Shimadzu LCMS Report: Sample Information

2013-12-4 15:33:51 1 / 5
Shimadzu LCMS Report

Sample Information
LCMS
Data File
Injection Volume
Vial#
Report Format File
: MC0944-059-3.lcd
:1
: 104
: LCMS Format 1.lsr
Date Acquired
Tray#
Method File
: 12/4/2013 3:31:10 PM
:1
: A60B40+-.lcm
Chromatogram
mV
ELSD
0.98
0.97
0.00
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
min
mAU
1.323
PDA Multi 1 254nm,4nm
0.776
500
0
0.00
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
min
mAU
PDA Multi 2 214nm,4nm
1.326
1000
500
0
0.00
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.25
2.50
min
Segment#1
1.320
TIC(+)@1 (1)
1.778
1.107
0.973
1.00
0.887
0.777
(x1,000,000)
4,790,790
3.00 (-0.033min Delay)
TIC(-)@2 (1)
0.00
0.25
0.50
0.75
1.00
1.25
1.50
1.75
2.00
2.100
1.927
1.988
1.781
0.777
1.321
1.52 (x1,000,000)
1,517,880
1.00 (-0.033min Delay)
2.25
2.50
min
Integration Results for DAD
D:\Data\user\MC0944-059-3.lcd
2013-12-4 15:33:51 2 / 5
ELSD
Peak#
Total
Ret. Time
Width at 10% Height
Height
Area
Area%
PDA Ch1 254nm

Peak#
Ret. Time
1
0.776
2
1.323
Total
Width at 10% Height

0.053
0.059
Height
27799
719330
747128
Area
48329
1440459
1488788
Area%
3.246
96.754
100.000
Width at 10% Height

0.066
Height
843696
843696
Area
1981889
1981889
Area%
100.000
100.000
PDA Ch2 214nm

Peak#
Ret. Time
1
1.326
Total
Mass Spectrum
419.1
348.0
Rt=0.777min Positive
50
100
150
200
250
300
350
400
450
625.8
490.0
512.1
441.0
389.0
279.0
216.2
60.0
132.1
167.0
100000
500
550
600
650
700
750
m/z
417.0
Rt=0.778min Negative
20000
100
150
200
250
300
350
400
450
500
550
600
650
772.6
726.8
688.5
647.7
608.6
559.5
531.1
488.0
452.9
355.7
312.5
272.5
207.6
228.5
148.7
113.5
10000
700
750
m/z
274.2
30000
100
150
200
250
300
350
400
450
500
550
600
650
700
782.5
746.4
709.0
673.9
646.6
610.9
535.1
557.7
492.0
460.3
419.3
362.5
319.7
230.2
111.0
167.1
186.3
83.3
10000
318.2
20000
750
m/z
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200
400
450
500
550
600
650
700
753.9
712.0
684.6
629.7
588.0
350
534.9
300
419.4
260.6
250
347.7
150
295.2
100
167.2
130.2
83.2
10000
194.9
216.1
20000
493.8
438.0
750
m/z
250
300
500
550
600
650
700
753.0
709.5
669.5
626.5
450
591.5
400
560.7
350
504.0
448.2
200
396.8
150
342.2
360.0
100
231.8
1000
195.0
2000
153.0
129.0
3000
309.1
279.1
750
m/z
330.0
2000000
1000000
50
100
150
200
250
300
350
400
450
500
550
600
650
700
750
m/z
327.9
400000
300000
100
150
200
250
300
350
400
450
757.0
679.1
72.8
385.8
100000
463.9
200000
500
550
600
650
700
750
m/z
2013-12-4 15:33:51 4 / 5
100
150
200
250
300
350
400
450
500
550
600
650
796.3
750.5
702.5
677.7
604.3
510.6
428.9
1000
360.6
2000
276.6
166.9
187.1
3000
309.3
330.1
216.1
4000
504.1
5000
576.7
6000
110.2
83.3
700
750
m/z
480.0
40000
30000
250
300
350
500
550
600
650
700
778.3
751.7
718.2
661.0
636.9
450
577.7
400
517.9
371.7
331.6
291.8
242.0
200
266.6
173.7
144.5
150
445.9
100
396.7
50
116.5
10000
60.0
20000
750
m/z
692.0
250
300
350
400
450
500
550
600
775.4
700
750.8
650
564.5
522.9
480.3
425.8
446.6
353.2
373.9
283.4
239.5
200
689.5
150
647.8
100
165.6
109.7
5000
750
m/z
677.9
400
450
500
550
600
650
700
757.5
693.2
637.7
599.0
350
536.6
300
490.2
250
429.4
355.2
227.6
201.8
200
302.7
150
255.1
100
157.8
107.8
10000
750
m/z
2013-12-4 15:33:51 5 / 5
250
450
500
550
600
650
711.4
679.0
646.4
568.4
400
516.7
350
443.6
309.7
300
479.7
742.3
764.0
200
402.8
150
337.7
356.9
100
241.4
140.5
1000
201.5
100.7
2000
86.7
700
750
m/z

Shimadzu LCMS Report: Sample Information

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2013-12-4 15:33:51 1 / 5

Shimadzu LCMS Report

PDA Multi 1 254nm,4nm

Integration Results for DAD

Width at 10% Height

PDA Ch1 254nm

Width at 10% Height

Width at 10% Height

PDA Ch2 214nm

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