Yee 20309-987 10/17/05 494795 10/17/05 01925200 WILL CALL 1 SHIP TO: soto To: NITOR METAL, S.A. NITOR METAL, S.A. CARRETERA VIA LOS POLONES CARRETERA VIA LOS POLONES SECTOR LA FLORIDA ALI PRIMERA SECTOR LA FLORIDA ALI PRIMERA ANACO EDO ENZAOTEGUI ANACO EDO ENZAOTEGUI 1 413015. 50NQT Pc 1 4130 NQ&T Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -75 Deg. F Rough Machined 1/4" to finish: 15.50"0D x Solid x 9.50"0AL TAG: Item# 7 (WO# 20309-987, PO# 01925200) HEAT# P2166-1 2 413023.00NQT pc. 4130 NQ&T Forging per FSM 2005-06, Rev, K, dtd 3/27/01, Charpies 20/15 @ -75 bee’ \ Rough Machined 1/4" to finish: 23.00"0D x Solid x 5.00"0AL TAG: Item# 3 — (WO# 20607-986, PO# 01925200)"HEAT# P2930-1 wen == 3 413021. 50NQT 4130 NQ&T Forging per 3/27/01, Charpies 2 to finis TAG: Item (Wo# 20796-9898 Deg. F Saw Cut x14.625" Block 0) HEAT# P4616-2 4 413021.50NQT 4130 PC 1 FSM 2005-06, Rev. K, dtd Og 3/2) ¢ 20/15 @ -75 Deg. F Saw Cut to x 14.40" x 15.10" Block Tac! Wo} 88, PO# 01925200) HEAT# P4616-2 Continued on Next PageSTAR METALS, IWC. 2K HOUSTON. Tx. 77280.0460 20309-987 10/17/05 947-95 10/17/05 01925200 WILL CALL 2 SHIP TO, SOTO NITOR METAL, S.A. NITOR METAL, S.A. CARRETERA VIA LOS POLONES CARRETERA VIA LOS POLONES SECTOR LA FLORIDA ALI PRIMERA SECTOR LA FLORIDA ALI PRIMERA ANACO EDO ENZAOTEGUI ANACO EDO ENZAOTEGUI VENEZUELA 5 413021. 50N 6 413021.50N VENEZUELA Qt PC 1 4130 NQ&T Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -15 Deg. F Rough Machined 1/4" to finish: 21.50"0D x Solid x 17.125"0AL TAG: Item# 4 (WO# 20796-988, PO# 01925200) HEAT# P4616-2 QT PC 2 4130 NQ&T Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -75 Deg. Rough Machined 1/4" to finish 21.50"0D x Solid x 22.00"0AL > TAG: Item# 5 & 6 — 7 (Wo# 20796-988, PO# 01925200) HEAT# P4616-2 INVOICE NO. 43390 DATE 10-17-05 AMOUNT $14872.00 SHIP WEIGHT: 9111 144324 NICA24FIVE STAR METALS, INC. EOE eae Pe ee ast INVOICE Houston, TX. 77280-0460 INVOICE No: 43390 CUSTOMER CODE: 144324 Nic424 To: SHIP To: NITOR METAL, S.A. NITOR METAL, S.A. CARRETERA VIA LOS PILONES CARRETERA VIA LOS PILONES SECTOR LA FLORIDA ALT PRIMERA SECTOR LA FLORIDA ALI PRIMERA ANACO EDO ANZOATEGUI, VENEZUE! ANACO EDO ANZOATEGUI, VENEZUELA inv pare Sa VIA Foe TERMS (10F70s WILL CALL ORIGIN PAYMENT IN ADVANCE Fou wo SALESWAN CUSTONER P.O. 20796-988 FSM (01925200 Payable in Houston, Harris County, Texas in United States Dollars cuanmry TEM NUMBER DESCRIPTION unt price [UW | —exrennep pmce T 413021. SONOT 2557.0000 BC 2557.00 4130 NQ&T Block Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -75 Deg. F, Saw Cut to finish: '14.625" x 14.625" x 14.625" Block TAG: Item# 1 1 413021. 