20 nm

20 nm

30 nm

80 nm

60
50
40
30
20
10
0

15.0
ppm (11)
60
50
40
30
20
10
0

15.0
ppm (11)

10.0

5.0

0.0

100

50

10.0
ppm (11)

5.0

0.0

-5.0

10.0

5.0

0.0

Tranamltance (%)

90
80
70
60

50

3500

3000

2500 2000 1500

Wave No. (cmG 1)

1000

Tranamltance (%)

90
80
70
60
50
40
30
20

4000

3500

3000

2500

2000
1500
Wave No. (cmG 1)

1000

500

50 nm

170 nm

1-CNTs (MWCNTs+Aspartic) -DWP (H) -FA (60)

50

0
8.0
ppm (y 1)

100
f-CNTs: MWCNTs+Aspartic
acid in DMF

300

200

100

15.0

10.0

5.0

0.0

300
250
1-CNT (H2SO 4+HNOS)
-DMP-FA

200
150
100
50
0

15.0
DDM (y1)

10.0

5.0

0.0

7.0

6.0

5.0

4.0

3.0

2.0

1.0

0.0