-226
TRG
D-3 DIS
pCifl
3.72E+OO
9.92E-01
4.94E-01
OK
17
RA-226
TRG
PZ-100-SD TOT
pCUI
1.87E+OO
5.07E-01
1.83E-01
OK
Cl
18
RA-226
TRG
PZ-100-SD DIS
pCUI
1.SSE+OO
4.66E-01
1.25E-01
OK
"c
19
RA-226
TRG
PZ-112-AS TOT
pCi/I
2.27E+OO
7.40E-01
2.57E-01
OK
20
RA-226
TRG
PZ-112-AS DIS
pCi/I
1.19E+OO
5.22E-01
3.77E-01
OK
(Q
N
N
Ctl
Q.
Q.
"'c"
~
~I
LCS
Flag
Sample
Desc
.g
LCS
Nuclide
""""
Work Order: 13-07098-Ra226-1
Lb
Fraction
.~
Printed: 7/25/2013 8:13 AM
Page 1 of 3
"E
"
"'c
Client
Results
Error Estimate
MDA
LCS
Known
1.03E+01
103.42
OK
MDA
- Flag
"'
OK
NA
OK
:;;;
"
a.
c
~!!!
t.-.jl
""..i,~
Fl.ag
OK
Cl
c
;:
Blank
OK
Eberline Services
(
c
.E
.g
01
Sample
Sample
Sample
Aliquot
Radiometric
%Rec
Mean
%Rec
Grav
%Rec
SAF
Sep to
Datemme
Date
RA-226
LCS
07/16/13 00:00
1.00E+OO
96.26
0.00
96.26
7/23/2013 12:55
02
RA-226
MBL
07/16/13 00:00
1.00E+OO
86.08
0.00
86.08
7/23/201312:55
03
RA-226
DUP
07/09/13 12:25
1.00E+OO
94.11
0.00
94.11
7/23/2013 12:55
04
RA-226
TRG
07/09/13 10:42
1.00E+OO
94.79
0.00
94.79
7/23/201312:55
05
RA-226
TRG
07/09/1310:42
1.00E+OO
94.72
0.00
94.72
7/23/201312:55
cu
06
RA-226
TRG
07/09/13 10:50
1.00E+OO
55.95
0.00
55.95
7/23/201312:55
07
RA-226
TRG
07/09/13 10:50
1.00E+OO
68.85
0.00
68.85
7/23/201312:55
08
RA-226
TRG
07/09/1311:40
1.00E+OO
84.58
0.00
84.58 '
7/23/201312:55
09
RA-226
TRG
07/09/1312:13
1.00E+OO
88.65
0.00
88.65
7/23/201312:55
10
RA-226
TRG
07/09/13 12:13
1.00E+OO
96.25
0.00
96.25
7/23/201312:55
11
RA-226
DO
07109/1312:25
1.00E+OO
100.00
0.00
100.93
7123/2013 12:55
12
RA-226
TRG
07109/13 12:25
1.00E+OO
86.83
o.oo
86.83
7/23/201312:55
,,;
.5
13
RA-226
TRG
07109113 13:36
1.00E+OO
89.06
.0.00
89.06
7123/201312:55
t:
14
RA-226
TRG
07/0911313:36
1.00E+OO
95.00
0.00
95.00
712312013 12:55
15
RA226
TRG
07109113 13:42
1.00E+OO
87.86
0.00
87.86
7123/2013 12:55
Q)
E
Q)
16
RA-226
TRG
07109113 13:42
1.00E+OO
82.17
0.00
82.17
7/23/2013 12:55
c:
17
RA-226
TRG
0710911314:32
1.00E+OO
97.47
0.00
97.47
7/23/201312:55
Cl
18
RA-226
TRG
0710911314:32
1.00E+OO
98.37
0.00
98.37
7/2312013 12:55
19
RA-226
TRG
07/09113 14:46
1.00E+OO
96.04
0.00
96.04
7/23/201312:55
20
RA-226
TRG
0710911314:46
1.00E+OO
89.82
0.00
89.82
7/23/2013 12:55
""
CD
c:::
Q.
Q.
"'c:
~I
Nuclide
Work Order: 13-07098-Ra226-1
Dase
.!!!
Lb
Fraction
Printed: 7/25/2013 8:13 AM
Page 2 of 3
g>
E
Q)
Q)
.5
Cl
c:
UJ
~~!
(J,~.b
-Ji
~-)
Sept1
Date/Time
Eberline Services
<(
0
.i1
.g
8
01
RA-226
LCS
02
RA-226
03
Halflife
Count
Bkg
CPM
170 3.13 E+02
1.30 E-02
19.4
MBL
07/24/1312:43
A_Spec
Alpha_010
170 3.62 E+OO
1.40 E-02
19.7
RA-226
DUP
07/24/1312:43
A_Spec
Alpha_011
170 3.08 E+01
7.00 E-03
20.5
04
RA-226
TRG
07/24/13 12:43
A_Spec
Alpha_012
170 3.17 E+01
2.00 E-03
19.9
05
RA-226
TRG
07/24/13 12:43
A_Spec
Alpha_013
170 4.18 E+01
7.00 E-03
18.7
06
RA-226
TRG
07/24113 12:43
A_Spec
Alpha_014
170 1.09 E+01
1.80 E-02
18.5
07
RA-226
TRG
07/24/1312:43
A_Spec
Alpha_015
170.02 7.98 E+OO
6.00 E-03
14.8
08
RA-226
TRG
07/24/13 12:44
A_Spec
Alpha_033
170 9.80 E-01
6.00 E-03
18.5
09
RA-226
TRG
07/24/1312:44
A_Spec
Alpha_034
170 1.08 E+02
0.00 E+OO
18.6
10
RA-226
TRG
07/24/13 12:44
A_Spec
Alpha_035
170 9.60 E+01
0.00 E+OO
18.3
11
RA-226
DO
07/24/13 12:44
A_ Spec
Alpha_036
170 2.73 E+01
4.00 E-03
19.1
12
RA-226
TRG
07/24/1312:44
A_Spec
Alpha_037
170 1.47 E+01
2.00 E-03
17.8
.;
.5
13
RA-226
TRG
07/24/13 12:44
A_Spec
Alpha_038
170 1.01 E+02
4.00 E-03
17.2
-i::
14
RA-226
TRG
07/24/1312:44
A_Spec
Alpha_039
170 9.90 E+01
6.00 E-03
19.7
15
RA-226
TRG
07/24/13 12:44
A_Spec
Alpha_040
170 5.57 E+01
2.00 E-03
19
16
RA-226
TRG
07/24/1312:44
A_ Spec
Alpha_041
170 5-71 E+01
1.10 E-02
19.8
17
RA-226
TRG
07/24/1312:44
A_Spec
Alpha_042
170 5.35 E+01
3.00 E-03
18.5
18
RA-226
TRG
07/24/13 12:44
A..;..Spec
Alpha_045
170 6.18 E+01
1.00 E-03
19.1
"
;;,
19
RA-226
TRG
07/24/13 12:44
A_Spec
Alpha_046
170 3.68 E+01
1.00 E-03
17.9
20
RA-226
TRG
07/24/13 12:44
A_Spec
Alpha_047
170 2.16 E+01
8.00 E-03
18.2
"l'""
CD
cu
Cl.
Cl.
-"
"'"c
E
"
"'c
::;
"'
Cl
Cl
c
c
'"''~
Counting
OatelTime
Alpha_004
$:.\,
Sample
Desc
A_Spec
t,1~
Nuclide
07/24113 12:43
t;l~I
Lob
Fraction
Carrier
N
N
~I
Work Order: 13-07098-Ra226-1
Detect
.~
Printed: 7/25/2013 8:13 AM
Page 3 of 3
(days)
nme
Counts
Eff
Count Room Report

13-07098-Ra226-1 (pCi/I) in WA
Tracer ID: Ba-Ga
Internal
Fraction
Printed: 7/24/201312:28 PM
Page 1 of 1
,-(\....r-'
Sample
Desc
Client
ID
Sample
Date
Sample
Aliquot
01/)
LCS
LCS
07116113 00:00
1.0000
0.9214 ''
915.5353
397.0000
02
MBL
BLANK
07116113 00:00
1.0000
0.9118
905.9964
351.3000
03
DUP
1-4 TOT
07109113 12:25
1.0000
0.9114
905.5989
04
TRG
PZ-111-SD TOT
07109113 10:42
1.0000
0.9096
05
TRG
PZ-111-SD DIS
07109113 10:42
1.0000
Tracer
Tracer
Radiometric
Aliquot (g)
ACT(dpm)
Tracer (pCi)
Radiometric
%Rec
SAF
1'
SAF
2'
96.26
2.40 I. 1.00
86.08
2.27
1.00
383.9000
94.11
2.55
1.00
903.8104
385.9000
94.79
2.37
1.00
0.9105
904.7047
386.0000
94.72 . 2.44
1.00
902.7174
227.5000
55.95
3.50
1.00
902.8168
280.0000
68.85
6.24
1.00
'
06
01
TRG
S-5 TOT
07109113 10:50
1.0000
0.9085
TRG
S-5 DIS
07109113 10:50
1.0000
0.9086
'
'
08-?)TRG
FB @ PZ-110-SS TOT
07109113 11 :40
1.0000
0.8957
889.9989
339.1000
84.58
2.08
1.00
09
TRG '
PZ-110-SS TOT
07109113 12:13
1.0000
0.9078
902.0219
360.2000
88.65
2.37
1.00
10
TRG
PZ-110-SS DIS
07109113 12:13
1.0000
0.9090
903.2142
391.6000
96.25
2.37
1.00
11
DO
1-4 TOT
07109113 12:25
1.0000
0.9076
901.8231
410.0000
100.93
3.61
1.00
12
TRG
1-4 DIS
1.0000
0.9114
905.5989
354.2000
86.83
3.82
1.00
13
TRG
PZ-100-SS TOT
07109113 13:36
1.0000
0.9086
902.8168
362.2000
89.06
2.31
1.00
14
TRG
PZ-100-SS DIS
07109113 13:36
1.0000
0.9057
899.9352
385.1000
95.00
2.27
1.00
TRG
D-3 TOT
07109113 13:42
1.0000
0.9055
899.7365
356.1000
87.86
5.26
1.00
07109113 13:42
1.0000
0.9046
898.8422
332.7000
82.17
6.13
1.00
15
16
(A~
..,,1,~]
!JI
TRG
D-3 DIS
07109113 12:25
'
17
TRG
PZ-100-SD TOT
07109113 14:32
1.0000
0.9066
900.8295
395.5000
97.47
2.37
1.00
18
TRG
PZ-100-SD DIS
07109113 14:32
1.0000
0.9067
900.9289
399.2000
98.37
2.12
1.00
19
TRG
PZ-112-AS TOT
07109113 14:46
1.0000
o.9063
900.5314
389.6000
96.04
5.10
1.00
20 I, 11i'RG
PZ-112-AS DIS
07109113 14:46
1.0000
0.9059
900.1339
364.2000
89.82
3.40
1.00
~~
I
'
Eberline Services
Isotope
Sol#
Ra-226
Ra-Sb
Page 1 of 1
Printed: 7/19/2013 8:56 AM
Activity
dpmlg
44.0671
Solution
Date
1
1
7/19/20131
Approx
Addition
Analysis Code
Date
Technician
Ra226
7/19/2013 8:54
JWOLFE
LCS
Volume
Used (g)
0.5001
MS
LCSD
MSD
Volume
Used (g)
Volume
Used(g)
Volume
Used(g)
0.5188
Tracers
LCS
Known
pCi
Em"
Estimate
10.301
Solution
Date
Volume
Used(g)
Approx
Addition
0.4741
Tracer
Isotope
Sol#
01
Ba-133
Ba-Ba
993.635 7/19/2013
. 0.9214
1.0200
02
Ba-133
Ba-6a
993.635 7/19/2013
0.91.18
1.0200
03
Ba-133
Ba-6a
993.635 7/19/2013
0.9114 .
1.0200
04
Ba-133
Ba-6a
993.635 7/19/2013
0.9096'
1.0200
Ba-133
Ba-Sa
993.635 7/19/2013
0.9105
1.0200
Ba-133
Ba-6a
993.635 7/19/2013
0.9085
1.0200
--0. 968::i g
-0.8957
06
07
Ba-133
Ba-Sa
993.S35
7/19/2013
0.9086
1.0200
08
Ba-133
Ba-Sa
993.635 7/19/2013
0.8957
1.0200
09
Ba-133
Ba-6a
993.635 7/19/2013 I
10
Ba-133
Ba-6a
993.635 7/19/2013
0.9078
1.0200
0.9090
1.0200
.J
:.H.::rrr.:.~
::i
-0. 9090
~1
-?.:!.
-e.":.!e76 s
-0. 91 :i..::\. :J
-0 .. ;".1121:36
Ba-133
Ba-6a
993.635 7/19/2013
0.9114
1.0200
13
Ba-133
Ba-6a
993.635 7/19/2013
0.9086'
1.0200
14
Ba-133
Ba-Sa
993.635 7/19/2013
0.9057
1.0200
15
Ba-133
Ba-Sa
993.635 7/19/20131:.
0.9055
1.0200
16
Ba-133
Ba-Sa
993.635 7/19/2013
0.9046
1.0200
-J.~ln
17
Ba-133
Ba-Sa
993.635 7/19/2013
0.9066
1.0200
-tl. 9:166
-0 '305"t :J
__ ..,._ """''""""''' ...
n
Ba-133
Ba-6a
19
Ba-133
Ba-Sa
Ba-133
Version 2.0 08/99
Ba-Sa
993.635 7/19/2013
993.635 7/19/2013
I
I
993.635 7/19/2013
0.9067
1.0200
0.9063
1.0200
0.9059
1.0200
..
i~I~ 5i::':G :.1

ti " ~i 1:::.::} ' .:.1
-0. 90s6 s~
12
20
~~
(,.)
g
90':!16 ;J
-Ott9i05 9
-~~I~
1.0200
18
0.000
0.9076.
....
0.00
--o'.:: 114
993.635 7/19/2013
'
Estimate
921.4 9
ti. :.111;;:; '3
Ba-Sa
..
0.000
MSD
Error
Known
pCi
1Zi ..
Ba-133
11
0.001
LCSD
Error
Estimate
LCS
fraction
05
MS
Added
pCi
Activity
dpmlg
WffiiE!SS -Initials
Te
9046 '.:)
::J
-0. 9E.1E:t S
-ti. '3063 3
-0, :H:J::1'3 '3
Matrix Spike
Added
pCi
o.oo!
Error
Estimate
0.000
Eberline Analytical
Work Ord
13-01oss
Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
I
i:!:~I
1.~
"'"I
.,j
I 1
Sample
Client ID
LCS
Type
Analysis Code
Rpt Units
Lab Deadline
Technician
Ra226
liters
8/6/2013
JWOLFE
Muffle Data
Comments
Technician
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
I -NoofDils
Post/Pre -
.
...
..
.
.
.
.
..
..
.
.
'
.
.
.
..
.- ---
.
.
..
Aliquot
Net Equiv
1.0000E+OO 1.0000E+OO
1.0000E+OO . 1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
.1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
.1.0000E+OO
1.0000E+OO t.OOOOE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OQ
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
MS Aliquot Data
NetEqulv _
Aliquot
H-3 Solids Only

Water Added
H3 Dist
(ml)
Aliq
.
.
.
-
..
I
_
Ratio
...
Aliquot Data
Oil Factor
...
.
Dilution Data
..
Ratio_ _.-::::-._-,:'.
BLANK
1-4 TOT
PZ-111-SD TOT
PZ-111-SD DIS
S-5TOT
S-5 DIS
FB@ PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
1-4 TOT
1-4 DIS
PZ-100-SS TOT
PZ-100-SS DIS
D-3TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
Printed: 711912013 8:48 AM
Page 1 of 1
Aliquot Worksheet
Jl AJ:i%-
Date_;~
J3
Eberline Services - Oak Ridge

Version 1.0 9/1999
Printed: 7/23/2013 6:22 PM

Page 1 of 1
Gravimetric Worksheet
Gravimetric
Carrier
Analysis
Code
Work Order
Carrier Cone
Technician
(mg/ml)
Ra226
TRetec Engineering Management Support, Inc.
Sample
tllll
tuJi
'~-;;Ji
(J(JJ
Technician:
Client ID
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
LCS
BLANK
DUP
PZ-111-SD TOT
PZ-111-SD DIS
S-5 TOT
S-5 DIS
FB @ PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
1-4 TOT
1-4 DIS
PZ-100-SS TOT
PZ-100-SS DIS
D-3 TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
(ml)
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
,~ LI'-"~
Filter Data
Carrier Data
Carrier Added
Fraction
LWALKER
Date:
Filter Tare
(g)
0.0226
0.0224
0.0224
0.0225
0.0227
0.0224
0.0227
0.0225
0.0224
0.0227
0.0224
0.0224
0.0225
0.0225
0.0225
0.0226
0.0225
0.0226
0.0225
0.0225
.-:/-, ).3 I / 3
--
Gravimetric
Filter Final
(g)
0.0293
0.0287
0.0296
0.0291
0.0295
0.0331
0.0375
0.0283
0.0290
0.0293
0.0334
0.0339
0.0289
0.0288
0.0363
0.0373
0.0291
0.0285
0.0361
0.0329
%
Recovery
Filter-Net
(g)
.
.
..
0.0067
O.Q0.63.
0.0072
o..oo.6s
0.0068
0.0107
0.0148
0;005s
... 0.0066
.. 0.0066
0.0110
0.0115
0.0064
0.0063
0.0138
0.0147
0.0066
0.0059
0.0136
.
0.0104
..
.~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1307098A-RA
01
Shelf 2
Ra
Detector Name:
Alpha_004

4
Env. Background:
System Bkgd 62748

Reagent Blank:
<not performed>

2.400E+OOO
Generic Div. Factor:
7/24/2013 12:55:40 PM
7/24/2013 12:43:34 PM
170.0 minutes
170.0 minutes
Sample Size:
Generic Mult. Factor:
Sample Date/Time:
0.9626 +/0.1940 +/0.1868 +/-

0.0000
0.0036 on 12/15/2012 11:26:46 AM
0.0034
Control Certificate Name: Ra226 Ra-Sb

RA-226
0.430887 +/Peak Match Tolerance:
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5.530
4.689
Net
Pk Area
554.07
312.79
1.000E+OOO
AREA
0.028779
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
8.37
11.13
4. 93
2.21
FWHM
(keV)
0.00E+OOO
0.00E+OOO
11.0
4.9

Nuclide
Id
conf.
Energy
(keV)
RA-224
RA-226
0.969
0.988
5685.50*
4785.00*
Activity
(pCi/liter )
1.98E+001 +/- 4.32E+001
l.07E+001 +/- l.25E+OOO
MDA
(pCi/liter
3.79E-001 +/- 8.26E-001
2.72E-001 +/- 9.80E-003
rte
1/{)5/tJ
3379
0000063869.CNF

start:
1:3493.l(kev)
stop : 1024:6486.9(kev)
Acq. Start :wed Jul 24 12:43:34 2013
60
55
50
45
40
35
Vl
+-'
c::
8 30
25
20
15
10
11.1...1".1.;.iJ11
0
3500
i
Ila
(,Ji
():)
oo!
ROI Type: 1
,1l~,j1 .:,
\,.11!1
1
4000
4500
1 \1 1:~
:11:1.11!1
1
W'
111.11.11
. 11111,11111 ..
1
1if1 1l. \ I ' 11 1 \
1\
' "I' L,I lu, .. '111 .

,'I1'!1 u m:i i l!1
l I
, n i llvf~
1.
1.
I JI
1
5000
Energy(kev)
5500
6000
6500
Channel Data Report
7/24/2013
Page
4:50:53 PM
*******************************************************
*****
P E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10201
Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10201
3
0
2
1
3
2
0
2
0
0
1
3
1
3
0
1
2
2
2
0
0
2
7
2
1
3
2
0
3
2
2
1
2
3
1
2
4
3
6
1
3
5
3
3
4
10200
0
0
3
0
3
3
1
0
1
1
1
0
1
4
3
1
3
2
1
1
2
3
1
3
3
2
2
4
2
3
1
4
1
3
1
6
3
1
3
3
6
3
2
2
3
1
0
1
1
0
1
1
0
1
1
3
1
2
1
1
6
4
1
4
4
2
4
4
3
1
1
1
5
2
2
1
1
2
2
4
6
3
3
2
2
3
4
7
6
3
2
1
0
1
1
2
1
0
3
1
2
0
2
4
0
1
6
1
2
3
2
1
5
2
1
1
6
2
3
1
1
0
0
1
6
3
4
5
6
2
3
5
4
1
4
4
2
1
1
0
1
3
1
1
1
0
0
0
1
1
2
1
0
3
2
3
5
0
5
1
2
0
2
3
2
1
1
5
5
3
2
3
6
2
2
2
4
4
2
2
2
0
2
0
0
0
0
0
2
0
1
0
1
0
2
1
1
2
0
1
2
5
3
4
2
1
0
0
1
2
3
3
3
3
4
3
5
3
4
0
0
2
1
5
1
2
1
5
2
0
1
2
0
3
1
3
1
2
0
2
0
0
3
2
1
2
2
1
2
1
4
4
2
4
1
4
5
3
5
0
3
1
0
4
1
3
0
1
2
6
3
4
4
4
1
3
1
2
1
2
1
2
1
1
1
2
1
1
1
3
1
4
5
3
1
1
1
4
1
3
6
4
1
5
4
2
1
5
2
1
2
2
1
4
3
1
2
1
3
2
2
m_3a1
Channel Data Report

369:
7/24/2013
5
Sample Title:
4:50:53 PM
5
Page
0
01
Channell------l-------l-------l-------l-------1-------1-------1-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
2
3
6
3
2
6
5
6
5
2
0
1
1
2
3
2
3
2
3
3
2
2
5
2
6
5
6
5
5
3
2
5
8
7
7
8
6
4
7
9
4
5
3
4
5
2
6
2
2
5
9
5
8
5
5
3
4
4
4
4
5
6
1
2
3
1
1
2
2
4
8
4
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3
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4
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5
9
5
B382
Channel Data Report

801:
7/24/2013
4
Sample Title:
4:50:53
5
Page
PM
4
01
Channell------l-------l-------l-------1-------1-------1-------l-------I
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5
~383
~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
BLANK
l307098A-RA
02
Shelf 2
Ra
Detector Name:
Alpha_OlO

10
Env. Background:
System Bkgd 62749

Reagent Blank:
<not performed>

2.270E+OOO
7/24/2013 12:55:40 PM
7/24/2013 12:43:29 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.8608 +/
0.1967 +/
0.1693 +/
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
5 .526
4.526
0.0000
0.0036 on 12/15/2012 11:26:40 AM
0.0031
AREA
REPORT
Pk Area
Net
Pk Area
Error %
3.26
3.62
l . OOOE+OOO
FWHM
(keV)
Ambient
Backgnd
Backgnd
3.74
2.38
0.00E+OOO
O.OOE+OOO
166.13
137.02
Reagent
2.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.967
0.916
5685.50*
4785.00*
Activity
(pCi/liter )
l.22E-00l +/- 3.34E-00l
l.29E-00l +/- l.76E-001
MDA
(pCi/liter
3.58E-00l +/- 7.84E-00l
2.9lE-OOl +/- l.04E-002
0000063849.CNF

start:
1: 3505 .l(kev)
Stop : 1014:6498,0(kev)
Acq. Start :wed Jul 24 12:43:29 2013
60
55
50
45
40
35
Vl
+-'
<=
8 30
25
20
15
10
l,fl I
0
'
4000
~
~ii
I.!
00
(,111
ROI Type: 1
4500
5000
Energy(kev)
5500
Hi/, /,
6000
6500
Channel Data Report
7/24/2013
4:51:04 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
02
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Channel Data Report

369:
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fiJ387
Channel Data Report

801:
7/24/2013
Sample Title:
Page
4:51:04 PM
02
Channell------l-------l-------l-------l-------1-------1-------1-------I
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tit(/\
~~-/'"\pexSample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Env. Background:
Reagent Blank:
Al pha
TM
I-4 TOT-DUP
1307098A-RA
03
Shelf 2
Ra
Alpha_Oll
11
System Bkgd 62750

<not perforrned>
Sample Size:

2.550E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:43:30 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.9411 +/0.2051 +/0.1930 +/-
PEAK
Energy
(MeV)
RA-224
RA-226
5.479
4.599
2:50:46 PM
0.350 MeV
Nuclide
0.0000
0.0035 on 7/20/2013
0.0033
1. OOOE+OOO
Net
Pk Area
AREA
REPORT
Pk Area
Error %
8 .11
30.81
81. 93
36.10
Ambient
Backgnd
2.89
1.19
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
2.6
2.6
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.945
0.956
5685.50*
4785.00*
Activity
(pCi/liter )
3.60E-001 +/- 9.26E+001
l.08E+OOO +/- 3.91E-001
MDA
(pCi/liter
3.89E-001 +/- l.OOE+002
2.31E-001 +/- 7.80E-003
'3389
0000063854.CNF

Start:
1:3640.l(kev)
Stop : 1024:6315.3(kev)
Acq. start :wed Jul 24 12:43:30 2013
60
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Vl
+-'
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8 30
25
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10
11_\ 1\
4000
ll!l1
"''
!0
!;;,!
~.
ROI
Type: 1
4500
N1fl,\
5000
Energy(kev)
lL A J .\
5500
6000
Channel Data Report
7/24/2013
4:51:15 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
03
Elapsed Live time:

Elapsed Real Time:
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;391
~-
Channel Data Report

369:
7/24/2013
1
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f"
??>-i'j
~.;J;.;jL
..,,.
Channel Data Report

801:
7/24/2013
0
Sample Title:
4:51:15
0
PM
1
Page
0
03
Channell------l-------l-------l-------l-------1-------1-------1-------J
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2
1
111393
1fA
~~-/"'\pexSample Description:
Spectrum File:
Sample Geometry:
Al pha
TM
PZ-111-SD TOT
1307098A-RA
04
Shelf 2
Ra
Detector Name:
Alpha_Ol2

12
Env. Background:
System Bkgd 62751

Reagent Blank:
<not performed>
Sample Size:

2.370E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:43:31 PM
170.0 minutes
Sample Date/Time:
170.0 minutes
0.9479 +/0.1989 +/0.1886 +/-

Energy
(MeV)
RA-224
RA-226
0.0000
0.0034 on 12/11/2011
0.0033
2:21:56 PM
0.350 MeV
PEAK
Nuclide
1. OOOE+OOO
Net
Pk Area
5.592
4.599
9.83
31. 66
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
63.14
35.05
0.17
0.34
0.00E+OOO
O.OOE+OOO
FWHM
(keV)
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.988
0.956
5685.50*
4785.00*
Activity
(pCi/liter )
4.15E-001 +/
l.05E+OOO +/
l.07E+002
3.71E-001
k,
1/').S)O
MDA
(pCi/liter
l.76E-001 +/- 4.53E+001
l.59E-001 +/- 5.41E-003
0000063852.CNF

Rea1 Time :10200.000 sec
start:
1:3502. l(kev)
stop : 1024: 6535. 3(kev)
Acq. start :wed Jul 24 12:43:312013
60
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+-'
<:::
8 30
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~
! ,\
4000
&,_~
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tJ1
ROI Type: 1
4500
5000
Energy(kev)
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6500
Channel Data Report
7/24/2013
4:51:26 PM
Page
*******************************************************
*****
p E C T R A L
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*****
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Sample Title:
04
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Channel Data Report

369:
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1
ffl397
,.,,
i-%'
Channel Data Report

801:
7/24/2013
0
Sample Title:
4:51:26
0
Page
PM
0
04
Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
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897:
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!!1338
~~.Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-111-SD DIS
1307098A-RA
05
Shelf 2
Ra
Detector Name:
Alpha_013

13
Env. Background:
Reagent Blank:
System Bkgd 62752

<not performed>
Sample Size:

2.440E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:43:32 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.9472 +/0.1869 +/0.1770 +/-

PEAK
Energy
(MeV)
Net
Pk Area
5.477
4.576
RA-224
RA-226
0.0000
0.0035 on 12/15/2012 11:26:45 AM
0.0033
0.350 MeV
Nuclide
1.000E+OOO
10.77
41. 81
AREA
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
69.42
30.81
3.23
1.19
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
5.7
2.8
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.944
0.945
5685.50*
4785.00*
Activity
(pCi/liter )
4.99E-001 +/- 1.28E+002

1.53E+OOO +/- 4.74E-001
/JC
'?/)s/0
MDA
(pCi/liter
4.22E-001 +/- 1.08E+002
2.41E-001 +/- 8.72E-003
0000063851.CNF
start:
1 3547. 5(kev)
stop : 1014 6438.l(kev)
Acq. Start wed Jul 24 12:43:32 2013
60
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+"'
c:
8 30
25
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II

1! [\
'
4000
l<!.1
Q.1
ROI Type: 1
4500
'II'
'I /\ill!
,\ i
l"i\-11\I ,jI
,j1;;!1:]
5000
Energy(kev)
5500
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Channel Data Report
7/24/2013
Page
4:51:35 PM
*******************************************************
*****
S P E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
05
Elapsed Live time:

Elapsed Real Time:
10200
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Channel Data Report

369:
7/24/2013
2
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B4m2
Channel Data Report

801:
7/24/2013
0
Sample Title:
4:51:35
0
Page
PM
0
05
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Sample Description:
Spectrum File:
Sample Geometry:
S-5 TOT
1307098A-RA
06
Shelf 2
Ra
Detector Name:
Alpha_014

14
System Bkgd 62753
Env. Background:
Reagent Blank:
<not performed>

3.500E+OOO
7 /23/2013 12:55:40 PM
7/24/2013 12:43:32 PM
170.0 minutes
Sample Size:
Sample Date/Time:
0.5595 +/0.1846 +/0.1033 +/-
PEAK
RA-224
RA-226
0.0000
0.0034 on 12/15/2012 11:26:44 AM
0.0019
0.350 MeV
Energy
(MeV)
OOOE+OOO
170.0 minutes

Nuclide
1.
AREA
REPORT
Net
Pk Area
Pk Area
Error %
5.511
4.587
-0.59
10.94
726.33
68.27
Ambient
Backgnd
Reagent
Backgnd
4.59
3.06
0.00E+OOO
0.00E+OOO
FWHM
(keV)
5.9
2.9
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.961
0.950
5685.50*
4785.00*
Activity
(pCi/liter )
-6.72E-002 +/- 1.73E+001
9.83E-001 +/- 6.72E-001
MDA
(pCi/liter
1.18E+OOO +/- 3.03E+002
8.02E-001 +/- 2.92E-002
0000063855.CNF

