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Vaal University of Technology Faculty of Engineering and Technology Department: Chemical Engineering Baccalaureus Technologiae: Engineering: Chemical
Vaal University of Technology Faculty of Engineering and Technology Department: Chemical Engineering Baccalaureus Technologiae: Engineering: Chemical
SUBJECT CODE
808509006
DATE
JUNE. 2007
DURATION
3 HOURS
EXAMINER
Dr PO OSIFO
MODERATOR
Mr WA du Plessis
MARKS
TOTAL: 131
FULL: 125
REQUIREMENTS:
Calculators
Graph paper must be provided
INSTRUCTIONS:
Answer all questions
Number clearly and correctly
ENGLISH QUESTION PAPER CONSISTS OF: 4 TYPED PAGES PLUS ANNEXURE
1, 2, 3, 4, 5, 6, 7, & 8
Question 1
(a)
[32]
State whether the behavior between shear stress and shear rate is time independent
for the following fluids. Explain briefly the effect of increasing shear rate on their
apparent viscosity.
i)
thioxotropic
ii)
rheopectic
iii)
shear thinning
iv)
shear thickening
[8]
(b)
Show that the pressure drop through a centre line for non-Newtonian fluid
obeying Power Law flowing through a pipe is:
Where
(c)
The apparent
viscosity of the modified fluid is equal to the viscosity of the original liquid at
shear rate of 1000 s"1. Determine the liquid maximum velocity in the pipe and
also the velocity if the liquid is a Newtonian liquid.
[12]
Question 2
(a)
[32]
Show that the frictional pressure drop for fluid of density p flowing through a
straight pipe of diameter D and length L is:
APS
L
2fpV2
D
(b)
[8]
(c)
Water (p = 988 kg/m and JJ, = 1 cP) is steadily pumped between two reservoirs.
The difference in elevation of the two reservoir surfaces is 30 m. All the piping is
51 mm diameter steel and its length is 122 m. if the volume flowrate is 0.006
m3/s. Find the power required to run the pump. The steel pipe roughness is e =
0.000051 m.
2
Open globe
valve
30 m
p entrance
Fully open
gate valve
= 6.90
= 1.0
[12]
Question 3
(a)
[20]
(c)
[4]
A crude oil with a viscosity of 0.5 cP and specific gravity of 0.895 is flowing
through a 0.1 m inside diameter horizontal pipe. An orifice meter consisting of an
orifice plate and a differential mercury-glycol manometer (mercury is the
manometric liquid (specific gravity 13.6) and glycol (specific gravity 1.15) is the
sealing liquid) is used to measure the volumetric flowrate of crude oil. If the
manometer reading is 0.6m, corresponding to a volumetric flow rate of 1.3 x 10"3
m3/s, estimated the diameter of the orifice and also the power lost due to the
pressure drop by the orifice plate. Assume Co = 0.61.
[16]
Question 4
(a)
[22]
A spray dryer containing a hot air (80 C, viscosity = 0.018 cP) is used to dry a
molten detergent sprayed from the top of the dryer. The molten detergent formed
into a small size particle before it gets to the bottom of the dryer which is 30 m
high. If the particle diameter is 1 mm and a density of 1200 kg/m3, what would
be the terminal velocity of the particles assuming free settling? Mw of air is 29
kg/kmol
[12]
(b)
A bed has a height of 5.0 m and a void fraction of 0.33. A gas with a density of
1.25 kg/m3 and dynamic viscosity of 1.5 x 10"5 N s/m2 flows steadily through it.
The size of particles in the bed is 0.005 m diameter and the sphericity Os is 1.
The pressure drop is 150 N/m2. Calculate the superficial velocity.
[10]
Question 5
[25]
(a)
[5]
(b)
A curve-blade turbine with six blades is installed centrally in a vertical tank. The
tank is 2 m in diameter; the turbine is 0.66 m in diameter and is positioned 0.66 m
from the bottom of the tank. The turbine blades are 82.5 mm wide. The tank is
filled to the depth of 1.83 m with a base solution at 65.5 C which has a viscosity
of 15 cP and density of 1200 kg/m3. The turbine is operated at 150 r/min. The
width baffled rod is 198 mm.
(a)
(b)
What would be the power requirement be in the vessel if the tank is unbaffled?
[10]
Annexure 1
1.
Momentum correction factor
(3=! Ju2dS
SV 2 s
2. Kinetic correction factor
2sJ
a=
SV
3.
Flow measurement
V1^
4.
-=jx'pD''
K=D\gp(pyp)
For Re < 1
C D = 24/Re,
u t = gDp(Pp ~P\
FD = 3
For 1000<Re>200,000
C D = 0.44,
5.
