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Abstract—Several models that describe the behavior of ionic Electroactive polymers (EAPs), particularly ionic
polymer–metal composite (IPMC)-based actuators can be found polymer–metal composites (IPMCs), have been around for
in the literature. The response of IPMC transducers as a function many years, because they have the very interesting capabilities
of modifying quantities is a matter of interest; however, it has
not been investigated. It is reasonable to argue that environmental of transforming electrical energy into mechanical energy, and
humidity and temperature represent the main modifying parame- vice versa [9]–[11], making them privileged candidates for the
ters. In fact, humidity changes the behavior of IPMC transduc- realization of artificial muscles.
ers, working as both sensors and actuators, because it changes Although the number of proposed applications grows at an
the Young modulus of the devices and, hence, their mechanical impressive rate, full exploitation of unique IPMC properties in
response. The influence of temperature is suspected, because poly-
mer characteristics are often influenced by this quantity. In a motion applications has not yet been possible because of some
previous paper, the authors proposed a dynamic model and investi- unsolved drawbacks from which they suffer.
gated the scaling effect of geometrical parameters, giving evidence Moreover, the full exploitation of IPMCs has been limited
of the excellent agreement between estimations that were obtained by incomplete knowledge of their working principles, which
using the proposed model and corresponding observations. In this makes it impossible to have a clearly defined design proce-
paper, the response of IPMC actuators to both temperature and
relative humidity is analyzed, giving interesting information that dure. In previous papers, the authors proposed models that
both integrates IPMC models and allows for a better exploitation can guide the design of devices with the desired performance
of IPMCs. [12], [13]. In the referenced papers, the need to investigate the
Index Terms—Actuators, materials testing, measurement influence of environmental parameters on IPMC performance
system data handling, modeling, transducers. was outlined as a concluding remark [13]. To the authors’
knowledge, a complete characterization of IPMC transducers
as a function of modifying quantities has not yet been ac-
I. I NTRODUCTION
complished, and few analyses can be found in the literature
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894 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
where [13]
Lclamp length of the clamped part of the IPMC;
Lt total free length of the IPMC (without considering
Fig. 1. Scheme of the model for describing the electromechanical conversion the length of the pinned part);
in an IPMC actuator.
Ls point where the force or the deflection is measured;
w and t dimensions of the IPMC cross section;
η equivalent permittivity that corresponds to the two
capacitive branches;
Y Young modulus;
d coupling electromechanical coefficient;
Γ value that depends on the solution of the charac-
teristic equation of the clamped beam for the first
mode;
ρ IPMC density.
In (1) and (2), the quantities d and Y have to be identified
as a function of the sample being tested and the modifying
quantities.
Fig. 2. Equivalent electrical circuit for an IMPC-based actuator.
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 895
TABLE I
CHARACTERISTICS OF THE ACTUATOR FOR THE
CHARACTERIZATION PROCESS
TABLE II
MODIFYING INPUTS AND THEIR VARIATION RANGE
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896 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Fig. 6. Top: train of symmetric step inputs and amplitude modulated noise
voltage signal used as input to the IPMC actuator to characterize the dynamic
Fig. 4. Setup for the characterization of the IPMC actuator. part in its model. Bottom: relative current response.
Fig. 5. Top: triangular voltage signal at 25 mHz, which was used as an input to
the IPMC actuator to characterize the nonlinear element in its model. Bottom:
relative current response.
6) one laser sensor that reveals the IPMC free deformation Fig. 7. Top: step voltage signal (3.0 V) that was used as an input to the
that was produced under the effect of an applied voltage; IPMC actuator to characterize the blocked force. Bottom: relative force that
was developed by the IPMC actuator and measured by the load cell.
7) one load cell that reveals the IPMC developed force that
was produced under the effect of an applied voltage.
In Fig. 4, a real view of the developed system is shown,
including the LM35 temperature sensor by the National Semi-
conductors and the HIH 3610 Honeywell humidity sensor. The
GSO-10 Transducers Techniques load cell was used to measure
the developed blocking force, whereas the Baumer OADM
12U6460/S35A laser sensor was used for the measurement of
the IPMC displacement.
A. Voltage-to-Current Transduction
Identification of the electric circuit (see Fig. 2) that models
the currents that flow in the various branches requires two
different measuring surveys [13].
The first measurement is needed for the identification of the
nonlinearity, and this task can be achieved by forcing on the Fig. 8. Top: swept sinusoidal voltage signal (peak-to-peak value 5 V,
50 mHz–50 Hz, 10 s) that was used as an input to the IPMC actuator to
actuator a triangular voltage signal at very low frequencies to characterize the free deflection. Bottom: relative free deflection.
neglect the capacitive behavior of the IPMC actuator.