50NOT. 2629.0000 PC 2629.00 4130 NQ&T Block Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -75 Deg. F, Saw Cut to finish: "14.40" x 14.40" x 15.10" Block TAG: Item# 2 1 413021. 50NOT 2734.0000 PC 2734.00 4130 NO&T Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -75'Deg. F Rough Machined 1/4" to finish: 21.50"OD x Solid x 17.125*OAL TAG: Item# 4 2 413021. 50NQT 3476.0000 PC 6952.00 4130 NQ&T Forging per FSM 2005-06, Rev. K, dtd 3/27/01, Charpies 20/15 @ -75'Deg. F Rough Machined 1/4" to finish: 21.50"0D x Solid,x 22.00*OAL TAG: Item# 5 & 6 SUBTOTAL —14872.00 TOTAL TAXES 0:00 TOTAL FREIGHT 0:00 SALES TAX EXEMPTION NUMBER: EXPORT TOTAL ~14872.00Five Star Metals, Inc. P.O. Box 800460 + Houston, Texas 77280-0460 + 713 466-1491 + FAX 713 466-6027 CUSTOMER: NITOR METAL, S.A. CERT. NO.: P4616-2 CARRETERA VIA LOS POLONES REC. DATE: 09/28/2005 SECTOR LA FLORIDA ALI PRIMERA SHIP DATE: 10/17/2005 ANACO EDO ENZAOTEGUI VENEZUELA W.O. NO.: 20796-988 P.O. NO.: 01925200 ory. FSM NO. DESCRIPTION wr. EA. 1 PC 413021.50NQT 4130 NQ&T FORGING PER 735 Las FSM 2005-96, REV. K, DTD 3/27/01, CHARPIES 20/15 @ -75 DEG. F SAW CUT TO FINISH: 14.625" X 14.625" X 14.625" BLOCK TAG: ITEM #1 TEST BAR SIZE: 4" X 4" X 8" BAR DIA: 0.505 MELT PRACTICE: EFVD/LR REDUCTION RATIO 4.2:1 NO WELD REPAIRS NOTE: ALL FORGINGS HAVE BEEN HEAT TREATED IN THE SAME HEAT TREAT LOT UNLESS OTHERWISE STATED, YIELD STRESS IS 0.2% OFFSET. GAUGE LENGTH IS 2" FOR 1/2" BAR. CHEMICAL ANALYSIS PHYSICAL PROPERTIES HEAT NO.: P4616-2 CODE: #29 YIELD STRENGTH: 86,168 MILL: ELLWOOD TENSILE STRENGTH: 107,743 00.33 CR: 01.07 ELONGATION: 26.00% MN: 00.55 MO: 00.23 RED. OF AREA: 73.00% + 00.009 CU: 00.18 TEST BAR BRINELL: 228/235 00.002 AL: 00.015 FORGING BRINELL: 224/231 00.23 VA: 00.028 10MMK10MMCHARPY: 84/68/85 2 00.17 cB: ‘TEST TEMP.: -75F LCVN FE: BAL : JOULES : MLE: .047/.040/.049 r SHEAR FRAC.: 65/60/70 DELTA FERRITE RETAINED AUSTENITE: HEAT TREATMENT: FORGINGS &, TEST BAR NORMALIZED: 1675F 20.00 HRSAIR QUENCH: 1600F 20.00 HRS WTR TEMPER: 1200F 23.00 HRS AIR QUENCHANT: WATER START TEMP: 64F END TEMP: 88F We hereby certify that all test results and procedure information contained herein are correct