F D =0.055:ru t Djip
Minimum fluidization
\.75pV2OM
ut= 1^
gD p ( P p
-p)
0169509773
i CJ q C> o
i o o' o o"
4ii
'
in* SphorH
DUkj
,_ Cvllnc on
ico
_i
10
**"
C ih
l.o
0,!
mm-.
_
V*
nirnfir
Tm ' f| T M " mP
.. 1 ill,. rJ IILI ' HI 11
,1
,1 Jl;III 1 1 III
*
III 1
n.
i MM
Drag coefficients for sphorcs, disks, and cylinders. [By permission from J. H. Perry and
D, W. Green (eds.), Chemical Engineers'Handbook, 7th ed.. p. 6-51. Copyright, 1997,
McGraw-Hill Book Company,]
Io
~'
0169509773
Aimcxure3
0.33
0.33
d.33
0.33
0.25
0.29
0,2
0.12S
FIGURE 9.12
Power number N, versm A/,, for nU-bltida turbine*. {After Chudaetk1 *; O / . f o W M Wiih Ihe dinhd
portion of eurvo D, (he vuliie of N, reud from tho fifluro must be multiplied by /V-.
Curva
A
B
Pitch
T,S:1
1.SH
S,
S,
O.30 0.SO
0.30 0.30
S,
1.0
1.0
I !
10*
N^ m O'.nola
TCURE 9.13
P t U I D MBCHANtCS
i|
TABLE 9J
Values of constants Kc and ATr for baffled tanks having four baffles at tank
wall, with width equal to 10 percent of the tank
diameter
Fiflure
rj three blAdea
Pitch ].0*
Pitch | . 5 "
Turbine
Six-btade dlik" (S, - 0 . 2 5 , ^ - 0 2 )
cU,hdM(ff4Wj
Six pitched blades" (45* SA ~ o >)
Four pitched blade." (45*. St . " o n
laLpaddlertworlJiaa*'"^
41
55
6S
70
i.
Lines
9.12
LO
40.0
0,32 9.13
0,87
VI
18.0
5.7J
4.B0
1.63
T27"
1.70
0.35
To:*69E061360017S312328 P.9'13
0169509773
\
10'"
'
"I
'
o - Absolute roughneea, m
10* L. di-lnBldaplpodtamotor.m
. 10*
10*
Figure 2.2
Plot of-^fRe" against Reynolds numbor
111
W
FIGURE 7.7
Plot of exponent/i versus Re,, for Eq. (7,46).
1.0
" - ^
o.s
0,6
'i
> S
0.2
MCM- 0,5
P
0.6
0-7
0-8
0.9
FIGURE 8.19
Ovorull pressure loss in orifice mcicra. (After American Society of
1.0
To:*69206136EI017631S3S8 P. 10'13
0169509773
Viscosities of Liquids'
No,
Liquid
No.
1
Acetaldehyda
2
Acetic ucid, J00%
3
Acetic nnhyclride
4
Acetone, 100%
5
Ammonin, 100%
6
Ammonia, 26%
7
Amyl acctolo
8
Amyl alcohol
9
Aniline
10
Aniaole
..-. .
11
Benzene
,
12
Blphenyl
13
Brine, CaCJj, 25%
14
Brino, NuCl, 25%
15
Bromlna
16
Butyl acetate
17
Butyl alcohol ~
18
Cnrbon dioxides
19
Carbon disulflda
20
Cnrbon tetrachlorlda
21
Chlnrobenzuno
22
Chloroform
23
m-Crcsol
24
25
26
27
2a
29
30
31
63
64
65
12.2
8.9
9.1
13,8
14.3
16.6
11.5
No.
Liquid
A'
3.2*
15.2
25,8
24,8
21.3
13,7
12.7
12.3
Toluene
Trichlorocthylena '
Vinyl ttcemto
Wnter
oXylcno
m-Xylcno
/-Xylono
13,7
14,8
14,0
10,2
13.5
13,9
13,9
10.4
10,5
7.0
70
71
72
73
74
75
Dicbloroeihune
Dichloromethane
Ethyl ucetale
Bthyl nlcohol.l00%
Bthyl alcohol, 95%
Bthyl alcohol. 40%
Ethyl benzeno
Liquid
66
67
68
69
15.2
12.1
12-7
14.5
12.6
10.1
II, 8
7.5
8.1
12.3
-12.5
12,0
6.6
10,2
14.2
12.3
8,6
ll.fi
16.1
12.7
12,3
J4.4
2.5
2.9
13.2
J4.fi
13.7
10.5
9,8
6.5
13.2
Cyclohcxnnol
No.