Rea1 Time :10200.000 sec
Start:
1:3507. 9(kev)
stop : 1024:6512.2(kev)
Acq. start :wed Jul 24 12:43:32 2013
60
55
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45
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35
V>
c:
8 30
25
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4000
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ROI Type: 1
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4500
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11.
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6000
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Channel Data Report
7/24/2013
4:52:14 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
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06
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~4!16
Channel Data Report

369:
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4:52:14 PM
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~4B7
Channel Data Report

801:
7/24/2013
0
Sample Title:
Page
4:52:14 PM
06
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c!J(J\
~~_.:!!S'f"\pexSample Description:
Spectrum File:
Sample Geometry:
Al pha

TM
S-5 DIS
1307098A-RA
07
Shelf 2
Ra
Detector Name:
Alpha_Ol5

15
Env. Background:
System Bkgd 62754

Reagent Blank:
<not performed>

4.000E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:43:33 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.6885 +/
0.1477 +/
0.1017 +/

PEAK
Energy
(MeV)
RA-224
RA-226
6:27:27 PM
0.350 MeV
Nuclide
0.0000
0.0027 on 7/20/2013
0.0018
1. OOOE+OOO
Net
REPORT
Pk Area
Error %
Pk Area
5.518
4.598
AREA
5.49
7.98
88.08
74.39
FWHM
(keV)
Ambient
Reagent
Backgnd
Backgnd
0.51
1. 02
O.OOE+OOO
0.00E+OOO
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 964
0.955
5685.50*
4785.00*
Activity
(pCi/liter )
7.26E-001 +/ 1.87E+002
8.31E-001 +/ 6.19E-001
MDA
(pCi/liter
6.94E-001 +/- 1.78E+002
6.56E-001 +/- 2.32E-002
0000063850.CNF

start:
1 3490.S(kev)
stop : 1024 6558.S(kev)
60
55
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45
40
35
.....,
Vl
r::
8 30
25
20
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0
'
3500
1<1~1
t;'Jb,
,.~
'i.m~I
ROI Type: 1
1!1
4000
4500
5000
Energy(kev)
,\
Jl_
5500
.IA
6000
6500
Channel Data Report
7/24/2013
4:54:59 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
07
Elapsed Live time:

Elapsed Real Time:
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8411
Channel Data Report

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fgA,12
Channel Data Report

801:
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0
Sample Title:
4:54:59
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0
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07
Channell------l-------l-------l-------l-------1-------1-------1-------I
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~~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
FB @ PZ-110-SS TOT
1307098A-RA
08
Shelf 2
Ra
Detector Name:
Alpha_033
04026479A
91132
Env. Background:
Reagent Blank:
System Bkgd 62765

<not performed>

2.080E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:02 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.8458 +/
0.1848 +/
0.1563 +/

PEAK
Energy
(MeV)
RA-224
RA-226
2:31:30 PM
0.350 MeV
Nuclide
0.0000
0.0032 on 7/20/2013
0.0027
l.OOOE+OOO
Net
Pk Area
5.462
4.675
AREA
REPORT
Pk Area
Error %
0. 49
0.98
416.98
294.85
FWHM
(keV)
Ambient
Backgnd
Backgnd
0.51
1.02
O.OOE+OOO
0.00E+OOO
Reagent
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.937
0.984
5685.50*
4785.00*
Activity
(pCi/liter )
2.19E-002 +/- 5.64E+OOO
3.46E-002 +/- l.02E-001
MDA
(pCi/liter
2.35E-001 +/- 6.04E+001
2.22E-001 +/- 7.63E-003
0000063861.CNF
Live Time
Real rime
Start:
l
stop : 1014
Acq. start
60+
10200.000 sec
10201.500 sec
3447.l(kev)
6496. 6(kev)
wed Jul 24 11: 44: 01 2013
I_
55
50
45
40
35
..,c:"'
8 30
25
20
15
10
;'!;
;Ji
L
0
3500
l~I
.w,~.,
......
1:.11
ROI Type: 1
4000
4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
7/24/2013
4:55:10 PM
Page
*******************************************************
*****
S P E C T R A L
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
08
Elapsed Live time:

Elapsed Real Time:
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10202
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~41 ':t
Channel Data Report

801:
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Sample Title:
Page
4:55:10 PM
08
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0
0
0
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0
0
0
0
0
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0
0
0
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0
0
0
0
0
0
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0
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0
0
0
0
~~.Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-110-SS TOT
1307098A-RA
09
Shelf 2
Ra
Detector Name:
Alpha_034
040264798
91136
Env. Background:
System Bkgd 62766

Reagent Blank:
<not performed>

2.370E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:03 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
0.8865 +/0.1856 +/0.1645 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5.506
4.586
0.0000
0.0032 on 12/16/2012
0.0029
5:49:43 PM
0.350 MeV
Nuclide
1. OOOE+OOO
Net
Pk Area
35.32
108.00
AREA
REPORT
FWHM
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
0.68
0.00
0.00E+OOO
0.00E+OOO
33.35
18.95
(keV)
3.7
4.5

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.959
0.950
5685.50*
4785.00*
Activity
(pCi/liter )
l.71E+OOO +/- 4.40E+002
4.12E+OOO +/- 7.94E-001
MDA
(pCi/liter
2.73E-001 +/- 7.03E+001
2.29E-001 +/- 7.81E-003
0000063860.CNF

start:
I: 3439. l(kev)
stop : 1024:6479.9fkev)
Acq. Start :wed Ju 24 12:44:03 2013
60
55
50
45
40
35
"'
<=
+"'
3 30
25
20
15
10
0
'
3500
!iE~I
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1<:1
ROI Type: 1
'
4000
4500
5000
Energy(kev)
5500
6000
Channel Data Report
7/24/2013
4:55:19 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
09
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ty421
Channel Data Report

369:
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~422
Channel Data Report

801:
7/24/2013
0
Sample Title:
4:55:19
0
PM
0
Page
1
09
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~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-110-SS DIS
1307098A-RA
10
Shelf 2
Ra
Detector Name:
Alpha_035
04026477A
58771
Env. Background:
System Bkgd 62767

Reagent Blank:
<not performed>
Sample Size:

2.370E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:05 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.9625 +/0.1826 +/0.1757 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
AREA
Error %
20.00
96.00
44.91
20 .11
5:49:42 PM
REPORT
Pk Area
Net
Pk Area
5.514
4.591
0.0000
0.0032 on 12/16/2012
0.0031
1. OOOE+OOO
FWHM
Ambient
Backgnd
Reagent
Backgnd
0.00
0.00
O.OOE+OOO
O.OOE+OOO
(keV)
2.9
3.7
Nuclide
Id
conf.
Energy
(keV)
RA-224
RA-226
0.962
0.952
5685.50*
4785.00*
Activity
(pCi/liter )
9.07E-001 +/- 2.33E+002
3.43E+OOO +/- 7.00E-001
MDA
(pCi/liter
2.72E-001 +/- 6.99E+001
2.14E-001 +/- 7.34E-003
0000063862.CNF

start:
l:J463.4(kev)
Stop : 1024:6473.S(kev)
Acq. start :wed Jul 24 12:44:05 2013
60
SS
so
4S
40
3S
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ROI Type: 1
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4000
4SOO
SOOD
Energy(kev)
ssoo
6000
Channel Data Report
7/24/2013
Page
4:55:28 PM
*******************************************************
*****
SPECTRAL
DAT A
R E P 0 R T
*****
*******************************************************
Sample Title:
10
Elapsed Live time:

Elapsed Real Time:
10200
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ill-4 26
Channel Data Report

369:
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Sample Title:
Page
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10
Channell------l-------1-------1-------1-------l-------l-------l-------I
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Sample Geometry:
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11
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Ra
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84167
System Bkgd 62768
Sample Description:
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Reagent Blank:
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3.610E+OOO
7 /23/2013 12:55:40 PM
7/24/2013 12:44:06 PM
170.0 minutes
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170.0 minutes

1. 0000 +/-
0 .1910 +/0.1910 +/-
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
1. OOOE+OOO
AREA
Error %
13 .32
27.32
55.28
38.04
2:31:37 PM
REPORT
Pk Area
Net
Pk Area
5.537
4. 637
0.0000
0.0033 on 7/20/2013
0.0033
Ambient
Backgnd
0.68
0.68
Reagent
Backgnd
FWHM
(keV)
0.00E+OOO
0.00E+OOO
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.971
0.972
5685.50*
4785.00*
Activity
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MDA
(pCi/liter
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2.83E-001 +/- 9.63E-003
U429
0000063863.CNF

start'
1: 3452. 9(kev)
Stop ' 1024:6474.2(kev)
Acq. Start :wed Jul 24 12:44:06 2013
60
55
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5500
6000
Channel Data Report
7/24/2013
5:00:46 PM
Page
*******************************************************
*****
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DAT A
RE P 0 R T
*****
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611132
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801:
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TM
I-4 DIS
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12
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Alpha_037
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91133
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3.820E+OOO
7 /23/2013 12:55:40 PM
7/24/2013 12:44:08 PM
170.0 minutes
170.0 minutes

0.8683 +/0.1783 +/0.1548 +/-
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RA-224
RA-226
3:28:25 PM
0.350 MeV
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0.0000
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RA-226
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4785.00*
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9.59E-001 +/
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start:
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stop : 1024:6468.S(kev)
Acq. Start :wed Jul 24 12:44:08 2013
55
45
40
35
....c:
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25
20
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(,Ji
ROI Type: 1
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4500
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ILL/;!
l,ll
5000
Energy(kev)
5500
6000
Channel Data Report
7/24/2013
5:00:56 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
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Elapsed Live time:

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Channel Data Report

801:
7/24/2013
0
Sample Title:
5:00:56
0
PM
0
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12
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....Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-SS TOT
1307098A-RA
13
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_038
04026478B
91134
System Bkgd 62770
<not performed>
Sample Size:
Sample Date/Time:

2.310E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:09 PM
170.0 minutes
170.0 minutes

0.8906 +/0.1722 +/0.1533 +/-
PEAK
Energy
(MeV)
RA-224
RA-226
5.495
4.599
5:13:35 PM
0.350 MeV
Nuclide
0.0000
0.0030 on 5/11/2013
0.0027
1. OOOE+OOO
AREA
REPORT
Pk Area
Error %
Net
Pk Area
11. 32
101.32
60.27
19.55
Ambient
Backgnd
0.68
0.68
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
3.0
3.4
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.953
0.956
5685.50*
4785.00*
Activity
(pCi/liter )
5.73E-001 +/- 1.47E+002

4.04E+OOO +/- 8.03E-001
MDA
(pCi/liter
2.86E-001 +/- 7.35E+001
2.25E-001 +/- 7.75E-003
NA.39
0000063859.CNF

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Acq. Start :wed Ju 24 12:44:09 2013
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5500
6000
6500
Channel Data Report
7/24/2013
5:01:06 PM
Page
*******************************************************
*****
p E CTR AL
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
13
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";"'
Channel Data Report

369:
7/24/2013
1
Sample Title:
Page
5:01:06 PM
1
13
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Channel Data Report

801:
7/24/2013
1
Sample Title:
5:01:06
0
Page
PM
0
13
Channell------l-------l-------1-------1-------1-------l-------l-------I
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~-~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-SS DIS
1307098A-RA
14
Shelf 2
Ra
Detector Name:
Alpha_039
06027396A
83109
Env. Background:
System Bkgd 62771

Reagent Blank:
<not performed>

2.270E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:11 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
0.9500 +/0.1965 +/0.1867 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
0.0000
0.0034 on 4/20/2013
0.0032
2:01:25 PM
0.350 MeV
Nuclide
1. OOOE+OOO
Net
Pk Area
5.493
4.588
7.81
98.98
AREA
REPORT
Pk Area
Ambient
Reagent
Error %
Backgnd
Backgnd
1.19
1.02
O.OOE+OOO
O.OOE+OOO
76.13
19.82
FWHM
(keV)
3.0
7.4

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.952
0.950
5685.50*
4785.00*
Activity
(pCi/liter )
3.19E-001 +/- 8.21E+001
3.19E+OOO +/- 6.41E-001
MDA
(pCi/liter
2.69E-001 +/- 6.93E+001
2.03E-001 +/- 6.89E-003
0000063865.CNF

Start:
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stop : 1024: 6497. l(kev}
Acq. Start :wed Jul 24 12:44:11 2013
,l,
4000
3500
lllii
&,"l:m.
II>
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ROI Type: 1
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4500
5000
Energy(kev)
5500
6000
6500
Channel Data Report
7/24/2013
5:01:17 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
14
Elapsed Live time:

Elapsed Real Time:
10200
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-mttl!E
Channel Data Report

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7/24/2013
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-~447
Channel Data Report

801:
7/24/2013
0
Sample Title:
5:01:17
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PM
0
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14
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~~Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
D-3 TOT
1307098A-RA
15
Shelf 2
Ra
Detector Name:
Alpha_040
06027396B
91135
Env. Background:
System Bkgd 62772

Reagent Blank:
<not performed>
Sample Size:
1.000E+OOO +/- 0.000E+OOO liter

4.000E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:13 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.8786 +/
0.1900 +/
0.1669 +/
PEAK
Energy
(MeV)
RA-224
RA-226
5:49:33 PM
0.350 MeV
Nuclide
0.0000
0.0033 on 12/16/2012
0.0029
1. OOOE+OOO
Net
Pk Area
5.515
4.636
24.49
55.66
AREA
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Reagent
Backgnd
Backgnd
40.09
26. 37
0.51
0.34
0.00E+OOO
0.00E+OOO
3.7
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 962
0. 971
5685.50*
4785.00*
Activity
(pCi/liter )
1.97E+OOO +/- 5.08E+002
3.53E+OOO +/- 9.39E-001
MDA
(pCi/liter
4.23E-001 +/- 1.09E+002
3.04E-001 +/- 1.03E-002
0000063864.CNF
Live Time
Real Time
start:
l
Stop : 1024
Acq. Start
60
10200.000 sec
10201.600 sec
3459.0(kev)
6497.l(kev)
wed Jul 24 12:44:13 2013
55
50
45
40
35
Vl
+-'
c::
8 30
25
20
15
10
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1::.
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ROI Type: 1
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5000
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5500
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6500
Channel Data Report
7/24/2013
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Page
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*****
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~451
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61152
Channel Data Report

801:
7/24/2013
0
Sample Title:
5:01:25
1
PM
1
Page
0
15
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!l!.:153
_jfApex-Alpha
D-3 DIS
l307098A-RA
16
Shelf 2
Ra
Sample Description:
Spectrum File:
Sample Geometry:
Detector Name:
Alpha_041
05026930A
91087
Env. Background:
System Bkgd 62773

Reagent Blank:
<not performed>
Sample Size:

4.000E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:15 PM
170.0 minutes
170.0 minutes
Sample Date/Time:
0.8217 +/0.1978 +/0.1626 +/-

PEAK
Energy
(MeV)
RA-224
RA-226
5.532
4.595
5:49:31 PM
0.350 Mev
Nuclide
0.0000
0.0034 on 12/16/2012
0.0028
l.OOOE+OOO
Net
Pk Area
25. 98
57.13
AREA
REPORT
Pk Area
Ambient
Error %
Backgnd
Reagent
Backgnd
FWHM
(keV)
39.33
26.42
l.02
l.87
O.OOE+OOO
O.OOE+OOO
3.7
3.0

Id
Conf.
Energy
Nuclide
RA-224
RA-226
0.970
0.954
5685.50*
4785.00*
(keV)
Activity
(pCi/liter )
2.l5E+OOO +/
3.72E+OOO +/
5.53E+002
9.92E-00l
MDA
(pCi/liter
5.2lE-00l +/
4.94E-00l +/
l.34E+002
l.67E-002
0000063868.CNF
start:
1 l452.7(kev)
stop : 1024 6506.6(kev)
60
55
50
45
40
35
V>
+-'
c:
8 30
25
20
15
10
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3500
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ROI Type: 1
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'
4000
4500
5000
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5500
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6000
6500
Channel Data Report
7/24/2013
5:01:35 PM
Page
*******************************************************
*****
E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
16
Elapsed Live time:

Elapsed Real Time:
10200
10202
Channell------l-------l-------l-------1-------1-------1-------l-------I
1:
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S457
Channel Data Report

801:
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1458
~A
~~-/"'\pex-
Al pha
TM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-SD TOT
1307098A-RA
17
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_042
050269303
84185
System Bkgd 62774
<not performed>
2.370E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:17 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.9747 +/0.1846 +/0.1799 +/-

Energy
(MeV)
RA-224
RA-226
5:49:29 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0031
l.OOOE+OOO
Net
Pk Area
5.497
4.571
AREA
REPORT
Pk Area
Error %
7.98
53.49
74.39
26.95
Ambient
Backgnd
1. 02
0.51
FWHM
(keV)
Reagent
Backgnd
0.00E+OOO
0.00E+OOO
4.5
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.954
0.942
5685.50*
4785.00*
Activity
(pCi/liter )
3.53E-001 +/- 9.09E+001

l.87E+OOO +/- 5.07E-001
MDA
(pCi/liter
2.79E-001 +/- 7.18E+001
l.83E-001 +/- 6.24E-003
_@,459
0000063867.CNF
Real Time :10201.SOO sec
start:
1:3450.2(kev)
stop : 1024: 6505. 5(kev)
Acq. start :wed Jul 24 12:44:17 2013
60+
SS
so
45
40
3S
Vl
.....
c:
8 30
25
20
lS
10
s
0
'
3SOO
~r,1!1
ill
m
~ii
ROI Type: 1
4000
4SOO
sooo
Energy(kev)
ssoo
6000
6SOO
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[,,...
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411
~
Apex-Alpha
Sample Description:
Spectrum File:
Sample Geometry:
PZ-100-SD DIS
1307098A-RA
18
Shelf 2
Ra
Detector Name:
Alpha_045
04026482A
91131
Env. Background:
System Bkgd 62775

Reagent Blank:
<not performed>

2.120E+OOO
7/23/2013 12:55:40 PM
7 /24/2013 12:44:19 PM
170.0 minutes
170.0 minutes
Sample Size:
Sample Date/Time:
0.9837 +/
0.1909 +/
0.1878 +/

Energy
(MeV)
RA-224
RA-226
2:31:26 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 7/20/2013
0.0033
1. OOOE+OOO
Net
Pk Area
5 .490
4.590
9.15
61.83
AREA
REPORT
FWHM
(keV)
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
68.23
24.97
0.85
0.17
O.OOE+OOO
O.OOE+OOO
3.0
3.0
Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.951
0.951
5685.50*
4785.00*
Activity
(pCi/liter )
3.47E-001 +/- 8.93E+001
l.85E+OOO +/- 4.66E-001
MDA
(pCi/liter
2.27E-001 +/- 5.84E+001
l.25E-001 +/- 4.26E-003
0000063856.CNF

start:
1:34S3.7(kev)
stop : 1024:6489.l(kev)
Acq. start :wed Jul 24 12:44:19 2013
35
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+-'
<=
:::s
8 30
25
15
10
5
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3500
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4000
4500
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5000
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5500
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I I
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II hi!
6000
MA
Channel Data Report
7/24/2013
5:01:55 PM
Page
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p E C T R A L
DAT A
RE P 0 R T
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18
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ti1466
Channel Data Report

369:
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1
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mLts7
Channel Data Report

801:
7/24/2013
0
Sample Title:
5:01:55
0
Page
PM
0
18
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~~Apex-Alpha
PZ-112-AS TOT
1307098A-RA
19
Shelf 2
Ra
Sample Description:
Spectrum File:
Sample Geometry:
Alpha_046
040264828
58762
System Bkgd 62776
<not performed>
Detector Name:
Env. Background:
Reagent Blank:
1.000E+OOO +/
O.OOOE+OOO liter
4.000E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:21 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
0.9604 +/
0.1789 +/
0.1718 +/

PEAK
Energy
(MeV)
RA-224
RA-226
0.0000
0.0031 on 12/16/2012
0.0030
5:49:23 PM
0.350 MeV
Nuclide
1.000E+OOO
REPORT
Pk Area
Net
Pk Area
5.569
4.566
AREA
Error %
20.83
36.83
Ambient
Backgnd
43.15
32.38
0.17
0.17
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Id
Conf.
Energy
Nuclide
RA-224
RA-226
0.982
0.939
5685.50*
4785.00*
(keV)
Activity
(pCi/liter )
1.63E+OOO +/- 4.19E+002
2.27E+OOO +/- 7.40E-001
MDA
(pCi/liter
3.27E-001 +/- 8.40E+001
2.57E-001 +/- 8.86E-003
I..
0000063857.CNF

Start:
1:3453.l(kev)
Stop : 1024:6515.4\keV)
Acq. start :wed Ju 24 12:44:21 2013
60+
55
so
45
40
35
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.....
s::::
8 30
25
20
15
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3500
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4000
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4500
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,!!,
5000
Energy(kev)
5500
6000
6500
Channel Data Report
7/24/2013
5:03:56 PM
Page
*******************************************************
*****
p E C T R A L
DAT A
RE P 0 R T
*****
*******************************************************
Sample Title:
19
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Blt71
Channel Data Report

369:
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0
0
0
0
1
1
1
0
0
0
0
0
0
0
1
1
0
0
1
0
0
2
0
0
0
0
0
1
0
0
0
1
0
0
0
0
1
0
Channel Data Report

801:
7/24/2013
0
Sample Title:
5:03:56
0
PM
0
Page
0
19
Channell------l-------l-------1-------1-------1-------l-------l-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
~-473
~A
Al pha
~~..s/'"\pex-
TM
Sample Description:
Spectrum File:
Sample Geometry:
PZ-112-AS DIS
1307098A-RA
20
Shelf 2
Ra
Detector Name:
Alpha_047
02030596A
91086
Env. Background:
System Bkgd 62777

Reagent Blank:
<not performed>

3.400E+OOO
7/23/2013 12:55:40 PM
7/24/2013 12:44:24 PM
170.0 minutes
Sample Size:
Sample Date/Time:
170.0 minutes
0.8982 +/0.1822 +/0.1636 +/-
0.350 MeV

PEAK
Nuclide
Energy
(MeV)
RA-224
RA-226
1. OOOE+OOO
Net
Pk Area
AREA
5:49:21 PM
REPORT
Pk Area
Error %
15.66
21.64
5.546
4.580
0.0000
0.0032 on 12/16/2012
0.0029
Ambient
Backgnd
50.15
43.66
0.34
1.36
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
2.9
4.4

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.974
0.947
5685.50*
4785.00*
Activity
(pCi/liter )
l.09E+OOO +/
l.19E+OOO +/
2.81E+002
5.22E-001
MDA
(pCi/liter
3.34E-001 +/- 8.59E+001
3.77E-001 +/- l.30E-002
0000063866.CNF

start:
1: 3457. 9(kev)
Stop : 1024:6467.7(kev)
Acq. Start :wed Jul 24 12:44:24 2013
60
55
50
45
40
.,,
....,
35
r::
8 30
25
20
15
10
3500
'
!ill
t~~.
~-iJ
U11
ROI Type: 1
'
~ /j\ if\ ,\ !
'
4000
4500
,,\
5000
Energy(kev)
1\
!, I, M1.11.i,\ ii r'
5500
6000
Channel Data Report

369:
7/24/2013
1
Sample Title:
5:07:26
0
PM
1
Page
0
20
Channell------l-------1-------1-------1-------l-------l-------l-------I
377:
385:
393:
401:
409:
417:
425:
433:
441:
449:
457:
465:
473:
481:
489:
497:
505:
513:
521:
529:
537:
545:
553:
561:
569:
577:
585:
593:
601:
609:
617:
625:
633:
641:
649:
657:
665:
673:
681:
689:
697:
705:
713:
721:
729:
737:
745:
753:
761:
769:
777:
785:
793:
0
0
0
0
1
1
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
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0
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0
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0
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0
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0
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0
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0
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0
0
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0
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0
0
0
0
0
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0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
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0
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0
0
0
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0
0
0
0
1
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
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0
0
0
0
0
0
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0
0
0
0
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0
0
0
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0
0
0
0
0
1
1
0
0
0
1
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0
0
0
0
0
0
1
0
0
1
0
0
0
0
0
0
0
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0
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0
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0
0
0
0
0
0
0
0
0
0
0
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0
0
0
0
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1
0
0
0
0
1
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
t}J477
Channel Data Report

801:
7/24/2013
0
Sample Title:
5:07:26
0
PM
0
Page
0
20
Channell------l-------l-------l-------l-------1-------1-------1-------I
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
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0
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0
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0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
~478
Page 1 of 2
--=
lt'Apex-Alpha
7/24/2013 5:43:41 AM
'l
QA SUMMARY REPORT

Date
Time
: 7/24/2013
: 5:43:41 AM
CHAMBER
Alpha 001
Aloha 002
Alpha 003
Aloha 004
Aloha 005
Alpha 006
Aloha 007
Alpha 008
Aloha 009
Alpha 010
Aloha 011
Alpha 012
Alpha 013
Aloha 014
Alpha 015
Aloha 016
Alpha 017
Aloha 018
Aloha 019
Alpha 020
Aloha 021
Alpha 022
Aloha 023
Alpha 024
Aloha 025
Alpha 026
Aloha 027
Alpha 028
Aloha 029
Aloha 030
Aloha 031
Aloha 032
Aloha 033
Aloha 034
Alpha 035
Aloha 036
Alpha 037
Aloha 038
Alpha 039
Aloha 040
Aloha 041
Aloha 042
DEVICE
2lf
2lf
2lf
2lf
2lf
2lf
21f
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analv.tl OODC
Aloha Analvstl OODC
Alpha Analv.t l OODC
Aloha AnalvstlOODC
Aloha AnalvstlOODC
Aloha Analvstl OODC
Alpha AnalystlOODC
Aloha Analvstl OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Passed
Passed
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
7/24/2013 5:25:26 AM
7/24/2013 5:25:27 AM
7/24/2013
7/24/2013
7/24/2013
7/24/2013
7/24/2013
7/24/2013
5:25:28 AM
5:25:29 AM
5:25:29 AM
5:25:30 AM
5 :25 :3 1 AM
5:25:32 AM
7/24/2013 5:25:33 AM
7/24/2013 5:25:34 AM
7/24/2013
7/24/2013
7/24/2013
7/24/2013
5:25:34 AM
5:25:35 AM
5:25:36 AM
5:25:37 AM
7/24/2013 5:25:38 AM
7/24/2013 5:25:38 AM
7/24/2013 5:25:39 AM
7/24/2013 5:25:40 AM
7/24/2013 5:25:42 AM
7/24/2013 5:25:43 AM
7/24/2013 5:25:45 AM
7/24/2013 5:25:46 AM
7/24/2013 5:25:48 AM
7/24/2013 5:25:50 AM
7/24/2013 5:25:52 AM
7/24/2013 5:25:54 AM
7/24/2013 5:25:56 AM
Page 2 of 2
CHAMBER
Aloha 043
Alpha 044
Aloha 045
Alpha 046
Aloha 047
Alpha 048
DEVICE
PARAMETER
Aloha Analvst!OODC
Alpha Analyst! OODC
Aloha Analvst!OODC
Alpha Analyst! OODC
Aloha AnalvstlOODC
Alpha Analyst! OODC
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Passed
Passed
7124/2013 5:43:41 AM
DATE
7/24/2013
7/24/2013
7/24/2013
7/24/2013
5:25:58 AM
5:26:00 AM
5:26:02 AM
5:26:05 AM
APPROVED BY:
APPROVAL DATE:
iil48ill
6/12/12
Page
12:16:17 PM
*************************************************************************
*****
L I B R A R Y
L I S T I N G
R E P 0 R T
*****
*************************************************************************
Radium
Nuclide
Name
Half-Life
(Seconds)
Energy
(keV )
P0-218
RN-222
RA-226
5.049E+Ol0
5.049E+Ol0
5.049E+Ol0
6003.000*
5490.000*
4785.000*
= key
TOTALS:
Ra-226, Po-218, Rn-222

Energy
Uncert. (keV
0.000
0.000
0.000
line
3
Nuclides
Energy Lines
Yield
( %- )
99.9800
99.9200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
SECTION XI
ANALYTICAL DATA (RADIUM-228)
Eberline Services
Analysis Sheet
Printed: 8/5/2013 10:17 AM

Page 1 of3
13-07098
Ra228
Run 1
Run
I Sample
Desc
Client
ID
01
LCS
LCS
02
MBL
BLANK
7/15/2013
03
DUP
Ra228
Analysis Code
Date Received
Internal
Fraction
13-07098
Work Order
Login
'
=i_-
8/6/2013
Client I Engineering Management Support, Inc.

