Compound

(ppm) (J (Hz))

6.56 (8) (d, 1H, H2), 6.92 (8) (d, 1H, H3), 6.89 (s, 1H, H5),
4.77 (15) (d, 1H, H7a), 4.00 (15) (d, 1H, H7b), 4.56 (m, 1H,
H10a), 4.40 (m, 1H, H10b), 3.66 (m, 1H, H8a), 3.58 (m, 1H, H8b),
3.26 (m, 1H, H11a), 3.19 (m, 1H, H11b), 2.76 (m, 1H, H9a), 2.55
(m, 1H, H9b), 2.20 (s, 1H, 4-CH3).

9.03 (sb, 1H, Mo-OH), 6.59 (8) (d, 1H, H2), 6.95 (8) (d, 1H,
H3), 6.91 (s, 1H, H5), 4.82 (15) (d, 1H, H7a), 4.03 (15) (d, 1H,
H7b), 4.57 (m, 1H, H10a), 4.40 (m, 1H, H10b), 3.67 (m, 1H, H8a),
3.58 (m, 1H, H8b), 3.26 (m, 1H, H11a), 3.19 (m, 1H, H11b), 2.77
(m, 1H, H9a), 2.56 (m, 1H, H9b), 2.49 (2H, CH2 of 4-ethyl ),
1.13 (8) (t, 3H, CH3 of 4-ethyl ).

9.05 (sb, 1H, Mo-OH), 6.60 (8) (d, 1H, H2), 7.14 (8) (d, 1H,
H3), 7.08 (s, 1H, H5), 4.80 (15) (d, 1H, H7a), 4.07 (15) (d, 1H,
H7b), 4.59 (m, 1H, H10a), 4.40 (m, 1H, H10b), 3.68 (m, 1H, H8a),
3.60 (m, 1H, H8b), 3.27 (m, 1H, H11a), 3.20 (m, 1H, H11b), 2.77
(m, 1H, H9a), 2.55 (m, 1H, H9b), 1.23 (s, 9H, 4-t-Bu).

8.81 (sb, 1H, Mo-OH), 6.95 (s, 1H, H3), 7.12 (s, 1H, H5), 4.75
(14) (d, 1H, H7a), 4.04 (14) (d, 1H, H7b), 4.54 (m, 1H, H10a),
4.40 (m, 1H, H10b), 3.65 (m, 1H, H8a), 3.47 (m, 1H, H8b), 3.31
(m, 1H, H11a), 3.17 (m, 1H, H11b), 2.81 (m, 1H, H9a), 2.58 (m,
1H, H9b), 1.31 (s, 9H, 2-t-Bu) 1.23 (s, 9H, 4-t-Bu).