| peeves ENHANCING Or PERSONAL oN Aquaflex® SF-40 A Versatile Hair Fixative PolymerERFORMANCE- ENHANCING FRODUCTS PERSONAL CARE. INTRODUCTII Aquaflex SP-AO resin is designed to rreet the needs of the global hair care market. Aquafiex $F-40 resin is a new patentee, mutti-use, high performance, versatile. global hair fixative polymer. It is cffectiva in $84 VOC, AAS VOC and anhyttrous hair spray pump and aerosol systems. ‘Acuafiex SF-40 resin possesses a unique combination of characteristics; it is a water-soluble hair fixative polymer With nigh propetant tolerance. Aquafiex SF-40 gives superior hold at lov solids levels in high humidity conditions and does not require neutralization. Products can be created with a flexible or stiff feel, just ‘by modifying the percent salics in the formulation, Key features of Aquaflex SF-40 resin: @ Effective in 55% VOC, 80% VOC and anhydrous systems © Yields both floxible fool and stiff Yeo! finished products @ Requires no neutralization © Extremely high propellant tolerance © Hydrolytically stable © Has excellent high humidity curl retention © Provides superior holding at low solids © Low tack © Fast dry times © Suitable for either pump or acrosol systems @ Low solution viscosity in 55% VOC formulations. When formulators are faced with reducing VOC's, they must remove alcohol and/or propellants. and replace these ingredients with water or non-VOC propellants. By increasing the water cantent of Nair spray formulations, the Formulator may be faced ‘with the following issues: larger particle size. poor spray Patterns, can corrosion, polymer hydrolysis, and compatiblity issues with solvents, propetants and additive ingredients, Performance of the hair spray is also compromised with decreased hald, increased tackiness. beading on the hair. style droop and longer dry times. In high VOC systems, when replacing alcohol with more propellant, formulators can encounter hydrocarbon intolerance with certain polymars. ‘Aquafiex SF-40 resin, a new product from Internationa! Specialty Products (ISP), solves most of the formulation problems associated with adding more water or more propellant.CONSUMERS’ NEEDS Consumers require a hair spray that remains in place under the highest humidity conditions, that ismot wet and sticky on their hair, and maintains their style after comb through. ‘A new type of hair spray consumer is also emerging: one who realizes that he or she does not have to sacrifice hold for a hairstyle that is flexible to the tauch. FORMULATORS’ NEEDS | ‘The objective of the formulation chemist is to find a product that meets all necessary regulatory requirements as well as the performance demands af the marketplace. In the USA, this translates into developing hair sprays Which meet low VOC requirements and match the performance of current products. Aquaflex" SP-40 resin atlows the formutator to accomplish both goats In Europe. the current trends are flexible products with good hold, Aquaflex SF-40 resin affers flexible film and excellent curl retention. It has high hydrocarbon tolerance, making the cest of the formulation lower. Aquaflex SF-40 resin is compatible with up to 60% hydrocarbon propeltant, dependent upon the ethanol ‘used. With 200 proof ethanol, 60% hydrocarbon tolerance is achieved, while 40% hydrocarban tolerance Is achieved If 190 proof ethanol is used, In regions where a crunchy, stif fect hair style is preferred, formulatars can develop this type of product by adjusting the solids content of the Aquatlex SF-40 resin in the system, or by blending other ISP pyrralidane