Project
West Lake OU-1
04
TRG
PZ-111-SD TOT
05
TRG
PZ-111-SD DIS
06
TRG
S-5 TOT
07
TRG
Activity Units
pCi
08
, TRG
09
TRG
07/16/13 00:00
1.0000E+OO
44
07/09/13 12:25
1.0000E+OO
07/09/13 10:42
1.0000E+OO
36
07/09/13 10:42
1.0000E+OO
45
07/09/13 10:50
45
07/09/13 10:50
1.0000E+OO
43
07/09/13 11 :40
1.0000E+OO
41
07/09/1312:13
1.0000E+OO
-r:
S-5 DIS
FB @ PZ-110-SS TOT
_.....
1.0000E+OO
PZ-110-SS TOT
-
--
WA
10
TRG
PZ-110-SS DIS
E904.0
11
DO
1-4 TOT
Method
1.0000E+OO
--!
Matrix
07/16/13 00:00
Repo rt Leve I
Aliquot Units
Sample
Aliquot
1-4 TOT
Lab Deadline
Sample
Date
CPM
I
I
07/09/13 12:13
1.0000E+OO
07/09/13 12:25
1.0000E+OO
44
07/09/13 12:25
1.0000E+OO
46
07/09/13 13:36
1.0000E+OO
46
07/09/13 13:36
-+
Instrument Type
Radiometric Tracer
Alpha/Beta GPC
12
TRG,
Ba-133
13
TRG
1-4 DIS
PZ-100-SS TOT
....,.
Radiometric Sol#
Tracer Act (dpm/g)
Carrier
Ba-Ga
993.635
14
PZ-100-SS DIS
TRG
15
D-3 TOT
TRG
Yttirum
16
, TRG
34
17
TRG
18
TRG
1.0000E+OO
43
07/09/13 13:42
1.0000E+OO
PZ-100-SD TOT
39
07/09/13 14:32
1.0000E+OO
39
07/09/13 14:32
1.0000E+OO
45
07/09/13 14:46
PZ-112-AS TOT
TRG
PZ-112-AS DIS
1.0000E+OO
I
-----------t-
20
07/09/1313:42
D-3 DIS
PZ-100-SD DIS
TRG
43
'
19
=t_
1.0000E+OO
45
07/09/13 14:46
1.0000E+OO
l\!ll
t":~.
00
~~
j-----~
**Actual mass exceeded the calibration cuive range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 8151201310:17 AM
Page 2 of3
13-07098
Ra228
Run 1
Internal
Fraction
Sample
Desc
01
LCS I
02
,_____1
03
-397.0
-i
90~+
I Radiometric I Grav Carrier I

% Rec
351.3
Added (ml)
Grav Filter
Tare (g)
Grav Filter
Final (g)
II
Grav Filter
Net (g)
Grav
%Rec
96.26!
2.0001
0.09541
0.15371
0.05831
86.08 1
2.0001
0.0962
0.1542 1
0.0~80 85.~9r
2.000
0.0957
0.1546
0.0589;
Mean
%Rec
SAF
SAF
65741 _ 82.53! 1.00 I 1.00

73.4211.00 I 1.00
385.91
94.791
2.000
0.0957
0.1518
0.056; -,':5ol-''2or_ 1.00
1.00
0.9105
90'-7
386.0 '
94-nr--
2.ooo
0-0<>58
0.1511
0.0553
81.32l_77.03
1.00
1.00
0.9085 .
902.7
55.951
2.000
o.0964
o.1542
0.0578
85.o~j
47.56, 1.00
1.00
0.9086
902.8
68.85!
2.0001
0.0958
0.1522
0.0564
82.94~1
'
0.8957
890.0
339.1
2.000
0.0962
0.1526
0.0564
82.94
70.16[ 1.00
1.00
TRG '
0.9078
902.0
360.2 _----,;;:;;;\
2000
0.0964
0.1515
0.0551
8103, _71.8311.00
'1
1.00
903.2
391.6
2.000
0.0957
0.1509
0.05521
0.0963
- o.1517'
-~RG
TRG
915.5
Radiometric
Tracer (pCi)
903 8
I
.
1--~~RG
0.9214 I
Tracer Total
ACT (dpm)
0 9096
~TRG
09
383.9
IDUP1
-'----1-.:'"G
1_ 06 ! TRG
'
0.9118 1
0.9114 ! W s . 6
MBL
1.
Tracer
Aliquot (g)
~90
I ~
1
. 227.5
280.0 .
96.251
1.00 I 1.00
81.18t 78.13
o.0~~82.231
1.00 I 1.00
1.00
1.00
901.81
410.0
0.9114
905.6
354.2
86.83 !
2.000
0.0960
0.1507
0.0547
80.44; .. 69.851 1.00
1.00---1
TRG
1.00 I 1.00
13
TR~0.9086
902.8 .
362.2
89.06
2.000
0.0960
0.1509
0.0549
80.~41
71.91
1.00
1.00
14
TRG
0.9057
899.9
385.1
95.00
2.000
0.0960
0.1521
0.0561
82.5Qf7a.37
1.00
1.00
1---:;5
TRG
0.9055
899.7
356.1
87.86
2.000
. 0.0964
O~ 1540
0.0~-8~ 74.43 .. 1.00
1.00
16
I TRG
0.9046
898.8
332.7
2.000
0.0924
0.1~
0.0556
81~ 67.19
17
I TRG ro.9066
900.8 ,
395,;t-97.47 -
2.000
0.0928
0.15001
0.0572
18
2.000
0.0929
0.1509
0.05801
19
2.000
0.0927
0.1509
0.05s;r-;;5.59'
82.2011.00_i.2.00
0.0927)
0.1514]
o.o587l
77.54
'
20
-~67
TRG ~~63
TRG
TRG ,
o.9059
900.1 ,
82.171
39~:2
_98.37!
389.~96.04
900.9
900.5
364.2~G.ooo
1.00
1.00
84.121
81.9911.00
1.00
85.291
83.90.
86.321
1.00~~
1.00
!l'.:U
4~::fi,
ih::i.
0.9076
~2 I
(i\)1
____12~0 I
-100.9~.ooo
8~1.52
1.00
Eberline Services
Analysis Sheet
Printed: 8/5/2013 10:17 AM

Page 3 of 3
13-07098
Ra228
Run 1
Internal
Fraction
j Sample
Desc
01
LCS
02
i MBL
03
CUP
04~G
05
TRG
~-
Rough Prep
Date
Rough Prep
By
+
. l
-----=+
Prep
Date
07/19/13 08:57
07/19/13 08:57
TRG
TRG
10
TRG
11
DO
12
TRG
13
TRG
14
TRG
15
TRG
16
TRG
17
TRG
18
TRG
-----
19
TRG
wTTRG
--+--
i-
:_
--+
..
-----1---
[
i
Sep to
By
Sep t1
Date/Time
Sep t1
By
JWOLFE
07/23/13 12:55
LWALKER
07/31/13 04:18
TSMITH
JWOLFE
07/23/13 12:55
LWALKER
07/31/13 04:18
TS MITH
TSMITH
LWALKER ' 07/31/13 04:18
07/19/13 08:57
JWOLFE
: 07/23/13_12:55
LWALKER
07/19/13 08:57
JWOLFE_
07/19/13 08:57
JWOLFE
\ 07/23/13 12:55 . LWALKER
07/19/13 08:57
JWO_~
07/19/13
--
JWOL~ffi7/23/1312:55
f---
09
'
Sep to
Date/Time
07/19/13 08:57
08
Prep
By
08:5~0LFE
07/19/13 08:57
07/31/13
04~*~SMITH
TS~~TH
07/31/13 O~*MITH
07/23/13 12:55 . LWALKER _ 07/31/13 04:18_
07/23/13 12:55
LWALKER
07/31/1~ 04:18
i 07/23/13 12:55
LWALKER
07/~1/13 04:18
TSMITH_
07/23/1312:55
LWALKER
07/31/13 04:18
TSMITH
JWOLFE
TSMI~
07/19/13 08:571
JWOLFE
07/23/13 12:55
LWALKER
07/31/13 04:18
TS MITH
07/19/13 08:57
JWOLFE
' 07/23/13 12:55
LWALKER
07/31/13 04:18
TS MITH
JWOLFE --rom3113 12:55
07/19/13 08:57
LWALKER
07/31/13 04:18
TSMITH
-----
07/19/13 08:57
JWOLF-~7/23/13 12:55
LWALKER
07/31/13 04:18
TS MITH
07/19/13 08:57
JWOLFE
, 07/23/13 12:55
LWALKER
07/31/13 04:18
TS MITH
07/19/13 08:57
JWOLFE
j 07/23/13 12:55
LWALKER
07/31/13 04:18
TSMITH
--
07/19/13 08:57
JWO~ 07/23/13 12:55 , LWALKER
07/31/13 04:18
TS MITH
07/19/13 08:57
JWO~-- 07/23/13 12:55
LWALKER
07/31/13 04:18
TS MITH
07/19/13 08:571
JWOLFE
LWALKER
07/31/13 04:18
TSMITH
07/19/13 08:57
07/23/13 12:55
JWO~ 07/23~1312:55
--
LWALKER
07/19/13 08:57
JWOLFE
07/23/13 12:55
LWALKER
07/31/13 04:18
TSMITH
07/31/13 04:18
TS MITH
~~rllt
t".r.a<.
t~~l
Eberline Services
-~
Client
Identification
Activity
Units
Results
Error Estimate
MDA
LCS
Known
LCS
%R
LCS
Flag
119.50
OK
RPO
Flag
MOA
Flag
LCS
pCi/I
1.06E+01
8.26E-01
9.69E-02
02
RA-228
MBL
BLANK
pCi/I
2.43E+OO
4.24E-01
1.07E-01
03
RA-228
DUP
1-4 TOT
pCi/I
3.00E+OO
4.42E-01
1.02E-01
04
RA-228
TRG
PZ-111-SD TOT
pCl/I
3.72E+OO
5.0GE-01
1.08E-01
OK
05
RA-228
TRG
PZ-111-SD DIS
pCi/I
4.77E+OO
5.76E-01
1.07E-01
OK
06
RA-228
TRG
S-5TOT
pCi/I
5.52E+OO
7.98E-01
1.75E-01
OK
07
RA-228
TRG
S-5 DIS
pCi/I
4.01E+OO
6.16E-01
1.46E-01
OK
08
RA-228
TRG
FB@ PZ-110-SS TOT
pCi/I
2.86E+OO
4.67E-01
1.20E-01
OK
09
RA-228
TRG
PZ-110-SS TOT
pCi/I
4.11E+OO
5.57E-01
1.20E-01
OK
10
RA-228
TRG
PZ-110-SS DIS
pCUI
5.20E+OO
6.02E-01
1.14E-01
OK
11
RA-228
DO
1-4 TOT
pCl/I
5.20E+OO
5.91E-01
1.07E-01
OK
12
RA-228
TRG
1-4 DIS
pCUI
5.89E+OO
6.75E-01
1.27E-01
OK
J
.E
13
RA-228
TRG
PZ-100-SS TOT
pCill
1.99E+OO
8.43E-01
1.GOE+OO
OK
t0
14
RA-228
TRG
PZ-100-SS DIS
pCl/I
7.37E-01
6.58E-01
1.33E+OO
OK
15
RA-228
TRG
D-3 TOT
pCi/I
4.81E+OO
9.62E-01
1.GOE+OO
OK
16
RA-228
TRG
D-3 DIS
pCi/I
6.18E+OO
1.03E+OO
1.60E+OO
OK
17
RA-228
TRG
PZ-100-SD TOT
pCi/I
1.35E+OO
6.65E-01
1.27E+DO
OK
18
RA-228
TRG
PZ-100-SD DIS
pCi/I
6.71E-01
6.21E-01
1.25E+OO
OK
19
RA-228
TRG
PZ-112-AS TOT
pCi/I
3.39E+OO
6.92E-01
1.09E+OO
OK
20
RA-228
TRG
PZ-112-AS DIS
pCi/I
1.96E+OO
7.51E-01
1.40E+OO
OK
co
c.
8.84E+OO
OK
NA
OK
c.
..
..
"
(/)
c:
~1
<:J
"'c:
~
:;;
"'
c:
..
c:
13
,t"~,
t~~
IJn
a,
c:
w
Blank
Flag
OK
LCS
"
Oesc
Sample
RA-228
cu
;;;
c
Nuclide
Work Order: 13-07098-Ra228-1
01
&
"'""
Lob
Fraction
Printed: 8/5/2013 10:19 AM
Page 1 of 3
OK
Eberline Services
~
c
,E I
.g
8
-~
Work Order: 13-07098-Ra228-1
G'"
Sep to
DatefTime
Sept1
Nuclide
Sample
Desc
Sample
Sample
Date
Aliquot
01
RA-228
LCS
07/16/13 00:00
1.00E+OO
96.26
85.74
82.53
1.00
7/23/201312:55
7/31/2013 4:18
02
RA-228
MBL
07/16/13
oo:oo
1.00E+OO
86.08
85.29
73.42
1.00
7/23/2013 12:55
7/31/2013 4:18
03
RA-228
DUP
07/09/13 12:25
1.00E+OO
94.11
86.62
81.52
1.00
7/23/201312:55
7/31/2013 4:18
04
RA-228
TRG
07/09/13 10:42
1.00E+OO
94.79
82.50
78.20
1.00
7/23/201312:55
7/31/2013 4:18
05
RA-228
TRG
07/09/13 10:42
1.00E+OO
94.72
81.32
77.03
1.00
7/23/2013 12:55
7/31/2013 4:18
06
RA-228
TRG
07/09/13 10:50
1.00E+OO
55.95
85.00
47.56
1.00
7/23/2013 12:55
7/3112013 4:18
RA-228
TRG
07/09/13 10:50
1.00E+OO
68.85
82.94
57.11
1.00
7/23/2013 12:55
7/31/2013 4:18
08
RA-228
TRG
07/09/13 11:40
1.00E+OO
84.58
82.94
70.16
1.00
7/23/201312:55
7/31/2013 4:18
09
TRG
07/09/13 12:13
1.00E+OO
88.65
81.03
71.83
1.00
7/23/201312:55
7/31/2013 4:18
10
RA-228
RA-228
TRG
07/09/13 12:13
1.00E+OO
96.25
81.18
78.13
1.00
7/23/2013 12:55
7/31/2013 4:18
11
RA-228
DO
07/09/13 12:25
1.00E+OO
100.93
81.47
82.23
1.00
7/23/2013 12:55
7/31/2013 4:18
12
RA-228
TRG
07/09/13 12:25
1.00E+OO
86.83
80.44
69.85
1.00
7/23/2013 12:55
7/31/2013 4:18
13
RA-228
TRG
07/09/13 13:36
1.00E+OO
89.06
80.74
71.91
1.00
7/23/2013 12:55
7/31/2013 4:18
14
RA-228
TRG
07/09/1313:36
1.00E+OO
95.00
82.50
78.37
1.00
7/23/201312:55
7/31/2013 4:18
"'".."
15
RA-228
TRG
07/09/13 13:42
1.00E+OO
87.86
84.71
74.43
1.00
7/23/201312:55
7/31/2013 4:18
16
RA-228
TRG
07/09/13 13:42
1.00E+OO
82.17
81.76
67.19
1.00
7/23/2013 12:55
7/31/2013 4:18
"'
""'"'
""'
~
17
RA-228
TRG
07/09/13 14:32
1.00E+OO
97.47
84.12
81.99
1.00
7/23/2013 12:55
7/31/2013 4:18
18
RA-228
TRG
07/09/13 14:32
1.00E+OO
98.37
85.29
83.90
1.00
7/23/2013 12:55
7/31/2013 4:18
19
RA-228
TRG
07/09/13 14:46
1.00E+OO
96.04
85.59
82.20
1.00
7/23/201312:55
7/31/2013 4:18
20
RA-228
TRG
07/09/13 14:46
1.00E+OO
89.82
86.32
77.54
1.00
7/23/2013 12:55
7/31/2013 4:18
Lb
Fraction
T"'
00
N
ca
.;
.E
"!:'.
0
a.
a.
~I
Printed: 8/5/2013 10:19 AM
Page 2 of 3
..
07
Radiometric
%Rec
%Rec
Mean
%Rec
SAF
Date/Tlme
-
-
::;;;
"
UJ
"
c,
1<!!1
.Ii:~~.
O")
,,,,,_~
Eberline Services
0:
{:
8
.~
"
Printed: 8/5/2013 10:19 AM
Page 3 of 3
Work Order: 13-07098-Ra228-1
Lb
Fraction
Nuclide
Sample
Oesc
Counting
Date/Time
01
RA228
LCS
02
RA-228
03
Halflife
(days)
Count
Bkg
Detect
Carrier
07/31/13 08:18
L84110R
A1
120
629 0.00196688
0.4776
M8L
07/31/13 08:18
LB4110R
A2
120
127 0.001681312
0.4699
RA-228
DUP
07/31/13 08:18
L84110R
A3
120
178 0.00237914
0.4809
04
RA-228
TRG
07/31/13 08:18
L84110R
A4
120
208 0.002347269
0.4732
N
N
05
RA-228
TRG
07/31/13 08:18
L84110R
81
120
264 0.002208604
0.4754
rx:
06
RA-228
TRG
07/31/13 08:18
L84110R
82
120
185 0.002084176
0.4658
07
RA-228
TRG
07/31/13 08:18
L84110R
83
120
163 0.002208398
0.4713
08
RA-228
TRG
07/31/13 08:18
L84110R
84
120
145 0.002425977
0.4773
09
RA-228
TRG
07/31/13 08:18
L84110R
C1
120
210 0.002480706
0.4705
10
RA-228
TRG
07/31/13 08:18
L84110R
C2
120
287 0.002817592
0.4676
11
RA-228
DO
07/31/13 08:18
L84110R
C3
120
298 0.002511178
0.4614
12
RA-228
TRG
07/31/13 08:18
L84110R
C4
120
293 0.002817505
0.4714
13
RA-228
TRG
07/31/13 08:17
L84110A
81
120
284 1.533333333
0.4626
14
RA-228
TRG
07/31/13 08:17
L84110A
82
120
195 1.283333333
0.4691
15
RA-228
TRG
07/31/13 08:17
L84110A
83
120
429
1.55
0.449
16
RA-228
TRG
07/31/13 08:17
LB4110A
84
120
450 1.333333333
0.4619
17
RA-228
TRG
07/31/13 08:17
LB4110A
C1
120
232 1.283333333
0.4667
18
RA-228
TRG
07/31/13 08:17
L84110A
C2
120
189
1.25
0.4578
19
RA-228
TRG
07/31/13 08:17
LB4110A
C3
120
312
0.95
0.4699
20
RA-228
TRG
07/31/13 08:17
L84110A
C4
120
276
1.4
0.4692
co
cu
-=~
0
""""
::s
"'c
~
~I
"
"
E
Time
Counts
Eff
CPM
Cl
~
:;;
Cl
;::
"c
"
c;,
c
w
~Ell
'~~.
(!~
~),)I
---
Count Room Report

Internal
Fraction
I
1
Sample
Desc
13-07098-Ra228-1 (pCi/I) in WA
Tracer ID: Ba-6a
Client
ID
01
LCS
LCS
02
MBL
BLANK
Sample
Date
-+
'
07/16/13
1.0000
0.9096
903.8104+--=_85.9000
94.79
1.00
1.00
1.0000
0.9105
904.7047 '
94.72
1.00
1.00
0.9085
902.7174
55.95 . 1.00
1.00
TRG
S-5 TOT
07/09/13
10
TRG
PZ-110-SS DIS
,r.~~~~jt
386.0000
p1-- 22:.5000
0.9086
902.8168 H0.0000
68.85
1.00
1.00
1 0000
0.8957
889.9989 '
339.1000
84.58
1.00
1.00
1 0000
0.9078
902.02~360.2000
88.65
~09/131213 - ~000
1.0~Bi
0.9090
903.21421
96.25
1.00 . 1.00
~9/13 11 :40
09/13 12*1
391.6000
---------
11
DO
1-4 TOT
07/09/13 12:25I1.0000
0.9076
901.8231
410.0000
100.93
1.00
1.00
12
TRG
1-4 DIS
07/09/1312:~~1.0000
0.9114
905.~--
354.2000
86.83
1.00
1.00
13
TRG
PZ-100-SS TOT
07/09/1313:36
'
1.0000
._________l__
0.9086
902.8168
362.2000
89.06
1.00
1.00
01109113 13:36
899.9352 .
385.1000
95.00
1.00
1.00
0.9055 .
899.736sla56.1000
87.86
1.00
1.00
0.9046
898.8422 ~32.7000
82.17
1.00
14
TRG
PZ-100-SS DIS
15
TRG
16
TRG
1.0000
D-3 TOT
07/09/13 13:42_~
1.0000
D-3 DIS
07/09/13 13:42
1.0000
1.0000
0.9067
900.9289
07/09/13 14:46 ;'
1.0000
0.9063
1.0000
0.9059
T~__PZ-10~-SD DIS
07/09/13 14:32
19
TRG
TRG
07/09/13
PZ-112-ASTOT
.
PZ-112-AS DIS
'
900829~t-395.50d
18
1~
0.9066
TRG
PZ-100-SD TOT
14:3~! 1.0000
17
20
CI'.)
10:5~~-0000
1.0000
t~
07/09/1310:50 '
1.00
1.00
06
'
1.00
1.00
07/09/13 10:42
PZ-110-SS TOT
86.08
905.9~51.3000
94.11
PZ-111-SD DIS
TRG
1.00
,.
SAF
383.9000
TRG
09
1.00
397.0000 .
905.5989
05
FB @ PZ-110-SS TOT
96.26
,.
0.9114
07/09/1310:42
TRG
SAF
1.0000
PZ-111-SDTOT
08
915.5353
I
Radiometric
%Rec
07/09/13 12:25
TRG
S-5 DIS
0.9214
Radiometric
Tracer (pCi)
0.9118
04
TRG
Tracer
ACT{dpm)
1.0000
1-4 TOT
07
Tracer
Aliquot (g)
00:0~-~0000
DUP
Sample
Aliquot
07/16/13 00:00 .
03
-
Printed: 8/5/2013 10:17 AM

Page 1 of 1
07/09/13 14:46
399.2000
900.531~~1-- 389.6000
- -----r----------.
364.2000
900.1339 i
--
1.00
1----..
9747
1.00
1.00
98.37
1.00 ' 1.00
96.04
1.00
1.00
89.82
1.00
1.00
Eberline Services
Analysis Code
oate
iechnician
Ra228
7/19/2013 8:56
JWOLFE
LCS
Isotope
Sol#
Ra-228
Ra-11
Page 1of1
Printed: 7119/2013 8:57 AM
Activity
dpmlg
Solution
Date
37.8641
7/19/2013
Approx
Addition
Volume
Used(g)
0.530
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
LCS
Known
pCi
8.84
0.5184
iecfinician Initials
1-----t------j---
---
MS
Error
Estimate
Added
pCi
0.451
I Estimate
Error
o.ool
LCSD
0.000
MSD
Error
Estimate
Known
pCi
0.00
0.000
-l----j----1----+----+
Tracers
Activity
dpm!g
Solution
Date
Volume
Used(g)
Approx
Addition
fraction
Isotope
Sol#
01
Ba-133
Ba-6a
993.635 7/19/2013
0.9214
1.0200
02
Ba-133
Ba-6a
993.635 7/19/2013
0.9118
1.0200
993.635 7/19/2013 .. .. 0.9114
1.0200
03
Ba-133
Ba-6a
04
Ba-133
Ba-6a
993.635 7/19/2013 .
0.9096
1.0200
05
Ba-133
Ba-6a
993.635 7/19/2013
0.9105
1.0200
06
Ba-133
Ba-6a
993.635 7/19/2013
0.9085
1.0200
07
Ba-133
Ba-6a
0.9086
1.0200
08
Ba-133
Ba-6a
993.635 7/19/2013
0.8957
1.0200
09
Ba-133
Ba-6a
993.635 7/19/2013
0.9078
1.0200
10
Ba-133
Ba-6a
993.635 7/19/2013
0.9090
1.0200
11
Ba-133
Ba-6a
993.635 7/19/2013
0.9076
1.0200
0.9114
1.0200
I'
Tracer
LCS
.,~-
l:i!!1
~11;
w
r<lll
'J
993.635 7/19/2013
..
12
Ba-133
Ba-6a
993.635 7/19/2013
13
Ba-133
Ba-6a
993.635 7/19/20131::
0.9086
1.0200
14
Ba-133
Ba-6a
993.635 7/19/2013
0.9057
1.0200
15
Ba-133
Ba-6a
993.635 7/19/2013
0.9055
1.0200
16
Ba-133
Ba-6a
993.635 7/19/2013
0.9046
1.0200
17
Ba-133
Ba-6a
993.635 7/19/2013
0.9066
1.0200
18
Ba-133
Ba-6a
993.635 7/19/2013
0.9067
1.0200
19
Ba-133
Ba-6a
993.635 7/19/2013
0.9063
1.0200
20
Ba-133
Ba-6a
993.635 7/19/2013 I>
o.9059
1.0200
Version 2.0 08/99
Witness Initials
Matrix Spike
Added
pCi
Error
; Estimate
o.ool
0.000
Eberline Analytical
Lab
Fraction
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
Client JD
Type
LCS
BLANK
1-4 TOT
PZ-111-SD TOT
PZ-111-SD DIS
S-5 TOT
S-5 DIS
FB@ PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
1-4 TOT
1-4 DIS
PZ-100-SS TOT
PZ-100-SS DIS
D-3 TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
~~:ti,
,_,.
Rpt Units
Lab Deadline
Technician
Ra228
liters
8/6/2013
JWOLFE
Dilution Data
I
No of Dils
Aliquot Data
.....
' ..
Oil Factor -
Ratio
..
..
- -';<----- - .....
- -"-;-----
,-,';.-,
.. .
I. .
..
'
..
.
.
.....
..
-.;;_.__ --_ .:_
..
..
.....
.
.
.
....
..
Comments
Technician
..
.
Page 1 of 1
Analysis Code
Muffle Data
- ~atio
- - Post/Pre
Sample
(/.ll
l\ll
Printed: 7/19/2013 8:49 AM
Aliquot Worksheet
_J~ Cv~
Date
':f-,fL /~
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+1JO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
MS Aliquot Data
.
Net Equ_iv
1.0000E+OO
1.0000E+OO
1'DOOOE+OO
1.0000E+.00
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+1l0
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0oOdE+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
Aliquot
Net Equiv_
H-3 Solids Only

Water Added
H3 Dist
(ml)
Aliq
Eberline Services - Oak Ridge

Version 1.0 9/1999
1Nork Order
TRetec
Fraction
Client ID
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
LCS
BLANK
DUP
PZ-111-SD TOT
PZ-111-SD DIS
S-5 TOT
S-5 DIS
.
FB @ PZ-110-SS TOT
PZ-110-SS TOT
PZ-110-SS DIS
1-4 TOT
1-4 DIS
PZ-100-SS TOT
PZ-100-SS DIS
D-3 TOT
D-3 DIS
PZ-100-SD TOT
PZ-100-SD DIS
PZ-112-AS TOT
PZ-112-AS DIS
~-
2
5
...0
Technician:
~~
Printed: 7/31/2013 7:35 AM

Page 1 of 1
Gravimetric Worksheet
Sample
Type
LCS
MBL
DUP
TRG
TRG
TRG
TRG
TRG
TRG
TRG
DO
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
TRG
Analysis
Code
Gravimetric
Carrier
Carrier Cone
(mg/ml)
Technician
Ra228
Yttirum
34.0000
TSMJTH
Filter Data
Carrier Data
Carrier Added
(ml)
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
2.0000
Date:
Filter Tare
(g)
0.0954
0.0962
0.0957
0.0957
0.0958
0.0964
0.0958
0.0962
0.0964
0.0957
0.0963
0.0960
0.0960
0.0960
0.0964
0.0924
0.0928
0.0929 i
0.0927
0.0927
__J_1].}__;_!J_
Gravimetric
Filter Final
(g)
0.1537
0.1542
0.1546
0.1518
0.1511
0.1542
0.1522
0.1526
0.1515
0.1509
0.1517
0.1507
0.1509
0.1521
0.1540
0.1480
0.1500
0.1509
0.1509
0.1514
Filter Net
. (g)
"<
0.0583
.
.
.,.
.
.
.
'
.
..
'
..
..
0.0580
0.0589
0.0561
0.0553
0.0578
0.0564
0.0564
0.0551
0.05.52 ..
0.0554
0.0547
0.0549
0.0561
0.0576
0.0556
0."0572
0.0580
0.0582.
0.0587
%
Recovery
85.74
85.29
86.62
82.50
81.32
85.00
82.94
82.94
81.03
81.18
81.47
80.44
80.74
82.50
84.71
81.76
84.12
85.29
85.59
86.32
<:...--
7111111
Sheet1
(!!)
Detector ID
Sample ID Alpha
Beta Count Time
Voltage
120
1400
1307098-09
8
210
C1
1400
1307098-10 13
287
120
C2
120
1400
1307098-11 22
298
C3
120
1400
293
1307098-12
10
C4
120
1400
10
629
1307098-01
A1
1400
7
127
1307098-02
120
A2
1400
178
120
9
1307098-03
A3
1400
208
1307098-04 11
120
A4
1400
264
120
6
1307098-05
81
1400
185
120
1307098-06 12
82
1400
163
120
1307098-07 13
83
120
1400
9
145
1307098-08
84
~ill
ti:~.
~~4~
Page 1
TOD
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
7/31/13 10:18
Sheet1
fl?/117
Detector ID Sample ID Alpha

