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ASTM
ASTM
Vivek Chaudhary
Manisha Gupta
Mohd. kashif
Grp No-4
Objective
To carry out the ASTM distillation of given gasoline sample(ASTM D86).
Apparatus/Materials Used
Theory
This method gives the distillation range of petroleum products. It is applicable to organic
liquids such as hydrocarbons,oxygenated compounds,chemical intermediates and blends
thereof.
The distillation charactristics give a broad indication of fuel type.Being a measure of voltality
,they determine the system of fuel metering required (wick feed,carburation or
atomization),and are indicative of the vapourisation behaviour of fuels in storage (vapour loss
& vapour lock),and in piston-engine manifolds (uniformity of distribution to cylinders).The
extent of the distillation range for any given fuel is representative of the availability of that fuel
from the parent crude oil.
The IP designation of ASTM distillation is IP123/83 and the corresponding ASTM designation
is ASTM D86-78
Observations:
• Room temperature=25.0oC
• Temperature of condenser bath=29.0oC
• Volume of gasoline sample taken=100.0 ml
Sources of errors/precautions
• Temperature of te condenser bath was not equal to 0.0 oC.It was equal to 29.0 oC
,which is very high as compared to 0.0 oC.
• Heating rate was not equal to the prescribed heating rate in ASTM
INTERNATIONAL manual.According to the prescribed heating rate ,2 drops per
second of condensate should fall in the cylinder .In the experiment performed , just
one drop was falling in the cylinder in one second.
• Capacity of the flask for holding the gasoline sample was not equal to 200 ml.
• Thermometer readings should be read carefully.