rocucts in the formulation. rN ad Aquafiex SF-40 is a terpolymer of vinyicaprotactam: {VCL). Vind Pyrrolidane (VF) and Dimethylaminopropy! ‘methacrylamide (DMAPA) and is supplied as 40% solits in-ethanol. Vinylpyrrolidone and DMAPA acrylates are welrproven building blocks of hair care potymers providing a pseudo-cationic nature at low pH ano water solubility. The incorporation of Vinyicaprolactamn into the structure results in outstanding hytrocarbon compatibility, by virtue of the sequence of five -CH2- Coroups in its rina. Structurally, Aquaflex SF-40 resin can be represented as: INCI Name: PVP/VinylcaprolactariDMAPA Acrylates Copolymer CAS No: 180005-72-5 a” eee Relative Viscosity * 130-140 % Solids: 38.0 -42.0 ‘% Moisture 2.0 max, ‘Color (APHA) 100 max. pH (50% solution in D.1. HO) 70-85 Haze (NTU) 20 max, ‘Specific Gravity @ 25°C 0.9165 (as is) Refractive Index @ 25°C.=598 nm 1.427 (as Is) Mw (Relative to PEO standards) (37,500 Polydispersity (Wy / Mad 34 Tere) 138 (oven-dried) 1% polymer solution in ethanol with @,051A LINQ, in ‘Cannon-Fenske tube size 75. NOTE: The above is typical of current production, ‘Sales specifications are available upon requestaU ete) Rea | ee ioe Lag er We) cy With the irtraduction of Aquafex® SF-40, ISP has Many of the same attributes which make Aquaftex developed a hair ative resin which will meet all the ‘SF-40 an excetient hair spray resin, suct as exe feel Needs of consumers and formulators outlined in this ‘and long lasting hold, make it a superior resin for gees. brochure. It allows the farmulator to substitute water spray gels, mousses and other styling products. for alcohol or propellant without the inherent problems _—_in adaftion to the fhative characteristics mentioned, these have caused in the past. It does not require consumers are also looking for products with good neutralization. Aquaflex SF-40 resin is a liquid, stying properties, namely, good comabilty. bocifying making processing easier. Thus. Aquaflex SF-40 satisfies effects. negligible tack and shine, Aquafler SF-40 resin the consumer, the formulator and government ives the formutstor a product to address the nosds of regulations for low VOC, asit is equally effective in 55% this market. VOC, 80% VOC and anhydrous systems. PERFORMANCE DA’ Aquafiex SF-40 is a film former with outstanding performance as.a hair fixative, Its high hokding power per Unit weight of resin means that it can be formulated at lower levels (as low as 1.5% solids) than most traditional fixative polymers. This holding ability is maintained under high humidity conditions, despite the pelymer’s solubility in water. Figure 4 llustrates curl retention properties of Aquafiex SF-A0 in a 4% resin solids pump formulation Asdepicted below. the tresses cons'stently maintained high hold even at a wide range of VOC bevels, Figure 1: Curl Retention Study - Four Cell - 4 Hr, StudyAquatles* SF.40 exhibits negligible tack in systems ranging from high to low VOC. Figure 2 llustrates the tack of an optimized 5% VOC pump spray as compared to other VOC levels. The data in figure 2:clearly shows that the addition of water does not increase tackiness. Any VOC level product based on Aquaflex SF-40 resin can achieve low tack by pump optimization, Figure 2: Tack Duration Aquaflex SF-40 Subjective Evaluation 60.07 50.0 4 g 40 i 3004 & 200 “ iz ool Tack Duration 1H Aqueous Pump (25% voc) Ml 55% VOC 80% vor © Box voc DB High voc Figure 3. Hair characteristic measurements of Aquafiex SF-A0 at a full range af VOC resins. Figure 3: Hair Characteristics Aquaflex