and true as cont: company. ed in the records of the BY:Five Star Metals, Inc. P.O. Box 800460 + Houston, Texas 77280-0460 + 713 466-1491 + FAX 713 466-6027 CUSTOMER: NITOR METAL, S.A CERT. NO.: 4616-2 CARRETERA VIA LOS POLONES REC. DATE: 09/28/2005 SECTOR LA FLORIDA ALI PRIMERA SHIP DATE: 10/17/2005 ANACO EDO ENZAOTEGUI VENEZUELA W.O. NO.: 20796-988 P10. NO.: 01925200 ory. FSM NO. DESCRIPTION Wr. EA. 1 PC. 413021.50NQT 4130 NQ&T FORGING PER FSM 2005-06, REV. K, DTD 3/27/01, CHARPIES 20/15 @ -75 DEG. F SAW CUT TO FINISH 14.40" X 14.40" X 15.10" BLOCK TAG: ITEM #2 TEST BAR SIZE: 4" X 4" X 8" BAR DIA: 0.505 MELT PRACTICE: EFVD/LR REDUCTION RATIO 4.2:1 NO WELD REPAIRS NOTE: ALL FORGINGS HAVE BEEN HEAT TREATED IN THE SAME HEAT TREAT LOT UNLESS OTHERWISE STATED, YIELD STRESS IS 0.2% OFFSET. GAUGE LENGTH IS 2" FOR 1/2" BAR. CHEMICAL ANALYSIS PHYSICAL PROPERTIES HEAT NO.: P4616-2 CODE: #29 YIELD STRENGTH: 86,168 MILL: ELLWOOD TENSILE STRENGTH: 107,743 C: 00.33 CR: 01.07 ELONGATION: 26.00% MN: 00.55 MO: 00.23 RED. OF AREA: 73.00% PH: 00.009 CU: 00.18 TEST BAR BRINELL: 228/235 SU: 00.002 AL: 00.015 FORGING BRINELL: 224/231 SI: 00.23 VA: 001928 10MMX10MMCHARPY: 84/68/65 NI: 00-17 cB: TEST TEMP.: -75) N FE: BAL JOULES : MLE: .047/.040/.049 SHEAR FRAC.: 65/60/70 DELTA FERRITE RETAINED AUSTENITE: ‘T_TREATMENT: _FORGINGS_§ TEST BAR NORMALIZED: 1675F 20.00 HRS AIR QUENCH: 1600F 20.00 HRS WIR TEMPER: 1200F 23.00 HRS AIR QUENCHANT: WATER START TEMP: 64F END TEMP: 88F We hereby certify that all test results and procedure information contained herein are correct and true as contained in the records of the ‘company . BY:Five Star Metals, Inc. P.O. Box 800460 + Houston, Texas 77280-0460 + 713 466-1491 + FAX 713 486-6027 CUSTOMER: NITOR METAL,S.A CERT. NO.: P4616-2 CARRETERA VIA LOS POLONES REC. DATE: 09/28/2005 SECTOR LA FLORIDA ALI PRIMERA SHIP DATE: 10/17/2005 ANACO EDO ENZAOTEGUI VENEZUELA W.O. NO.: 20796-988 P.O. NO.: 01925200 ory. FSM NO. DESCRIPTION Wr. EA. 1 PC 413021.50NQT 4130 NQ&T FORGING PER 841 1 FSM 2005-06, REV. K, DTD 3/27/01, CHARPIES 20/15 @ -75 DEG. F ROUGH MACHINED 1/4" TO FINISH: 21.50"0D X SOLID X 17.125"OAL TAG: ITEM #4 4" X 4" xX 8H BAR DIA: 0.505 EFVD/LR REDUCTION RATIO 4.2:1 NO WELD REPAIRS NOTE: ALL FORGINGS HAVE BEEN HEAT TREATED IN THE SAME HEAT TREAT LOT UNLESS OTHERWISE STATED, YIELD STRESS IS 0.2% OFFSET. GAUGE LENGTH IS 2" FOR 1/2" BAR. CHEMICAL ANALYSIS PHYSICAL