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Parameters for condition monitoring of oil service Two ways are available to an operating engineer 1. To make periodic oil tests to establish trends and classify them. 2. To conduct dissolved gas analysis to assess the internal condition of transformers PARAMETERS TO BE CHECKED ARE:
1. 2. 3. 4. 5. 6. 7. 8. FLASH POINT DIELECTRIC DISSIPATION FACTOR SPECIFIC RESISTANCE NEUTRALISATION. MOISTURE CONTENT SLUDGE % BREAK DOWN VOLTAGE D.G.A.
PHYSICAL CONTAMINATION
1. Dust, fibre, metallic, particles, other solid impurities. 2. Dissolution of varnish. 3. Free and dissolved water.
CHEMICAL DETERIORATION Oxidation resulting in acids sludges and polar impurities. CONTAMINATION OF GASES a) Dissolved air from atm. Nitrogen, co2 b) Generated in oil, methane, ethane, acetylene, ethylene etc.Before the oil is put in the transformer, its properties should be fully ensured.
Catalyst RH (Hydrocarbon) R* + O R* + H (Free radical) RO2* (Peroxy radical) RO2* + RH RO2*H+ R* (Hydro per oxide)
2 RO2* R* + RO2* 2 R*
Oxidation products (Higher Temperature metal Ions as catalyst favours the reaction)
Hydrocarbon RH first produces a free radical R. The radical R now combines with the available oxygen giving peroxide RO2. First product of oxidation peroxides reacts with any hydrocarbon (RH) giving hydro peroxide RO2H and another free radical R. this type of chain propagation continues till the chains are broken adding suitable inhibitor.
SERVICE OIL TESTS The service oil tests to be conducted are furnished below: Service oil tests as per IS: 1866 2000
Sl. No. 1 Interfacial Tension 2 Neutralisation Number 3 Moisture content (ppm) 4 Flash point Acid present in the oil Reveals total water content or cellulosic deterioration. Sudden drop in flash point indicates of unsatisfactory working condition of transformer. Indicated deterioration Sludge present in the oil. TESTS INFORMATION PROVIDED BY TESTS
Sludge
Dielectric strength
Resistivity
Reveals ppm of combustible gases dissolved in the oil to assess the internal condition of the transformer.
INSTALLATION DATA
Filled on. Commissioned on.. Maximum load... Maximum oil temperature.. Normal load Normal Oil Temperature
MAINTENANCE OF DATA 1. Date of sampling.. 2. Topping up done up. Type and quantity of oil added 3. Note on abnormal operations... 4. Oil filtered on... 5. Breather reconditioned on 6. Physical observation
7. Tests conducted: a. Interfacial Tension. b. Neutralisation Number c. Moisture content (ppm) d. Flash point e. Sludge f. Dielectric Dissipation Factor g. Dielectric Strength h. Resistivity
TABLE 1: APPLICATION AND INTERPRETATION OF TESTS ON OIL IN TRANSFORMERS AS PER IS: 1866 1983 Sl. N o. 1
Equipment voltage
Characteristic
Action if outside permissible limit Recondition it the value of dielectric dissipation factor permits, reclaim if not. Reclaim
All voltages
0.1 * e12
0.2 1.0
Sl. No
Characteristic
Equipment voltage
0.5
Reclaim
No perceptible sludge Decrease in flash point 15c (max) of the initial value, minimum value 125 c
Reclaim
Flash point
All voltages
Sl. N o
Equipment voltage
All voltages 145 kv + above < 145 kv > 72.5 kv < 72.5 kv > 145 kv < 145 kv
Electric strength
Is: 6792
Water content ppm, max Specific resistance @ 90, 10 E12 ohm, cm Tan delta @90, max
Is: 335
Is: 6103
Is: 6262
IS: 1448
0.5
IS: 6104
0.015
125
ALL VOLTAGE
IS: 1866
NIL
GENERAL Properties Breakdown voltage Moisture Dielectric dissipation factor Volume resistivity IFT Condition Low High High Filtration as above if the cause is moisture or other Low Low Reclamation Remedies
NV
HIGH
FP
LOW
SLUDGE %
HIGH
DE-SLUDGING
SUGGESTED LIMITS FOR IN SERVICE OILS GROUP I BY VOLTAGE CLASS, BASED ON IS: 1866-1983 LIMITS
___________________________________________________
VOLTAGE CLASS PROPERTIES 145 KV & ABOVE 50 (MIN) 0.1 (MAX) 0.015 (MIN) 0.2 (MAX) 25 (MAX) 0.1x1012 72.5 KV & < 145KV 40 (MIN) 0.1 (MAX) 0.015 (MIN) 1.0 (MAX) 35 (MAX) 0.1x1012 BELOW 72.5 KV 30 (MIN) 0.1 (MAX) 0.015 (MIN) 1.0 (MAX) 35 (MAX) 0.1x1012
ELECTRIC STRENGTH NEUTRALISATION VALUE (mgKOH/g) INTERFACIAL TENSION N/m DIELECTRIC DISSIPATION FACTOR AT 90 C WATER CONTENT, ppm SPECIFIC RESISTANCE Ohm-cm
Suggested limits for in service oils group ii by voltage class (reconditioning) based on IS: 1866-1983 LIMITS
PROPERTIES VOLTAGE CLASS - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -------------145 KV & 72.5 KV BELOW ABOVE & < 145KV 72.5 KV
< 50 0.1 UPTO 0.5 < 0.015 (MIN) > 0.2 < 40 0.1 UPTO 0.5 < 0.015 (MIN) > 1.0 < 30 0.1 UPTO 0.5 < 0.015 (MIN) > 1.0
Electric strength Neutralisation Value (mg.KOH/g) Interfacial Tension N/m Dielectric dissipation Factor At 90 C Water Content, ppm Specific resistance Ohm-cm
TABLE IV Suggested values for in-service oils group II by voltage class (reconditioning) based on IS: 1866 (1983)
LIMITS Voltage Class Properties 145 Kv & Above
Electric Strength < 50 Neutralisation Value 0.1 (mg KOH/g) Upto 0.5 Interfacial Tension < 0.015 N/m Dielectric Dissipation > 0.2 Factor at 90 C Water Content, ppm > 25 Specific Resistance < 0.1 Ohm-Cm
Below 72.5 Kv
< 30 0.1 Upto 0.5 < 0.015 > 1.0 > 35 < 0.1
GROUP III OILS: To categorize under group III, the parameters should be well beyond the limits proposed in table IV. Such oils should be initially filtered under vacuum and temperature to verify whether the properties improve or not. If properties like Dielectric Dissipation Factor, Interfacial Tension do not improve on filtration, then there is a case for oil to be replaced.
IFT
Acidity
18 38
0.0321 0.0392
0.914E12 0.046E12
30 30
0.1 0.3
4 5
220 / 11 220 / 11
27 35
0.0108 0.263
2.75E12 0.912E12
30 30
0.1 0.1
IFT
Acidity
45 47 11 8 24
30 30 30 30 25
Acidity
IFT 10 10 15 10 15 15 10
29 -
24 29 37 44
Acidity
IFT
44 30 39 33 29
10 15 15 10 15
Contd
5 5 5 5 5
33 / 11 33 / 11 33 / 11 33 / 11 33 / 11
63 27 22 18 15
15 10 10 10 10
CONCLUSIONS
a. In view of the importance of service oil tests, all tests have to be carried out as per IS: 1866 systematically and periodically, as a part of maintenance schedule, as no single test is a reliable indicator. b. The periodic testing will help O & M personnel to build up databank and case histories of power Transformers. c. Periodic testing will help to know the oil condition as well to know growing of any incipient faults by Dissolved Gas Analysis. d. The preventive maintenance followed by all utilities will result not only savings in O & M costs but also prevent any premature breakdown / Failures besides improving the overall system reliability.
Test required to assess the level of oil degradation Screening tests: - Laboratory evaluation can be minimised by performing screening tests at site. The tests are: 1. Appearance i. Colour ii. Visible particles iii. Haziness or cloudiness 2. Acidity by colour CPRI acidity testing kit 3. Interfacial tension test By field method 4. Quality index By Myers method
A portable acidity testing kit was developed by cpri to quickly check the acidity of transformer oil at site Procedure: A) 1.1 ml of oil in a test tube. B) Add 1ml of rectified spirit. C) Shake well D) Add 1 ml. of alkaline solution E) Add few drops of universal indicator F) Match the colour with the colour chart to arrive at the acidity value. Advantages: Test can be performed by semi skilled personnel at the site of transformer / remote areas.
<72.5
72.5 to 170
> 170
Appearance
Clear, free from sediment and suspended matter 0.89 0.89 0.89
140
140
140
0.03
0.03
0.03
Water content, ppm, min Interfacial tension, N/m, min Dielectric Dissipation Factor @ 90 C, 40-60 Hz, max Resistivity, ohm-cm, min Breakdown voltage, kV, min Oxidation stability of uninhibited oil Neutralisation value, Mg.KOH/g, min Sludge (% by Mass), max oxidation stability of inhibited oil - induction period
20 35 0.015 6 40
15 35 0.015 6 50
10 35 0.010 6 60
0.4 0.1
0.4 0.1
0.4 0.1