SF-40 ‘Subjective Evaluation Stiffness Aromat ya) NI pyar 2 ss BE Aqueous Pump (2.5% VOC) ML 55% VOC 60% VOC Pump @ 88% voc Pump © High vocAquaflex* SP-40 is an extremely versatile resin, yielding both flexible hold and stiff feel finished products. ‘Stifiness represents how the tress feels to the tauch. This parameter is important to some consumers, as the Stfmess of the tress has been equated with the effectiveness of the product. To meet the needs of this consumer, Sprays based on Aquafiex SF-dO resin can be made stiffer by increasing the percent solids in the formulation, or by [blending it with other ISP pyrrolidone based polymers like PVP K-30 for aerosols and PYPIVA E-735 for pumps. ‘or gum rosin. Figure 4 ilustrates that a 55% VOC pump spray with 3.5% resin solids level of Aquaflex SF-40 is as stiff as two commercially avalable 80% VOC pump hair sprays based on acrytamide. when measured by Oynamic Hair Spray Analysis techniques. Figure 4 Stttness profile versus two commercial BO% hair sprays based on acrylamide eee s le = : eae — feet eee a Sas me | SES A new hair spray trend is occurnng. 4 fast growing consumer segment realizes It does not have to sacrifice hold for a product that is flexible to the touch, This segment requires products that exhibit good hold, and are also flexible. Faure 5 ilustrates the resin at 4% resin solids versus three commercial products based on acrylate dimethicone capalymer. ‘The Aquaflex SF-40 aerosol product exhibited higher stiffness than the natural and extra hold product. but was more ‘flexible than the maximum hold preduct. Ifequivalent stifiness § required, a higher resin load can be used. Conversely, reducing the resin load wil rhake the product more flexible, supporting the claim that Aquaflex SF-40 is a versatile resin. Figure 5: Comparison of Stitiness Ratios for a $5% VOC Aquafiex SF-40 Formulation ws. ‘Natural Hold. Extra Hold. and Maximum Hod Commercial Aerosat Systems ‘Based on Aerylate Dimethicone Cepalymer. ‘Serene ag Oma a9 er‘The fetlowing section ilustrates how problems commonly 28sociated with the addition of more water ‘Yo-a formulation are resaheed in systems based on ‘Aguatiex’ SF-40 hair fixative polymer. HYDROLYTIC STABII One of the problems encountered upon switching a hair fiative formulation from an antydrous system to a water containing system is the hytrolytic stability of the resulting product, Aquaflex SF-40 resin was designed specifically to circumwent these problems. ‘The polymeric structure of Jiquaflex SF-40 contains cithor acid functionality or ester groups that could hydrotyze te acids. The aming groups. which impart ‘edditional holding characteristics to the resin, are ‘attached to the polymer backbone through hydrolytically stable amide linkages. CORROSION RESISTANCE For low VOC aerosol products, the addition of water to the hair spray system increases the potential for corrosion. When manufacturing. only deionized water should be used in the compaunding, Tap water containing as little as 15 ppm of chlorido will accelerate corrosion, In addition, both liquid and vaper phase inhibitors are needed in the formula. The use level for liquid phase inhibstors is 0:1 - 0.4% and for vapor phase inhibitors 0.1 - 0.3% After extensive corrosion screening, the following inhibitors have been shown to be effective in'55% VOC systems: Ingredient Inhibits Corrosion in Dimethyl Oxazclidine Vapor Phase Ammonium Hydroxide Vapor Phase MEA Borate and MIPA Borate Liguid Phase MOLECULAR WEIGHT The molecular weight of Aquafiex SF-40 resin was specifically designed