The input voltage and relative absorbed current for the afore- pair of humidity and temperature values in Table II. A total of
mentioned case study are shown in Fig. 5. 20 measuring surveys were performed for each pair of modify-
As reported in Fig. 5, a number of measurements were ing quantities. This approach allowed us both to obtain a mean
performed by applying the same input voltage signal for any model and to estimate the measurement dispersion.
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 897
Fig. 9. (a) From the top: the current that was absorbed by the actuator for the input voltage signal in Fig. 6, the laser sensor output when a swept sinusoidal
voltage signal is applied to the actuator, and the load cell conditioned output when the actuator is forced by a step voltage signal. (b) Zooms for the same quantities.
The aforementioned input signal allows for the identification branches, can be identified using input signals that force the
of parameters in the static part of the electrical model. The dynamic response of the actuator in the frequency range of
dynamic part of the model, which comprises the two capacitive interest. The signal consists of a sequence of steps with different
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898 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Fig. 10. Comparison of the predicted and measured absorbed current, the standard deviation of the residuals, and the 3σ confidence level.
amplitudes and a sequence of samples of amplitude modulated Note that the swept signal that was adopted can solicit only
noise. This choice proved to be the most adequate for the the first resonant frequency. The proposed electromechanical
identification process. model is based on the theory of the cantilever beam, which is
The input signal and the relative current response are shown not accurate over this frequency without corrections. Moreover,
in Fig. 6. the application for the IPMC actuator does not require a work-
Again, 20 different measurements were performed for each ing frequency that is higher than this frequency.
pair of humidity and temperature values in Table II. The measurements of both the blocked force and the free
Once the electric circuit has been identified, it is possible deflection were also performed 20 times.
to estimate the fraction of absorbed current that produces the
mechanical reaction and use it for the estimation of either
IV. D ATA P ROCESSING
free deflection or blocking force after the identification of the
electromechanical parameters of the model has been performed. The collected data were used to identify relevant parameters
1) Electromechanical Transduction: To identify the parame- in the IPMC actuator model and the corresponding model
ters that appear in the electromechanical models (1) and (2), mea- uncertainty. The dependence of the identified model on the
surements of the blocking force and free deflection are needed modifying inputs was also of interest. For each pair of modify-
[13], [17], and (1) and (2) must simultaneously be solved. ing inputs (temperature and humidity), the model of the actuator
For the case of the blocking force, a step voltage (0 V÷3 V) was identified, and its uncertainty was estimated.
with a duration of 10.0 s was applied to the IPMC actuator, and The identified model was used for the estimation of the
the developed force was measured by using the load cell. The actuator output. The estimated values were therefore compared
input signal and relative force developed by the DUT are shown with the recorded values to obtain the model residuals.
in Fig. 7. A statistical analysis of the model residual was performed
To measure the free deflection that was needed for the model to obtain a type-A estimation of the actuator uncertainty [19]
estimation, a swept sinusoidal voltage signal with a peak-to- by using the experimental value of the standard deviation of
peak amplitude that is equal to 5.0 V, a frequency of 50 mHz– the residuals. Once the standard deviation was estimated, the
50.0 Hz, and a duration that is equal to 10.0 s was applied to the coverage factor k = 3 was used to compute the 3σ confidence
IPMC actuator, and the free deflection was measured by using level as a function of the modifying inputs.
the aforementioned laser system. The input voltage and relative One typical example of an available signal set is shown in
free deflection measured by the laser displacement sensor are Fig. 9(a), along with the signal that was predicted by the model.
shown in Fig. 8. Fig. 9(b) zooms in on the results that were obtained, thus better
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 899
Fig. 11. Comparison of the predicted and measured free deflection, the standard deviation of the residuals, and the 3σ confidence interval.
Fig. 12. Comparison of the predicted and measured blocking force, the standard deviation of the residuals, and the 3σ confidence interval.
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900 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Fig. 13. Comparison of (a) the predicted and measured resonant frequency and (b) oscillation amplitude, the standard deviation of the residuals, and the
3σ confidence level.
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 901
Fig. 15. Resonant frequency of the actuator with different humidity levels at a fixed temperature.
Fig. 16. Blocking force that was developed by the actuator with different humidity levels at a fixed temperature.
Fig. 14 shows the average IPMC actuator deformation for humidity on both the amplitude of the resonance value and the
20 recordings. corresponding frequency value.