PROPERTIES HEAT NO.: P4616-2 CODE: #29 YIELD STRENGTH: 86,168 MILL: ELLWOOD TENSILE STRENGTH: 107,743 C: 00.33 CR: 01.07 ELONGATION: 26.00% MN: 00.55 MO: 00.23 RED. OF AREA: 73.00% PH: 00.009 CU: 00.18 TEST BAR BRINELL: 228/235 SU: 00.002 AL: 00.015 FORGING BRINELL: 224/231 SI: 00.23 VA: 00.028 10MMX10MMCHARPY: 84/68/85 NI: 00.17 cB TEST TEMP.: -75F LCVN PE: BAL : JOULES : : ML E: .047/.040/.049 SHEAR FRAC. : 65/60/70 DELTA FERRITE: RETAINED AUSTENITE: HEAT : FORGINGS & TEST BAR NORMALIZED: 1675F 20.00 HRS AIR QUENCH: 1600F 20.00 HRS WIR TEMPER: 1200F 23.00 HRS AIR QUENCHANT: WATER START TEMP: 64F END TEMP: 88F We hereby certify that all test results and procedure information contained herein are correct and true as contained in the records of the company . BY:Five Star Metals, Inc. .0. Box 800460 + Houston, Texas 77280-0460 + 713 466-1491 + FAX 713 466-6027 CUSTOMER: NITOR METAL, S.A CERT. NO.: P4a6i6-2 CARRETERA VIA LOS POLONES REC. DATE 09/28/2005 SECTOR LA FLORIDA ALT PRIMERA SHIP DATE: 10/17/2008 ANACO EDO ENZAOTEGUI VENEZUELA W.0. NO.: 20796-988 P10. NO1: 01925200 ory. FSM NO. DESCRIPTION TOTAL Wr. 2 Pcs 413021.50NQT 4130 NQ&T FORGING PER FSM 2005-06, REV. K, DID 3/27/01, CHARPIES 20/15 @ -75 DEG. F ROUGH MACHINED 1/4" TO FINISH 1.50"OD X SOLID X 22.00" OAL TAG: ITEM #5 & #6 TEST BAR SIZE: 4" X 4" X 8" BAR DIA: 0.505 MELT PRACTICE: EFVD/LR REDUCTION RATIO 4.2:1 NO WELD REPAIRS NOTE: ALL FORGINGS HAVE BEEN HEAT TREATED IN THE SAME HEAT TREAT LOT UNLESS OTHERWISE STATED, YIELD STRESS IS 0.2% OFFSET. GAUGE LENGTH IS 2" FOR 1/2" BAR. CHEMICAL ANALYSIS PHYSICAL PROPERTIES HEAT NO.: P4616-2 CODE: #29 YIELD STRENGTH: 86,168 MILL: ELLWOOD TENSILE STRENGTH: 107,743 C: 00.33 01.07 ELONGATION: 26.00% MN: 00:55 00.23 RED. OF AREA: 73.00% PH: 00.009 00-18 TEST BAR BRINELL: 228/235 SU: 00.002 00.015 FORGING BRINELL: 224/231 SI: 00.23 00.028 | LOMMX10MMCHARPY: 84/68/85 NI: 00.17 TEST TEMP.: -75F LCVN FE: BAL JOULES: M LE: .047/.040/.049 SHEAR FRAC.: 65/60/70 DELTA FERRITE RETAINED AUSTENITE: :__FORGINGS & TEST BAR NORMALIZED: 1675F 20.00 HRS AIR QUENCH: 1600F 20.00 HRS WIR TEMPER: 1200F 23.00 HRS AIR QUENCHANT: WATER START TEMP: 64F END TEMP: 88F We hereby certify that all test results and procedure information contained herein are correct and true as contained in the records of the company. BY:FIVE STAR METALS, INC. P.O. Box 800460 Ph, 713-466-1491 INVOICE Houston, TX. 77280-0460 