1. The document outlines the operating procedure for a Thermogravimetric Analyzer (TGA).
2. It involves setting gas pressures, taring the balance, selecting diagnostic programs, loading empty crucibles and samples, starting the analysis which measures moisture and temperature-dependent weight changes, and viewing final results.
3. Precautions include using high quality gas cylinders, avoiding disturbing the TGA machine, and ensuring proper software and hardware are used.
1. The document outlines the operating procedure for a Thermogravimetric Analyzer (TGA).
2. It involves setting gas pressures, taring the balance, selecting diagnostic programs, loading empty crucibles and samples, starting the analysis which measures moisture and temperature-dependent weight changes, and viewing final results.
3. Precautions include using high quality gas cylinders, avoiding disturbing the TGA machine, and ensuring proper software and hardware are used.
1. The document outlines the operating procedure for a Thermogravimetric Analyzer (TGA).
2. It involves setting gas pressures, taring the balance, selecting diagnostic programs, loading empty crucibles and samples, starting the analysis which measures moisture and temperature-dependent weight changes, and viewing final results.
3. Precautions include using high quality gas cylinders, avoiding disturbing the TGA machine, and ensuring proper software and hardware are used.
2. Switch on the TGA & leave it on for 15 to !"in for balance stabili#ation . $o%ble &lic' on the TGA software. Go to $ia(nostics ,& )a'e *alance tare & +ress o' ,. Now select the Go to Option- Diagnostic Program - select .SO 5. Now clic' on wei(hts, it will as' for A"o%nt of sa"+le to test, (ive the n%"ber of sa"+les & o'. .nstr%"ent will (ive where to +%ts the sa"+le +osition. After this lid will o+en, /o% need to +%t the e"+t/ cr%cibles at the res+ective +osition on the screen. Alwa/s +%t the e"+t/ cr%cible at ! +ositions. 0. Now follow the instr%ctions on the screen caref%ll/ ()eans e"+t/ cr%cibles +lacin( & their res+ective "eas%re"ents then sa"+le +lacin( & their res+ective "eas%re"ents & then cr%cible +lacin( & their res+ective "eas%re"ents. 1. After this .nstr%"ent as' to clic' on 232&4T.52 b%tton (sto+ beco"es e6ec%tive) 7. Then re(%late the (as flow, +ress o'. 8. Then actual wor starts. 1!. See the left side corner window of software for c%rrent stat%s of )achine. 11. Once the te"+ reaches to !"#- $oisture starts % gi&es the results as soon as wei(ht stable. Then 'urnace start heating towar(s )$ measurements* & (ives the res%lts within 1 "in%ets after reachin( of 8!! 12. Then instr%"ents (o to +"" (egree % start increasing towar(s Ash temp. & res%lt will dis+la/ after (ettin( stable wei(ht loss. 1. Once all anal/sis will co"+lete * Instrument starts 'or cooling ( 75! to ,!! to 5! )& (ives indication of co"+ilation of wor' & read/ for ne6t anal/sis !,- .ou can &iew the result in Data /ase Data Report* select the particular ID % tae the printout i' nee(e(- Precaution % care while operating the TGA 1. 4se (ood 9%alit/ c/linders 2. Don0t (istur/ the position o' the TGA machine, 1INCE 23ANCE IN IN1TA33ED IN1IDE* Tr/ to avoid hand +%ttin(: e6tra +ress%re on the table where the "achine has been installed . 4se +ro+er sta/ili4e(* proper earthling suppl5 for the "achine Alwa/s %se the (ood 9%alit/ UP1 ' or PC (since so'tware % communication /oar(s o' TGA installe( in the PC6- ,- Please tae care o' TGA so'tware (ongle e5 72ac si(e o' PC6* missing o' which not a/le to operate TGA-