to deiver a spray pattern with good Particle size while maintaining the hold characteristics ‘that make it an effective hair spray at any VOC level Refer to the summary chart for details SOLUBILITY Aquaflex SF-40 resin is soluble in water, ethanol, anc low VOC mixtures. Since itis soluble in water as well as. alcohol, Aquaflex $F-40 is easily removed from the har by shampoo in hat of cold water. The incorporation of \vinylcaprolactam into the polymer leads to increased hydrocarbon compatibility and improved solubility,HYDROCARBON TOLERANCE Aquafiex* S#-40 resin has excellent compatibiity wth all types of aerosol propellants. In high VOC formulations, dependent upon the ethanol used. Aquaflex SF-40 is, ‘compatible with up to 60% hycrocarbon propellant. With 200 proof ethanol, 60% hydrocarbon tolerance is achieved. while 40% hydrocarbon tolerance is achieved with 190 proof ethan, Aquaflex SF.40 resin is also compatibie up to 80% with DME. ‘Tnisis a crttcal feature in partsof the world where systems tend to have a high degree of propellant andt high hydtrocerbon tolerance is necessary. Figure 6 reflects, ‘the absolute tolerance of the polymer in different propellant systerns. This ceearlyillustrates that Aquaflex SF-40 is extremely propellant tolerant at levels above ‘thase normally usd Figure 6: Propellant Compatibility Aquafiex SF-40 @ 5% Solids % Propellant eS88ee8ees ot 1 0c A4G MDME [11523 MI CAP 40 Paget The broad solubility spectrum of Aquaflex SF-40 resin allows considerable flexbilty in the formulation ofall types of hair Ficatives and styling products. in pump sprays, the ppolyrner may be blended with virtually any ratio of alcohol to water. Sods lewols up te 5% are possible without arty spray characteristic deterioration. In water-based styling products, Aquafiex SF-40 exhibits ‘good curl retention under extreme humidity conditions and provides bodifying. and shine benefits. ei Teale) Aquafiex SF-40 resin is easy to incorporate into. formutatiens and is compatible with most common cosmetic ingredients, Neutralization is not required. Aquaflex SF-40 is supplied as a solution, making processing easier since there isno dissolving stage. ‘The reiatively law viscosity of the ethanolic solution supplied makes the product easily purnpable. ‘The following formulations were selected fram our Global Technical Service Laboratories to illustrate this polymer's formulating flexbiity. Formulations imparting a Soft feel through to a stiff feel in both pumps, aerasols and mousses are included.Flexible Hold 55% VOC Pump Hair Spray ‘with Aquaflen SF-40_ Formula 10596318 Ingredients: we % 0 Alcohol 40-8 200") 80.50 Water 41,95 Aquafiex F-40 730 FUP! vinyt Caprotactarrd DMAPA Acsylates Copotymer Cyclomethicore 08 Total 100.00 Resin Sots: 3.00 Procedure: 1. Add alcoho! ard water to main tank. ‘Start moana, 2, Aaks the Aquattex SF-49 and mix until completely dessatved, 3 Add the remaining ingredient; ‘mixing unti uniforen. Pump Used: Seaquist Euromist Il (160 me. output) 0,018" 0.010" Deep 0.060" Tubing 1.9. ‘ Calmar Mark V1 VEL 31 Flexible Hold 80% VOC Pump Hair Spray ‘with Aquaflen SF-40) Fermuta 10596-32-8 Ingredients: we. 9% SD Alcohial 4048 (2007 7550 Water 1695 Aquatiex S¥-40 130 VPI vinyl Caprotactary DAUAPA Acrylates Copolymer Cyclomethicone ‘aos Total 100.00 ‘9% Resin Solids: 3.00 Procedure: 1, Add alcohol and water te main tank, ‘Start moing. 2, A Une Aquafiex SF-a0 2nd mix Until completely disse. ‘3. Ada the remaining ingredient: ‘mixing until uniform. Pump Used: Seaquist Euromist It (160 mel. output} 0.018" %0.010" Deep 0.060" Tubing FORMULATIONS Flexible Hold High VOC Pump Hair Spray with Aquafiex SF-40 Formula 10596-53 Ingredients: WE. SD Alcohol 40-8 (200°) 92.45 Aquafiex SF-40 750 PvPr nyt Capretactarn’ MAPA scrylates-Copolymer Cyciomethicone 05, Tetal 4100.00 Se ResinSoids: 3.00 Procedure 1. Ad aleohol to main tank. ‘Start mang 2. Ade the Aquaftex SF-€0 and ric Until completely cessatre. 83. Ad the remaining ingrediont: ‘ming until uniform. Pump Used: Seaqulst Euromist It (160 mel, output) 0.018" X 0,010" Deop 0.660" Tubing 10.Stiff Feel Stiff Feel Stiff Feel 55% VOC 80% VOC jh VOC Pump Hairspray Pump Hairspray Pump Hairspray with Aquafies SF-40 resin, with Aquaflex SF-40 resin, ‘with Aquafiex SF-A0 resin, and PVP K-30 and PVP 1-30 ‘and PVP K-30 Formula 10596-30-8 Formula 10596-28 Formula 10596:29 Ingredients: Wt | Ingredients: ‘We. 9 | Ingredients we 6 [5 Aicohol 40.8 (2007) 4150. | SO Aone! 40-8 (200) aso | SD Alcohol 40:8 (2007 710 water es | Water 14960 | Aquaflex SF-40 1250 ‘Aquaflex SF-40 12.80 | Aquatiex:5f-40 12.50 | FVPrViny! Caprotactamy PVP Vinyl Caprolactarn! PAPI Ving Caprotactarnd DMA Aerytates Coponymer DMAPA Acrylates Copotymer DMAPA Acrylates Copolymer Pur K30 030 PvP K30 20 | PpyPK.30 ogo | vr Pp iP Dirnothicene Copoht 010 ‘Dimethicone Copoiyol 0.05 | Dimethicone Copotya! 010 — Total ‘100.00 Total 100.00 Total 100.00 ‘% Resin Solds| 5.30 ‘% Resin Solids: 5.30 Procedure: Procedure: 1. std alconol and water to rain tank. | 1. dl alcotal to rain tari Start mizing. Start mixing 2. Add the Aquaflex SF.A0 and mix 2 Add the Aquaflex $40 and mix until completely dissolved. until completely dissolved, until completely dissolved. 3. Add the PVP K-39, end mix until 3. Add the PVP K-30 and Dimethicone | 3. Add the PVPIK-30 and Denethicone homogeneous. (Copotyok: mic until uniform. CCopatyal mix until uniform, 4. Add the remaining ingrediant: mixing until unifoer. Pump Used: Pump Used: ‘Seaguist Euromist II (160 mcl.output) | Seaquist Euromist tl (160 mel. output) Purp Used OIE" K 0.010" Deep 0.060" Tubing LO. | O.018" x o.010" Deep @.060" TuDIRg LO. Seaquist Curomist I (100 met. outpat) 0.018" x 0.010" Deep 0.060" Tubing LO. o Colmar Mark Vi WL 31 FORMULATIONSFlexible Hold 55% VOC Aerosol Hair Spray with Aquaflex SF-40 resin Formula 19529-131-8 logredients Wt. 56 | Ingredients: wow Water aiss | water 16.55 50 Alcohot 40-0 (200) 15.50 | SO Alcon 40:8 (200°) 40.50 Aquatiex 5F-40 7.50 | Aquafien st 40 730 PAPI Vinyl €aprotactamy MAPA Acrylates Copotymer Bimethicane Copatyal 0.25 | Bimethicone Copotyot 02s Ammonium Hynde 0.10 | Ammonium Hyeiroxie 0.10 MEA Borate and MIPAorate 0.10 | MEABbrate and MIPA Borate 0.10 (nner Exner 35.00 | Dimetryt Eter 38.00 Total i000 Total "700.00 ‘6 Resin Solids: 3.00 % Resin Sols; 3.00 Procedure: Procedure: 1, Aid alcoho! and water to main tank | 1, Add aicohol and water te main tank, Start mixing. Start moxng, 2. Add the Aquaflex SFO arct mix 2, Add the Aquaflex $F-80 and mix tunti'completely dissolved. until completely dissolved. 3. Add the Dimethicone Copayol, ‘Ammonium Hydroxide, and MEA Borate/MlIPA Borst inetvicualy. Flexible Hold 80% VOC Aerosol Hair Spray with Aquattex SF-40 resin Formula 1059627 3. Add the Dimethicone Copolyl Acnerienium Hydeoscl, and MEA BorateMIPA Borate individually. ‘Mex unta hemagenaus after each ‘Mix unt homogenous after each ‘adaition. addition. <4. Fil inta cans and pressurire 4, Filinto cans and pressurize ‘Valve Used, ‘Valve Used: ‘Seaquist ST-74 ‘Seaqust ST-74 ‘018° x Capliory Boay x O.O1S VT 101030" 1D or OOS" x Capitiary body x 0015" VT x 0.080" 