INVOICE No: 43389 CUSTOMER CODE: 144324 NIc424 To: SHIP TO: NITOR METAL, S.A CARRETERA VIA LOS PILONES SECTOR LA FLORIDA ALI PRIMERA ANACO EDO ANZOATEGUI, VENEZUE! NITOR METAL, S.A CARRETERA VIA LOS PI SECTOR LA FLORIDA AL ~ LONES | T PRIMERA ANACO EDO ANZOATEGUI, VENEZUELA inv pare ‘SHIP Via Foe. TERMS 10/17/05 WILL CALL ORIGIN PAYMENT IN ADVANCE Femw.o. ‘SALESMAN ‘CUSTOHER P-. 20607-986 FSM 01925200 Payable in Houston, Harris County, Texas in United States Dollars ‘oun | ITEM NUMBER / DESCRIPTION uwrewice [Uw | exrenoeo price] 413023. 0ONOT 991.0000 PC 991.00 4130 NO&T Forging per FSM 2005-06, Rev. K dtd 3/27/01, Charpies 20/15 @ -75 Deg. F | Rough Machined 1/4" to finish: | 23.00"0D x Solid x 5.00"OAL TAG: Item# 3 | SUBTOTAL 991.00 TOTAL TAXES 0.00 TOTAL FREIGHT 0.00 SALES TAX EXEMPTION NUMBER: EXPORT TOTAL — 951.00Five Star Metals, Inc. P.O, Box 800460 + Houston, Texas 77280-0460 * 719 466-1491 + FAX 713 466-6027 CUSTOMER: NITOR METAL, S.A. CERT. NO.: 2930-1 CARRETERA VIA’ LOS POLONES REC. DATE: 06/27/2005 SECTOR LA FLORIDA ALI PRIMERA SHIP DATE: 10/17/2005 ANACO EDO ENZAOTEGUI VENEZUELA W.0. NO.: 20607-986 P10. NO.: 01925200 ory. FSM NO. DESCRIPTION Wr. EA. 1 PC. 413023.00NQT 4130 NO&T FORGING PER 558 LBS. FSM 2005-06, REV. K, DTD 3/27/0 CHARPIES 20/15 @ -75 DEG. F ROUGH MACHINED 1/4" TO FINISH: 23.00" OD X SOLID X 5.00" OAL TAG: ITEM #3 TEST BAR SIZE: 4" X 4" X 8" BAR DIA: 0.505 MELT PRACTICE: EFVD/LR REDUCTION RATIO 6.5:1 NO WELD REPAIRS NOTE: ALL FORGINGS HAVE BEEN HEAT TREATED IN THE SAME HEAT TREAT LOT UNLESS OTHERWISE STATED, YIELD STRESS IS 0.2% OFFSET. GAUGE LENGTH IS 2" FOR 1/2" BAR. CHEMICAL ANALYSIS PHYSICAL PROPERTIES 2930-1 CODE: #1 YIELD STRENGTH: 80,553 ELLWOOD TENSILE STRENGTH: 104,036 00.32 01.07 ELONGATION: 23.00% 00.56 00.23 RED. OF AREA: 68.00% 00.014 00-17 TEST BAR BRINELL: 215/216 00.005 00.015, FORGING BRINELL: 214/224 90.23 00.027 LOMMK10MMCHARPY : 42/25/29 00.14 TEST TEMP.: -75F LCVN BAL JOULES MLE: .027/.016/.020 SHEAR FRAC.: 5/0/0 DELTA FERRITE: RETAINED AUSTENITE: HEAT TREATMENT: FOR NORMALIZED: 1675F 21.00 HRS AIR QUENCH: 1600F 21.00 HRS WIR TEMPER: 1200F 25:00 HRS AIR QUENCHANT: WATER START TEMP: 71F END TEMP: 91F We hereby certify that all test results and procedure information contained herein are correct and true as contained in the records of the company. BY:1 FIVE STAR METALS, INC. P.O. Box 800460 Ph. 713-466-1491 INVOICE Houston, TX. 