Scribd Logo
Upload

Welcome to Scribd!

  • C Realizata Iso Sulfat

    Uploaded by

    Corina Stanculescu
    3 views3 pages
    This document contains information from the calibration of a sulfate spectroscopic tube method. It presents the calibration curve data including the measured concentrations, standard concentrations, and residuals from 10 calibration standard measurements ranging from 20-200 mg/L sulfate. The calibration curve was highly linear with an R2 value of 0.99905. Method performance statistics are also reported including the calibration sensitivity (slope), intercept, standard residual deviation, standard method deviation, and method coefficient of variation, all indicating good method accuracy and precision over the calibration range.

    Original Description:

    laborator chimic

    Original Title

    c Realizata Iso Sulfat

    Copyright

    © © All Rights Reserved

    Available Formats

    XLS, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    Report this Document
    This document contains information from the calibration of a sulfate spectroscopic tube method. It presents the calibration curve data including the measured concentrations, standard concentrations, and residuals from 10 calibration standard measurements ranging from 20-200 mg/L sulfate. The calibration curve was highly linear with an R2 value of 0.99905. Method performance statistics are also reported including the calibration sensitivity (slope), intercept, standard residual deviation, standard method deviation, and method coefficient of variation, all indicating good method accuracy and precision over the calibration range.

    Copyright:

    © All Rights Reserved
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    3 views3 pages

    C Realizata Iso Sulfat

    Uploaded by

    Corina Stanculescu
    This document contains information from the calibration of a sulfate spectroscopic tube method. It presents the calibration curve data including the measured concentrations, standard concentrations, and residuals from 10 calibration standard measurements ranging from 20-200 mg/L sulfate. The calibration curve was highly linear with an R2 value of 0.99905. Method performance statistics are also reported including the calibration sensitivity (slope), intercept, standard residual deviation, standard method deviation, and method coefficient of variation, all indicating good method accuracy and precision over the calibration range.

    Copyright:

    © All Rights Reserved
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 3

    CURBA DE ETALONARE SO4

    tub Spectro
    DATA: 0.6.02.07
    INDICATOR: SO4
    METODA DE ANALIZ: Merck 14548
    DOMENIUL DE MSUR: 20-200 mg/l
    CONC. ETALON MERCK: 1001 mg/l toleranta 2 TERMEN DE VALABILITATE:
    CERTIFICAT CALITATE:
    CONC. SOL: ETALON DE LUCR 1001 ppm

    i C stand C realiz Yi1 Yi2 Yi3 Yi4 Yi5 Yi6 Yi7 Yi8 Yi9 Yi10
    1 20 18.9 18.160 19.060 18.910 19.360 19.060 19.960 19.210 17.870 18.610 18.910
    2 40 37.8
    3 60 59.6
    4 80 80.8
    5 100 102.3
    6 120 122
    7 140 139.9
    8 160 160.4
    9 180 180.8
    10 200 196.2 196.670 195.330 196.070 196.970 196.820 195.930 195.780 196.370 196.220 196.520
    suma 1100.000 1098.700 ext. -extincia
    media 110.000 109.870 X/ ; Y/
    *2- ridicat la patrat
    N Xi-X/ Yi-Y/ (Xi-X)(Yi-Y) (Xi-X)*2 (Yi-Y)*2 Y^ Yi-Y^ (Yi-Y^)*2 (Xi-X/)*2
    10 -90.000 -90.970 8187.3000 8100.0000 8275.5409 19.9327 -1.0327 1.066526 8100.000000
    -70.000 -72.070 5044.9000 4900.0000 5194.0849 39.9188 -2.1188 4.489262 4900.000000
    -50.000 -50.270 2513.5000 2500.0000 2527.0729 59.9048 -0.3048 0.092933 2500.000000
    -30.000 -29.070 872.1000 900.0000 845.0649 79.8909 0.9091 0.826446 900.000000
    -10.000 -7.570 75.7000 100.0000 57.3049 99.8770 2.4230 5.871076 100.000000
    10.000 12.130 121.3000 100.0000 147.1369 119.8630 2.1370 4.566639 100.000000
    30.000 30.030 900.9000 900.0000 901.8009 139.8491 0.0509 0.002592 900.000000
    50.000 50.530 2526.5000 2500.0000 2553.2809 159.8352 0.5648 0.319054 2500.000000
    70.000 70.930 4965.1000 4900.0000 5031.0649 179.8212 0.9788 0.958026 4900.000000
    90.000 86.330 7769.7000 8100.0000 7452.8689 199.8073 -3.6073 13.01242 8100.000000
    suma 32977.0000 33000.0000 32985.2210 1098.7000 31.20497 33000.000000
    b= 0.9993 y=a+bx b- msur a sensibilitii metodei (panta dreptei)-indice de performan de execuie a met.analiz
    a= -0.0533 a-proba martor calculat(ordonata la origine)

    Sy= 1.9750 3.90062E+00 abaterea standard rezidual (indice de performan care descrie exactitatea etalonrii)

    Sx0= 1.9764 abaterea standard a metodei (indice de performan de execuie a metodei de analiz pe domeniu de lucru)

    Vx0= 1.7967 coeficientul de variatie a metodei


    C m asurata m g/l

    250

    200
    f(x) = 0.9993030303x - 0.0533333333
    R = 0.9990539712
    150

    100

    50

    0
    0 50 100 150 200 250
    C standard mg/l
    Y/i

    You might also like