1D ‘Button: ST 150 Misty 0.023" Misty orifice ‘O.018" x Capiary Booy x 0.018" YT 0.030" 1 Button: SST 150 Misty 0.023" Misty erifico FORMULATIONS Flexible Hold High VOC Aerosol Hair Spray with Aquafiex SF-40 resin Formula 10596-26 Ingredients: wi ‘SD Alcohol 40-8 (200°) S128 Aquaflen SP-40 730 PYPr Vin! Capraisctar 1 Add alcohol to main tank, Start mang, 2. Rad the Aquaflex SF-a0)and mix ‘ntl completely dissolved 3. Add the Dimethicone Copal, ‘mic thar oughly. Fillinto cans and pressurize. Vatee Used: Seaquist $T-74 0.018" x Capilary Body x 0.015°VT 0,030" 1D Button: SST 150 Misty 0.023" Misty onticeStiff Feel Extra Hold 55% VOC 80% VOC Aerosol Hair Spray Aerosol Hair Spray With Aquafiex SF-A0 resin, ‘with Aquaflex SF-40 resin and PP K-30 Formula 10529-133 Formula (0474-283, Ingredients: We % SSD Alcohal $08 (200°) 39.00 Water 15.70 ‘Aquatiex SF-90 10.00 PVP) Vinyl Caprotactamy DMAPA Acryiates Copolymer Dimethicone Copelycl ou MEA Borate / MIPA Borate 0. Arieronium Hytroxide 0.19 Total 100.00} Dimetnst Ether 38.00 % Resin Solids: 580 Total 400.05 % Fesin Solids: 4.00 Procedure: Procedure: 1, Acid alcohol to main tank, 1) Add alcohol and water to main tank. Start mixing. ‘Start mixing. 2, fad the Aquaflex SF-49 and mix 2, Add the Aquafiex:SF-40 and mix ‘until completely dissoived, ‘until completely dissolved, 3. Aad the P¥P K-30. ana moc unt 3. Acd the Dimethicone Copoty. hornogeneous. Mix thoroughly and vat 4, Pil into cans and pressurize Iharnogeneaus. 4. Add the MEA Borate/ MIPA Borate Valve Used: ‘and Ammonium Hydroxide. Seaquist ST-74 Max thoroughly between each adeitien 0.013" x Capitary Body 0.015" VTx and unti hemegeneeus, (050K LD. 5. Fil into cans and pressurize. Button: ST-1500.023" Misty orifice ‘Valve Used: ‘Seaquist ST-74 ‘Q.O18" x Capillary Body £0,018" VT 0.990" 10 Button ‘ST 150 Misty 0.023" Misty orifice FORMULATIONS Stiff Fee! High VOC Aerosol Hair Spray with Aquaflex SF-40 resin and PVP K-30 rormus 10300-25 Ingredients: Wt % SO Alcott 40-8 (2007) 5085 ‘Aquaflen SF-40 1275 PVP ¥inytCaproiactamy DA acrylates Copoymer Pve na 040 PvP Prepanefaobutane (2080) 30.00 Total 100.00" % Resin Solids, 5.50 Procedure: 11 Add akabo to main tank, Start ming 2. Add the Aquaflex SF-#0 and mix nti completely dissohed. 3. Add the PVP K-30.and mix unt homogeneous. 4. Pllinto cans and pressure. Vane Used: Seaqust ST-74 0.01.3" x Capalary Boy x 0.018" VT x 0.050" 1.0. Button: ST 150 0,023" misty erficeQuick Dry, Extra Hold 55% VOC Aerosol Hair Spray with Aquafiex SF-40 resin ‘and Escalol® S77 Formula 1046-87 Ingredients: We. 96 ‘Water a7 ‘SD Alcohol 23-4 2052 ‘Aquatiex S40 10.00 [PVP Vin! Caprotactar /BMAPA ‘Acrylates Copabyner Dimethicone Copal a0 PPG-12-PEG-6S Larolin a0 Escalol® 577 aor Beraephenore-4 Ammonium Hycroxide ous MEA Borate and MIPA Borate 0.15 Dimethy! Ether 30.00 Total 1000 %ResinSoids: 4.00 Procedure: |) Add alcohol and water to main tank. Start mixing, 2 dd the Aquaflex $F-49 and enix until complete dissohed. |. Add the Dimethicone Copoty. PPG: 12-PEG-65 Lanoin, and Escalol $77 Indeidually, Mix until heenogenious after each addition. 44, Ad the Aenmonium Hydroxide ant [MEA BorsteiM4IPA Borate separately, ‘and mix until completely dissolved. '. Fill into cans and pressurize. Vane Used Seaquist ST-74 0.018" x Capttary Body x 0.015" VT 6.030" 1 Button: ST-150 Misty 0.023" Misty enfice FORMULATIONS Extra Hold 55% VOC Aerosol Hair Spray ‘with Aquaffex SF-0 resin Formula 10396-1 Ingredients: we ‘SD Alcohol 40-8 (200°) 25 ‘water 11.99 Aquatiex SF-49 ens ‘PvP Viry Caprotactam fom ‘cryiates Copolyner ‘Giycerin 0.10 PEGTS Lanalin 0.10 Panther oot MEA Borate/MiIPA Borate 020 ‘aenmoniura Hyeiraide Isobutane Hydrofiuorecarbon 1524 Total "100.00 Resin Solis: 3,90 Procedure: 1, Ad alcoho! an water to rain tank, ‘Start mixing. 