77280-0460 INVOICE NO: 43388 CUSTOMER CODE: 144324 NICA24 0: SHIP TO: NITOR METAL, S.A CARRETERA VIA LOS PILONES SECTOR LA FLORIDA ALI PRIMERA ANACO EDO ANZOATEGUI, VENEZUE! NITOR METAL, S.A SECTOR LA FLORIDA AL ANACO EDO ANZOATEGUI CARRETERA VIA LOS PILONES I PRIMERA » VENEZUELF inv pare SHIP Via Fos. TERMS 10/17/05 WILL CALL ORIGIN PAYMENT IN ADVANCE Feu wo, ‘SALESMAN CUSTOMER P.O. 20309-987 FSM 01925200 Payable in Houston, Harris County, Texas in United States Dollars ouanrny | ITEM HUMBER DESCRIPTION [—“unrrpnice [UW exrennen pace | T 413015. SONOT 809.0000 Pc 809.00 | 4130 NQST Forging per FSM 2005-06, Rev. K, | dtd 3/27/01, Charpies 20/15 @ -75'Deg. F | Rough Machined 1/4" to finis | 15.50"0D x Solid x 9.50"0AL | TAG: Item# 7 | | SUBTOTAL 809.00 TOTAL TAXES 0.00 TOTAL FREIGHT 0.00 SALES TAX EXEMPTION NUMBER: EXPORT TOTAL 809.00Five Star Metals, Inc. P.O. Box 800460 + Houston, Texas 7280-0460 + 713 466-1491 + FAX 713 466.6027 CUSTOMER: NITOR METALS, S.A CERT. NO.: P2166-1 CARRETERA VIA LOS POLONES REC. DATE: 06/10/2005 SECTOR LA FLORIDA ALI PRIMERA SHIP DATE: 10/17/2005 ANACO EDO ENZAOTEGUI VENEZUELA W.O. NO.: 20309-987 P.O. NO.: 01925200 ory. FSM NO. DESCRIPTION wr. EA. 1 PC. 413015.50NQT 4130 NQ&T FORGING PER 530 LBS. FSM 2005-06, REV. K, DID 3/27/01, CHARPIES 20/15 @ -75 DEG. F ROUGH MACHINED 1/4" TO FINISH 15.50" OD X SOLID X 9.50" OAL TAG: ITEM #7 TEST BAR SIZE: 4" X 4" X 8" BAR DIA: 0.505 MELT PRACTICE: EFVD/LR REDUCTION RATIO 7.6:1 _ NO WELD REPAIRS NOTE: ALL FORGINGS HAVE BEEN HEAT TREATED IN THE SAME HEAT TREAT LOT UNLESS OTHERWISE STATED, YIELD STRESS IS 0.2% OFFSET. GAUGE LENGTH IS 2" FOR 1/2" BAR. CHEMICAL ANALYSIS PHYSICAL PROPERTIES HEAT NO.: P2166-1 CODE: #14 YIELD STRENGTH: 87,604 MILL: ELLWOOD TENSILE STRENGTH: 110,268 C: 00.33 : 01.07 ELONGATION: 23.00% MN: 00.55 00.23 RED. OF AREA: 67.00% PH: 00.012 00.17 TEST BAR BRINELL: 234/237 SU: 00.002 00.014 FORGING BRINELL: 231/234 SI: 00.26 001028 10MMX10MMCHARPY: 52/30/33 NI: 00.14 TEST TEMP.: -75F LCVN FE: BAL SOULE! MLE: .034/.024/.026 SHEAR FRAC. : | 25/5/5 DELTA FERRITI RETAINED AUSTENITE: \T_TREA’ ':_FORGIN( TEST BAR EORNALIEED NeiSF ae 00 FRE AIR QUENCH: 1600F 15.00 HRS WIR TEMPER: 1200F 17.00 HRS AIR QUENCHANT: WATER START TEMP: 77F END TEMP: 92F We hei certify that all test results and procedure information contained herein are correct and true as contained in the records of the company. BY: