Professional Documents
Culture Documents
of Chemical
Engineering
ISSN 0104-6632
Printed in Brazil
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Vol. 22, No. 01, pp. 143 - 152, January - March, 2005
Abstract - The filtering hydrocyclone is a solid-liquid separation device patented by the Chemical
Engineering Department at the Federal University of Uberlndia, which consists of a hydrocyclone whose
conical section was replaced by a conical filtering wall. The objective of this work is to compare the
performances of the filtering hydrocyclones designed by Bradley and by Rietema. The experimental results
obtained with the filtering hydrocyclones under the same operational conditions as those used with the
conventional device allow the conclusion that performance of the Bradley and Rietema types is significantly
influenced by the filtering medium. Rietemas filtering hydrocyclones had a lower volumetric feed flowrate
than the conventional device and Bradleys filtering hydrocyclones showed increases in this same variable. In
both designs, overall efficiency was influenced by the underflow-to-throughput ratio.
Keywords: Filtering hydrocyclone; Solid-liquid separation; Hydrocyclone.
INTRODUCTION
Hydrocyclones, also known as liquid cyclones, are
an important device for the separation of solid-liquid
suspensions (Svarovsky, 1984). The principle
employed is centrifugal sedimentation, i.e., the
particles in the suspension are subjected to centrifugal
forces, which causes their separation from the fluid.
Like centrifuges, which make use of the same
principle, hydrocyclones do not have moving parts,
require a low installation and maintenance investment
and are simple to operate. Hence, these devices are
widely utilized in mineral, chemical, petrochemical,
textile and metallurgical industries.
Aiming at combining two separation processes,
researchers in the Chemical Engineering Department
at the Federal University of Uberlndia proposed a
modification of the conventional hydrocyclone
(Barrozo et al., 1992). The conical section of a
hydrocyclone of Bradleys design was replaced by a
conical filtering wall. The resulting equipment was
*To whom correspondence should be addressed
144
Di
Feeding
L1
Overflow
Cylindrical section
Glass
Filtering section
Angle
Filtrate
Underflow (Du)
Figure 1: Trajectory of suspension for the conventional hydrocyclone and filtering device scheme
MODELLING
Residence Time Theory
There are several theories for the describing the
separation that takes place in hydrocyclones. Perhaps
one of the best known is the residence time theory
(Svarovsky, 1981). In this approach, first proposed
by Rietema (1961), a particle of a given size will be
collected if the time it remains inside the cyclone is
equal to or greater than the time necessary for it to
reach the wall. Under some assumptions, the
residence time theory yields Eq.(1) for the prediction
of cut size in cyclones:
DC
d50
=K
DC
Q ( s )
0.5
(1)
DC
Q ( s )
0.5
F ( R L ) G(C V )
(2)
where
F( R L ) =
1
1 + 1.73R L
G ( C V ) = e(
4.5CV )
(3)
(4)
D
R L = B U
DC
(5)
145
K
0.016
0.039
B
54.6
145
P
u c2
2
(8)
Km
where Rm is the filtering medium resistance and AL
is the lateral area of the cone surface, which might be
expressed as a function of the lowest radius.
Rm =
( L L1 )( Dc Dinf )
2
(9)
Conical Filtration
dP
QF
=
dr K m A L
AL = 2r ( L L1 ) +
Eu
7000
1200
(6)
C
2.61
4.75
.Rm
dr
QF
(10)
2 ( L L1 ) Pm
4
R m ln 1 +
Dinf + Dc
(11)
2 ( L L1 ) Pm
4
Q F ln 1 +
Dinf + Dc
(12)
Brazilian Journal of Chemical Engineering Vol. 22, No. 01, pp. 143 - 152, January - March, 2005
146
Dc = 3.10-2
= 0.26.10
-2
QF
L L1 = 7.09.10
-2
Patm
Dinf = 0.5.10-2
Figure 2: Filtrate radial flow across the filtering cone (dimensions in meters - not drawn to scale)
EXPERIMENTAL
dStk =
Material
The particulate material used was pyrochlore
(65% Nb2O5), which has a suitable density (s =
4030 kg.m-3). The particle size distribution of the
samples was determined by the gamma-ray
attenuation unit. Am241 was the radioactive source
utilized. The relationship between the beams counted
by the equipment and the volumetric solids
concentration (CV) in a given suspension may be
derived from Lamberts equation. Eq. (13), for
example, was obtained for pyrochlore aqueous
suspensions:
I
Cv = ( 42.74 0.55 ) ln o
I
18H
( s l ) gt
I
I
X = ln o ln o
I
I
t
(14)
(15)
(13)
Hydrocyclones
147
1.00
0.90
0.80
0.70
o
--D' :
n:
R:
0.60
Exp. Data
RRB Model
14.32 microns
0.73
0.998
0.50
0.40 7
11
15
19
23
27
31
35
39
43
47
51
55
59
63
67
dStk (microns)
Do/DC
L/DC
Angle
Rietema
0.28
0.34
5.00
200
Bradley
1/7
