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  • Three Solvents by Using The Directions Which Follow. Record Your

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    JassanitoElia
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    The document describes procedures for (1) testing the solubility of various compounds in water, ethanol, and ethyl acetate and (2) recrystallizing impure acetanilide. For the solubility test, samples of 5 compounds will be added to 3 solvents and observations will be made about solubility when cold or heated. For the recrystallization, impure acetanilide will be dissolved in hot water and filtered to remove insoluble impurities like sucrose, sand, or carbon black. The filtered solution will then be cooled to obtain purified acetanilide crystals.

    Original Description:

    organic chemistry lab report

    Original Title

    Crystal Ization

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    The document describes procedures for (1) testing the solubility of various compounds in water, ethanol, and ethyl acetate and (2) recrystallizing impure acetanilide. For the solubility test, samples of 5 compounds will be added to 3 solvents and observations will be made about solubility when cold or heated. For the recrystallization, impure acetanilide will be dissolved in hot water and filtered to remove insoluble impurities like sucrose, sand, or carbon black. The filtered solution will then be cooled to obtain purified acetanilide crystals.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
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    5 views2 pages

    Three Solvents by Using The Directions Which Follow. Record Your

    Uploaded by

    JassanitoElia
    The document describes procedures for (1) testing the solubility of various compounds in water, ethanol, and ethyl acetate and (2) recrystallizing impure acetanilide. For the solubility test, samples of 5 compounds will be added to 3 solvents and observations will be made about solubility when cold or heated. For the recrystallization, impure acetanilide will be dissolved in hot water and filtered to remove insoluble impurities like sucrose, sand, or carbon black. The filtered solution will then be cooled to obtain purified acetanilide crystals.

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    © All Rights Reserved
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    of 2

    Part1:choiceofsolvent

    Testthesolubilityof:
    (a)naphthalene()
    (b)aspirin()
    (c)acetamide()
    (d)sucrose()
    (e)benzoicacid()
    ineachofthreesolventsbyusingthedirectionswhichfollow.Recordyour
    observationsSforsolubleIforinsolubleandtheapperance
    .Havetheseresultsinitialledbythedemonstratorbeforeyouleave.
    1Weigh0.5gofthesolidtobetested(onthetoploadingbalanceto2decimalplaces),
    anddividethesampleintothreeequalportions.
    2Stironeportionwith2mLofwaterinatesttubeandrecordthesolubility.
    NOTE:Ifthematerialfailstodissolve,heattheaqueousmixtureusingthehotplateor
    steambathasyourheatsource,andrecordthesolubilityinhotwater.
    3Stirasecondportionofsolidwith2mLofcoldethanolandnotethesolubility.
    Ifitfailstodissolve,heatthemixtureinasteambathandnotetheresult.Usethelast
    portionofsolidtotestitssolubilityin2mLofcoldethylacetate,andifitfailsto
    dissolve,theninethylacetateheatedinasteambath.
    Part2(a): RECRYSTALIZATIONOFIMPUREACETANILIDE
    1Fluteapieceoffilterpaperandplaceitintoastemlessfunnel.Setthefunnelina
    beaker.
    2FitaBchnerfunneltoafilterflask.(SeeFigure1).Becertaintoclamptheapparatus
    toaretortstandwithathreeprongclamp.
    3Placeapieceofweighedfilterpaperintothefunnel,withthecurvedsurfaceofthe
    paperfacingawayfromtheceramicsurface.
    Thefilterpapershouldlieflat,coveringalltheholes.Checkthatthetrapforthevacuum
    containsnoliquid(disassembletrapanddiscardtheliquidbeforeyoubegin)
    4Obtaina1gsampleoftheimpureacetanilideprovided,whichmaycontainanyorall
    ofthefollowingcontaminants:sucrose,sand,shreddedcork,carbonblackanddirt.
    5Addenoughhotwatertotheimpuresolidina50mLErlenmeyerflaskuntilthe
    entirewhitesolidhasdissolved,allthewhile,keepingthetemperatureofthemixture
    above90C.

    Howmuchwaterisneeded?(Theapproximateanswertothisquestionmaybe
    obtainedbyconsideringthedatafromchemicalhandbooksonthesolubilityof
    acetanilide,4.3gto100mLofwaterat90C.)Recordthevolumeofwaterthatyou
    actuallyused(..)
    Whenyoufeelthattheentirewhitesolidisinsolution(remember,someinsoluble
    impuritiesmaybepresent!),pourthehotmixturethroughthefilterpapertodoagravity
    filtrationwhichremovesinsolubleimpurities(seeFigure2).
    Ifcrystalsforminthefunnelduringthisprocess,use12mLofhotwatertodissolve
    them.
    6Keepthesolutionhotbyplacingthesetuponthesteambathwhileliquidisbeing
    addedtothefunnelabove.
    Whenalltheliquidhasbeenfiltered,rinsetheremainingsolidandthefilterpaperdown
    withasmallquantityofhotwater,thenremovethefunnel.Recordtheappearanceofthe
    insolubleimpurities,ifany.Whatdoyouthinkthisresidueis?Discardtheresidueinthe
    regulargarbagepail.

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