Liquid
10.2
11.9
14,2
14.4
7.1
4.8
14.2
12.8
7,2
2.0
.13.9
12.5
18.4
1B.7
13.5
10.9
18.3
15.9
16.6
13.2
11.0
17.2
0.3
7.5
13.1
12.4
10.2
20,8
24.3
76
32
Ethyl chloride
33
Bthyl ether
34
Ethyl formate
35
Ethyl iodide
36
Bthylone glycol
37 . Formic acid
38
Proon-12
39
Olyccrol, 100%
40
Olycerol. 50%
41 ' Hepiano
42
Hcxana
43
Hydrochloric ncid, 31,5%
44
Iuobutyl A l c o h o l
Kerosene
Linseed oil, raw
Mercury
Mothnnol, 100%
Methyl ncotnio
Methyl chloride
Mothyl othyl koiono
Nupthalenc
Nitrfeacid, 95%
Nitric;, add. 60%
Nitrobenzene
Nitnotolucnc
Octane
Octyl alcohol
Psnwne
Phenol
Sodium
16.4
.13.9
8.8
13.0
111
10,6
10-9
To:*6920613600176312328 P.11'13
0169509773
t
.
Tomporatura
!$;
y '
Vlscotily
Cnntlpoliaj
r- 100
r 80
Dag. C Dog.F
200 - 380
190-
180 - - 360
170 - - 340
160 - - 320
> 40
150 - - 300
140 - - 2 H 0
130 - 260
120- - 240
110 -220
100 - 200
30
r 10
28
90 - i
00 - - 1B0
7 0 - - 160
60 - - UO
50 - - 120
40
30 -
- 100
26
24
-4
22
20
- 2
ia
16
U
- 00
>
(
12.
20.-60
10>-40
10'
S
6
-20
-10- 0
4
0.2
2
2
-30 - f
r o.B
-20
To:*692061360017S312328 P.12'13
0169509773
APPENDIX W
No.
Gas
Y 'i /
No.
Gun
14,3
13.0
14.9
20.0
29
30
31
Freon-113
Helium
Hcxane
Hydrogen
3Hj H- Nj
Hydrogen bromide
Hydrogen chloride
Hydrogen cyanido
Hydiogen iodide
Hydrogen Bulfide
Iodine
Mercury
Methane
Methyl ulcohol
Nitric oxida
Nitrogen
Nitrosyl chloride
Nitrous oxide
Oxygen
Pennine
Propane
Propyl alcohol
Propylene
Sulfur dioxido
Tbluene
2,3,3-Trimelhylbuuine
Water
Acetic add
7.7
2
3
Acoiono
Acetylene
8.9
Air
5
6
7
8
.12
13
Ammonin
Argon
Benzene ~
Dromlne
Butane
Butylene
Carbon dioxide
Carbon disulfiilo
Carbon monoxide
14
Chlorine
15
16
17
Chloroform
Cyanogen
Cyclohcxnno
Ethane
Bthyl acetate
Ethyl alcohol
Ethyl chloride
Bthyl ether
Eihylcnc
Fluorine
Froon*11
Preonl2
Prcon-21
Preon-22
10
11
18
19
20
21
22
23
24
25
26
27
28
-"A
9,8
11.0
8.4
10.5
.'
32
16.0
22,4
13.2 .
33
34
8.9
9.5
19.2
13.7.
13-0
16.7
36
37
38
39
8,0
16,0
40
n.o
9.0
20.0
8.9
9.2
9.2
9.1
8.5
9.2
8.5
8.9
9.5
7.3
15,7
15.2
12.0
41
42
43
44
45
46
1.3.0
15.1
23.8
IQ.6
15.1
8.5
8.9
9.2
18.4
14.5
13.2
14.2
15.6
11.1
16.6
10.H
15.3
17.0
10.1
35
47
48
49
50
51
52
53
54
55
56
Xenon
X
11,3
10.9
&.6
11.2
11.2
y
14.0 .
20.5
11.8 *
12.4
17.-2'
8iS
2bl9'
8.B
I8."7
14.9
9.8
9.0
8.6
9.0
5.3
9.9
8.5
10.9
10,6
21.3
18.018,4
22.9
15.5
15.6
20.5
20.0
8,0
17.6
8.8
19.0
21.3
L2.8
12.9
L3.4
13.8
1.7-0
12.4
n.o
7.0
9.7
8,4
9.0
9.6
8.6
9.5
8.0
9.3
10.5
16.0
23.0
1074
~"
~ "
I o : *b3CO&iOOi3t)i i D J i c o c o
0169509773
8: Viscosities of Gnaoa
1075
- L1
Tamparaluro
Vlscoilty'
ContipoUos
Dag, C, Dag. F.
-100 -
p 0.1
- 0.09
- 0,0Q
- 0.07
r 0.06
\- 0,05
- 0,03
- 0.02
-001
- 0.009
- 0.008
-
10 12 14 16 IB
- 0.007
r-O.006
'- 0.005
ViscoBities of gases nnd vnpors nt 1 fltmj for coordinates, sec tnble on previous page.
T l