1/5
6.8
90
148
B2
11
10.63.10
6.5.10
6.37.10
4.95.10
R3
11
4.54.10
RC
11
where
DU
RL
R1,R2,R3
RC
1.01
RC R1 R2 R3 P B2 B1 BC
RC R1 R2 R3 P B2 B1 BC
13.4
20.8
23.4
18.4
17.4
0.26
2.91
17.1
28.4
34.4
39.2
35.4
33.2
R2
11
DU :0.003 m
48.5
50.8
52.0
30.3
45.6
R1
0.579.10
DU : 0.004 m
40.6
44.5
RL(%)
48.0
DU : 0.005 m
BC
11
29.4
Rm (m )
P
11
29.5
-1
RC R1 R2 R3 P B2 B1 BC
DU
RL =
0.5
1.69 8.66.106 ( R m D C ) DC
1
2
exp 0.69+1.06.10 21 ( R m DC )
(16)
D
0.1 U 0.167
DC
0.174.109 R m D C 5.315.109
(17)
where
D
0.1 U 0.167
DC
1.362.109 R m DC 3.185.109
filtering
147000 Pa
117600 Pa
RC R2
P
B2
R1 R3 B1 BC
176400 Pa
184
154
178
125
140
165
145
168
313
263
145
124
133
108
248
271
250
270
285
268
350
293
88200 Pa
R1 R3 B1 BC
RC R2
P
B2
153
design,
303
the
209
176
200
on
RC R2
P
B2
R1 R3 B1 BC
R1 R3 B1
P
RC R2
P
B2
Hydrocyclones
6071
5021
4284
Eu
Depending
384
( R m DC )0.092
317
290
1.66
D
RL = U
DC
309
345
where
149
1791
1874
1967
R1
R2
R3
1200
RC
B2
B1
BC
Hydrocyclones
150
Eu =
(18)
16 ( L L1 )
0.0119 + 0.0296R
L
4
DC R m ln 1 +
DC + Dinf
where
Overall Efficiency
0.174.109 R m D C 5.315.109
( 0.73)
DC
(19)
where
10221 Re 16394
D
0.1 U 0.167
DC
DU : 0.003 m
59
74
65
63
62
RC R1 R2 R3 P B2 B1 BC
77
79
83
RC R1 R2 R3 P B2 B1 BC
66
73
73
62
74
75
84
90
89
85
77
78
76
79
DU : 0.004 m
64
DU : 0.005 m
71
0.63 D U
Eu = Re( )
RC R1 R2 R3 P B2 B1 BC
Hydrocyclones
DC
Q ( s )
(1 R L )
exp ( 4.5C V )
0.5
(20)
'
DC
d50
= ( 0.036 0.001)
DC
Q ( S )
0.5
(21)
1
exp ( 4.5C V )
1 + ( 0.51 0.12 ) R L
CONCLUSIONS
The experimental results obtained with the
filtering hydrocyclones under the same operational
conditions as those for the corresponding
conventional devices, allow the following
conclusions to be drawn.
The performance of the hydrocyclones of
Bradleys and Rietemas designs is significantly
influenced by the filtering medium. The underflowto-throughput ratios of both filtering devices
underwent changes in relation to the corresponding
conventional devices increasing for Rietemas
filtering hydrocyclone and decreasing for Bradleys
filtering hydrocyclone. While Rietemas filtering
hydrocyclones had a lower volumetric feed flowrate
than the conventional device, Bradleys filtering
hydrocyclones showed increases in this same
variable. While the Euler numbers for Rietemas
filtering hydrocyclones increased move under the
same operational conditions, than that of the
conventional device, for the Bradleys filtering
hydrocyclones they decreased. In both designs,
overall efficiency was influenced by the underflowto-throughput ratio. For Rietemass filtering
hydrocyclones the underflow-to-throughput ratio
contributed to the increase overall efficiency. The
overall efficiency of the Bradleys filtering
hydrocyclones decreased compared to the
conventional device, due to the reduction in solids in
the underflow stream. Filtration and design were
equally important at the same degree for
understanding the separation process in the filtering
hydrocyclone.
B and C
CV
DC
Di
Dinf
DO
DU
'
d 50
Eu
g
H
I
Io
It
K
Km
l
L
L1
P
Patm
Q
QF
Re
RL
Rm
t
uc
NOMENCLATURE
AL
dStk
d 50
(m2)
(-)
(m3solid/
m3suspension)
(m)
(m)
(m)
Stokes diameter
cut size
reduced cut size
(m)
(m)
(m)
Euler number
gravity
position of gamma-ray
measurement
gamma-ray beams
counted for suspension
gamma-ray beams
counted for pure water
gamma-ray beams
counted for suspension
as a function of time
parameter in Eq.(1) and
Eq.(2)
filtering medium
permeability
vortex finder length
hydrocyclone length
length of the cylindrical
section of the
hydrocyclone
pressure of gas inside
the filtering cone
atmospherie pressure
volumetric feed
flowrate
volumetric filtrate
flowrate
Reynolds number
underflow-tothroughput ratio
filtering medium
resistance
time
speed of the suspension
in the cylindrical area
cumulative mass
fraction
(-)
(-)
(m)
(-)
(-)
(-)
(-)
(m2)
(m)
(m)
(m)
(kg m-1s-2)
(kg m-1s-2)
(m3 s-1)
(m3 s-1)
(-)
(-)
(m-1)
(s)
(m s-1)
(-)
Greek Letters
(m)
(m)
151
, s
Brazilian Journal of Chemical Engineering Vol. 22, No. 01, pp. 143 - 152, January - March, 2005
(m)
(kg m-1s-2)
(kg m-1s-1)
(-)
(kg m-3)
152
ACKNOWLEDGMENTS
It is necessary to acknowledge our gratitude to the
Postgraduate Program in Chemical Engineering at the
Federal University of Uberlndia, to the FAPEMIG,
CNPq and to the CAPES, Brazilian institutions that
made available the resources necessary for the
development and conclusion of this work.
REFERENCES
Allen, T., Particle Size Measurement, 5th ed.,
London: Chapman and Hall, 524p. (1997).
Barrozo, M.A.S., Damasceno, J.J.R. and Lanna, A.E.,
Estudo do Desempenho de um Hidrociclone