In Fig. 15, the same working conditions as in Fig. 14 are con- A similar dependence was observed when the blocking force
sidered to show the IPMC behavior in the frequency domain. was analyzed. The data that were obtained in this case are
It shows the modulus of quotient of the cross power spectral shown in Fig. 16.
density between the applied voltage and the deformation and One example of the behavior of the IPMC actuator as a
the power spectral density of the applied voltage. Note that, function of the environmental temperature is shown in Figs. 17
although the actuator is nonlinear, it shows a sharp resonance. and 18. In this second analysis, the environmental humidity is
Moreover, the results show the effect of the environmental fixed to 80%, whereas the environmental temperature varies
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902 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Fig. 17. Resonant frequency of the actuator at different temperatures and a fixed humidity level.
Fig. 18. Blocking force that was developed by the actuator at different temperatures and a fixed humidity level.
in the range of interest. Based on a perusal analysis of the As outlined in Section III, two modifying inputs were consid-
results, it is possible to conclude that, for the considered range ered. For any pair of modifying inputs, a set of measurements
of temperature values, no clear trend can be recognized. was performed to obtain the model parameters and the uncer-
In the following section, the complete set of investigated tainty estimation of this model.
working conditions and the results that were obtained will be In Table IV, the whole set of identified model parameters is
presented to show the dependence of the IPMC actuator on the shown as a function of both temperature T and humidity H.
modifying quantities and the uncertainty that was estimated for All the parameters and symbols that were adopted refer to
the model that describes the IPMC-based actuator. the electromechanical models (1) and (2).
As far as the uncertainty estimation is concerned, a Type-A
estimation was performed. In the following figures, the results
V. R ESULTS AND D ISCUSSION
that were obtained in the uncertainty estimation will be shown.
In this section, the results on the characterization of the IPMC For each quantity of interest, the respective uncertainty is
actuator as a function of the modifying inputs will be presented. reported as a function of the modifying input values.
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 903
TABLE IV
MODEL PARAMETERS AS A FUNCTION OF THE MODIFYING INPUTS
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904 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Fig. 19. Surface that was generated by collecting the information on the uncertainty estimation of the absorbed current in different working conditions.
Fig. 20. Surface that was generated by collecting the information on the uncertainty estimation of the IPMC deformation in different working conditions.
Fig. 19(a) reports the uncertainty due to the model that Figs. 22 and 23 emphasize the performance of the model in a
was adopted as a function of both temperature and humidity, working condition that is critical because of the presence of a
whereas Fig. 19(b) reports the experimental confidence level resonance.
that was obtained by using the considered coverage factor As mentioned in the previous section, the modifying in-
k = 3. puts cause changes in the performance of the actuator. These
Fig. 20 gives the results that were obtained in the estimation changes are much more evident when the humidity changes,
of the uncertainty with regard to the IPMC deformation. whereas no important variations are shown when the tempera-
Based on the analysis in Figs. 19(a) and 20(a), it is possible to ture changes. Fig. 24 gives the results that were obtained, with
observe that the standard deviation of both the absorbed current the free deflection and the blocking force being a function of
and the free deflection increases with the humidity level. temperature and humidity, respectively.
Fig. 21 gives the uncertainty estimation results with regard
to the IPMC blocking force. In this case, the dependence of the
VI. S UMMARY AND C ONCLUSION
model uncertainty on the humidity level is not present.
Fig. 22 gives the uncertainty estimation results with regard to Full exploitation of IPMC actuators requires models of the
the capability of the model to estimate the resonant frequency devices to be available, along with the corresponding uncer-
of the IPMC in the cantilever configuration. tainty estimation. In this paper, the characterization of a set
In Fig. 23, the uncertainty of the model for the estimation of IPMC-based actuators has been performed to investigate
of the IPMC deformation at the resonant frequency is shown. variations in model parameters due to the effects of external
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 905
Fig. 21. Surface that was generated by collecting the information on the uncertainty estimation of the IPMC blocking force in different working conditions.
Fig. 22. Surface that was generated by collecting the information on the uncertainty estimation of the resonant frequency in different working conditions.
Fig. 23. Surface that was generated by collecting the information on the uncertainty estimation of the amplitude deformation at resonant frequency in different
working conditions.