2, Ad the Aquilex SF-40 and mix until completely cssatved. 3. Add the Gyoenn, PEG-75 Lanotin, ‘and Panthexal. ‘Mix thoroughly between each addition ‘and unti hemogenceus, A, Ade the MEA Borate /MIPA Borate ‘and Ammaniuim Hydrext0 ‘Mix thoroughly between each addition and unti homogeneous. 5. Fil inta cans and pressurize: Isobutane fist, then ‘Mydreftuorecarbon 52a. ‘Valve Used: Seaquist $1.74 0.018" x Capillary Body x 0.015" YT 0.030" I Button: ‘ST-150 Misty 0.023" Misty once Conditioning Styling Mousse Normal Hold swith Aquaflex SF-40 resin Formula 19596:37 Geemaben It Prepyene Gal (re Dizol Urea (an Methylparaton (ard) Peepytparaben Propane / Isobutane (2080) Total 100.00 Procedure: ‘Add water to main tank. Start miaing and dissolve Oleth 20, 2 Add the remaining ingredients in Order listed anc ma until completely ‘issolwd between each ackstion. 3. Alinto cans and pressure Standard mousse vahe and actuator recommended,Ultra Hold Styling Mousse Natural Styling / Conditioning Mousse with Shine with Aquaflex SF-40, Ceraphyl® 69, with Aquafiex SF-40 resin Ceraphyl® 65, Ceraphyi® 41, Formula CH-90125-5 Germaben® Il, and Surfadone® LP-200 Formula ¢-9620-CH Ingredients: Wee Ingredients: We % i an | Oth 20 os0 ‘Aqusflex SF-49 730 PNPMing! Caprotactarn! DIMAPA Acrylates Copolymer Metty/ Gluceth-10 1 Dimetticone Copayet 0.10 Panthenol C1215 Alt Lactate Propane Isobutane 20/80) 8.00 Germaben® I 9.50 — Tota! 100.00 Methylparaben (and) Propyiparaben Cetrenenium Chieiso 050 Surfadone® LP.300 010 Laura Pyrroicone Propane/ Isobutane (20/00) #00 Total 100.00 Procedure: Procedure: 1, Add wate to main tank. Start mixog | 1. aaa water to mai tank Start mixing sacl enone Oath 20, ‘and cissoive Oieth 20. 2. Add the remaining ingredionts in ‘order listed ard mix until completely disselved between each addition. 3. Fil into-cans and pressurize, 2, fla the remaging ingredients in order Rsted and mbcuntit cormpletety dissolved between each addition. 8. Filinto cans aad pressurize ‘Standard mousse valve and actuator enna Standard mousse valve and actuator recommended‘The table below summarizes Key performance characteristes of hair fuative and styling polymers and Hlustrates haw Aquaflex* SF-40 resin performs at different VOC levels. Polymer(s) Tested Aqueous SS% VOC BO VOC = BBKH VOC High VOC Flim Clarity 5 5 4 3 5 (=Car. i=Opaqee) Hard Film 6H 6H 6H 6H 6H (eHare3es0mt) pH 760 8.00 850 8.60 8.30 (oR aston) —_(1oRRAMatN) (10M ten) High Humidity Curt Retention 99% 899% 98% 939% 94% Scirin 0 FOAM High Humidity Curl Retention 989% 63% 36% 90% 93% A (0 HF ‘Quick Drying (Dry Time) 48 seconds 24 seconds Si seconds 41 seconds. 36 seconds, Low Tack (Duration of Tack) 25 seconds 1S seconds 23 seconds 11 seconds 1 seconds Stiffness 26 8 712 72 60 (aS Aso Non-Flaking (Gn Comb) 7 8 8 8 8 ((Oene fatog. taba cored) Non-Flaking (On Hair) 3 8 3 8 10 (ste fakcg. (ata cones) Shiny 8 9 9 9 9 (1am. Good Combatuity 4 8 5 5 8 {10n0 comb dria, corn as) ‘Curl Snap 9 9 9 9 6 (1o-migh cur ome eu Particle Size Dlv.0.5)" 26um eam ‘96um 4m ‘i6um Spray Pattern (Inches) 412 4 4 4 342 Sprayability Sometaege fe sproy fee spr0y fe spray very fine spray parties ‘Spray Rate (gramsisecond) 16 1a 13 15 is *seagat Euro Aaya, Cray sca Caf Garman nt Sarde re rae cerewost0 aap icrerotin Spoealy eae. ‘are outst en Aaya 540 covered US. Pate Ho. 56595 andrea patents nd