Beta Count Time
Voltage
B1
1307098-13 17
284
120
1400
1307098-14 15
195
B2
120
1400
1307098-15 10
429
B3
120
1400
B4
1307098-16 14
450
120
1400
C1
1307098-17 13
232
120
1400
1307098-18 12
189
C2
120
1400
1307098-19 12
312
C3
120
1400
C4
1307098-20 10
276
120
1400
~~~
~~.
t!l
(,,1,~1
Page 1
TOD
7/31/13 10:17
7/31/13 10:17
7/31/13 10:17
7/31/13 10:17
7/31/13 10:17
7/31/13 10:17
7/31/13 10:17
7/31/13 10:17
Eberline Analytical
t;-ll1
I"
00
i-:;~,
GPC Detector Report
Printed: 7/31/2013 7:07 AM

Page 1 of 1
(ALL Backgrounds)
Detector
Alpha/Beta
Calibration Date
Count Date
Bkg CPM
PFW
LB4110A - Al
Alpha
11/18/2007
7/31/2013
5.00E-02
LB4110A - A2
Alpha
11/18/2007
7/31/2013
LB4110A - A3
Alpha
11/18/2007
LB4110A - A4
Alpha
LB4110A - Bl
LCL
Mean
UCL
-2.14E+Ol
2.84E-01
2.19E+Ol
1.50E-Ol
-l.82E+Ol
2.55E-01
l.87E+Ol
7/31/2013
8.33E-02
-1. 77E+Ol
2.17E-01
1.81E+Ol
11/18/2007
7/31/2013
6.67E-02
l.92E+Ol
11/18/2007
7/31/2013
8.33E-02
-l.88E+Ol
-9.70E-02
2.37E-01
Alpha
7.51E-02
2.47E-Ol
LB4110A - B2
Alpha
11/18/2007
7/31/2013
l.50E-Ol
-7.82E-02
7.23E-02
2.23E-Ol
LB4110A - B3
Alpha
11/18/2007
7/31/2013
1.17E-01
-6.31E-02
5.35E-02
l.70E-01
-l.41E-Ol
7.88E-02
2.98E-01
-l.49E-01
8.88E-02
3.27E-Ol
LB4110A - B4
Alpha
11/18/2007
7/31/2013
5.00E-02
LB4110A - Cl
Alpha
11/18/2007
7/31/2013
6.67E-02
LB4110A - C2
Alpha
11/18/2007
7/31/2013
5.00E-02
-l.77E-Ol
8.69E-02
3.51E-01
LB4110A - C3
Alpha
11/18/2007
7/31/2013
1.83E-01
-1. 72E-01
l.OlE-01
3.73E-01
LB4110A - C4
Alpha
11/18/2007
7/31/2013
8.33E-02
-6.27E-02
6.84E-02
l.99E-Ol
LB4110A - Dl
Alpha
11/18/2007
7/31/2013
5.00E-02
-5.36E-02
8.35E-02
2.21E-01
LB4110A - D2
Alpha
11/18/2007
7/31/2013
6.67E-02
-7.0lE-02
6.07E-02
l.91E-01
l.90E-Ol
LB4110A - 03
Alpha
11/18/2007
7/31/2013
3.33E-02
-4.83E-02
7.09E-02
LB4110A - D4
Alpha
11/18/2007
7/31/2013
5.00E-02
-5.73E-02
7.04E-02
l.98E-01
LB4110R - Al
Alpha
11/24/2006
7/31/2013
1.90E-04
-9.84E-02
1.0lE-01
3.0lE-01
LB4110R - A2
Alpha
11/24/2006
7/31/2013
9.52E-05
-8.92E-02
7.65E-02
2.42E-01
-7.34E-02
7.72E-02
2.28E-01
LB4110R - A3
Alpha
11/24/2006
7/31/2013
1.27E-04
LB4110R - A4
Alpha
11/24/2006
7/31/2013
6.34E-05
-5.27E-02
7.lOE-02
l.95E-01
LB4110R - Bl
Alpha
11/24/2006
7/31/2013
1.24E-04
-9.44E-02
6.15E-02
2.17E-Ol
LB4110R - 82
Alpha
11/24/2006
7/31/2013
l.24E-04
-6.94E-02
6.34E-02
l.96E-01
LB4110R - 63
Alpha
11/24/2006
7/31/2013
1:56E-04
-6.48E-02
6.99E-02
2.05E-Ol
LB4110R - 64
Alpha
11/24/2006
7/31/2013
9.33E-05
-6.41E-02
7.02E-02
2.05E-01
-7.69E-02
7.36E-02
2.24E-Ol
-7.56E-02
7.llE-02
2.18E-01
LB4110R- Cl
Alpha
11/24/2006
7/31/2013
1.23E-04
LB4110R - C2
Alpha
11/24/2006
7/31/2013
9.19E-05
LB4110R - C3
Alpha
11/24/2006
7/31/2013
l.53E-04
-8.80E-02
8.44E-02
2.57E-Ol
LB4110R - C4
Alpha
11/24/2006
7/31/2013
3.06E-05
-6.20E-02
8.13E-02
2.25E-01
LB4110R - Dl
Alpha
11/24/2006
7/31/2013
O.OOE+OO
-l.02E-01
7.0SE-02
2.43E-01
LB4110R - D2
Alpha
11/24/2006
7/31/2013
O.OOE+OO
-7.73E-02
7.00E-02
2.17E-01
LB4110R - D3
Alpha
11/24/2006
7/31/2013
O.OOE+OO
-8.24E-02
6.97E-02
2.22E-Ol
LB4110R - D4
Alpha
11/24/2006
7/31/2013
O.OOE+OO
-7.46E-02
7.45E-02
2.24E-Ol
L65100 - 1
Alpha
7/10/2006
10/26/2007
5.00E-02
-l.56E-02
9.58E-02
2.07E-01
C-
/11111?
Eberline Analytical
GPC Detector Report
Detector
$.":.."t,
!JI
tr~
Alpha/Beta
Calibration Date
Count Date
Bkg CPM
PFW
LCL
Mean
UCL
LB4110A - Al
Beta
11/18/2007
7/31/2013
6.80E+OO
-2.90E+02
7.63E+OO
3.05E+02
LB4110A - A2
Beta
11/18/2007
7/31/2013
3.93E+OO
-3.04E+Ol
2.59E+OO
3.56E+Ol
LB4110A - A3
Beta
11/18/2007
7/31/2013
1.70E+OO
-5.03E+Ol
2.63E+OO
S.56E+Ol
LB4110A - A4
Beta
11/18/2007
7/31/2013
7.18E+OO
-3.25E+Ol
3.19E+OO
3.89E+Ol
LB4110A - Bl
Beta
11/18/2007
7/31/2013
1.53E+OO,
-1.04E+Ol
3.24E+OO
1.69E+Ol
LB4110A - B2
Beta
11/18/2007
7/31/2013
1.28E+OO.
-7.65E+OO
2.00E+OO
l.16E+Ol
2.61E+OO
LB4110A - B3
Beta
11/18/2007
7/31/2013
1.SSE+OO
1.14E-Ol
1.36E+OO
LB4110A - B4
Beta
11/18/2007
7/31/2013
1.33E+OO.
-7.64E+OO
l.98E+OO
1.16E+Ol
LB4110A - Cl
Beta
11/18/2007
7/31/2013
1.28E+oo.
-5.40E+OO
2.12E+OO
9.64E+OO
LB4110A - C2
Beta
11/18/2007
7/31/2013
i.2sE+oo.
3.82E-Ol
1.27E+OO
2.lSE+OO
LB4110A - C3
LB4110A - C4
Beta
11/18/2007
7/31/2013
9.SOE-01
l.46E+OO
2.45E+OO
Beta
11/18/2007
7/31/2013
l.40E+OO
4.71E-Ol
-1.76E+OO
2.lOE+OO
S.97E+OO
LB4110A - 01
Beta
11/18/2007
7/31/2013
1.SBE+OO
-2.32E+OO
2.57E+OO
7.4SE+OO
-6.4SE-Ol
l.56E+00
3.77E+OO
l.28E+OO
-4.27E-Ol
4.48E+OO
7.67E+OO
l.37E+OO
3.17E+OO
LB4110A - 02
Beta
11/18/2007
7/31/2013
1.75E+OO
LB4110A - 03
Beta
11/18/2007
7/31/2013
4.27E+OO
LB4110A - 04
LB4110R - Al
Beta
11/18/2007
7/31/2013
1.28E+OO
Beta
11/24/2006
7/31/2013
1.97E-03
-6.lOE+Ol
3.68E+OO
6.83E+Ol
1.68E-03
-4.84E+Ol
2.02E+OO
S.24E+Ol
LB4110R - A2
la
Printed: 7/31/2013 7:07 AM

Page 1 of 1
(ALL Backgrounds)
Beta
11/24/2006
7/31/2013
LB4110R - A3
Beta
11/24/2006
7/31/2013
2.38E-03.
-4.48E+Ol
2.74E+OO
5.03E+Ol
LB4110R - A4
Beta
11/24/2006
7/31/2013
2.35E-03.
-4.47E+Ol
l.99E+OO
4.87E+Ol
LB4110R - Bl
LB4110R - B2
Beta
11/24/2006
7/31/2013
2.21E-03
-4. 70E+Ol
2.02E+OO
S.llE+Ol
Beta
11/24/2006
7/31/2013
2.08E-03
-4.70E+Ol
2.0SE+OO
S.llE+Ol
LB4110R - B3
Beta
11/24/2006
7/31/2013
2.21E-03
-4.68E+Ol
2.66E+OO
5.21E+Ol
LB4110R - B4
Beta
11/24/2006
7/31/2013
2.43E-03.
-4.71E+Ol
l.92E+OO
5.lOE+Ol
LB4110R - Cl
Beta
11/24/2006
7/31/2013
2.48E-03
-4.69E+Ol
2.97E+OO
S.29E+Ol
LB4110R - C2
LB4110R - C3
Beta
11/24/2006
7/31/2013
2.82E-03
-4.69E+Ol
2.72E+OO
S.23E+Ol
Beta
11/24/2006
7/31/2013
2.SlE-03.
-4.74E+Ol
2.52E+OO
5.24E+Ol
LB4110R - C4
Beta
11/24/2006
7/31/2013
2.82E-03.
-5.35E+Ol
2.95E+OO
5.94E+Ol
LB4110R - 01
Beta
11/24/2006
7/31/2013
O.OOE+OO
-4.4SE+Ol
S.58E+OO
S.57E+Ol
LB4110R - 02
Beta
11/24/2006
7/31/2013
O.OOE+OO
-4.79E+Ol
l.88E+OO
S.16E+Ol
LB4110R - 03
Beta
11/24/2006
7/31/2013
O.OOE+OO
-5.12E+Ol
S.56E+OO
6.23E+Ol
LB4110R - 04
Beta
11/24/2006
7/31/2013
O.OOE+OO
4.76E+Ol
2.24E+OO
S.20E+Ol
LBSlOO - 1
Beta
7/10/2006
10/26/2007
4.52E+OO
-3.19E-01
1.SBE+OO
3.48E+OO
r111117
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)
Detector
Eff
PFW
LCL
Mean
UCL
-0.0136
0.2157
0.4451
Alpha
11/18/2007
7/31/2013
0.2408
LB4110A - A2
Alpha
11/18/2007
7/31/2013
0.2061
-0.0511
0.1739
0.3990
LB4110A - A3
Alpha
11/18/2007
7/31/2013
0.2079
-0.0745
0.1631
0.4007
0.2207
-0.0529
0.1818
0.4166
Alpha
11/18/2007
7/31/2013
LB4110A - Bl
Alpha
11/18/2007
7/31/2013
0.2182
0.1944
0.2244
0.2544
LB4110A - B2
Alpha
11/18/2007
7/31/2013
0.2120
0.1924
0.2214
0.2503
0.2293
0.1276
0.2323
0.3370
Alpha
11/18/2007
7/31/2013
LB4110A - B4
Alpha
11/18/2007
7/31/2013
0.2222
0.2089
0.2364
0.2639
LB4110A - Cl
Alpha
11/18/2007
7/31/2013
0.2209
0.1976
0.2208
0.2439
LB4110A - C2
Alpha
11/18/2007
7/31/2013
0.2241
0.1971
0.2252
0.2533
LB4110A - C3
Alpha
11/18/2007
7/31/2013
0.2538
0.2233
0.2494
0.2756
LB4110A - C4
Alpha
11/18/2007
7/31/2013
0.2255
0.1969
0.2257
0.2544
LB4110A - Dl
Alpha
11/18/2007
7/31/2013
0.2230
0.2030
0.2329
0.2629
7/31/2013
0.2446
0.2277
0.2581
0.2885
0.2311
0.2635
0.2959
0.2343
LB4110A - D2
Alpha
LB4110A - D3
Alpha
11/18/2007
7/31/2013
0.2429
LB4110A - D4
Alpha
11/18/2007
7/31/2013
0.1824
0.1643
0.1993
11/18/2007
LB4110R - Al
Alpha
11/24/2006
7/31/2013
0.2363
0.2005
0.2387
0.2769
LB4110R - A2
Alpha
11/24/2006
7/31/2013
0.2167
0.1869
0.2203
0.2537
LB4110R - A3
Alpha
11/24/2006
7/31/2013
0.2149
0.1929
0.2245
0.2560
LB4110R - A4
Alpha
11/24/2006
7/31/2013
0.2387
0.2125
0.2455
0.2785
LB4110R - Bl
Alpha
11/24/2006
7/31/2013
0.2163
0.1831
0.2257
0.2683
LB4110R - B2
Alpha
11/24/2006
7/31/2013'
0.2061'
0.1754
0.2170
0.2586
0.2421
0.2014
0.2438
0.2862
0.2744
LB4110R - B3
Alpha
11/24/2006
7/31/2013
LB4110R - B4
Alpha
11/24/2006
7/31/2013
0.2150
0.1883
0.2313
LB4110R - Cl
Alpha
11/24/2006
7/31/2013
0.2072
0.1833
0.2150
0.2467
0.2204
0.1931
0.2245
0.2559
0.2033
0.2394
0.2755
0.2619
LB4110R - C2
Count Date
LB4110A - Al
LB4110A - B3
""t'lt!l
Calibration Date
LB4110A - A4
ti'.t~I
Alpha/Beta
Printed: 7/31/2013 7:07 AM
Page 1of1
Alpha
11/24/2006
7/31/2013
LB4110R - C3
Alpha
11/24/2006
7/31/2013
0.2328
LB4110R - C4
Alpha
11/24/2006
7/31/2013
0.2084
0.1827
0.2223
11/24/2006
7/31/2013
0.0000
0.0080
0.2003
0.3927
0.4459
LB4110R - Dl
Alpha
LB4110R - D2
Alpha
11/24/2006
7/31/2013
0.0000
0.0097
0.2278
LB4110R - D3
Alpha
11/24/2006
7/31/2013
0.0000
0.0096
0.2238
0.4380
LB4110R - D4
Alpha
11/24/2006
7/31/2013
0.0000
0.0063
0.1804
0.3544
LB5100 - 1
Alpha
0.3368
0.3332
0.3455
0.3578
7/10/2006
10/26/2007
c..--
lt?/11/
Eberline Analytical
GPC Detector Report

(ALL Efficiencies)
Detector
1:0
"1t-J
Calibration Date
Count Date
Elf
PFW
LCL
Mean
UCL
LB4110A - Al
Beta
11/18/2007
7/31/2013
0.5560
0.2101
0.5625
0.9150
LB4110A - A2
Beta
11/18/2007
7/31/2013
0.4944
0.1610
0.4647
0.7683
LB4110A - A3
Beta
11/18/2007
7/31/2013
0.4648
0.0889
0.4572
0.8255
LB4110A - A4
Beta
11/18/2007
7/31/2013
0.5225
0.1416
0.4890
0.8364
LB4110A - Bl
Beta
11/18/2007
7/31/2013
0.5103
0.4635
0.5299
0.5962
LB4110A - B2
Beta
11/18/2007
7/31/2013
0.5081
0.4632
0.5269
0.5906
LB4110A - B3
~!!l
.~~'
Alpha/Beta
Printed: 7/31/2013 7:07 AM
Page 1of1
LB4110A - B4
LB4110A - Cl
11/18/2007
7/31/2013
0.5265
0.3162
0.5314
0.7466
Beta
11/18/2007
7/31/2013
0.5284
0.4919
0.5540
0.6160
Beta
11/18/2007
7/31/2013
0.5085
0.4510
0.5026
0.5543
Beta
LB4110A - C2
Beta
11/18/2007
7/31/2013
0.5056
0.4291
0.5010
0.5730
LB4110A - C3
Beta
11/18/2007
7/31/2013
0.6061
0.5289
0.5906
0.6523
LB4110A - C4
Beta
7/31/2013
7/31/2013
0.5215
0.5212
0.4577
0.4787
0.5248
0.5532
0.5920
0.6277
LB4110A - Dl
Beta
11/18/2007
11/18/2007
LB4110A - 02
Beta
11/18/2007
7/31/2013
0.5414
0.4890
0.5873
0.6857
LB4110A - 03
Beta
11/18/2007
7/31/2013
0.5931
0.5373
0.6150
0.6927
LB4110A - 04
Beta
11/18/2007
7/31/2013
0.4372
0.3849
0.4721
0.5594
LB4110R - Al
Beta
11/24/2006
7/31/2013
0.5611
0.4754
0.5675
0.6595
LB4110R - A2
Beta
11/24/2006
7/31/2013
0.5163
0.4166
0.5087
0.6009
LB4110R - A3
Beta
11/24/2006
7/31/2013
0.5268
0.4506
0.5386
0.6265
LB4110R - A4
Beta
11/24/2006
7/31/2013
0.5969
0.5033
0.5915
0.6798
LB4110R - Bl
Beta
11/24/2006
7/31/2013
0.5342
0.4461
0.5422
0.6383
LB4110R - B2
Beta
11/24/2006
7/31/2013
0:5046
0.4245
0.5196
0.6147
LB4110R - B3
Beta
11/24/2006
7/31/2013
0.5985
0.4936
0.5916
0.6896
LB4110R - B4
Beta
11/24/2006
7/31/2013
0.5184
0.4540
0,5490
0.6440
LB4110R - Cl
Beta
11/24/2006
7/31/2013
0.4613
0.4162
0.5017
0.5873
LB4110R - C2
Beta
11/24/2006
7/31/2013
0.5125
0.4439
0.5284
0.6129
LB4110R - C3
Beta
11/24/2006
7/31/2013
0.5626
0.4753
0.5706
0.6659
LB4110R - C4
Beta
11/24/2006
7/31/2013
0.4959
0.4259
0.5251
0.6243
LB4110R - Dl
Beta
11/24/2006
7/31/2013
0.0000
0.0183
0.4790
0.9398
LB4110R - 02
Beta
11/24/2006
7/31/2013
0.0000
0.0212
0.5383
1.0554
LB4110R - 03
Beta
11/24/2006
7/31/2013
0.0000
0.0205
0.5228
1.0251
LB4110R - 04
Beta
11/24/2006
7/31/2013
0.0000
0.0139
0.4303
0.8467
LB5100 - 1
Beta
7/10/2006
10/26/2007
0.4428
0.4555
0.4731
0.4906
c..
1-n117
SECTION XII
BARIUM-133 ANALYTICAL TRACER DATA
L-
configuration
Analyses by
Client ID .
Peposition Date
sample Date
Sample ID
Sample typ<il
Detector name
:
Elapsed live time:
Start channel
Sensitivity
C:i;it;ical level
I;lKl\.100' [GAMMA. SCUSR.ARCI'!IVE] SMP 13070$l60l

ll'EAK V16. 9 l?ll!J\.Kll:F'F V2. 2
-"
SPIKE
?1~
ClE3~BJ\.F!L~19357'7
24-JUL-201.3 QOiOO:OO ~cquisition date : 24-JUL-2013 07:47:36

J,307098-01
Samp:).e Quantity
l.OOOODE+DO tilter
FILT.ER
Sample Geometry
Q
Detector Geometry:
Elap$eq reai tim~:
E:nd eham:i,el
Gaui;;lilian
GE:3
0 OQ:l5:CJO.OO
2S
3.00()09
BAFIJ;,.
OOolS:OS.O~
:L0.00000
No
F:i,t
30.7S
2:J,l1
102
2
3
4
0
500
90
64
1
1
0
134
82
80
13
1
2
35.00
52.34
61,. 56
65.82
80.90
l:Ll.62
ll6.2l
l.60.31
206.25
276.SS
282.69
302.79
14
307.04
15
16
3:L0.69
1
0
0
333.53
337.72
93
17
:L
6
7
9
10
ll
:).2
ie
:L9
20
21
22
23
24
25
26
27
28
29
0
0
0
0
:L
:L
1
0
l
1
0
0
0
0
Q
0.6~
4096
Pk It
.CN
355.98
365.S:L
31\l3.67
3!Hi.7$
391..16
414.53
417.87
436.72
41!ifi. 04
472.SS
510.98
583.52
253
141
828
222
72
32
55
116
89
47
76
:L.41
l.73
1.67
1.51
1.52
1.68
1.46
1.94
1, 61
;n.io
2Ei
l.4 2.35l1!+00
35.'.!2
52.66
2~
14 5.$SE01
ii~
~a.as
57
57
!J
17
17
7
fi6.14
81.22
'77
111. !:13
116.53
l.60.63
108
115
:LSS
5$
5.67
206.56
202
62
13
14
13
276.$6
145
3Ei
18
1.78
1. 62
1. 50
272
272
298
298
298
330
330
352
362
31:3 l.
381
390
410
""':L 0
36
5411
;LO
116
198
18
13
:L6
12
35
30
23
27
1.99
1.64
1.S3
1.83
1.48
1.70
1.13 7
l9
19
1.73
l. 96
1. 89
36
121
20
1.90
1. 50
23
11
18
11
10
ll
1.85
0
0
3.94
2.58
54
45
l.44
21')3.00
303.09
307.34
31;1..()0
333.83
338.02
356.29
366.11
383.98
387.08
3Q:J,.47
414.93
418.1'7
437.02
HiS.34
433
464
473.17
511.28
470
508
583.82
581
2.3 (J.J,OliJ+OO
s.s
7.09E-02 3S.8
2.SlE;-01 8.3 2.33i+OO
1,57E-01 12.7
;l.20E-Ol 4.1
7 2.47E-01 9.7
5 8.04E-02 18.8
7 3.55E-02 49.5
10 6.06E-02 29.7
15 6.84E-02 16.0 2.59E+OO
15 1.42E02 56.9
19 1. 61.E-OJ,. 9.3 2.33E+OO
J,.9 4.00E-02 31.0
J,.9 1.04E-02 76.0
11 l.03E-01 :L2 .1 1.33E+OO
l.1 4.0SE-02 2'.$.7
9 6.04E-0l. 4.7
7 1.09E-02 96,. 3
9
9
6
18
l.8
1.29E-Ol.
2.2oE-01
5. 'il6E-02
4.98E02
3,95E-02
7 1.34E-01
12.9 1.44E+Ol.
9.4
19.9
22.1
29.6
9.3
'7 2.56E-02 31.:L
6 1.27E-02 $5.2
7 2.00E-02 23.6
7 1.22E-02 30.2
Summary of Nuclide Activity

Sample ID : 1307098-01
Acquil3ition date
Total m1mber of linef; in ;;pectrum

NumJ;ler o:t: unidentifieO. lines
N\lmber o:e lines tentatively iC!entified by NIP
l?age :
29
24
17.24\
Nuclide Ty)?e : FISSION

Nuclic;le
EA-133
Hlife
10,!;'SO'i
W\;d Mean
Qncoin:ec::ted
Decay pCi/f ilter
1.00
Total Activity
3.970E+02
3.970E+02
3.970E+02
3.970E+02
Nuclide Type ' NATURAL

Nuc+ide
!ilife
PA-2;!1 3. 48E-!04Y.
TH2~4
4.47E:+Q9).'
Wt;d Mean
Uncorrected
Decay pCi/filter
l.00
1.00
Wt;d Ml!an
Pecay Corr
pCi/filter
Wtd Mean
Pecay Corr
pCi/filter
3,0S6E+O;>
'7.S49E+02
3.036E+03
7.5491)+02
3.791E+O~
:3,791E+03
4.18BE+03
4.188E+03
~---..,.
Total Activity
Grand Total Activity :
"K" "' Key:).ine not found

"E" "' Manually edited
...
24;-JUL:!Wl.3 07: 4;7: 36
Decay Corr
2-sigmc;,
2-Sigma Error %Error Flagl3
0,706E+02
:l. 7. 79
DecOl.y Corr
4-Sigms,
2-Sigma Error %E:t:ror Flags
0.78!5El+03
J,.,35!5E+02
;a f)i. 8 7
17,$!5
-~-'"
"M" = Manually accepted

"A" "' Nuclide s~ecific abn. limit
NUcl.iQ,e 1,:l,ne A,ctivity J<.eport

Sample IP : 1307098-01
Page :
Nuclide Type: FISSION

Nuclide
BA-133
E11ergy
01.09
302.84
356.01
Uncorrect.Eild'Pecay Corr
%A:bn
33.00*
17.S()
60.00
Final Mean for
24-JUL>-2013 07:4(1::.16
%Eff
pCi/filter
1.899E+01 . 3.970!!!+02
6.222E+OO 3,923E+Q2
5.860E+OO 4.645E+02
3 Valid
Peaks~
pCi/filter
3.970E+02
3.924E+02
4.645E+02
:?-~ligma
%Error
17,79
27.78
16.60
Stati.u;
OK
OK
OK
3,970E+02+/- 7.061E!+01 ( 17.79%)
Nuclide Type: NA,TU!IJ\L
Nuclide
PA-231
Energy
9,2S
10.11
2!)3.67
302.67
%Al:'Jn
42.00*
20. 20
1.60
2,30
Final Mean for

TH-234
63.29
2 Valid Peaks
3.80*
Final Mean for
uncorrected Pecay Corr 2-Sigma

pCi/filter pci/filter %Error
l.OOOE+02 ----- Line Out Of Range ---l.OOOE+02 ----- Line Out Of Range ---6.406E+OO 3. 756E+02
3.756E+02 115.18
6.224E+OO 3.036E+03
3.036E+03 25.87
%Eff
2.648E+01
1 Valid
3.036E!+03+/- 7.854E+02 ( 25.87%)
7.549E+02
Peaks~
s t<i\ t 1.,1$
Ab:!lent
Absent
OK
OK
'7.549EJ+02
17.95
OK
7.549E+Q2+/- 1.355E+02 ( 17.95%)
Flag: "*" "' Keylinei
85S1
combined AGtivity-MDA Report

Sample ID ; 1307098-01
Acquisition date
Page ;
4
24-JUL-2013 0747;36
Activity
(pCi/filter)
.!\.ct <!rror
MDI',
(pCi/t:ilter)
MDA E!)rro:r
Act/MDA
Nuclide
l3A-13 3
PA-231
TH-234
3.970E+Q2
3,036E+03
7.549E+Q2
7.061E+Ol
7.854E+02
1.355E+02
2.212E+01
3.194;E+QO
l.361E+02
3.383E+OO
4.542Jll-02
'7.311E+OO
17.946
950.530
!5. 546
Act err<;ir
MP/l;
(pCi/tilter)
error
Act/MDA
6.04'0E+OO
l,129E+02
l.558E+OO
3.490E+01
1.053E+Ol
9.SSOE+OQ
1.951E+D2
2.886E+OO
5.610E+01
l.989E+Ol
1.091E+OO
1.609E+01
4.104E-02
4.535E+OO
9.779E01
-0.()97
Non-rdentif ied Nuclides
Nuclide
C0-57
CD-109
PA-234
Nl?-237
AM-241
Key-Line
Activity I<. L,
(pci/filter)Ided
-9. 26'.!.E-O:J.
-4, 044E+OO
3.40BE+OO
9,576E-Ol
3.389E+Ol
M\')A
-o.o::a
1.181
0.017
1.704
VAX/VJV!S P@<tk
Search
ConfiliJration
A,naJ;yseia l:Jy
Client IP
Depoi;;H:ion :Oat;e
Sa,mple Pate
l
Samp:Lfl IP
sa.mple type
Petflctor name
:
El,ai;io;ed live time
Stll.rt;. channel.
seni;iit;ivity
C:rit;i.9al l<:JVel
L.-
-'j7/~
Rep<;:>rt Genera,t;:ed. 24-JUl',,c20l3 08 'J.8: 40. 01
PKA.J,90: [GAMMA.$GUSR.A,RC}l'):VE]SM!? J,:30709802 GJ;1;3 BAFIJ;., 193579.CN
l?!!J]'.!< VlG. 9
Et.AfiK
l?EAK!!J!!'V V2. 2 .
24,-JlJI.-:20;1.3 0():00:00
130709iJ-02
F:T:I.TER
GE3
0 QO:l-5:00,0Q
25
3.0000Q
No
Aoquisition ~ate :
SampJ,\:l Quantity
S<!.mple Geometry
Petector Gleometry:
Elapsed reaJ, time;
En~ ch!!'!'ln\Sl
<:>&ssian
24iJl.ll:..-20;1.J Oil: 03; J,9

i.000001+00 filter
0
:SAF'IL
0 00:15:04.49
Q.5%
4096
lQ.00090
Fi,t
1
2
;:!
3
4
5
6
7
8
0
l
l
l
l
l
0
l
10
ll
12
13
14
l5
16
17
1
0
0
0
0
1
1
18
19
20
2l
42
23
24
25
2<?
5
5
0
4
4
0
30,74
34. !ls
52.87
58,82
6l-.82
65.54
80.S2
83,EiS
93.0'7
1.11.EiO
l-15.54
l60.53
476.96
303.15
322.33
333.54
337.59
3!/l,77
3S5.90
31L3.53
386. 74,
414,43
4,3Ei.!!5
467.4,9
472.29
510.52
4,(:153
a1
56Q
90
75
lll
ll?
34
231
l-Ol
'733
28
33
65
74
40
25
196
53
26
49
121
20
72
20
16
76
49
49
'77
44
52
l.5
14,
20
sos
0
6
20
31
25
l9
ll
84
185
88
24
2
3
19
1. 43
1.ss
2. 3 0
l..50
1. 51
1. 52
1. 54
1.41
1. 22
1.!:)9
l.60
l.l6
1.54
1.1Ei
4.98
l.83
1. 83
:)..84
1.55
2,09
1.49
1. SHI
1. 22
2.57
2.58
l. 69
3:L.06
35,27
53.19
59.l-4
62.14
65.86
Sl.l.4
84,QO
513.38
111.9l
ll5.85
l.60,85
277.27
303.46
322.63
333.84
337.SlO
352.08
356.20
383,84
3$7.Q4
414.73
43'7.15
467.79
4'72.551
Sl0.82
26
:;l6
49
Stl
SS
58
7Ei
76
89
l07
l07
157
2 '7 4,
300
3lf.l
32 ll
328
351
35l
38l
38l
412
434
4Ei2
462
~06
19
19
9
12
12
l2
ll
11
'7
ll3
HJ
6
9
7
10
l-4
14
12
12
9
9
'7
'7
14
l4
10
2.J.7E+QO
1L2;lE-Ql
1.00E-Ol
2.121-02
2,571-01
l.12El-0:).
S.14EOl
3.l-31-02
3.EiSE-02
2.lBE-01
2.3 1.QSE+()l
4;.9
23.7
4, 9. 2 l..10E+Ol
8.9
16.5
4.1 1.191,l;+Ol
67,l
4'7. s
9,2 2.79$+00
;;.s~rn:-o:a
:as.o
2.92E-02
5.46E-02
l.35E-01
2.lSE-02
8.04E-02
2.27E-02
1.75E-02
5.64E-Ol
9.:.lOE-02
2.06E-01
3.45E-02
9.?SIE:-02
2.68E-02
8 .42lhQ3
2.0SE-02
!;)6. l
28.4
13.3
43.4
14.3
38.9
20.0
4.5
16,6
8,4
28.9
l-2.3
24. ;t
49.8
3)_.9
2.12El+OO
1.llE+OO
6.l3E+OO
7.00E-01
Summary of Nucli~e Activity

Sample IP : l307Q98-02
Acquisition d?.te
Total number Of lines in spectrum

Number of \mident:U:ied lines
Number o:e lines tent?.tively identified by NIP
Nuclide '.l"ype ' F!$SION
NucliO.e
EA-l.33
Hlif e
10.SOY
Wtd Mean
Uncorrected
Decay pci/filter
1.00
Total Activity
Page :
26
2l
Wtd M\llan
Decay Corr
pCi/filter
3.S12E:+02
3.513Et02
3.5l2E+02
3.S;L3E+02
:I.9.23%
Dt;!eay C<::>rr
4-l.li11ma
2-Sigma Error tErro:i:: Flags
17.SS
Q.627E+02
Nc;1ide Type : NATURAL

Nuqli.G.e
TH-234
AM-24l
IUife
4.47E+Q9'i
432.20Y
Wtd M(:)an
Uncorrectec;'l
Pecay pCi/filtt;Jr
1. 00
1. 00
Total Activity
Gr?.nd Total Activity '
Wtd Mean
Pecay corr
pCi/fi1ter
6.899E+02
S.505E+OO
S.505E+OO
6,954E+02
6.9:;i4E+04
l,047E+03
l,047E+03
Flags: "K" " Keyline not found

"l.ll" .. Manu<;1.1ly eC!ited
6.S99E+02
24-JUL-2013 08:03:l9
2-Sigma
Pi!:lCiiloY Corr
2-sigma Error t)l]rror
1.317E+02
;1.9.09
98.65
5.43:LE+OO
"M" "' Manuai1ly aqcepted

"A" "' Nuelide :;ip;;cifii;:: abn. limit
Page :
Nuclide L.:i.n Act~.vity Report

Sample :i:o : 1307()98-02
Acquisition date
Nticlic;!e Type' J1'I$Sl'ON
N\J,Glide
!>A-13 3
Ene~gy
a1.oo
%Abn
:n.oo*
302.fH
17.80
356.01
60,00
!''inal Mean for
Qncorrec;ited Decay c9:i:i: <a-Sigma

pci/filter pCi/filter %Jllr:i:-or
3.SJ.3E!+02 l 7. S!?
1.89SIE+O:L 3.S;l.2Et02
3.291,E+02 33.57
6,222E+OO 3.29l)l:+02
l6.34
s.860E+OO 4.3'.36E+02
4.~36E+O;>
%Eft:
