Preparation of the NaOH Solution

Mass of NaOH before standing

= NaOH before standing (g) beaker
(g)
= 111.490 g 110.970 g
= 0.520 g
Mass of NaOH after standing = NaOH after standing (g) beaker (g)
= 111.500 g 110.970 g
= 0.530 g
Standardization of the NaOH solution
TRIAL I
Volume of NaOH solution
= Final reading of buret - Initial
reading of buret
= 13.80 mL 0.00 mL
= 13.80 mL
Converting the Volume (mL) to Volume (L)
Volume (liters)

= Volume (mL) x
= 13.80 mL x

1L
1000 mL

1L
1000 mL

= 0.01380 L
Moles of potassium acid phthalate =
=
Moles of NaOH solution

Massgrams
Molar Mass

0.150 g
204.2g/mol

= 0.000735
= Moles of (HKC8H4O4) x

Mole Ratio of NaOH

Mole Ratio of HKC8H4O4
= 0.000735 mol x

1 mol NaOH
1 mol KHC8H4O4

= 0.000735 mol
Molarity (NaOH)

Moles (NaOH )
Volume (liters)

0.000735 mol
0.01380 L

= 0.053 M
TRIAL II
Volume of NaOH solution
reading of buret

= Final reading of buret - Initial

=27.20 mL 13.80 mL
= 13.40 mL
Converting the Volume (mL) to Volume (L)
Volume (liters)

= Volume (mL) x
= 13.40 mL x

1L
1000 mL

1L
1000 mL

= 0.01340 L
Moles of potassium acid phthalate =
=
Moles of NaOH

Massgrams
Molar Mass

0.150 g
204.2g/mol

= 0.000735
= Moles of (HKC8H4O4) x

Mole Ratio of NaOH

Mole Ratio of HKC8H4O4
= 0.000735 mol x

1 mol NaOH
1 mol KHC8H4O4

= 0.000735 mol
Molarity (NaOH)

Moles (NaOH )
Volume (liters)

0.000735 mol
0.013 4 0 L

= 0.055 M
Average Molarity (NaOH)

Molarity ( NaOH ) TRIAL I+ Molarity ( NaOH ) TRIAL II

2
0. 0 53+0.0 55
= 2
= 0.54 M
Titration of Soft drink samples with NaOH solution
Soft drink sample 1 TRIAL I
Volume of NaOH used (mL)
= Final reading of buret - Initial
reading of buret
= 7.20 mL 0.00 mL
= 7.20 mL

Moles of NaOH

= Molarity x Volume (NaOH)

= (0.054 mol/L) (7.20/1000) L
= 0.003888 L or 3.89x10-4 L
Soft drink sample 1 TRIAL II
Volume of NaOH used (mL)
= Final reading of buret - Initial
reading of buret
=
=
Moles of NaOH
=
=
=
Soft drink sample 2 TRIAL I
Volume of NaOH used (mL)

7.70 mL 0.00 mL
7.70 mL
Molarity x Volume (NaOH)
(0.054 mol/L) (7.70/1000) L
0.004158 L or 4.16x10-4 L
= Final reading of buret - Initial

reading of buret
Moles of NaOH

=
=
=
=
=

Soft drink sample 2 TRIAL II

Volume of NaOH used (mL)

18.40 mL 7.20 mL
11.20 mL
Molarity x Volume (NaOH)
(0.054 mol/L) (11.20/1000) L
0.0006048 L or 6.05x10-4 L
= Final reading of buret - Initial

reading of buret
Moles of NaOH

=
=
=
=
=

Acidity of Soft drinks

Soft drink sample 1 TRIAL I
Moles of citric acid

17.20 mL 7.70 mL
9.50 mL
Molarity x Volume (NaOH)
(0.054 mol/L) (9.50/1000) L
0.000513 L or 5.13x10-4 L
= Moles of (NaOH) x

Mole Ratio of citric acid

Mole Ratio of NaOH
= 3.89x10-4 L x

1 mol citric acid

1 mol NaOH

= 3.89x10-4 L
Soft drink sample 1 TRIAL II
Moles of citric acid
= Moles of (NaOH) x

Mole Ratio of citric acid

Mole Ratio of NaOH
= 4.16x10-4 L x

1 mol citric acid

1 mol NaOH

= 4.16x10-4 L
Average molarity of acid (M) =

Molarity of citric acid TRIAL I+ Molarity of citric acid TRIAL II

2
0.0195 M +0.0208 M

= 2

= 0.0202 M
Soft drink sample 2 TRIAL I
Moles of citric acid
= Moles of (NaOH) x

Mole Ratio of citric acid

Mole Ratio of NaOH
= 6.05x10-4 L x

1 mol citric acid

1 mol NaOH

= 6.05x10-4 L
Soft drink sample 2 TRIAL II
Moles of citric acid
= Moles of (NaOH) x

Mole Ratio of citric acid

Mole Ratio of NaOH
= 5.13x10-4 L x

1 mol citric acid

1 mol NaOH

= 5.13x10-4 L
Average molarity of acid (M) =

Molarity of citric acid TRIAL I+ Molarity of citric acid TRIAL II

2
0.0303 M +0.0251 M

= 2

= 0.0280 M
Mass of citric acid present in an 8 ounce bottle (g)
Soft drink sample 1 8 ounces
= 0.24 L
Mass
= (Molar mass) (Molarity) (0.24 L)
= (193.132 g/mol) (0.202 M) (0.24 L)
= 0.936 g
Soft drink sample 2 8 ounces
= 0.24 L
Mass
= (Molar mass) (Molarity) (0.24 L)

= (193.132 g/mol) (0.280 M) (0.24 L)

= 1.30 g