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906 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Fig. 24. Blocking force and the magnitude of the ratio free deflection/applied voltage in different working conditions.
influential quantities, i.e., temperature and environmental hu- Note that the results are linked to the investigated interval
midity. The investigated IPMC actuators showed a strong de- of variations for the modifying quantities, which are depen-
pendence on the humidity level of the environment, whereas no dent on the envisaged applications, i.e., biomedical applica-
significant dependence emerged as a function of the environ- tions of the IPMC actuators. Nevertheless, such dependencies
mental temperature. can arise if larger intervals of variation are of interest for
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BRUNETTO et al.: CHARACTERIZATION OF TEMPERATURE AND HUMIDITY INFLUENCE ON IPMC ACTUATORS 907
Fig. 24. (Continued.) Blocking force and the magnitude of the ratio free deflection/applied voltage in different working conditions.
applications other than the ones that have been considered in [12] C. Bonomo, L. Fortuna, P. Giannone, S. Graziani, and S. Strazzeri, “A
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[14] F. Bauer, S. Denneler, and M. Willert-Porada, “Influence of temperature
The authors would like to thank the Consorzio Catania and humidity on the mechanical properties of Nafion 117 polymer elec-
Ricerche, Catania, Italy, for providing the membranes that were trolyte membrane,” J. Polym. Sci. B, Polym. Phys., vol. 43, no. 7, pp. 786–
795, Feb. 2005.
used in this paper, as part of a project collaboration activity. [15] S. Nemat-Nasser, “Micromechanics of actuation of ionic polymer–metal
composites,” J. Appl. Phys., vol. 92, no. 5, pp. 2899–2915, Sep. 2002.
[16] M. Shahinpoor, Y. Bar-Cohen, T. Xue, J. O. Simpson, and J. Smith, “Ionic
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mer transducers,” Ph.D. dissertation, Virginia Polytechnic Inst. State
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N. Ferraro, “A MEMS-based flexible sensor and actuator system for
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Mater. Struct., vol. 17, no. 1, p. 13, Feb. 2008. DOI:10.1088/0964-1726/
17/01/015014. Paola Brunetto received the M.S. degree in automa-
[8] M. Shainpoor, Y. Bar-Cohen, J. O. Simpson, and J. Smith, “Ionic tion engineering in 2006 from the Università degli
polymer–metal composites (IPMCs) as biomimetic sensors, actuators and Studi di Catania, Catania, Italy, where she is cur-
artificial muscle: A review,” Smart Mater. Struct., vol. 7, no. 6, pp. R15– rently working toward the Ph.D. degree in ingegneria
R30, Dec. 1998. elettrica elettronica e del controllo dei sistemi com-
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damentals,” Smart Mater. Struct., vol. 10, no. 4, pp. 819–833, Aug. 2001. Elettronica e dei Sistemi.
[10] S. Nemat Nasser and J. Y. Li, “Electromechanical response of ionic She is the author or a coauthor of several scientific
polymer–metal composites,” J. Appl. Phys., vol. 87, no. 7, pp. 3321–3331, papers, many of which were presented at interna-
Apr. 2000. tional conferences or were published in reviewed
[11] Y. Bar-Cohen, X. Bao, S. Sherrit, and S.-S. Lih, “Characterization of journals. Her research interest is focused on IPMC
the electromechanical properties of ionomeric polymer–metal composite materials.
(IPMC),” in Proc. SPIE Smart Struct. Mater. Symp., 2002, vol. 4695, Paola Brunetto is a member of the Italian Association for Electrical and
pp. 286–293. Electronic Measurements (GMEE).
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908 IEEE TRANSACTIONS ON INSTRUMENTATION AND MEASUREMENT, VOL. 59, NO. 4, APRIL 2010
Luigi Fortuna (F’00) received the M.S. degree in Salvatore Graziani received the M.S. degree in
electric engineering from the Università degli Studi electronic engineering and the Ph.D. degree in
di Catania in 1977. electrical engineering from the Università degli
Since November 1994, he has been a Full Pro- Studi di Catania, Catania, Italy, in 1990 and 1994,
fessor of systems theory with the Dipartimento di respectively.
Ingegneria Elettrica, Elettronica e dei Sistemi, Uni- Since 1990, he has been with the Dipartimento di
versità degli studi di Catania, Catania, Italy, where Ingegneria Elettrica, Elettronica, e dei Sistemi, Uni-
he has been the Dean of the Faculty of Engineering, versità degli Studi di Catania, where he is currently
since November 2005 and is currently the Coordina- an Associate Professor of electric and electronic
tor of the Ph.D. courses in electronic and automatic measurement and instrumentation. He has been a
engineering. He is also in charge of a series of coauthor of several scientific papers and one book.
contracts with public and private companies. He is the author of more than His research interests include sensors and actuators, signal processing, multi-
350 scientific publications, seven of which were books published by interna- sensor data fusion, neural networks, and smart sensors.
tional editors. He is the holder of ten industrial patents. His research interests
include robust control, nonlinear science and complexity, chaos, cellular neural
networks, soft-computing strategies for control, robotics, micronanosensor and
smart devices for control, and nanocellular neural networks modeling.
Prof. Fortuna is Fellow of the IEEE Circuits and Systems Society.
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