3 V<\lid Peaki;i"
Nvolide
TH-2:34
Energy
63.29
%APn
3.80*
Final Mean for
AM-241
59.54
35.90*
Final Mean for

Flag: """ " Keyline
uncqn:ected
P1Gi!?,Y
Co:i:-r 2-Sigma
%Bf!
pCi/filter
pCi/fi1ter
2.6481+01
6.899E+02
6.899B+02
1 Valid Pe&ki;>
2.a93B+Ol
l Valid
OK
iirE:rror
19.09
Statu!ll
OK
6. 8Sl9E+02+/- 1. 317E:+02 ( 19. 09%)
5.5051+00
Peak~ ~
Status
OK
OK
3.S13E+02+/- 6.269E+01 ( J.7.85%)
Nuclide Type: NA'l'\JAAL
5.505B+OO
:?4-Y-UL-20J.3 08:03:J.9
S/8.65
OK
5.5Q5EtOO+/- 5.43lB+OO ( 98.65%)
Coml?iried A.ctivi ty-MPA Report

Sample IP : 1307098-02
----
Ide~tified
Nuclide@
Activity
Ni;:lide
(pCi/filter)
BA-133
3.5l.3EJ+02
6.!l99E+02
\3.505E+OO
TK-234
AM-241
l?a!:fe :
4
24-JUL-2013 08:03:19
A.ct e;rroi:
MDA
(pCi/filt!ll;:)
MPA er'l;'or
A.ct/MPA
(5.269E+01
1.317E+02
5.43:1.E+Oo
l.7!Ji2Et0l
1.1'.l5EJ+02
1.097E+tl1
2. S95EHJO
6.094E<1-00
5.393E-Ol
19.934
tl.0130
MPA
()tCi/filt!i!r)
MPA errqr
A.ct/MPA
l..044E+Ol
1.598Et02
3.614E+OO
2,795E+OO
4. 441:)i;lt01
l..1Sl3E+QO
L316E+01
5.140E-02
3.976E-02
3.599))]+00
().5(.12
Non-Identified Nuclides
1\ey-Line
Nur;;Jide
C0-57
CD-109
PA-231
PA-234
NP-237
Activity K.J:,, Act er:lfor

(pCi/filter)Ided
3.561E-01
8,040E+OO
3. 3941',:+QO
2.900E+OO
"7.195l))+QO
fi. 460E+OO
1.l32E>1-02
1.814E+OO
l,536E+QO
3.22.(!E+Ol
0.034
-o.oso
0.939
1.002
-0.162
c:::::--
1J
Dl\AlQOc [G!'MMA,.SCUSR.ARCHIV~]SMP 130709803 ~lll3_QhFir':J:;~~
PEAK V:J.Ei.9 PEA.KEF!l' v2.2
VAX./VM,s l!'el(lk Seareh Repo:i;ot ~;;:;rmrat;ec;J. il4JUir2013 9\1'37: 03. 37
con!iguration
Analysee by
Client ID
Dep9f?ition :Oi:i.te
Sample Pate
Sizimple +o
Sample type
Det.!lctor ni!\me
Elapsed live time:
St;:;i.rt charp:J.e l
Sensitivity
Critioal level..
J?k It
1
2
3
4
5
3
3
3
0
0
Ekgnd
FW~M
Channel
Left
;l7. 81
Sj:l.
41,
1.43
30.7S
34.85
45.77
52.91
lll9S
510
1.8
76
1.42
1.75
28.13
31..1{)
:n
70
l.. :21
55
235
103
144
10$1
117
4.37
61, so
0
0
65.90
8 0. 92
94.30
10
11
1
1
1
0
;J,OS, 78
s
12
13
l4
1;5
16
17
l8
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
'.H
24-JU12013 QQ:OO:OO Ac~uisition Qate : 24.qqL-201~ OB:21:41

130709$03
$aniple Quan.t:i, ty
1..oQOOOE+QO f:i,lter
F;J:;r,,TER
Sample Gee>metry
0
Peteotor Geometry: J!IA!l'It.
GE3
0 90:15:00.00
Elapsed real t:i,me: 0 00:15:05.05 Q.6%
En(J. channe i
4096
25
3.0QOOO
l0.00000
Gaussian
:Wo
Area
Ener;fy
6
7
I4 TQT
as
as
1.29
1. 42
49
1, 57
1.97
1. 59
46
1.59
43
1.60
1.13
2.45
ll.l.. $3
115.54
801
Sl.
l.4
188
47
161.61
23
"10
0
0
1
1
204.58
276.21
302.85
17
49
!>2
27
123
:n
307.53
35
1.2
3l0.86
11
98
1.88
1.62
1.81
1. 81
1. \13
:no. se;
11
;LO
333.73
337.9).
81
355.9l
383.sS
471
208
12
ll.
39
20
1.0
S4
56
25
2
4
2
12
l.2
1
9
0
20
1,93
1.94
18
4
2
3
0
2
2
2
2
2
2
0
0
1
1
0
0
386.76
390,75
4l4.72
417.95
421.06
436.92
458.62
467,54
471.82
510.45
608,08
20
134
86
2.21
2.22
1.41
1.. 85
l.. 82
1.87
2.08
2.09
2.09
1,49
1.10
35.17
46.09
53.23
61. 82
66.22
81.24
94.61
109.1.0
112.14
ll,S.85
27
27
44
50
58
65
7(1,
90
107
107
107
204,89
160
201
276.Sl
303.16
273
299
307.84
299
299
328
328
328
352
161.~3
311.16
33l..17
334.04
338 ':;?2
356.21
3113.66
;>87.06
391. 06
415.02
418.25
421.36
437.22
458.92
~6l
381
381
409
409
409
433
456
464
2.18
46/.84
472.12
510.74
3.40
608.37
605
464
507
J?w
Cts/Sec
~Err
;J,<l S, 63E- 02 lS.5

;1.4 2.1:).E+OQ 2.4
14 5. 67E 01 5,2
6 1. 98E 02 78.2
B 6. 081,1:-02 :34. 9
7 2.6l.E-Ol 10.7
5 9.77E,-02 :n .1
10 8.90E-Ol 4.3
1(1
S.70E-02 3 !l '7
17 1. S4E-02 93.Q 2.91E+OO

17 2.09E01 9.4
17 5.20E02 31.5
5 2.55E04 59.1
7 1. 93E-02 78.4
7 5.49E-02 22.3
15 l.. 37ll!01 l(), 4 7, 09lll01
15
15
14
14
3,84E02
1.23E-02
1.1.7E02
9.00E-02
25.7
74.Q
5<'i.S 2.;)2E+OO
14.2
14 2.211):02 41. 9
9 5.24Jll01 5.2
16 l.49EOl 10.1 9.48E+OO
16 2.31EOl S.5
16 s.96E02 20.0
20 6,25E-02 13.7 ;i.46E+OO
2.73E02 34.7
1.36E02 54.5
20
20
9
6
11
11
9.61E02 12.4
l.33E02 28.9
2,22E-02, 30.2 l. l.4E+OO

8.12lll03 67.4
7 l,.94E-02 29.8
7 l,.Q2lllQ2 41. 0
summary qf N\lclid<'I Activity

sample ID : 1307099-03
Acquisition date
Total nl,lmber of lines. i.n spectrum

Number of unidentified lines
N\lmber of lines tentativel.y identified by NID
Page :
2
24-JUL-2013 08:21:41
34
30
4
11.76%
N\lcl.ide Type : FISSION

Nuc},ide
BA-133
Hlife
l0.50Y
Wtd Mean
Qncorrected
Deocay pCi/filter
1.QQ
'l'otal Ac tivi ty
Wtd Mean
Decay Corr
pCi/filter
3.S39E+04
3.S39E+02
3.83SE+02
3.B:39E+02
Dec;ay corr
2-Sigma
2-Sigma Er:por %-Error Flags
0.693E+02
18.04
Nuclide Type : NATURAL

Nuclide
Hlif e
TH-'.?34
4.47E+09
Ai\1-24:).
432.20Y
Wt;d Me<>.n
Uncorrect'i'd
Decay pCi/filter
1. (j b 7.0Q6E+02
l.OQ
Wtd Meoan
nec;:ay corr
pCi/filter
7.006E+02
6.7B8E+01
6. 788E+O'.).
'J:'ot:al Ac tivi ty
7.68SE+02
7.6BSE+02
Grand Total Activity
1.1!;52E+03
1.1S2E+03
Flags: "K" = Keyline not f9und

"E" " Manuoi.lly edited
DeH;:ay Corr
2Sigmii\
2-sigma Error %Error Flag(?
1.57'7E+02
1.52lE+Ol
22.5l
22,41
"M" " M1'nually accepted

"A" = Nuclide specific abn. limit
Nuclide Line Activity Report

Sample !P : 1307098-03
Acquisition date
Page :
3
24-JUL-2013 06:21:41
Nuclide
Energy
61.00
302.84
356.01
EA-133
\Al:>n
33.00*
17,80
60.00
Pinal Mean for
Nucl.ide
Tf!2;34
Key1ine
pCi/filter
pci/filter
3.B39E+02
3.338E+02
4.025E+02
3.839E+02
3.33BE+02
4.025E+02
3 Valid Peaks
35.90*
Final Mean for
"*''
Uncorrected Decay Corr 2-Sigma
%Error
18.04
29,29
17.13
Valid Peaks
2.893E+Ol
Status
OK
7.006E+02+/- 1.577E+02 ( 22.51%)
6.788E+Ol
1 Valid Peaks
Stilt US
OK
OK
OK
3.839E+02+/ &.925E+Ol ( 1s.04%)
uncorreqtec;'l p,.cay Corr 2-Sigm;;.i.

%Eff
pCi/f ilter pci/filter %Erreir
2.648E+Ol 7.0()6E+02
'7,006E+02 22. 5J..
final Mean for
Flag:
1.899E+01
6.222E+OO
5.860E+OO
Energy
63.29
59.54
%Eff
6.788E+01
22.41
OK
6.788E+Ol+/- 1.521E+01 ( 22.41%)
C:Pmbinetj. A,ctivity-MDA Report

Sqmple XD : 1:307098-0:3
---- Xdentified
Nuclide
E.11.-133
TJ.l-<B4
AM-241
Nuclide
G0-57
CD-10$1
PA-231
PA-234
NP-237
i
4
da:21:41
P~ge
24-JU~-2013
Nucli~e~
MJ;IA
(pCi/filte;t:)
MDA error
Act/MPA
6.925E+Ol
1.S77!J:+02
1.521E+Ol
1.646E+01
1.571E+0:2
1.296:C::+o1
2. !';l 7E+OO
!l.439E+OO
6.3"/lE-01
23.324
4.459
5.239
Act erro:i:
MDA
(pci/fi1ter)
MPA ei:'ror
Act/MDA
5,952E+OD
1, 21 T!JJ+02
1.635E+QO
1.425$+00
3.023E+Ol.
@,904E+OO
1.512E+02
3.;266E+OO
2.75Sll:+OO
4.6Sl5E+Ol
l..131E+OO
l.24eiE+ol
4.646E-02
3.922E-02
3.795E+OO
dl,610
0.815
l.013
0.309
Activity
(pei/filterl
3.83'?E+02
7.006E+02
6.788E+01
Key-r,ine
Activity
l.\.:t..
(pci/filt@rl~ded
J.,354E+OO
-9,2::l6E+Ol
2.664E+QO
2.794E+OO
J.4SQE+01
0.137
C-
Tf1Jt tA---'
Conf igu:na.tion
Anal.y!!!ei> by
Cl:hmt IP
O!\AlOO: [GAMMA. SC!JS\\\.ARCHIVE] SM!? :J,307Q9$Q4 GE3_BAFI:L_:J,935S:L. CN

P~AK V:J.6.9
PEAKEFF V2.2
PZll:l,-SP TOT
Samp),.e ID
130'7096-04
Depo!'litio!'J, Pate
SamJ?l pat;e
Sample type
Detector name
24-JUL-201~
00100:00 Aequieition date :
Fil"./i'ER
3
3
0
30.77
34.91
0
l
46.16
!(32. 23
58.82
Gl.. 8 0
7
8
9
65.54
80. 9:;l
1.2
l
0
l3
14
:J,5
:).08.83
lll.82
115.83
260.25
277,04
302,37
333.64
16
355.99
17
18
376.17
19
20
2l
22
23
24
0
1
1
1
3
3
3
0
414.Sl
25
26
0
0
0
10
11
27
2(3
~83.5:3
386.77
390.80
A:re11-
!3kgnGl
1939
90
Sample Geom@t:ry
El'.\.apsec:!i rl0tl
i:;:nd channel
Gaussian
FWHM Ch.,,nnll!l,
11 2.66E-01
81.2$
77
108
46.4@
52.55
35.~U
63
94
1.. 5 0
1.!51.
l.56
1.7\1
24
1.59
109.14
206
40
37
40
27
39
1.59
1.60
ll2.;J.4
l:l,6.15
;l60.56
277,35
302.GS
333.9;l
3!:;6.30
10
44
9!l
75
492
14
151
215
45
51
57
38
22
19
7
ll
8
9
2.51
1,93
],,25
1.49
1. 70
6.53
], . 87
1.77
1.89
2.29
41!L 15
422.27
436.7],
469.60
510.90
;36
)..3
10
2. :;;o
111
1. 75
14
25
1.. 81
2.59
524.60
60!l.$6
2
1
2.22
Q.96
1.06
!l'it
58
1. 52
;n
Ctiii/See 'llE:io'W
62.12
65.86
87
74
38
63
1.7'7
S4
241
100
80$
Pw
0.5%
50
58
1. 3 SJ
l.59
24
Ll!lJ;t
time' 0 OO::l,$:04.57
40\116
io.00000
2.4 s.s1m+o~
5.3
7 4.321!:-02 43.0
!fi 7. :)..4)!1-02 24. $
11 2.97E-02 39.7 8.56E+OO
?a
31. 09
504
;u
08;38:00
1.ooooo!ll+Oo Ci1te'
Petector Geometry: EAFIJ:,
GllJ3
Elapsed J,ive time: 0 00:15:00.00

Start channel.
.25
3.QQOOO
sensitivity
C'\:itic;;al level
No
!?k It
24-JU~-2013
Sample Quantity
59.14
37(;).47
383.83
387.0.7
39)..],0
4 :J,5. 11 .
4:1,8.45
4:22.!37
437.01
499.90
s:u.. 19
524.89
609.15
27
27
43
sa
108
109
257
272
29$!
329
352
3 7:1,
380
3$0
360
411
411
411
432
464;
507
522
906
14 2.1sE+oo
V<! s.GOEO:l.
8.4
11 1.12E-01 16.3
7 8.95E-01 4.0
18 2.37E-02 37,5 4.59E+OO
19 2,29E-01 !l.6
18 4.16E-02 33.5
7 1.0GE-02100.5
9 4.93E-02 29.2
!! :l,,OSE-01 16.9
S ~l.35E-02
9 s.47E-01
18.~
4.8
9 i.s!lE)-02 e;2,3
19 J..6SE-01 9,~ 4.37E+OO
19 2.39E-01 8.4
19 4.99E-02 23.3
15 5.67E-02 19,8 3.16E+OO
15 4.0lE-02 29.1
l,..49E-02
l,23E-01
8.10E03
2.79E-02
5.87E-03
7 9.56E-03
15
9
8
8
6
56.6
1().:J,
96,:L
22.2
57.S
42.0
S511
summary of Nuclide Activity

Sample ID ; l30709S-04
)).cquisition date
'rota) number of lines in i;;pectrum

Number of lines tentatively identified by NID
Nuclide Type : FISSION
Nuclide
Hlifei
BA-133
1().50Y
Wtd Mean
Uncorrected
Decay pCi/filte:i:
1. 00
Total Activity
Nvc1ii;l.e
TH-234
AM-24:).
Hlife
4.47E+09Y
432.20Y
Total Activity
flage: "K"
"!]:''
=
=
23
Wtd Mean
Decay Cor:i:
pci/f ilter
3.859E+02
3.856E+02
3.859E+02
Wt::d Mei\1.n
UncorrecteC!
Decay pCi/filter
1. 00
1. 00
28
3.135BE+02
Nuclide Type ' NATURAL
Wt<:l. Mean
Decay Corr
pCi/filter
7. l,90E+02
6.951E+OO
'7,J.90E+02
6.$15:1.E+OO
7.259E+02
7.:(.59E+02
1.1121+03
1.1J.2E+03
Keyline not fourid

Me,nually ecUted
J?age ;
2
24-Jl.1Ir2013 08:3S:08
s
2-i;Jigma
Decay Corr
2-Sigma Erroz- ilf)llrro:r
0. 685]1:+02
J.7,75
;a-Sigma
Decay Cor:r
2-Sigma Error %Error Flags
1.J01E+02
5.S38E+OO
J.8,10
'79.68
"M'' = Manally accepted

"A" "' Ncl.ide speci:Eic abp. limit
Nuclicte
l?age ;
~ine Activity Rep9rt

Sample ID : 1307Q98-Q4
Nuclide Type: VISSION

Nuclide
BA-133
N1,1cJ.ide
TH-234
33.00*
302.84
17.!lO
356.01
60.00
AM-241
Energy
63.29
2.647E+02
4.205E+02
%Eff
pCi/fil,t;er
pCi/filter
2.&4SE+Ol
7.190E+02
7.190E+02
1 Valid l?eaks
35.90*
Final Mean for
Uncorrected Decay ('.!orr 2-<Jigma
pCi/fi1ter pCi/filter %Error .Status
1.899E+Ol 3.S58E+02
J,859E+02 17.75
OK
6.222E+OO
5.0601))+00
2.B93E+Ol
2.647E+02
4.205E+02
39.52
l6.71
Uncorrected Pecay Corr 2-Sigma
l Valid l?eakEJ "'
%Error
lS .10
OK
OK
Status
OK
7.190E+02+/- 1.301E+02 ( 18.10%)
&.9511+00
6.95:).E+OO
24-JU~-2013 08:36:08
%Eff
%Alon
Energy
81.00
Final Mean for
Acquieition date
79.6!3
OK
6.9511+00+/- 5.538E+OO ( 79.156%)
combined Activity-MDA Report

sample ID ' 1307098-04
Page :
24-JU4-2013 08:3a:()B
- - - - Identified N\t.:;:lidelil
Activity
(p!'.;i/filter)
BA-133
TH-234
AM-241
Nuc:J.ide
C0-57
CD-109
PA-231
PA-234
NP-237
3.859E+02
7.190E+02
6.951E+OO
Key-r.,ine
Activity K. i;,.
(pci/filter)Ided
-2.215E-01
-S.017E+O;L
3.204E+OO
4.204El+OO
-l..975E+OO
A<;:t
error
6,851El+Ol
1. 3 01E;+o2
S.538E+OO
Act error
6.552/j;+QO
9.710E+01
1. 672EHlO
1,421E+OO
2.959E+O'.l.
MDA
(pCi/filter)
MDA elro;iJ;"
Aot/MPA
1.67lE+Ol
l.251E+02
1,209E+01
2.$6l,E+OO
6.'717E+OO
5. 944E-Ol.
20.629
MDA
MDA error
A<;t/MPA
1.129E+Ol
1.55SE+02
3.384E+OO
2,871E+OO
4.755E+Ol
1.289E+OO
:J,..282E+Ol
4.8121!:-02
4.084E-0;2
3.844E+Oo
-0.020
-0.51$
0.947
'.)..464
-0.042
(pci/filter)
5.749
0.575
VAX/VMS Peak Search !'l,t!iport Generate<J, 24-J!Jt-2013 09:10:215.4'7

Configuration
Analyees by
Client ID
Deposition Date
sample Date
DKf\.lOQ: [QP\MMA.SCUSR.1\.RCHIV!lJ]$MP 130709805

P)i]A!< Vl-6. 9 PEA!<EFF V2 ':l
.
PZ-111--SP DIS
critical lev!j!l
No
Q__
G~3~BAFIL~~~
<14-JUL-2013 00:00:\lo A,oqlJisition date : 24-JUi;..2013 OS:SS:OO

130'7Q9il-05
1.0QOOQE+OO filter
Sample Quantity
Fl;J;.,TE:R
Sample tYP"l
Sample G<!lometry
0
Detec:tqr n\ll,rne
~eteetor Geometry, aAFJ:L
GE'.3
E1a.p!i!ec:l live time: 0 OQ:J,5:00.00
Elap$ed real time: 0 00:15:05.08 Q.6%
Sto/.:t't channe+
25
!'i:nd enannel
40116
3.00(l()Q
sensitivity
Gaussian
10.00000
sample IP
Pk J:t
),"it
Eiill."(l!Y
30.~0
S4.96
124
264
76
5
6
7
:).
:).
:).
115
58
50
805
80.82
83.68
92.16
12
l;l
0
0
14
15
l6
17
18
0
0
3
19
3
0
20
21
22
23
;:?4
0
1
25
307.62
333.66
3;ll;l.
25
355.99
364.29
37&.57
383.76
386.65
39l.24
27
1
l
:;!8
29
414.53
417.87
421,.84
436.89
467.93
30
5:1.1.52
26
69.86
57
81.14
84.QO
92.49
108.l4
ll2.04
llS.98
161.31
67
61.75
65.66
69.54
11
57
1. 54
52.37
107.83
lll.72
ll5.66
161.00
275,91
;303.07
48
62.()7
65.98
1.51
1. 54
s;,L 69
1.59
:l. 60
26
215
J,.3'$
?:!,
35. ;rn
86
10
:n .12
2 06"1
4.39
;11
18
22
18
186
31
37
66
84
21
10::3
25
497
:n.
19
J.05
187
45
40
26
9
ll4
25
14
60
43
61
30
55
58
59
35
44
28
9
16
1.s:a
1.41
1.99
1.59
1. SSl
l.60
1.3S/
1.82
l, :;l9
1.61
1.6$
2.22
26
1.51
1. 85
16
2.20
33
51
12
12
15
1.53
1.46
1.42
17
11
18
6
1.89
1.90
1. 90
1.50
1.62
3.63
276.22
303,36
307. 9:;l
;!33.97
338.55
356.29
364.60
376.87
394,06
396,915
391.54
4l4.83
418.17
422.14
437.19
468.23
511.82
57
76
76
91
107
107
107
158
271
300
306
328
32$
352
362
374
382
31J2
390
411
4ll
411
433
"163
507
16 2.30E+OO 2.3 3.!l9E+OO

ll 4.8SE-Ol 6.Q
8 7.44E-02 3l..3
16
16
16
11
11
6
14
14
14
7
2,93EOl 7.9 3.01E+OO

1.<lSE-01 l4.e
2.28E-02 64.1
!l.95E-01 3.9 9.59E+OO
2.06E-02104.e
~L40:E:-02 60.8
1.991-02 46.6 3.$21+00
2.0?E-01
9.5
3. 44lll-02 4:;l. 2
4.12E-02 39.2
9 7.:29E-O<l 20.6
7 9.29E-02 17.0
5 2.3lE-02 4J.9
2l l.14E-Ol 11,0 1.:;l9E+OO

21 2.81EO<l 37.3
SI S.52EOl
4.9
7 2.31E02 32.4
7 2.14!Z-02 40.1
I l.17E-01 13.2 2.0SE+Ol
8 :;l.OaE-Ol 8.8
6 4.95)1:-02 20.si
15 4.39E-02 22.4 l.l!E+OO
15 2.90E-02 36.3
15 1. 03E-OZ 77. 5
9 1.:;ll5E-01 10.8
10 2.SlE-02 36.8
9 l.57E!-02 41.9
8515
~l\,im11lary of Nuclide Activi ty

Sample IP : 13070~8-0S
Pagiil :
Acquisiti9n date
Total number of lines in spectrum

24-JUL-201J oe:SS:OO
30
26
13.33%

Nuclide
BA,-1,33
Hlife
10.SOY
Wtd Me<an
Qpcqrrected
Decay pCi/filter
1.00
'I'otro).. Activity
3.860E+02
3.860E+02
3.S60E+02
3.860E+tl2

Nuclide
'rH-234
Hlife
4,47E+OSIY
l'ltd Ml?an
tlncorr,ected
Decay pCi/filter
1.00
Total Activity
Wtd Moian
Decay Corr
pCi/f ilter
Wtd Mean
D@cay Corr
pCi/fiJ.ter
7.81ii5E+02
7.S65E+02
7.81ii5B+02
7.S6SE+02
l.172E+03
:J..173E+03
Flq.gs: "K" "' Keyline not found

"E" = Manually edited
Pecay Corr
2-Sigma
2-Sigma Error %Error
0.6BOE+02
17.1>2
;;:,Sigma
Decay Corr
:z,Sigma Er:i;or %li!+ror
1.3S2E+O;l
17.1,9
"M" = Manu<tl.ly accepted

"A" " Nuclide specific abn. limit
lll516
Nuclide Line Activity R,eport

Sample ID : 1307098-0S
P<!.ge :
Acquisition date
24-UL-2013 08:55;00
i.

Nuclide
BA-133
Energy
81.QO
302.84
356.0l
%Abn
33.00*
17.80
60.00
Final Mean for
uncorrected Decay corr 2-Sigmoi,

%EJ;f
pCi/filter pci/filter %Error
l.899E+Ol 3.860E+02
3.860E+02 17.62
6.222E+OO 2,268E+02
2.268E+D2 3!0!. 70
4.246E+02 l.6.79
5,860E+OO 4.246E+02
Valid
Peaks~
3.860E+02+/
Status
OK
OK
OK
6.SD3E+Ol ( 17.62%)
Nuclide Type: NATURAL

Nuclide
TH-231,l
Energy
63.29
%A.bn
3.80*
Final Mean for

Flag:
uncorrectel'.'l Dec;ay corr 2-Sigma

%Eff
pci/f ilter pci/f.ilter %Error
7.865E+02 17.19
2.648E+Ol 7.865E+02
l Valid peaks
status
OK
7.665E+D2+/- 1.352E+02 ( 17.19%)
''*" Keyline
8517
Combined Activity-MDA Report
Page :
Sp,mple ID : 1307098-05
Acquisition (late
24-JUL-2013 08:55:00
---- Identified Nuclides

Nuclide
BA-133
TH-234
Activity
Act er+or
MDA
(pC;L/f;ilter)
MPA er)'."or
Act/M0.1'.
6.803E+01
1,352E+02
1.697E+01
1.135E+Q2
2.59SE+OO
6.094E+OO
22.751
Act error
MDA
(pci/!i1ter)
6.!il31E+OO
1.092E+02
1.550E+00
1.53lE+OO
3.285E+Ol
9.764E+OO
l,.Q33E+Ol
::J..654E+Q2
3.1J,8E+OO
2.767E+OO
4.897E+Ol
l..928E+Ol.
(pCi/:Eilterl
3.860E+02
7,86:SE+02
6.932
Non-Identified N\tc1ides
Nuclide
c0-57
cD-109
PA-231
PA-234
NP-2:37
AM-241
l<ey-Line
Activity K, r,,.
(pci/:filter)Idect
-3.017E+OO
3. 631E.JO::J.
2.486E+OO
2.590E+OO
9.054'.E;+OO
3,810E+Ol
e:i;"rc;p;
Act/MD.i\.
l,.180E+OO
1.3641ll+01
4. 4351!]-0,2
-Q.:;?92
MDA
3.935E-02
3.959E+OO
9.477E-()l.
0,234
0. 797
0.936
0.185
1.!)77
Cont'. i g\,lf:'a t i<m

AnaJ.ysee by
c:J.ierit IP
Oeposit:i.on Pate
sarnple Pat"
sampJ,e :tP
sa,mpJ.e type
Detector name
:
Elapsed live time:
Start chan!'leJ.
sensitivity
critical level
P~lOO:
[GAMMA. SCUS!R.ARCHIVE] SMJ? J,307()9806 GE3 !llAF:J;:r,.

li'EAK V'J.,6,9 !i'EAKEFF V'J..2
~
~
24-yUL-2013 QO:QO:OO Acq\,lisition date : 24-Y'UL-2013 0911:).:-;15

1.QOQOOE+OQ filter
13\)709!l-06
S<>mple Quantity
Fl'.J:,.TER
Sample Geomet:i:-y
0
Detector Geometry: l?Fi.li'IL
GE,3
0 00:15:00.()0
Elapsed real time: Q 00:15:04.69 0.5%
25
End channel
40Sl6
27. till
18
30.83
34.95
61. 28
69.25
78.05
80.96
l:Ll.78
115.74
1!36.36
;l76.58
302.72
1155
3.04
J.07
307.lQ
14
20
288
5
6
0
3
7
8
9
3
2
2
10
11
0
0
12
3
3
13
14
l5
16
17
18
19
20
21
22
333.76
355.95
383.64
1
1
386.87
390.1,:17
4J,6.62
436.91
4168.21
5l{).76
0
0
0
10.00000
Fit
G<1Qssian
3.00000
No
Erie:t:!]Y
CJ.IT
SS. TOT
li'k It;
1
2
3
1935~4.
43
15
475
118
24
17
24
$15
85
115
34
61
44
11
1s
;; 2
52
56
1.43
1.41
;!i,3.J,3
31. l!'i
1,.93
35.27
91
1.23
59
30
1. 27
1.86
1.56
1.75
61,60
66.57
78,37
38
43
34
69
13
17
20
20
25
4
4
l
4
9
10
2
1. 76
3.23
1.77
l.!)6
2.19
1.13
). . 50
1. 76
1.87
1. 88
4.19
1.49
1,09
1,14
27
27
27
58
65
77
81. 28
77
112.:J.O
l:J.6. 0!)
186.67
276.89
303.03
307.41
334.06
356.25
3!l3.S)4
387,17
391.17
416.92
'i\37.21
4G8.51
Sl.1,08
108
108
179
275
2!'19
;2 9 9
330
3 52
3(12
382
382
411
434
465
508
;1.7 2.00111-02 39 . S 8.081)':+00
17 1.2eE+OO
17 3.38E-01
6 l.19EOl
s 4.78l'i)-0;2
12 :J.. 68E-02
12 5.27E-01
:J.3 1.3lE-Ol
13 2.?J.E-02
11 l.93E-02
6 2.66E,Q2
20 J..O;iE-01
20 l.52E-02
6 2.27E-02
9 3.2QE-O:J.
13 9,41E-02
l3 1.28E01
l3 3.75E-02
15 !;1.73E-02
7 4.BSE-0:,J
8 l.17E-02
7 l.fi7E02
3.Q
8.8
17.1
3;1.5
67.3 4.03E+OO
4.9
12.2 6.94E-01
49.7
95.7
31,6
12.1 l.26E+OO
71.4
40.7
6.7
10.l 6.6lE+OO
11.7
26.6
14,7
l9.3
60.6
:;! !l. 8
6513

Siiimple ID : 13070'iHl-06
.
P;;i.ge ;
Ac;;quisition <;late

22
18
18.18%

Nvclide
BA-133
Hlife
10.SOY
Wtd Mean
Uncorrected
Decay pCi/filter
:J.,00
Wtd Mean
Decay Corr
pci/filter
2.27!5E+02
2.275E+02
2.27SE+D2
2.275E+02
Total Activity
...
Decay cor:i:
:JSigma
2-Sigffla l!::i;ror %Error
0.424E+02
l!l.62
.,.~---...--
Nuclide Type ' NATUl'U\.L

NuGlide
AM-241
Hlif e
432.20Y
Wtc;l Mea!'l
Uncorn!cted
Decay pCi/filter
:l.. 00
Total Activity
Wtd Me1'.n
J;lec;:ay corr
pci/f ilter
3. l08E1,Ql
3,l08E+01
3.lOBF)+Ol
3 .108]1)+01
2.586E+02
2.586E+04
Flags, "K" "' Keylipe not found

"E" ~ Manually eoited
24-.;rm;..-2ol.3 09:'.l1:4".i
Decay Corr
:<l-$i9l!la
2-Sigma Error %EJrror
1.084E+Ol
34.86

"A" = Nuclide speci!ic al:m. limj,t
Ni.iclide Line Activity Report

Sample ID ' '.).30709<!06
Acquisition date
Page :
3
24JUL2013 09:1'.J.;45

Nuclide
BA133
Energy
111.00
302.84
356,01
%Abn
33. oo
1,7,80
60.00
Final Mean for
uncorrected Decay corr 2Sigma

%Eff
pC:i/filter pC:i/filter %Error
1.899E+01 2.27SE+02
2.27SE+02 18.62
6.222E+OO 2.568E+02
2.S69E+02 31.77
S.860:E+OO 2.463E+02
2.463E+02 19.07
Valid Peaks =
2.275E+02+/ 4.236E+01
status
OK
OK
OK
18. 62%)
Nuclide Type: NATUF.AL

Nuclide
AM-241
Energy
59,54
%Abn
35.90*
Final Mean for

Flag:
l,Jneorrect\lld Decay Corr 2Sigma

pCi/filter pCi/f ilter %!J:rro:i::
%Eff
2.8'll3E+Ol 3.lOfJE+Ol
3.108E+Ol 34. 98
1 Valid Peaks
3.108E+01+/ 1.084E+Ol ( 34.89%)
''*'' - Keyline
tfl521

Sample IP : 1307098-06
Nuclide
BA-13'.l
A."1-241
Page :
Acquisition date
24-JUL-2013 09:11:45
Activity
(pCi/filter)
Act error
MDA
(pCi/f ilter)
MPA error
Act/MDA
2.275E+02
3.:l.OSE+Ol
4.236E+Ol
l.084E+Ol
1.575E+O:l.
9.674E+OO
2.409E+OO
4.757)J!-01
:].4.441
3.213
Act error
MDA
(pCi/filtel'.')
MDA eJ;'rai;
Act/MD#'
4.971E+OO
9.009E+Ol
l.509E+OO
1.106E+OO
l.047E+02
2.563E+OJ,
7.803E:+OO
1.348E+02.
3.005E+OO
2.122E+OO
l.609E+02
3.984E+Ol
8. 9141):-01
l.lllE+Ol
-0.175
-0.401
0.688
0.601
1.403
-0.237
Nan-Identified Nuclides
Nuclide
C0-57
CD-109
PA-231
PA-234
TH-'.234
NP-237
Key-Line
Activity K.r.,.
(pCi/filter) I\led
-1.365E+OO
-5.401E+Ol
2.067E+OO
1.276E+OO
2.539E+02
-9.462E+OO
<~.274'E-02
3.019E-02
9.716E+OO
3.221E+OO
VA'Y./VM,S
Configu:i:-ation
Analyses l;ly
Clie;nt :ED
Deposition P;i,te
sampli!! Date
Sample ID
sample type
J;Jetector n.me
:
Elapse(;], live timE;l:
Str,i.rt <::hannl\ll
Sen(>itivit;y
c:ritical :Level
Pk It
1
2
3
l,
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
.26
27
28
1
1
0
0
3
3
0
0
1
1
0
0
0
0
2
2
0
l
1
0
0
9
6
0
0
c_
Peak search, 1'<l!po:i:t <ilenerated ;24 JUL 2 t)'.l.3 0$1:47:22.41)

DKA109:
[GJ\MW:.,SCUSR,1\,RC~IVS]SMP
PEAK V19.9
S-5 P:tS
PEAKEFF
V~.2
130709907 GE3
24Jttf,,-;l013 ()0:00:00 i\cqiii sit ion date

1307098-07
sample Quantity
sample oecnnetry :
D(l:lt;ector Geomet:);'y:
Elapse\i real time:
Jj:!'ld charme l-
FIL'l'Ell.
O)l::l
0 OO:'.l-5:00.00
25
3.0()000
\;ausi;i;i,n
~AFIL
11~
~
44 -J'0)'..-;')0:\.3
J.. tl(lOOOE+(lO
193565.CN
011:~2:05
filter
0
EAFII,
0 oo, is: 04. !iJ3

4(l9t)
10. oeo(H)
0. Slli
No
Energy
J,\re!ll.
!'lkgno
30.74
34.!'ll
52 ' "!"!
61.1s
65.54
80.93
92.67
11i.01
116.16
167.32
276.69
302.79
307.82
334.20
338.51
355.91
365.06
383.66
386.90
391.05
414.53
';117. 87
437.17
448.98
462.89
467.06
512.00
521.26
14.58
31-6
81
150
79
584
43
;1.94
25
62
51
4(;)
40
125
64
30
41
31
117
17
25
17
38'7
11
79
161
34
31
25
51
33
!3
9
6
17
27
9
72
33
:n
10
40
19
20
6
17
15
9
12
l2
9
2
0
2
0
0
l1Wf!M C\'lannel
Left
:;n. 06
26
26
49
58
58
l ,4t;l
1,45
3.$2
1.$1
:\.. 52
1. 60
1.135
l.65
l,.93
2.25
1. 54
1. Bo
1. 81
1.30
1. 36
1.57
2.74
2.09
1.38
1.25
1.$9
J.. 90
1.4$
1.24
;J .11
3.11
6.85
2.75
35,13
53.Q9
6;2.l,0
65.$6
81.25
92.99
'.l-1:;! .14
11,6.49
167.63
2"17' 00
3()3.09
308.J.3
334.111
338.82
356.22
36!5.36
383.97
387.ll
391.35
414.83
4lS.l7
437.47
449.28
46~.1.9
4(37.35
512.30
521.56
76
99
107
107
164
275
299
2 SJSJ
332
337
351
362
381
381
390
4l1
411
434
446
462
462
507
519
f'W
Cts/Sei:; %l!:J;"l:'
iis l.62l!l+OO
l6 3.Slli:Ol
9 9.90E02
11 1. IQ6!li 01
11 S.47E-02
10 6.491$-01
9 4.75E-0:;!
l,, 7 2.15E01
l i 2.73E-02
7 3.37E-02
7 3 .45E-02
15 l,30)l:-Ol
1$ J.,93E-02
6 2.76E-02
6 l.86E-02
lO 4.30E-01
6 1.22E-()2
9 8.82E-o2
9 J.,79E-01
5 3.74E02
l3 3.41li!-02
13 2. Sl.E-02
E! 5. 64E.-02
7 1.0l.E-02
ll 6.38E-03
11 1. 85E:-02
11 3.00E-02
7 1.00E-02
Ji':i, t
2.7 6.6;1E+OO
6 , Ii!
<ll. 9
11.2 S.ll?E+OO
11.s
s.s
:; 6. 9
8,4 ;J..34lll+OO
45,9
40.J.
34.7
9.6 2.30lll+OO
38.2
44.7
47.5
5.5
46.4
1$.0 2,57E+OO
8.8
23.0
:;!4. l 6.90E+OO
32.6
16.9
4l. 3
37.2 '.l...37E!+OO
34.6
19.2
313. ~
til523
S\Jmmary of Nl.J.C::l.ide I<,etivity

Sample Il:l i 13()7096-07
JJlage ;
Total nl,J.mber of line9 in spectr\Jm

of l,J.nidlilntified l,,ines
~c<umber
Nuolide Type : FISSION
Nuelide
BA-),33
Hlife
;L0.50
WtCl Mean
Uncorrected
Oecay pCi/filter
1. QO
'J:'otiiil. Aqtivity
Nuolide
Hlife
TH-234 4.47E+D9Y
2. 800E+02
2.BOOE+02
Wti;i Mean
UnoorrectwJ.
peycay pci/fi1ter
;J.,OO
Total Activity
24-yUL-2013 ()9;32:05
2a
24
Wtd Mean
Oecay Cor:r
pCi/fiJ,ter
2.80t1E+02
... ..,_:"",,.. ___ _
2,80t1E+02
Wt.cl. Mean
Dt\',cay corr
pCi/filter
4,464E+02
4.464E+02
4.464E+02
4.464E+02
264E+02
7.264E+02
'7.
Flags: "K" = Key1ine not found

"E" " Ma.rn.\iii,lly e<diteet
"M"
"A"
14.29%
Decay Corr
2-Sigma Erro:c
0.53SE+02
2-Sigma
%E!rror Flags
l~.23
:Oecay Corr
2-sigm<'I.
2-$igmii. Erro+ %Erroi' Flags
l.046E+D2
23.47
= Manually acoepted
= Nuclide specific: ak:m. limit
19524

Sample ID : ).307098-07
Nm:;lide
EA-l.33
Ene:rgy
81.. 00
302.84
:l56. Ql.
%.1\bn
:n. OO*
17.eo
60.QO
Fi.nal Mean t:o:i:-
Nuclide
Snergy
'L'H-234
63.29
"~"
%Ef'.f
1.699E+O:).
6. 222.E+OO
5.860E+OO
3.80*
2.64SBt01
24-JUL-2013
O'nGor:rected Deeay Cc;irr 2-Sigma

pCi/fi:J.ter pCi/filter %Error
2.800E+02
3.180E+02
3.3Q;lE+02
Valid Peak<; "
%Bff
%}\l:m.
Final Mean for

Flag:
Page :
Acqisition date
2,800E+02
3.180Jl]+02
'.).303E+02
Hl,23
28.12
17.56
Stats
OK
OK
OK
2.800E+02+/- 5. :38:?>E+Ol. ( 19.:23%)
unoorrectE1d Pecay Corr 2-Sigma.

pCi/fi1ter pCi/filter %Error
4.464E+02
1 Valid Peaks "
Q9;~2:05
4.464E+02
2;>.47
Stl.t9
OK
4.464E+02+/- 1.048E+02 ( 23.47%)
"' Keyline
ti525
Combined Ac:tivit;y-MPA Report

ID ; 1307098-07
Page :
S~mple
24-JQL-20l3 09:32:05

Nuclide
Activity
(pC:i/f ilterl
Act error
MDA
(pCi/filt!!r)
MDA error
Jl.ct;/MDA
:i. 800li:t02
4.464E+02
5.363E+ol
1. 04!lElt()2
1.6!lOE+Ol
8.774E+01
2. 5t;i9E+OO
4.713E+(l()
16.665
s. 0 !ill!
Act error
MDA
(pCi/fil\:'1,!r)
MDA erro:ic
Act/MDA
5.134,E+OO
1.022E+02
1.552Et00
1.321E+OO
2.S24E+Ol
'7.S17!'+00
8.148li)+QO
1.363Et02
3.063Et00
2.485E+QO
4.376E+Ol
l..532E+01
9.3091l1-01
1.12<lE+Q1
4.356E-02
3.534E-02
3.537E+OO
7.535E-O:L
-0,125
Nuclide
Key-Line
Activity K.L.
(pCi/filterlided
C0-:57
<i. 020E+OO
CD-109
PA-231
PA-234
NP-237
AM-241
-4.030E+Ol
2.013Elt00
2.602E+OO
1.125Et01
2.434E+Ol
-0.296
0.657
1.047
0. 2!')7
l.588
VAX/VMS Peak Search Report Generated 24-JUL-2013 10:03:25.11
Configuration
Analyses by
Client ID
Deposition Date
sample Date
Sample ID
Sample type
Detector name
:
Elapsed live time:
Start channel
Sensitivity
Critical level
pk It
1
2
3
4
5
6
7
8
3
3
0
1
1
1
1
0
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
0
0
0
0
1
1
0
0
0
1
1
0
0
0
0
0
0
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP 130709808

PEAK V16.9 PEAKEFF V2.2
FB PZ-110-SS TOT
24-JUL-2013 00:00:00
1307098-08
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Energy
Area
Bkgnd
30.74
35.09
52.22
61. 75
65.61
80.82
83.68
90.90
111. 20
116.51
160.82
227.40
276.83
302.73
307.55
332.78
356.02
377.63
383.53
386.75
391. 25
414.83
436.82
467.48
512.77
608.62
1859
422
58
248
92
707
18
20
116
66
40
12
50
116
26
44
452
15
96
178
45
26
87
27
19
12
73
86
101
64
62
53
35
86
171
61
55
31
29
20
17
59
22
11
15
26
11
36
2
2
4
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.46
1.66
2.61
1.51
1. 52
1.54
1.41
1.28
1.26
1.88
1.94
5.35
1.46
1.51
1.81
1.47
1.75
1.93
1.87
1.53
2.01
1.55
1. 59
1.94
3.30
2.58
31. 06
35.41
52.54
62.06
65.93
81.14
84. 00
91.22
111.52
116.83
161.14
227.71
277.13
303.04
307.86
333.09
356.33
377.93
383.83
387.05
391.55
415.13
437.12
467.78
513.07
608.92
GE3_BAFIL_1~~
24-JUL-2013 09:48:00
1.00000E+OO filter
0
BAFIL
0 00:15:04.72
4096
10.00000
0.5%
Left
Pw
Cts/Sec %Err
Fit
26
26
49
57
57
76
76
89
108
115
157
224
273
299
299
328
354
374
381
381
390
411
433
464
509
605
16
16
8
16
16
12
12
8
8
6
8
6
9
15
15
10
7
7
9
9
6
8
8
7
9
8
2.07E+OO 2.4
4.69E-01 5.9
6.46E-02 32.6
2.75E-01 8.0
1.02E-01 17.5
7.86E-01 4.2
2. 04E-02101. 6
2.27E-02 81.8
1.29E-01 21.6
7.36E-02 23.2
4.39E-02 36.8
1.37E-02 78.9
5.55E-02 24.1
1.29E-01 10.7
2.84E-02 31.1
4.85E-02 37.3
5.02E-Ol 5.0
1.61E-02 45.4
1.07E-01 13.7
1.98E-Ol 8.7
4.96E-02 21.0
2.84E-02 45.3
9.67E-02 11.1
3.04E-02 20.7
2.14E-02 29.8
1.33E-02 28.9
8.38E+OO
3.74E+OO
1.34E+Ol
2.70E+OO
2.06E+OO

Sample ID : 1307098-08
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.390E+02
_, ________
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.393E+02
Total Activity
=
3.390E+02
Wtd Mean
Decay Corr
pCi/filter
3.391E+02
---------
Decay Corr
2-Sigma
0.606E+02
17.88
3.391E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
15.38%
FISSION
Hlife
10.SOY
Nuclide Type
26
22
4
Page :
2
24-JUL-2013 09:48:00
---------
---------
7.393E+02
7.393E+02
1.078E+03
l.078E+03
Keyline not found

edited
= Manually
Wtd Mean
Decay Corr
pCi/filter
7.393E+02
Decay Corr
2-Sigma
l.288E+02
17.42

~528

Sample ID : 1307098-08
Acquisition date
Page :
3
24-JUL-2013 09:48:00

Nuclide
BA-133
Energy
81. 00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Corr 2-Sigm;i.

%Eff
pCi/filter pCi/f ilter %Error
l.899E+Ol 3.390E+02
3.391E+02 17.88
6.222E+OO 3.142E+02
3.143E+02 29.71
5.860E+OO 3.859E+02
3.860E+02 16.97
3 Valid Peaks
Status
OK
OK
OK
3.391E+02+/- 6.061E+Ol ( 17.88%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
11
Keyline

%EU'
2.648E+Ol 7,393E+02
7.393E+02 17.42
1 Valid Peaks ;
Status
OK
7.393E+02+/- l.288E+02 ( 17.42%)

Sample ID : 1307098-08
-
Acquisition date
Page :
4
24-JUL-2013 09:48:00
- - Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.391E+02
7.393E+02
6.061E+01
1.288E+02
MDA
(pCi/f ilter)
1.713E+01
1.096E+02
MDA error
Act/MDA
2.620E+OO
5.888E+OO
19.790
6.744
MDA error
Act/MPA
1.088E+OO
1.293E+01
4.356E-02
3.820E-02
3.772E+OO
8.804E-01
-0.105
0.148
0.874
1. 293
0.231
1.758
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-9.981E-01
2.328E+01
2.675E+OO
3.473E+OO
1.079E+01
3.148E+Ol
Act error
6.034E+OO
1.051E+02
1.496E+OO
1.402E+OO
3.069E+01
9.088E+OO
MDA
(pCi/filter)
9.526E+OO
1.568E+02
3.063E+OO
2.686E+OO
4.667E+01
1.791E+Ol
rg53~
c
Configul'.'ation
Analyses l;iy
Cli@nt ID
J;lepoi:;ition l;late
Sample :Date;
Sample ID
sample type
Petector name
Elap;;ed :Live t;ime:
Start channel
SE?nsitiv:ity
CJ'.';itioal level
Pk J;t
1
2
3
4
5
6
'7
2
0
2
2
I:lAFIL
Q 00:15;00.28
4096
2S
3.00000
1.922
98
44, 7
10"\
52.tp9
4"1
61.87
65.73
S0.96
83.96
lll.76
116.03
l.85.57
192.21
277.64
302.87
189
103
510
307.06
116
1.40
l..53
1. 8$
1.60
1. 6l
1. so
26
3!'i. 21
52.81
21,i
ia 4. 9711.h cii
46
57
57
12 2.lOE-01
61.98
307.l.6
299
329
20
355.9'7
516
356.08
329
3 Sl.
12
6
6
364 ':;!2
383.65
1.99
:2. 0 0
l.42
1.5)..
333.75
:n~.l.4
36
17
13
27
20
1.97
333.64
15
66
120
1. (;)6
383.75
386.89
205
1.82
43
3$7.00
391.40
380
39:\..29
414.72
32
1
1
0
41!!.07
23
411
411
42J... 72
436.!ll
46!!.11
472.90
510.90
14
95
414. !33
418.l.7
421,..83
437.0l.
17
0
0
6
6
0
l(;),00000
31.00
1.39
0.0%
Fit
17
16
Energy
30. 19
35.09
CN
No
164
J.. ;.;
27
28
petector Geometry:
Elapsed real time:
End channeJ.
Gaussian
31!>
0
2
2
2
21
22
23
24
25
26
GE2
0 00:15:00.00
37
19
20
l.OOOOOE+OO filter
52
11
12
1!3
l?arnple Quilintity
Sall\ple Geometry
14
10
13
14
1307095-09
FIJ;.Tl1JR
1.82
1.83
1. 815
1
1
1
?!~
G~2-~l\.JFIL_19~587.
24-JQL-2013 00:00:00 Acquisition date : 24-JGi-2013 09:35:19
65,84
81. 07
84.07
111.87
116.14
11!5.6B
J..92.32
277.75
302.98
1
2
PKAlO\'I: [GAMMA, SC!JSR. ARClilVE] SM!i> 130709809

PEAK V16,9 PEAKEFF V2.2
PZ-J,10-SS TOT
58
39
7J.2
31
153
33
55
49
34
42
;l2
12
23
:n
22
J.. 5
15
1. 50
1. 55
1.5'1
6
6
2.30
1.88
1.89
1. 89
B
0
1. 37
:ns.2s
364.33
76
76
108
loa
181
181
272
299
362
380
380
468.22
3.10
3.11
473.00
4J.l
434
464
464
12
3.79
51:)..00
505
15 2.14E+OO
2.4
6.1
~.44E+oo
9 5.24E-02 4l.S
'JJ ']
2.96E+OO
12 1.291!!:-0l 14.4
11 '7,\ilE-01 4,0 6.22E+OO
11 3.SOE-02 54.0
ll. l.70E-Ol ll.. 2 3.2!1E+OO
11 3.66E-02 37.5
19 3.SlE-02 32.9 1. 5SE+OO
l9 1.SSE-02 73.l
9 5.74E-02 25.6
13 l..82E-Ol 8.4 .l).56E+OO
13 l.68E-02 64.4
13 7.39E-02 l.5.7 9.'74E-Ol
13 2.26El-02 4 l.. 9
l('J 5. 7311!-01
4.8
7 1.3BJ.1J-02 65.3
l9 l..33E-01 l l. . Ii 6.7SE+OO
lS 2.2BEOl
16 4.731!!:-02 26.5
16 3.59E-02 22.s 1. 6BE+OO
l,6 2.60E-Q2 35.9
16 1.60E-02 43.3
7 1.0SE:-01 11. 5
12 2.48E-02 25.7 9.89E-01
12 l.37E-02 38.0
12 2.56E-02 36.6
s."

Sample IO : 1307098-0~
l!lage :
2
24-JUL-2013 09:35:19
Total number e:t; lines in speotrum

Number ot: lines tent<ative1y identified by N!P
Nuclide Type : F!SS!ON
Nuclide
EA-133
Hlife
10.SOY
Wtd Mi;ian
Uncorrected
Decay pCi/filter
1.00 3.60J.E+02
Total Activity
3.601,E+02
28
24
4
Wtd Mean
Deoy Corr
pCi/filter
3.i;i02E+02
:J.4. 29%
;a,sigma
I;lec;&y Corr
2-Sigma Error %lilrror Flags
0.691E+02
19.l~
3.602E+02
Nuclide Type ; NATURAL

Nuclide
HJ,ife
TH,234 4 .<i\7E+OSlY
Wtd Mean
Uncorr<l!cted
oecay pCi/filter
1.0o
Total Activity
Plass: "K"
"E"
=;
Wtd Mean
Deoay Corr
pC::i(Eilter
6.478E+02
6.478E+02
6.47BB+02
6.478E+02
1.008E+Q3
l,OOBE+03
Keyline not J;ound
= Manually edited
;a,Sigma
Decay Corr
2-Sigina Er:cor i!illlrror Flags
1,.391E+02
21.4~

"A" "' Nuclide specific abn. limit
1'1532
!!'age :
Nuclide Line Activity &eport

Sample lD : 1307098-09
Nuclide
Ty~e:
FISSION
Nuclide
Elnergy
%Al;Jn
BA-J..33
81.0()
302.84
356.0l
33.00*
17.80
Final
Nuclide
TH-234
Flag:
ME!<!l.rl
'lill~f f
f.iO. 00
fo:r
E:nergy
%Abn
63.29
J.80*
24-JUL-2013 Q9:3S:19
l.799E+Ol
7.560E+OO
7.170E+QO
UncorrecteQ. Decay Corr 2-Sigma

pCi/filter pCi/f ilter %E:rror
3.601E+02
3. 6S3Eh02
3. 59!1!!1+02
Vali\i Peaks "'
%Bff
2.~05E+Ol
3.602E,.02
3.653E+02
3. 599E.JO::l
l!il.19
31L 25
17.93
Statu:;;
OK
OK
OK
3,602E+t)2+/- G.91:3E:+Ol ( J,9.19%)
l.Jncorrectec;I Decay Corr 2-Sigma

pCi/filter pci/filter %-E:rror
6.47SB+02
6.479E,.02
2l..4S
"*" "' Keyline
lil533
J?age :
Combined Activity-MOA Report

Sample ID : 1307098-09
24-JOL-2013 09:35:19
---- !dentifitild Nucli<:'les ---

Nuclide
Activity
(pci/:Eilterl
Act erl'.'or
MDA
(pCi/filter)
MDA error
Act/MPA
3.602E+02
6.478E+02
6.913E+Ol
l.. 3 91E+02
:L.731E+O:l.
1.379E+02
2 ..\l<l\7E+OO
1.1'.')9E+Ol
20.soa
Act error
MDA
(pCi/tilter)
MDA error
Act/M!JA
Key-Line
Activity
Nuclide
C:::0-57
CP-109
J?A-231
PA-234
NP-23'7
AM-441
!C.L.
(pCi/filterl!de~
-9.488E-02
-4. 91Hlll)+01
2.895E+01
2.889!!!+00
-2.594E+Ol
2,045Et01
6. 01.4E+OO
1.107E+02
4.5'73E-c00
1.65SE+\JO
3.199E+Ol
1. oo:rn+o1
9.715!l:+OO
l.706Et02
S.930E+OO
'.l.020E+OO
4.61:l9E+Ol
1.S5$E+Ol
1.4!J;'.<Et00
1.959E+Ol
1.'701E-Ol
6.229!1:-02
s.294E+OO
1. 43$E+OO
L 698
-0.010
-0.293
3. 2441
0, 956
-0.$53
1.101
c____
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
sample ID
sample type
Detector name
:
Elapsed live time:
start channel
Sensitivity
critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
2
2
0
0
0
0
3
3
0
0
0
2
2
0
0
1
1
0
1
1
0
1
1
0
0
0
D
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130709810
PZ-llO-SS DIS
24-JUL-2013 00:00:00
1307098-10
FILTER
GE2
0 00:15:00.00
25
3.00000
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
GE2_BAFIL~~
24-JUL-2013 09:51:05
1.00000E+OO filter
0
BAFIL
0 00:15:00.29
4096
10.00000
0.0%
No
Energy
Area
Bkgnd
30.89
35.15
52.76
61.73
65.84
80.94
111.77
116.20
160.82
184.91
276.64
302.90
306.74
324.82
333.50
351.88
355.93
366.54
383.72
386.84
391.21
414.72
417.84
437.04
468.65
510.61
580.40
1989
440
48
196
66
774
213
48
20
31
43
154
21
99
61
10
506
19
95
163
43
42
23
89
17
28
8
SJ f)
112
120
101
82
41
37
82
84
38
16
22
15
33
6
9
16
20
26
20
9
13
16
12
6
0
FWHM Channel
1.39
1. 53
1. 5![1
1.71
1.31
1. 36
1. 89
1.88
1.42
3.11
1. 57
1.56
1. 97
2.10
1.40
1. 83
1.58
1. 81
1.86
1. 53
1.59
1. 88
1. 89
1.36
1.25
2.58
1.33
31.00
35,26
52.87
61.$5
65.95
Bl.OS
111. 89
116.32
160.93
185.02
276.75
303.01
306.85
324.93
333,61
351. 99
356.03
366.65
383,83
386.95
391.32
414.83
417.95
437.14
468.75
510.71
580.50
Left
26
26
50
59
65
77
107
107
156
182
273
298
298
322
329
350
350
362
381
381
390
411
4ll
433
465
506
578
PW
Cts/Sec %Err
15 2.21E+OO 2.3
15 4.SBE-tll 6.1
8 5.34E-02 40.6
6 2.lSE-01 11.3
5 7.32E-D2 26.2
7 8.60E-01 4.l
20 2.37E-01 8.4
20 5.33E-02 29.5
7 2.20E-02 79.1
8 3.47E-02 53.5
8 4.76E-02 29.6
18 l.71E-01 8.9
18 2.30E-02 48.8
6 8.89E-03 86.4
8 6.77E-02 20.9
12 1.l7E-02 39.2
12 5.63E-01 4.5
9 2.12E-02 43.9
9 1.tlSE-01 14.2
9 1.SlE-01 9.2
6 4.73E-02 23.6
10 4.64E-02 19.4
10 2.52E-02 38,4
8 9.90E-02 13,l
8 l.85E-02 43.6
11 3.06E-02 25.2
6 8.89E-03 35.4
Fit
6,23E+OO
2.56E+OO
1. 09E+OO
1. 66E+OO
7.22E+OO
2.17E+OO

Sample ID : 1307098-10
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pci/filter
1. 00
3.916E+02
Total Activity
:
---------
3.916E+02
--,~-----

=
=
Wtd Mean
Decay Corr
pCi/filter
3.916E+02
---------
Decay Corr
2-Sigma
0.756E+02
19.30
3.916E+02
NATURAL
Wtd Mean
Uncorrected
Nuclide
Hlife
Decay pCi/f ilter
TH-234 4,47E+09Y
6.726E+02
1. 00
...
Total Activity
6.726E+02
Flags: "K"
"E"
14.81%
FISSION
Hlife
l0.50Y
Nuclide Type
27
23
4
Page :
2
24-JUL-2013 09:51:05
l.064E+03
Keyline not found

Manually edited
Wtd Mean
Decay Corr
pCi/filter
6.726E+02
---------
Decay Corr
2-Sigma
2-sigma Error %Error Flags
24.44
l.644E+02
6.726E+02
l.064E+03
"P.." = Nuclide specific abn. limit

Sample ID : 1307098-10
Acquisition date
Page :
3
24-JUL-2013 09:51:05

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.60
60.00
Final Mean for

%Eff
pCi/filter pCi/filter %Error
l.799E+Ol 3.916E+02
3.916E+02 19.30
7.560E+OO 3.427E+02
3.428E+02 34.83
7.170E+OO 3.535E+02
3.535E+02 17.65
3 Valid peaks
Status
OK
OK
OK
3.916E+02+/- 7.561E+Ol ( 19.30%)

Nuclide
TH-234
Energy
63.29
'l;Abn
3.80*
Final Mean for

Flag:
11
11

%Eff
2.305E+Ol 6.726E+02
6.726E+02 44.44
1 Valid Peaks =
Status
OK
6.726E+02+/- 1.644E+02 ( 24.44%)
Keyline
~537

Sample ID : 1307098-10
Acquisj.tion date
Page :
4
24-JOL-2013 09:51:05
- - - - Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.916E+02
6.726E+02
7.561E+01
1.644E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.899E+Ol
1.619E+02
3.234E+OO
1.338E+01
20.621
4.155
MDA
(pCi/filter)
MDA error
Act/MDA
1.449E+OO
;2.081E+Ol
1.700E-01
6.639E-02
5.842E+OO
1.536E+OO
0. 479
-0.085
3.274
0.989
0.002
1.406
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-tine
Activity K.L.
(pCi/filter)Ided
4.521E+OO
-1.537E+Ol
2.923E+Ol
3.184E+OO
l,287E-Ol
2.791E+Ol
4.897E+OO
1.045E+02
4.567E+OO
1.775E+OO
3.172E+Ol
1.133E+Ol
9.433E+OO
1.812E+02
8.926E+OO
3.219E+OO
5.174E+Ol
1.985E+Ol
UJ538
a__
"?f'L....,__

Configuration
Analyses Joy
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
3
3
3
3
3
3
1
1
0
0
0
0
0
4
4
3
3
0
0
1
1
1
5
5
5
0
1
1
0
0
0
0
PKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130709811 GE2 BAFIL 193591.CN

I-4 TOT
24-JUL-2013 00:00:00
1307098-11
FILTER
GE2
0 00:15:00.00
25
3.00000
No
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
Energy
Area
Bkgnd
FWHM Channel
Left
Pw
28.16
30.91
35.05
52.81
61. 85
65.69
80.98
84.89
92.72
111.68
116.32
164.45
277.19
302.84
307.39
333.73
338.44
355.93
368.98
383.77
386.90
390.90
414.57
418.69
421.47
437.03
467.86
472.07
511.01
742.24
881.66
1173.74
42
1802
462
47
183
89
810
14
30
155
44
43
50
161
24
76
16
540
15
99
188
37
39
13
12
89
22
13
36
7
4
6
157
102
87
68
72
76
58
65
67
101
86
101
48
15
16
16
10
26
7
10
13
15
8
12
14
7
1
2
6
2
3
2
1. 66
28.28
1.40
31.03
35.17
1.68
52.92
1. 74
1.76
61.96
1. 77
65.80
1.41
81.09
85.01
1. 50
2.07
92.83
1.28 111.80
1. 70 116.43
7.41 164.57
1.73 277.30
1. 60 302.95
2.38 307.50
1.85 333.84
2.20 338.55
1.38 356.04
2.10 369.09
1. 86 383.87
1. 86 387.00
1.86 3 91. 01
2.76 414.68
2.51 418.80
2.77 421.58
1.51 437.14
1.93 467.96
1.93 472.18
2.08 511.11
1.66 742.34
1.39 881.76
2.81 1173.82
26
26
26
50
50
50
76
76
90
108
115
156
272
299
299
329
329
352
367
380
380
380
411
411
411
432
465
465
505
738
878
1170
14
14
14
20
20
20
12
12
7
7
6
13
10
18
18
14
14
8
6
15
15
15
14
14
14
10
14
14
12
7
6
7
24-JUL-2013 10:11:02
1.00000E+OO filter
0
BAFIL
0 00:15:00.29
4096
10.00000
Cts/Sec %Err
4.66E-02
2.00E+OO
5.13E-Ol
5.19E-02
2.04E-01
9.94E-02
9.00E-01
1.58E-02
3.28E-02
1. 72E-Ol
4.86E-02
4.78E-02
5.56E-02
1.79E-Ol
2.71E-02
8.49E-02
1.74E-02
6.00E-01
1.66E-02
1.09E-Ol
2.08E-Ol
4.06E-02
4.36E-02
1.42E-02
1.36E-02
9.83E-02
2.41E-02
1.45E-02
4.00E-02
7.22E-03
4.60E-03
7.0lE-03
0. 0%
Fit
58.5 1.0SE+Ol
2.5
5.8
31. 2 l.37E+OO
10.3
19.3
3.8 3.03E+OO
88.0
49.4
13.4
37.2
51.1
29.4
8.6 1. 20E+OO
43.2
14.1 1.47E+OO
54.1
4.6
38.6
13.3 2.57E+OO
8.9
27.4
22.5 1.28E+OO
71.2
63.3
12.l
22.2 8.39E-Ol
37.9
21.5
51.2
81.9
52.7

Sample ID : 1307098-11
Acquisition date

Nuclide Type
32
27
5
Page :
2
24-JUL-2013 10:11:02
15.63%
FISSION
Nuclide
Hlife
BA-133
10.50Y
NP-237 2.14E+06Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 4.100E+02
1. 00
2.010E+Ol
__ ,... ______
Total Activity
4.301E+02
Wtd Mean
Decay Corr
pCi/filter
4.100E+02
2.0lOE+Ol
---------
Decay Corr
2-Sigma
19.03
0.780E+02
3.547E+Ol
176.50
4.301E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
6.283E+02
1. 00
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
6.2B3E+02
---------
6.283E+02
6.283E+02
l.058E+03
l.058E+03
Flags: "K" = Keyline not found

Decay Corr
2-Sigma
1.423E+02
22.64


Sample ID : 1307098-11
Acquisition date
Page :
3
24-JUL-2013 10:11:02

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks
12.60*
Final Mean for

%Eff
1.799E+Ol 4.100E+02
4.100E+02 19.03
7.560E+OO 3.599E+02
3.600E+02 34.50
3.770E+02 17.73
7,170E+OO 3.770E+02
l.691E+Ol
4.100E+02+/- 7.804E+Ol ( 19.03%)
2.0lOE+Ol
1 Valid Peaks;
Status
OK
OK
OK
2.0lOE+Ol 176.50
OK
2.0lOE+Ol+/- 3.547E+Ol (176.50%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
"*" ;

%Eff
2.305E+Ol 6.283E+02
6.283E+02 22.64
1 Valid Peaks ;
Status
OK
6.283E+02+/- l.423E+02 ( 22.64%)
Keyline
m.541

Sample ID : 1307098-11
-
Acquisition date
Page :
4
24-JUL-2013 10:11:02
- - Identified Nuc1ides
Nuclide
BA-133
TH-234
NP-237
Activity
(pCi/filter)
4.100E+02
6.283E+02
2.0lOE+Ol
Act error
MDA
(pCi/fi1ter)
MDA error
Act/MDA
7.804E+Ol
1.423E+02
3.547E+Ol
1.899E+Ol
1.424E+02
5.170E+Ol
3.234E+OO
1.177E+01
5.837E+OO
21. 590
4.412
0.389
Act error
MDA
(pCi/fi1ter)
MDA error
Act/MDA
5.584E+OO
1.232E+02
4.502E+OO
1.834E+OO
9.698E+OO
9.323E+OO
1.670E+02
8.817E+OO
3.251E+OO
1.882E+Ol
1.432E+OO
1.917E+01
1.679E-01
6.705E-02
1.456E+OO
0.122
-0.265
3.254
0.809
1.065
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/fi1ter)lded
1.137E+OO
-4.421E+Ol
2.869E+Ol
2.631E+OO
2.003E+Ol
:~~~:r::::nsearchD~:::~
[:~~~:::s:~~~~:::~:M:o~::~::~::
GE2_BA~(_=t9~~"'?.cN.
by
Vl6.9
V2.2
Analyses
Client ID .
Deposition Date
Sample Pate
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
1
1
0
0
0
0
0
0
0
0
2
2
2
1
1
2
2
0
0
1
1
33
2
2
2
0
0
0
0
PEAK
I-4 DIS
PEAKEFF
24-JOL-2013 00:00:00
130709$-12
FILTER
GE2
0 00:15:00.00
25
3.00000
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
24-JUL-2013 10;26:42
1.00000E+OO filter
0
BAFIL
0 00:15:00.29
4()96
10.00000
0.0%
No
Energy
Area
Bkgnd
30.91
35.24
52.37
61.75
65.84
80.98
92.89
111.45
116.30
139.83
160.74
185.. 59
276 .38
302.78
307.55
311.20
333.73
337.90
352.06
355.94
364.86
376.40
383.72
386.93
390.95
414.74
417.69
421. 71
436.93
480.32
504.35
511.29
933.69
1946
443
53
186
89
700
31
176
43
20
26
39
61
141
22
10
101
27
12
481
17
18
109
182
44
21
21
96
74
95
60
67
136
95
105
74
118
47
53
40
17
19
18
11
12
11
76
9
0
0
0
0
11
36
9
0
3
3
10
9
9
9
5
FWHM Channel
1.42
1.64
2.99
1.46
1.47
1.29
2.45
1.25
2.05
4.43
2.02
3.99
1.89
1.82
1. 97
1.97
1.81
1.82
1.83
1.59
1.41
2.14
1.86
1.86
1.86
2.07
2.08
2.08
1.40
1. 47
2.07
1.56
1.33
31. 02
35.35
52.48
61.87
65.96
81.09
93.00
111.57
116.41
139.95
160.86
185.70
276.49
302.89
307.66
311.30
333.84
338.01
352.17
356.05
364.96
376.50
383.83
387.04
391.05
414.84
417.80
421.82
437.04
480.43
504.45
511. 3 9
933.78
Left
27
27
49
58
58
77
89
108
115
138
158
182
271
299
299
299
330
330
351
351
362
372
380
380
380
411
411
411
432
478
502
508
930
PW
Cts/See %Err
17 2.16E+OO 2.4
17 4.92E-01 5.11
8 5.93E-02 34.4
12 2.07E-01 9.6
12 9.85E-02 16.3
8 7.78E-01 4.8
8 3.44E-02 57.6
7 1.95E-01 12.3
6 4.78E-02 36.3
12 2.19E-02112.4
6 2.88E-02 46.4
7 4.37E-02 34.8
10 6.BOE-02 23.2
18 1.56E-01 9.4
18 2.43E-02 39.5
18 1.12E-02 81.9
12 1.13E-01 10.5
12 2.99E-02 28.1
11 1.35E-02 2.9
11 5.35E-01 4.6
6 1.92E-02 28.6
8 2.0lE-02 38.3
18 1.21E-01 11.8
18 2.02E-01 9.0
18 4.84E-02 22.0
15 2.29E-02 36.3
15 2.29E-02 37.6
15 8.15E-03 80.9
9 8.44E-02 13.5
5 7.78E-03 37.8
6 l.22E-02 30.2
8 4.00E-02 16.7
8 l.OOE-02 33.3
Fit
6.03E+OO
4.21E+OO
1.05E+OO
6.13E+OO
1.35E+OO
3.06E+OO
1.76E+OO

Sample ID : 1307098-12
Acquisition date

Nuclide Type
Nuclide
BA-133
33
29
4
Page :
2
24-JUL-2013 10:26:42
12.12%
FISSION
Hlife
10.SOY
Wtd Mean
Uncorrected
Decay pCi/f ilter
1. 00
3.542E+02
Total Activity
---------
3.542E+02
Wtd Mean
Decay Corr
pCi/filter
3.542E+02
---------
Decay Corr
2-Sigma
0.705E+02
19.91
3.542E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/f ilter
6.392E+02
1. 00
Total Activity
---------
Wtd Mean
Decay Corr
pCi/filter
6.392E+02
---------
6.392E+02
6.392E+02
9.934E+02
9.935E+02

Decay Corr
2-Sigma
1.363E+02
21. 33

"A" "' Nuclide specific abn. limit

Sample ID : 1307098-12
Acquisition date
Page :
3
24-JUL-2013 10:26:42

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Jl...bn
33.00*
17.80
60.00
Final Mean for

%Eff
l.799E+Ol 3.542E+02
3.542E+02 19.91
3.142E+02 35.35
7.560E+OO 3.142E+02
7.170E+OO 3.360E+02
3.360E+02 17.72
3 Valid Peaks =
Status
OK
OK
OK
3.542E+02+/- 7.052E+Dl ( 19. 91%)

Nuclide
TH-234
Energy
6~.29
%Abn
3.80*
Final Mean for

Flag:
"*" = Keyline

%Eff
pCi/f ilter pci/filter %Error
2.305E;+Ol 6.392E+02
6.392E+02 21. 33
1 Valid Peaks =
Status
OK
6.392E+02+/- 1.363E+02 ( 21.33%)

Sample ID : 1307098-12
Page :
Acquisition d;i.te
24-JUL-2013 10:26:42

Nuclide
BA-133
TH-234
Activity
(pCi I filter)
3.542E+02
6.392E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
7.052E+Ol
l.363E+02
l.817E+Ol
l.528E+02
3.094E+OO
l.262E+Ol
19.493
4.185
MDA error
Act/MDA
l.351E+OO
2.043E+Ol
l.676E-Ol
6.736E-02
5.869E+OO
l.457E+OO
-0.171
-0.342
3.060
1.288
-0.206
0.865
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-l.501E+OO
-6.089E+Ol
2.692E+Ol
4.207E+OO
-l.070E+Ol
l.629E+Ol
Act error
5.610E+OO
l.336E+02
4.519E+OO
l.655E+OO
3.790E+Ol
l.051E+Ol
MDA
(pCi/filter)
8.799E+OO
l.779E+02
8.SOOE+OO
3.266E+OO
5.198E+Ol
l.883E+Ol
<2-:
VAX/VMS Peak Search Report Generated 24-JUL-2013 10:2711.98

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARC!-lIVE) SMP 130709813 GE3_BAFIL_193592.CN

PZ-100-SS TOT
24-JUL-2013 00:00:00
1307098-13
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
30.75
35.08
52.60
61.67
65.71
80.82
83.68
93. 21
111. 31
116.62
160.95
277.08
302.81
306.35
334.46
355.91
366.66
376.83
383.44
386.74
391.46
414.87
420.53
436.83
468.75
509.95
512.45
2044
500
76
278
95
756
23
45
179
47
28
45
123
12
102
505
32
17
85
191
44
48
12
116
34
15
93
64
67
67
87
69
43
64
140
53
71
38
28
35
22
42
22
10
13
15
10
10
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
4
0
3
3
1
1
0
0
0
0
0
2
2
0
0
0
0
8
8
0
1
1
0
0
2
?(l.J{{()
10
7
6
Acquisition date :
Sa,mple Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
PW
31.07
35.40
52.92
61.99
66.03
81.14
84.00
93.53
111.63
116.93
J.61. 26
277.39
303.12
306.66
334.76
356.22
366.96
377.13
383.75
387.04
391.76
415.17
420.83
437.13
469.05
510.25
512.75
26
26
50
58
58
76
76
91
108
115
159
273
297
297
330
352
362
373
381
381
390
411
411
432
464
507
507
13
13
6
13
13
16
16
7
8
6
7
9
14
14
11
8
11
8
9
9
6
14
14
9
10
9
9
1.52
1. 62
1.90
1.46
1.67
1.54
1.41
1. 35
1.34
1. 81
1.55
1.83
1. 59
1.99
1.95
1.45
6.18
2.38
2.os
1.41
1.47
1. 89
1.90
1.49
1. 80
2.16
2.16
24-JUL-2013 10:11:51
l.OOOOOE+OO filter
0
BAFIL
0 00:15:04.35
4096
10.00000
Cts/Sec %Err
2.27E+OO
5.56E-Ol
8.49E-02
3.09E-Ol
l.05E-Ol
8.40E-Ol
2.55E-02
4.98E-02
l.99E-Ol
5.21E-02
3.14E-02
5.0lE-02
l.37E-Ol
l.34E-02
1.13E-Ol
5,61E-Ol
3.54E-02
1. 87E-02
9.45E-02
2.12E-Ol
4.86E-02
5.36E-02
1.38E-02
1.29E-01
3.SlE-02
l.65E-02
1.04E-02
0.5%
Fit
2.3 2.2SE+Ol
5.2
20.4
7.3
17.9
4.0
84.7
33.l
13.6
29.4
52.4
28.9
10.9
92.9
13.3
5.0
34.6
40.S
15.7
7.9
20.3
18.2
54.2
10.4
22.6
36.0
62.4
l.33E+OO
9.69E+OO
1.41E+OO
1.24E+01
3.63E+OO
4.50E-01
lil5d7

Sample ID : 1307098-13
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.622E+02
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/f ilter
1. 00
8.305E+02
Total Activity
=
---------
3.622E+02
Wtd Mean
Decay Corr
pCi/f ilter
3.622E+02
Decay Corr
2-Sigma
0.643E+02
17.76
-~-------
3.622E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
14.81%
FISSION
Hlife
10.SOY
Nuclide Type
27
23
4
Page :
2
24-JUL-2013 10:11:51
---------
Wtd Mean
Decay Corr
pCi/filter
8.305E+02
---~-----
8.305E+02
8.305E+02
1.193E+03
1.193E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
1.330E+02
16.02


Sample ID : 1307098-13
Acquisition date
Page :
3
24-JUL-2013 10:11:51

Nuclide
BA-133
Energy
81. 00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
Uncorrec;ted Decay Corr 2-Sigma

%Eff
l.899E+01 3.622E+02
3.622E+02 17.76
6.222E+OO 3.337E+02
3.338E+02 29.96
5.860E+OO 4.311E+02
4.312E+02 16.89
3 Valid Peaks
Status
OK
OK
OK
3.622E+02+/- 6.433E+Ol ( 17.76%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
"*"
Keyline

%Eff
2.648E+01 8.305E+02
8.305E+02 16.02
1 Valid Peaks
Status
OK
8.305E+02+/- 1.330E+02 ( 16.02%)

Sample ID : 1307098-13
Acquisition date
4
Page :
24-JUL-2013 10:11:51
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.622E+02
8.305E+02
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.433E+Ol
1.330E+02
1.900E+Ol
l.190E+02
2.906E+OO
6.390E+OO
19.060
6.981
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
1.129E+OO
1.325E+Ol
4.222E-02
4.139E-02
4.070E+OO
9.624E-01
0.000
-0.532
0.785
1. 524
-0.251
1. 947
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-l.338E-03
-8.544E+Ol
2.331E+OO
4.434E+OO
-l.262E+Ol
3.810E+Ol
6.130E+OO
l.101E+02
1.462E+OO
1.502E+OO
3.271E+Ol
9.641E+OO
9.884E+OO
1.607E+02
2.968E+OO
2.910E+OO
5.035E+Ol
1.957E+Ol
-:..r1e, If( ~

Configuration
Analyse01 by
Client IP
Deposition Date
Sample Date
Sample ID
sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
3
3
9
9
9
0
0
1
1
0
0
0
0
0
0
0
0
0
5
5
0
0
0
1
1
0
DKAlOO: [GAMMA.SCUSR.ARCHIVE)SMP 130709814 GE3 BAFIL 193595.CN

PZ-100-SS DIS
24-JUL-2013 00:00:00
1307098-14
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Energy
Area
Bkgnd
30.78
35.03
52.16
61.85
65.71
80.99
92.93
111.75
116.54
159.96
239.63
266.43
276.45
302.87
333.74
338.31
355.88
364.71
383.58
386.70
3 91. 23
415.22
436.85
467.74
471. 88
510.86
1950
539
72
252
160
803
37
197
30
49
20
9
54
99
63
18
485
19
75
149
43
40
86
30
10
19
69
55
92
68
78
96
84
50
52
63
44
26
25
65
36
20
20
16
32
51
21
31
9
5
4
6
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
Pw
31.10
35.35
52.48
62.17
66.03
81. 31
93.24
112.07
116.85
160.27
239.94
266.74
276.76
303.18
334.04
338.61
356.19
365.01
383.88
387.00
391.53
415.53
437.15
468.04
472.18
511.16
26
26
49
49
49
77
90
108
108
156
236
264
273
299
330
337
351
362
381
381
390
412
432
463
463
507
16
16
24
24
24
9
8
13
13
9
9
8
8
7
7
1.48
1.59
3.18
1.89
2.26
1. 77
1. 81
1.59
1.60
1.58
1.50
1.82
1.82
1.25
1.18
1.90
1.50
1.99
2.06
1.49
1.26
1.57
1.64
1. 93
1.94
2.14
10
7
9
9
6
9
8
14
14
8
24-JUL-2013 10:27:45
1.00000E+OO filter
0
BAFIL
0 00:15:04.58 0.5%
4096
10.00000
Cts/Sec %Err
2.17E+OO
5.99E-01
8.0lE-02
2.SOE-01
1.78E-01
8.93E-01
4.llE-02
2.18E-01
3.32E-02
5.49E-02
2.19E-02
l.03E-02
5.99E-02
1.lOE-01
6.96E-02
2.00E-02
5.39E-Ol
2.07E-02
8.37E-02
l.66E-Ol
4.79E-02
4.49E-02
9.57E-02
3.33E-02
1.llE-02
2.13E-02
2.3
4.9
25.8
8.3
12.7
4.2
45.9
9.3
43.l
32.2
65.2
98.7
21.2
15.1
19.2
44.1
4.9
42.6
18.2
10.1
23.9
28.9
12.2
20.2
50.6
31.8
Fit
7.35E+OO
S.27E+OO
3.41E+OO
l.15E+Ol
1.0lE+OO

Sample ID : 1307098-14
Acquisition date

Nuclide Type
Nuclide
BA-133
26
22
4
Page :
2
24-JUL-2013 10:27:45
15.38%
FISSION
Hlife
10.SOY
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.851E+02
Total Activity
---------
3.851E+02
Wtd Mean
Decay Corr
pCi/filter
3.851E+02
---------
2-Sigma
Decay Corr
0.688E+02
17.86
3.851E+02

Nuclic;le
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
7.509E+02
1. 00
Total Activity
Flags: "K"
"E"
---------
---------
7.509E+02
7.509E+02
l.136E+03
l.136E+03
Keyline not found

edited
= Manually
Wtd Mean
Decay Corr
pCi/filter
7.509E+02
"M"
"A"
Decay Corr
2-Sigma
l.346E+02
17.92
Manually accepted
specific abn. limit
= Nuclide
~552

Sample ID : 1307098-14
Acquisition date
Page :
3
24-JUL-2013 10:27:45

Nuclide
BA-133
Energy
81. 00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
l.899E+Ol 3.851E+02
3.B51E+02 17.86
6.222E+OO 2.687E+02
2.687E+02 36.63
5.860E+OO 4.141E+02
4.142E+02 16.75
3 Valid Peaks =
Status
OK
OK
OK
3.851E+02+/- 6.879E+Ol ( 17.86%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

%Eff
pCi/f ilter pCi/filter %Error
2.648E+Ol 7.509E+02
7.509E+02 17.92
1 Valid Peaks =
Status
OK
7.509E+02+/- 1.346E+02 ( 17.92%)
Flag: "*" = Keyline
lil553

: 1307098-14
Sample ID
Acquisition date
Page :
4
24-JUL-;ltl:t.3 10:27:45
- - - - Identified NUclides
Nuclide
BA-133
TH-234
Activity
(pci/filter)
3.851E+02
7.509E+02
Act error
6.879E+Ol
l.346E+02
MDA
(pCi/filter)
1.825E+Ol
1.153E+02
MDA error
Act/MDA
2.791E+OO
6.195E+OO
21.103
6.511
MDA error
Act/MDA
9.918E-01
1.469E+Ol
4.242E-02
4.030E-02
4.045E+OO
8.745E-Ol
-0.468
0.438
0.643
1.563
0.363
1.633
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-4.060E+OO
7.804E+01
1.919E+OO
4.428E+OO
1.815E+Ol
2.905E+Ol
Act error
5.961E+OO
1.128E+02
1.507E+OO
1.443E+OO
3.213E+Ol
8.790E+OO
MDA
(pci/filter)
8.682E+OO
1.781E+02
2.983E+OO
2.834E+OO
5.004E+Ol
1.779E+Ol
554
c:__

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample typ<e
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
24-JUL-2013 00:00:00
1307098-15
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
30.90
35.14
52.61
62.04
66.27
81.34
93.93
111.97
117.37
276.95
303.38
307.33
334.07
356.43
377.09
384.19
387.25
391.16
416.47
419.79
437.49
469.16
512.87
609.86
700.67
711. 54
1885
467
42
292
137
768
50
199
34
59
154
27
81
531
11
124
223
51
35
10
122
42
9
10
7
7
78
57
103
84
73
148
95
73
73
38
28
23
18
22
16
9
6
5
28
18
11
8
14
4
0
4
3
3
0
4
4
0
0
0
0
0
3
3
0
0
0
4
4
4
5
5
0
0
0
0
0
0
?;~'tr~
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130709815 GEl_BAFIL_l93593.CN

PEAK Vl6.9 PEAKEFF V2.2
D-3 TOT
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
31.13
35.37
52.84
62.27
66.50
81. 57
94.16
112.20
117.60
277.16
303.59
307.55
334.28
356.64
377.30
384.40
387.46
391.37
416.68
420.00
437.69
469.36
513.07
610.05
700.86
711. 73
27
27
50
58
58
77
90
109
116
273
300
300
331
351
375
382
382
382
413
413
434
462
508
606
698
708
1.54
1.73
2.83
1. 88
2.11
1. 92
1. 57
1.74
2.26
1.23
1. 80
1. 96
1.86
1.89
1.45
1.74
1.94
2.50
2.78
1.73
1.88
2.86
1.98
1. 01
2.83
1.67
Pw
24-JUL-2013 10:16:18
1.00000E+OO filter
0
BAFIL
0 00:15:00.27
4096
l0.00000
Cts/Sec %Err
13 2.09E+OO
13 5.19E-01
8 4.70E-02
14 3.25E-01
14 1.52E-Ol
10 8.53E-01
8 5.58E-02
6 2.21E-Ol
6 3.82E-02
8 6.54E-02
11 1.71E-Ol
11 3.05E-02
6 9.00E-02
12 5.90E-Ol
6 l.23E-02
14 1. 38E-Ol
14 2.48E-01
14 5.62E-02
10 3.94E-02
10 1. 12E-02
9 1.36E-Ol
15 4.61E-02
10 9.86E-03
7 1.06E-02
6 7.78E-03
6 7.68E-03
2.4
5.4
43.9
7.5
14.8
4.7
36.6
9.8
44.4
22.3
8.9
36.7
13.9
4.7
63.3
10.l
7.8
26.2
33.7
82.5
10.3
21.2
83.0
46.0
37.8
61. 0
0.0%
Fit
9.79E+OO
3.96E+OO
3.04E+Ol
2.43E+OO
9.31E+OO
5555

Sample ID : 1307098-15
-
Acquisition date

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
l . 00
3.561E+02
Total Activity
;
15.38%
FISSION
Hlife
10.SOY
Nuclide Type
26
22
4
Page :
2
24-JUL-2013 10:16:18
---------
3.561E+02
Wtd Mean
Decay Corr
Decay Corr
2-Sigma
pci/f ilter 2-Sigma Error %Error Flags
3.561E+02
19.31
0.688E+02
...,..,. _______
3.561E+02
NATURAL
Nuclide
Hlif e
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Pecay pCi/f ilter
l . 00
3.941E+02
____ ..,. ____
Total Activity
Wtd Mean
Decay Corr
pCi/filter
3.941E+02
---------
3.941E+02
3.941E+02
7.501E+02
7.502E+02
Flags: "K" ; Keyline not found

"E" ; Manually edited
2-Sigma
Pecay Corr
15.91
0.627E+02
"M" ; Manually accepted

"A" ; Nuclide specific abn. limit
msss

Sample ID : 1307098-15
Acquisition date
Page :
3
24-JUL-2013 10:16:18

Nuclide
BA-133
Energy
Bl.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.963E+Ol 3.561E+02
3.561E+02 19. 31
4.915E+OO 5.290E+02
5.290E+02 34.20
6.963E+OO 3.818E+02
3.818E+02 17.80
3 Valid Peaks =
Status
OK
OK
OK
3.561E+02+/- 6.878E+Ol ( 19.31%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
Uncorrected Decay Corr 2-sigma

%Eff
5.865E+Ol 3.941E+02
3.941E+02 15.91
1 Valid Peaks =
Status
OK
3.941E+02+/- 6.271E+01 ( 15.91%)
"*" = Keyline
~557

Sample ID : 1307098-15
Acquisition date
Page :
4
24-JUL-2013 10:16:18

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.561E+02
3.941E+02
Act error
6.878E+Ol
6.271E+Ol
MDA
(pCi/filter)
1.813E+Ol
5.170E+Ol
MDA error
Act/MDA
2.976E+OO
l.656E+OO
19.640
7.623
MDA error
Act/MDA
6.509E+OO
2.638E+Ol
3.632E-03
6.425E-02
7.579E+OO
1. 523E-Ol
-0.060
-0.378
0.000
2.441
0.566
1.687
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-l.257E+OO
-7.702E+Ol
O.OOOE+OO
8.346E+OO
3.522E+Ol
1.095E+Ol
Act error
l.324E+Ol
l.582E+02
O.OOOE+OO
l.617E+OO
3.915E+Ol
3.323E+OO
MDA
(pCi/filter)
2.085E+Ol
2.039E+02
l.933E-Ol
3.419E+OO
6.225E+Ol
6.490E+OO
0558
c_,-
VAX/VMS Peak Search Report Generated 24-JUL-2013 10:47:06,63
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
3
3
0
2
2
4
4
0
3
3
0
0
0
0
0
0
1
1
0
0
2
2
2
3
3
0
0
0
0
0
l {""14 (,,._..;
DKA100: [GAMMA.SCUSR.ARCHIVE)SMP 130709816 GEl_BAFIL 193596.CN

WEAK V16.9 PEAKEFF V2.2
D-3 DIS
24-JUL-2013 00:00:00
1307098-16
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Energy
Area
Bkgnd
30.92
35.19
52.17
61.92
65.85
81.22
84.71
93.33
112.07
116.27
162.50
186.32
205.01
224.04
277.19
303.19
333.93
338.62
356.52
366.02
384.15
387.15
391.70
415.34
418.83
437.58
468.48
473.26
511.47
912.33
2028
431
39
243
106
717
22
43
234
59
40
21
34
23
55
130
75
30
512
20
126
214
43
38
16
108
21
8
23
6
85
63
99
77
83
59
61
100
51
49
101
85
50
52
36
36
29
20
23
25
18
14
15
9
12
15
2
3
2
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
24-JUL-2013 10:31:49
1.00000E+OO filter
0
BAFIL
0 00:15:00.27
4096
10.00000
FWHM Channel
Left
Pw
Cts/Sec %Err
31.15
35.43
52.40
62.15
66.08
81.45
84. 94
93.55
112.30
116.50
162.72
186.54
205.24
224.25
277.41
303.40
334.14
338.83
356.73
366.23
384.36
387.35
391.91
415.55
419.03
437.79
468.68
473.47
511.67
912.50
27
27
49
58
58
76
76
90
106
106
157
183
201
218
273
300
330
330
352
362
381
381
381
409
409
433
466
472
507
910
13
13
7
13
13
13
13
9
15
15
11
8
2.25E+OO 2.3
4.79E-01 5.8
4.37E-02 44.7
2.70E-01 8.4
1.18E-Ol 17.9
7.97E-Ol 4.1
2.46E-02104.7
4.82E-02 44.0
2.60E-01 7.9
6.52E-02 25.3
4.48E-02 51.4
2.36E-02 78.0
3.77E-02 40.0
2.54E-02 62.8
6.16E-02 23.7
1.45E-01 11. 6
8.30E-02 15.9
3.32E-02 32.4
5.69E-01 4.7
2.23E-02 50.1
1. 39E-01 10.8
2.37E-01 8.2
4.76E-02 22.3
4.26E-02 23.7
1.82E-02 53.0
1.20E-01 11.7
2.37E-02 23.6
8.33E-03 48.3
2.53E-02 24.5
6.67E-03 40.8
1.57
1.71
2.57
1.59
1.74
1. 67
2.14
1.61
1.78
2.00
1.96
1.99
4.65
3.19
1.55
1.92
1.84
1.84
1.77
1.58
2.06
1.77
1. 91
2.29
2.30
1.73
1.83
1. 00
2.09
1. 88
10
9
7
17
17
9
9
17
17
17
16
16
10
6
5
10
5
0.0%
Fit
1.SOE+Ol
1.05E+OO
1. 68E+OO
1.07E+OO
2.34E+OO
3.61E+OO
2,34E+OO
-fJl559

Sample ID : 1307098-16
Acquisition date

Nuclide Type
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.326E+02
3.446E+Ol
1. 00
Total Activity
:
Wtd Mean
Uncorrected
Decay pCi/filter
3.279E+02
1. 00
Total Activity
=
---------
3.671E+02
Wtd Mean
Decay Corr
pci/filter
3.327E+02
3.446E+Ol
---------
Decay Corr
2-Sigma
18.74
0.624E+02
209.74
7.227E+Ol
3.671E+02
NATURAL
Nuclide
Hlif e
TH-234 4.47E+09Y
Flags: "K"
"E"
16.67%
FISSION
Nuclide
Hlif e
10.SOY
BA-133
NP-237 2.14E+06Y
Nuclide Type
30
25
5
Page :
2
24-JUL-2013 10:31:49
---------
---------
3.279E+02
3.279E+02
6.950E+02
6.950E+02
Keyline not found

edited
= Manually
Wtd Mean
Decay Corr
pCi/f ilter
3.279E+02
"M"
"A"
Decay Corr
2-Sigma
0.578E+02
17.61
= Manually accepted
= Nuclide specific abn.
limit

Sample ID : 1307098-16
Acquisition date
Page :
3
24-JUL-2013 10:31:49

Nuclide
BA-133
Energy
81.00
302.84
356.01
%-A.bn
33.00*
17.80
60.00
Final Mean for

NP-237
86.50
3 Valid Peaks =
12.60*
Final Mean for

%-Eff
pCi/f ilter pCi/filter %-Error
3.327E+02 18.74
l.963E+Ol 3.326E+02
4.915E+OO 4.475E+02
4.476E+02 37.28
6.963E+OO 3.682E+02
3.682E+02 17.86
1.532E+Ol
3.327E+02+/- 6.235E+Ol ( 18.74%-)
3.446E+Ol
1 Valid Peaks =
Status
OK
OK
OK
3.446E+Ol 209.74
OK
3.446E+Ol+/- 7.227E+Ol (209.74%-)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
"*"

%-Eff
pCi/filter pCi/f ilter %-Error
5.865E+Ol 3.279E+02
3.279E+02 17.61
1 Valid Peaks=
Status
OK
3.279E+02+/- 5.776E+Ol ( 17.61%-)
= Keyline
tll561

Sample ID : 1307098-16
- -
--
Acquisition date
Page :
4
24-JUL-2013 10:31:49
Identified Nuclides
Nuclide
BA-133
TH-234
NP-237
Activity
(pci/filter)
3.327E+02
3.279E+02
3.446E+Ol
Act error
MDA
(pCi/filter)
MDA error
Act/MDA
6.235E+Ol
5. 776E+l'.ll
7.227E+Ol
l.911E+Ol
5.B02E+Ol
5.335E+Ol
3.137E+OO
1.!!59E+OO
6.495E+OO
17.409
5.652
0,646
Act error
MDA
(pCi/filtel'.')
MDA error
Act/MDA
6.212E+OO
2.519E+Ol
3.632E-03
6.669E-02
1. 486E-Ol
0.317
-0.031
0.000
2.452
1.323
Nuclide
C0-57
CD-109
PA-231
PA-234
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
6.303E+OO
-6.036E+OO
O.OOOE+OO
8.701E+OO
8.380E+OO
1.160E+Ol
1.393E+02
O.OOOE+OO
1.699E+OO
3.230E+OO
l.990E+Ol
1.948E+02
l.933E-01
3.549E+OO
6.333E+OO
9562

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample !:El
S;;tmple type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
11
12
13
0
0
0
0
0
1
1
0
2
2
15
16
17
18
19
20
21
22
23
24
25
26
27
239
91
16
19
783
161
42
31
48
36
38
49
49
27
12
15
25.55
31.00
35.18
36.07
53.15
53.59
61. 72
65.89
66.34
79.67
81. 04
111.81
115.88
206.64
301.87
302.80
306.83
333.01
333.55
354.81
355.74
383.17
385.54
386.17
413.91
10
'J-4
15
12
17
85
69
22
12
0
0
8
8
0
1
8
9
48
63
28
1838
382
101
50
20.80
1
1
0
2
2
0
24-JUL-2013 10:56:58
1.oooooE+Oe filter
0
BAFIL
0 00:15:01.12 0.1%
4096
10.00000
No
Bkgnd
;:n... 2a
2
2
24-JUL-2013 00:00:00 Acquisition date :

1307098-17
Sam)?le Quantity
FILTER
Sample Geometry
Petector Geometry:
GE5
0 00:15:00.00
Elapsed real time:
25
End channel
3.00000
Gaussian
Area
~ ""'V-< ....__..,
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP 130709817 GE5 BAFIL 193605.CN

WEAK V16.9 PEAKEFF V2.2
PZ-100-SD TOT
EnerSJy
11
97
43
21
63
64
99
325
69
19
165
31
12
4
2
6
7
5
9
8
3
FWHM Channel
Left
Pw
0. !35
205.0()
209.57
1.29
0.74
0.68
0.62
0.75
0.30
0.66
0.72
0.66
0.24
0.65
0.87
0.49
0. 49
1.06
1. 06
0,48
1.33
1.10
1.12
1.13
0.72
1.27
1.29
0.21
302.88
342,96
351,46
515.44
519.66
597.60
637.63
642.00
769.90
783.01
1078.29
1117.29
1988.22
2902.00
2911.00
2949.68
3200.89
3206.00
3410.00
3419.00
3682.22
3704.89
3711. 00
3977.11
190
1!30
236
292
333
333
502
502
584
626
626
758
774
1067
1108
1975
2890
2890
2929
3186
3186
3398
3398
3667
3695
3695
3962
26 5.35E-02 26.2
26 "l.02E-02 18.2
25 3.llE-02 45.5
21 2.04E+OO 2.6
25 4.25E-01 7.6
25 1.12E-01 20.7
21 5.53E-02 18.7
21 1.03E-02 66.4
27 2.66E-01 8.5
27 l.OlE-01 19.1
27 1.77E-02103.2
17 2.14E-02 69.0
22 8.?0E-01 4.1
22 1.79E-01 12.4
20 4.64E-02 30.1
19 1.24E-02 64.2
26 l.OSE-01 12.3
26 4.82E-02 16.6
27 2.36E-02 37.0
26 6.97E-02 13.8
26 7.12E-02 11.4
32 1. lOE-01 18. 9
32 3.61E-01 5.9
26 7.64E-02 13.6
29 2.0SE-02 66.2
29 1.83E-01 8.3
29 3.47E-02 20.9
0.50
250.~1
Cts/Sec %Err
Fit
2.20E+OO
l.43E+OO
8.SOE-01
2.56E+OO
5.97E+OO
4.23E+OO
1. 61E+Ol
1. 57E+OO
'!l563

Sample ID : 1307098-17
Acquisition date

Nu.elide
BA-133
Hlife
10.SOY
Wtct Meaa
Uncorrected
Decay pCi/filter
l.Oo 3.955E+02
Total Activity
3.95SE+02
27
21
Wtd Meafl
Decay Corr
pCi/filter
3.955E+02
... .,.. "" - .,.. ,... ... -
l?age :
2
24-JUL-2013 10:56:58
22.22%
Decay Corr
2-Sigma
2-Sigma Errcr %Error Flags
l'/.30
0.684E+02
3.955E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd M@an
Uncorrected
Decay pCi/filter
1. 00
2 .159E+02
Total Activity
Wtd Mean
Decay Corr
pCi/filter
2.159E+02
2.159E+02
2.159E+02
6.114E+02
6.115E+02

Decay Corr
2-Sigma
2-Sigma Error %E:i:-ror Flags
17.49
0.378E+02


Sample ID : 1307098-17
Nuclide
BA-l33
Energy
!ll. 00
302.84
356.01
%Ahn
33.00*
17.80
60.00
Final Mean for
Acquisition date
Wage :
3
24-JUL-20l3 10:56:58
unee~~eeted Pecay eorr 2-sigm!l

%Eff
l.802E+Ol 3.955E+02
3.955E+02 17.30
2.575E+OO 2.844B+02. 2.845E+02 42.35
3.770E+02 18.64
4.312E+OO 3.770E+02
3 Valid Peaks=
Status
OK
OK
OK
3.955E+02+/- 6.843E+01 ( 17.30%)

Nuclide
TH-234
Energy
63.29
%Ahn
3.BO*
Final Mean for

Flag:
"*"
uncorrected Decay Corr 2-Sigma

%Eff
pCi/filter pCi/f ilter %Erro:r
8.750E+Ol 2.159E+02
2.159E+02 17.49
1 Valid Peaks =
Status
OK
2.159E+02+/- 3.776E+01 ( 17.49%)
Keyline
lli565
combined Activity-MDA Report

Sample ID : 1307098-17
Nuclide
BA-133
TH-234
Acquisition date
Act errpr
Activity
(pCi/fi1teJ:')
3.955E+02
2.159E+02
6.843E+Ol
3.776E+Ol
MDA
(pci/filter)
l..365E+OO
3.395E+Ol
:eiawe :
4
24-JUL-2013 10:56:58
MDA error
Act/MDA
2.009E-Ol.
4.368E-01
21l9.853
6.359
MDA error
Act/MDA
9.430E+OO
l.71SE+Ol
1. 63 7E-02
2.238E-02
3.576E+OO
2.SlOE-02
0.323
0.176
-0.172
1.471
-0.718
0.441
Non-Identified Nuclide$
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pci/filter)Ided
8.982E+OO
3.13BE+Ol
-2.SOOE-01
2.925E+OO
-2.910E+Ol
9.832E-01
Act error
l.399E+Ol
9.306E+01
8.243E-Ol
1.070E+OO
2.650E+Ol
l.228E+OO
MDA
(pCi/filter)
2.782E+Ol
l.785E+02
1.455E+OO
1.988E+OO
4.054E+01
2.229E+OO
-msss
c___
VAX/VMS Peak Search Report Generated 24-JUL-2013 11:29:40,97
Configuration
Analyees by
Client ID .
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical l~vel
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
2
2
2
0
2
2
0
2
2
6
6
6
0
5
5
5
0
0
5
5
5
2
2
0
0
6
6
3
3
1
1
0
J/1_yf;_>
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_ 130709818 GES BAFIL_l93615.CN

PEAK V16.9 JilEAKEFF V2 . 2
PZ-100 SD DIS
24-JUL-2013 00:00:00
1307098-19
FILTER
GES
0 00:15:00.00
25
3.00000
No
Energy
Are ill.
Bkgnd
19.87
20.80
22.16
30.99
35.12
36.02
53. 47
61.13
61.72
65.51
66.09
66.56
80.95
110.00
110.BB
111.86
192.33
231.3S
275.50
276.03
2'76.85
301.49
302.39
306.69
333.00
355.25
355.86
382.63
383.38
385.86
386.38
390.15
29
57
16
1944
360
106
22
33
183
48
45
22
791
31
29
162
11
14
31
20
11
22
192
34
56
280
62
60
28
69
99
24
3
9
7
85
26
9
23
13
27
21
16
24
17
11
14
10
17
7
10
6
0
3
3
0
6
10
9
4
4
8
6
4
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
Left
Pw
0.60
0.61
0.51
0.75
0,66
0.57
0.57
0.65
0.78
0.66
0.46
0.88
0.77
l.23
1.12
0.68
0.18
0.57
1.03
0.61
0.61
1.28
1.06
0.83
0.15
0.91
1. 03
1.16
0.97
1.16
1,16
0,60
186
186
186
290
330
330
510
585
585
628
628
628
763
1046
1046
1046
1B30
2206
2640
2640
2640
2890
2890
2934
3187
3398
3398
3666
3666
3695
3695
3736
36
36
36
26
196.01
205.02
218.00
302.80
342.40
351.00
518.42
592.00
597.60
634.00
639.57
644.10
782.13
1060.88
1069.40
1078.72
1850.89
2225.61
2649.00
2654.13
2661.96
2898.36
2907.00
2948.26
3200.78
3414.25
3420.08
3677.00
3684.21
3708.00
3713.00
3749.20
28
28
14
24
24
27
27
27
33
43
43
43
23
24
25
25
25
26
26
24
24
31
31
27
27
28
28
22
24-JUL-2013 11:13;34
1.00000E+OO filter
0
J:lAFIL
() 00:15:01.13
4096
10.00000
ets/sec %Err
3.19E-02
6.32E-02
1.74E-02
2.16E+OO
4.0QE-01
1.18E-01
2.45E-02
3.70E-02
2.04E-01
5.34E-02
5.0lE-02
2.39E-02
8.79E-01
3.4SE-02
3.21E-02
1.SOE:-01
l.17E-02
1.SSE-02
3.47E-02
2.26E-02
1.25E-02
2.43E-02
2.14E-01
3.78E-02
6.21E-02
3.12E-01
6.91E-02
6.66E-02
3.09E-02
7.69E-02
l.lOE-01
2.71E-02
33.1
22.6
27.9
2.6
6.6
16.1
45.2
42.7
10.0
24.4
27.5
73.6
3.8
41.5
63.l
9.5
83.6
44.B
23.6
37.3
28.5
40.1
5.8
17.1
15.9
6.9
28.7
14.8
32.3
18.2
12.5
25.1
0.1%
Fit
2.19E+OO
4.69E+OO
2.39E+OO
3.27E+OO
l.18E+OO
7.47E-Ol
6.03E+OO
6.83E-01
8.27E-Ol
2.05E+OO
:!11567

sample ID : 130709S-le
ll'aliJe :
2
;'14-JUL-2013 11:13:34

32
25

Nuclide
BA-133
Hlif e
10.SOY
Wtd Mean
Urn::orrected
Decay pCi/filter
1.00 3.992E+02
Total Activity
3.992E+02
Wtd MeiHl
Decay Corr
pCi/filter
3.992E+02
Decay Corr
2-$igma
17.04
0.680E+02
3.992E+02

Nuclide
!Uife
TH-234 4,47E+09Y
AM-241
432.20Y
Wtd Mean
Uncc:ri;rected
Decay pCi/filter
1. 00
1.655E+02
1.00 2.7B2E+OO
____ .,..,.. ___
Total Activity
Flags:
---------
l.683E+02
1.683E+02
5.675E+02
5.675E+02
K11 ; Keyline not found

"E" "' Manually edited
11
Wtd Mean
Decay Corr
pCi/filter
l.655E+02
2.7B2E+OO
Decay Corr
2-Sigma
2-Sigma Error %Errer Flag!ll
0.337E+02
20.35
2.37\'lE+OO
85.52
"M" ; Manually accepted

"A'' "' Nuclide specific: abn. limit

sample ID : 1307098-18
Acquisition date
Page :
3
24-JUL-2013 11:13:34

Nuclide
BA-133
Energy
81.()0
302.84
356.01
%Al::in
33.00*
17.80
60.QO
Final Mean for

%Eff
l.802E+Ol 3.992E+02
3.992E+02 17.04
l.259E+03 28.87
2.575E+OO l.259E+03
4.312E+OO 7.216E+Ol
7.217E+Ol 59.16
3 Valid Peaks =
Status
OK
OK
OK
3.992E+02+/- 6.802E+Ol ( 17.04%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag:
l Valid Peaks =
35.90*
Final Mean for

%Eff
8.750E+Ol l.655E+02
1.655E+02 20.35
l.OOOE+02
l.655E+02+/- 3.368E+Ol ( 20. 35%)
2.782E+OO
l Valid Peaks =
Status
OK
2.782E+OO
85.52
OK
2.782E+OO+/- 2.379E+OO ( 85.52%)
''*'' = Keyline
1l569

Sample ID : 1307098-18
Acquisition date
Page :
4
24-JUL-2013 11:13:34

Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filterl
Act error
3.992E+02
1.655E+02
2.782E+OO
6.802E+Ol
3.368E+Ol
2.379E+(J0
MDA
(pCi/filter)
l.188E+Ol
3.4B2E+Ol
1.625E+OO
MDA error
Act/MDA
1.750E+OO
4.479E-01
1.829E-02
33.596
4.754
1. 712
MDA error
Act/MDA
8.774E+OO
1.704E+01
1.521E-02
2.333E-02
3.394E+OO
-0.208
0.281
-0.472
0.350
-0.294
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
-5.393E+OO
4.981E+01
-6.382E-Ol
7.257E-01
-1.133E+Ol
Act error
1.495E+Ol
B.925E+01
8.376E-01
4.058E-01
2.248E+Ol
MDA
(pCi/filter)
2.588E+01
l.770E+02
1.351E+OO
2.072E+OO
3.848E+01
0>~1~
-:r\t.,
configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.A.RCHIVE]SMP_ 130709819 GE5 BAFIL 193625.CN

PZ-112-AS TOT
24-JUL-2013 00:00:00
J,307096-19
FILTER
GE5
0 00:15:00.00
25
3.00000
No
Pk rt
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
18.34
21.15
31.01
35.12
36.05
53.45
61.81
66.08
81.03
111.36
111.99
115.91
160.49
276.11
302.18
302.80
332.90
355.35
382.84
383.46
386.22
390.20
5
85
1904
380
55
33
200
100
772
63
130
34
23
38
53
51
53
372
59
44
144
20
13
24
112
10
1
40
59
29
53
31
33
28
15
10
7
4
13
12
9
13
19
11
0
0
0
2
2
0
0
0
0
1
1
0
0
0
1
1
0
0
1
1
0
0
Acquisition date :
Sample Quantity
sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
24-JUL-2013 11:32:22
l.OOOOOE+OO filter
0
BAFIL
0 00:15:01.13
4096
10.00000
FWHM Channel
Left
Pw
Cts/sec %Err
0.31
0.32
0.82
0.68
0.51
0.72
0.69
0.72
0.65
0.76
0.77
0. 31
0.56
1.02
1.06
1.06
1.19
0.86
1.16
1.16
0.79
0.73
174
201
290
333
333
506
584
625
766
1050
1050
1105
1533
2639
2891
2891
3185
3398
3668
3668
3697
3734
10
14
26
24
24
20
27
29
29
39
39
24
20
27
26
26
27
32
25
25
28
25
5.83E-03133.7
9.43E-02 16.4
2.12E+OO 2.7
4.23E-01 6.0
6.09E-02 20.7
3.66E-02 43.6
2.23E-01 11.4
1.llE-01 16.4
8.57E-01 4.2
7.03E-02 28.7
1.45E-Ol 12.6
3.82E-02 38.4
2.59E-02 37.2
4.19E-02 24.1
5.89E-02 20.6
5.69E-02 16.3
5.92E-02 19.0
4.13E-01 5.5
6.51E-02 18.0
4.94E-02 22.7
1.60E-01 10.3
2.21E-02 39.7
181. 39
206.29
302.91
342.37
351.34
518.26
598.51
639.46
782.89
1074.00
1080.00
1117.64
1545.40
2654.89
2905.00
2911.00
3199.79
3415.26
3679.00
3685.00
3711.46
3749.66
0.1%
Fit
8.32E-01
1.96E+OO
1.51E+OO
1.74E+OO
lil571

Sample ID , 1307095-19
Acquilid ti on date

Page :
2
24-JUL-2013 11:32:22
22
16
27.27%

Nuclide
BA-133
Hlif e
10.SOY
Wtd Mean
uncorrected
Decay pCi/filter
1.00 3.896E+02
Total Activity
3.896E+02
Wtd Mean
Decay Corr
pci/filter
3.896E+02
---------
Decay Corr
2-Sigma
17.43
0.679E+02
3.896E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pci/filter
1. 00
1. 809E+02
Total Activity
Flags: "K"
"E"
1.809E+02
1.809E+02
5.705E+02
5.705E+02
Keyline not found

edited
= Manually
Wtd Mean
Decay Corr
Decay Corr
2-Sigma
pCi/filter 2-Sigma Error %Error Flags
1.B09E+02
0.420E+02
23.20
_____ .., ___
"M"
"A"
Manually accepted
specific abn. limit
= Nuclide
Page :

Sample ID : 1307098-19
24-JUL-2013 11:32:22

Nuclide
BA-133
Energy
%Abn
81. ()0
302. 84
33.00*
17.80
60.00
356.01
Final Mean for
Uncorrect;;ed Decay Corr 2-Sigma

%Eff
1.802El+Ol 3.896E+02
3.B96E+02 17.43
2.575E+OO 3.357E+02
3.357E+02 41.92
4.315E+02 19.23
4.312E+OO 4.315E+02
3 Valid Peaks =
3.$9r;iE+02+/- 6.792E+01
Status
OK
OK
OK
17.43%)
Nuclide Type: NATUl'<AL

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
*"
Uncorrected Decay Corr 2Sigma

pci/filter pCi/filter %Error
8.750E+01 1.$09E+02
l.S09E+02 23.20
%Eff
1 Valid Peaks ;
Status
OK
1.809E+02+/- 4.197E+01 ( 23.20%)
Keyline
S573

Sample ID : 1307098-19
- -
Acquisition date
4
Page :
24-JUL-2013 11:32:22
- - Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filterl
Act error
6.792E+Ol
4.197E+Ol
3.896E+02
1.809E+02
MDA
(pCi/f ilterl
1.336E+Ol
1.730E+Ol
MDA error
Act/MDA
1.967E+OO
2.225E-01
29.169
10.459
MDA error
Act/MDA
8.332E+OO
l.746E+Ol
1.827E-02
2.328E-02
4.028E+OO
2.626E-02
-0.507
0.286
0.305
1.900
-0.090
0.191
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-1.246E+Ol
5.186E+Ol
4.953E-01
3.929E+OO
-4.123E+OO
4.459E-Ol
Act error
1.581E+Ol
9.184E+Ol
7.924E-01
1.302E+OO
2.544E+Ol
1.436E+OO
MDA
(pCi/filter)
2.458E+Ol
1.814E+02
1.623E+OO
2.068E+OO
4.566E+Ol
2.333E+OO
~-v-tl~3

configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Oetector name
Elapsed live time:
Start channel
Sensitivity
C:ritical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130709820 - GES BAFIL 193633.CN

PEAK V1!0. 9 PEAKEFF V2.2
PZ-112-AS DIS
24-JUL-2013 00:00:00
1307098-20
FILTER
GES
0 00:15:00.00
25
3,00000
No
Pk It
Energy
Area
Bkgnd
6.91
21.16
31.01
35.13
36.04
53.51
61.55
62.18
65.61
66.24
79.61
81.00
84.12
111.85
116.25
161.10
193.59
275.88
302.31
332.41
332.92
333.65
355,35
382.74
383.15
386.16
416.91
5
89
1991
352
70
37
154
91
32
38
65
721
32
155
33
16
12
34
112
33
13
27
367
12
93
129
14
8
21
75
35
18
27
10
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
0
7
7
0
1
1
1
1
1
1
0
0
0
0
0
0
0
1
1
1
0
1
1
0
30
32
12
13
17
42
39
25
17
11
12
1
3
2
9
6
8
14
9
Acquisition date :
Sample Quantity
Sample Geometry
Petector Geometry:
Elapsed real time:
End channel
Gaussian
24-JUL-2013 11:48:11
1.00000E+OO filter
0
BAFIL
0 00:15:01.09
4096
10.00000
FW!1M channel
Left
Pw
Cts/Sec %Err
0.27
0. 9()
0.84
0.70
0.72
0. 2 (l
0.65
0.65
0.66
0.66
0.69
0.70
1.11
0.90
0.37
0.61
0.11
0.29
0.72
1.21
1. 10
1.10
0.75
1.16
1.16
0.71
0.81
65
200
292
334
334
507
583
583
627
627
760
760
800
1067
1103
1535
1843
2636
2891
3184
3184
3184
3398
3666
3666
3696
3993
9
1$
26
25
25
18
30
30
23
23
35
35
20
21
26
20
22
25
27
30
30
30
30
29
29
25
21
S.26E-03121.9
!L 91E-02 16. 3
2.20E+OO 2.6
3.91E-01 6.6
7.72E-02 26.1
4.07E-02 32.9
1.71E-01 10.B
1.0lE-01 18.2
3.54E-02 43.2
4.24E-02 35.9
7.22E-02 18.0
8.0lE-01 3.9
3.56E-02 31. 9
1.72E-01 12.0
3.63E-02 47.5
1.76E-02 64.3
1.32E-02 72.7
3.82E-02 25.1
1. 25E-01 11. 0
3.68E-02 23.6
1.47E-02 64.9
3.03E-02 22.9
4.07E-01 5.5
1. 31E-02 77.9
1. 04E-01 10.5
1. 44E-01 10.2
1. 52E-02 49.0
71.67
2()8.38
'Hl2. 92
342.44
351.18
518.81
596.00
602.00
635.00
641. 00
769.33
782.67
812.57
1078.69
1120.84
1551.30
1863.04
2652.62
2906.25
3195.05
3200.00
3207.00
3415.17
3678.00
3682.00
3710.89
4005.93
0.1%
Fit
1. 7BE+OO
1.44E+OO
1.43E+OO
7.62E-01
6.46E-Ol
2.63E+OO

Sample ID : 1307098-20
Acquisition date
To~al number of lines in spectrum

Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00 3.642E+02
--.,,.-----.~-
Total Activity
;
22.22%
FISSION
Hlife
10.SOY
Nuclide Type
27
21
6
Page :
2
24-JUL-2013 11:48:11
3.642E+02
Wtd Mean
Decay Corr
pCi/filter
3.642E+02
---------
Decay Corr
2-Sigma
0.624E+02
17.13
3.642E+02
NATURAL
Nuclide
Hlife
Tl{-234 4.47E+09Y
Wtd Me;an
Uncorrected
Pe cay pCi/filter
1. 00 S.237E+Ol
Total Activity
-----..--.-
Wtd Mean
Decay Corr
pCi/filtE;r
8.237E+01
.... ..., ______ .,..
8.237E+Ol
8.237E+Ol
4.465E+02
4.466E+02

Decay Corr
2-Sigma
2-Sigma Error !!;Error Flags
3.02lE+Ol
36.68

"A" = Nuclide specific abn. J.imit
~576
Page :

Sample ID : 1367098-20
Nuclide
BA-133
Energy
81,00
302.84
356.01
%Aon
33.00*
17.80
60.00
Final Mean for
Nuclide
TH-234
Energy
63.29
%Ahn
3.80*
Final Mean for

Flag: ''*'' = Keyline
= 3.642E+02+/- 6.237E+Ol
Status
OK
OK
OK
17.13%)
Uneorrected Decay eor:ir 2-!Hgma

%Eff
pCi/filter :pCi/filtel:' %Error
8.750E+01 8.237E+Ol
8.237E+Ol 36.68
1 Valid Peaks
24-JUL-2013 11:48:11
Uneel'.'rected Deeay eeirr 2-!Hgma

%Eff
l.BCl2E+Ol 3.642E+02
3.642E+02 17.13
2.575E+OO 7.365E+02
'7.365E+02 34.38
4.312E+OO 4.255E+02
4.256E+02 18.14
3 Valid Peaks
Acquisition date
!'Jtatus
OK
8.237E+Ol+/- 3.D21E+Ol ( 36.68%)
Combined AGtivityM~A Report

sample IO : i30'1098-20
Pagi!il :
4
24-JUL-2013 1148:11

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act errer
3.642E+02
S.237E+Ol
6.237E+Ol
3.02l-E+Ol
MDA
{pCi/filter)
MDA error
Act/MDA
l..381E+Ol
2.397E+Ol
2.033E+OO
3.0S3E-01
26.371
3. 4<37
MD.I\
M1'A error
Act/MDA
9.782E+OO
1.'16"/E+Ol
1.568E-02
2.255E-02
4.147E+OO
2.631E-02
0.260
0.191
-0.305
2.060
0.203
0.394
Nuclide
C0-57
CD-Hl9
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
7.511E+OO
3.503E+Ol
-4. 2'11E-01
4.126E+OO
9. SHlE+Otl
9.20lE-Ol
Act errer
(pci/filter)
1.'181E+01
9.579E+Ol
!3.210E-01
l.356E+OO
2.S89E+Ol.
1.334E+OO
2.886E+Ol
1.1136E+02
1.393E+OO
2.004E+OO
4.70l.E+Ol
2.337E+OO

Engineering Management Support, Inc.: West Lake OU-1

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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

WORK ORDER #13-07098-0R

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

Chain of Custody & pH Check Sheet

Analytical Results Summary

Quality Control Sample Results Summary

Laboratory Technician's Notes

Analytical Data (Isotopic Uranium)

Analytical Data (Isotopic Thorium)

Analytical Data (Radium-226)

Analytical Data (Radium-228)

Barium-133 Analytical Tracer Data

Last Page Number

STANDARD OPERATING PROCEDURE

Eberline Services - Oak Ridge Laboratory

LABORATORY DATA SUPPORT CHECKLIST

Eberline Services Work Order

Date for Partial

First Technical Data Review

Data Entry/Electronic Deliverable

Electronic Deliverable Proof

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Date package approved by: :

REC'D JUL .15 2.0i3

Chain of Custody Record

Re lnqu1shea oy: (~ ignalure)

Recelvea by: {Signature)

Received by: (Signature}

Fir>+ (}:p/hll CJ~../

Sample Custodian Remarks (Completed By Laboratory)

Rollnqulshed by: (Signature)

(IO b9 completed b'f Jab)

(865) 481-o683 Phone (865) 493-4621 Fax

Oak Ridge Laboratory

Fxns 05,07,10,12,14,16,18 & 20 are DISSOLVED

Location r circle one l

MUST USE Fxn 11 as DUP

--"36, __ -- ----C- -45

Fxns 04,06,08,09,11,13,15,17 & 19 are TOTAL

1"""' -. ;_~ ...::::..

----. ------------------ ------------~---!

----- --- -----------------------------!----------------- --- ---+------ ----------1

Oak Ridge Laboratory

Re-Analysis: 2Fxns 04,06,08,09,11,13,15,17 & 19 are TOTAL

Fxns 05,07,10,12,14,16,18 & 20 are DISSOLVED

Original Lab Deadline: 08/13/13

Location (circle oneJ

Printed: 7126/2013 10:10 AM

Fxns 04,06,08,09,11,13,15,17 & 19 are TOTAL

MUST USE Fxn 11 as DUP

Location (circle one

Printed: 1111t2013 a:11AM

Oak Ridge Laboratory

MUST USE Fxn 11 as DUP

Location circle one

Fxns 05,07,10,12,14,16,18 & 20 are DISSOLVED

Fxns 04,06,08,09,11,13,15,17 & 19 are TOTAL

Printed: 7/17/2013 8:11 AM

Oak Ridge Laboratory

: -:-:-_:__:__ 1 - ~:~--- 1------------------------------------11-~__:_~--~--~:~1: ~ ~--- ~- :~~; - -~~-~---:lr_;:__--~;~~1~-:==i:t ~~~

Fxns 05,07,10,12,14,16,18 & 20 are DISSOLVED

MUST USE Fxn 11 as DUP

: -:-:-_:: 1 - ~:~--- 1------------------------------------11-~__:_~--~--~:~1: ~ ~--- ~- :; - --~---:lr_;:__--~;~~1~-:==i:t ~~~

1~----~~----~21 -<~2r-~-1-~~<~2r-~-1-~~-~4.~o~oo~o ---4-1--~