wd ore 9» 2 spando ed of fettous gedit. To peepae® a.oam ‘2 galt and + Nn Ih on a suena Sulphate cone) 9% Moht € 6 ol os k dioting i ‘ a oO, solution bY tittotng Find olay oF Kitrd« of FAS against stondard toy (losks beaker, busette + pipette, s 250m' Volurett +A gloss dod, Purmely @akch aloes Conic) Flask. buwette stand. tee, KMn Oy ss FAS Solution » dished ooo CPotacsium peemanganatc) » dil Hy $%%, 4 Theony i> Molecul mass of fas = 392 dooom! 4m Fas sequies 92g of FAS "250 ml 005M FAS Solution will eequi: Est x 0:08 $89 10006 ~ 43g of FAsilo fF Fexvous Ammonium 4: phate FAS) av Moht’s Aim i> To prepare o.o8m stondard solution ealt and to Find malaity of KMoO,, solution_| Chemicals 3 FAS Salution » distilled cakes Lerten —Tetunatumm—pensnangenaie) atl Husa Theaty ¢ Moleculat mass oF FAS = 392 |toooml 4M FAS tequites 299.4 of ERs “0GR-m) 0.05 M FAS Solution oil tequivte = 250 x0,0S X392. 1000 | = 4.9 g_of FAS (A) Peocedute fo Pre 4 i) paottation of shandatd calutinn of PASi= Ltoeight accukelly FAs Cohauk 4.09) on arobch ala: Teansfee the teighed quantity of FAS inplass—« Observation =~ Contval teodind m| to Lom) Volume of Kindy | End point eqquieed fo dhin Volume of Burette scartat | Find _ Solukton_t yy _ | dow) \ 1 5.8m! 4.4 en | 3:4 mt i i | gaat ep 4) Caleulattana, 8 * wt. of empty wotch giles = Og = 38.0929 - 9. wd. of cjakch glass FFAS = Wo4 ma 3Tta est of FAS Hansfetted + Corry > 494 © (ot. oF FAS peecert in 250m) Solution 24.89 wh of FAS present te Loam solution + Gory) kecdq 7 250 u . 4: 9X 1000 250 FIQ.E Molo’ of FAS = Wr 3 aga Mola ity of Fras. - 13 Acei beaker. sw lash the cnotch plas Hyice evewy dhame coith labout tol of diatilled carat we cand tango jal Ane ccoashing to the beakee containing es the ERS completely in Gate's. Thansfek Atnis _SoluHon From beaket Ae 25am | Nolumetiic Flask Using Funnel Rinse dhe beaket & Hmes oritn about tom) of qoatet and Atansfer it to volumeteic Flask Add distilled eaates 4a valum edeic Plost upto the matk. +n amake dhe volume 9501 Siciase dhe flask tuith catk and shake The 5 lgjash all the appakatus Woith toatet.. [Rinse dhe butethe att KMnd, solution Pill it coith KMnCy Solution up tn zea mark, i) Rinse dhe pipette saith FAg olution. pipette out domi. ae PAS In a Clean Conical Black. iw) Add one sect ibe of clill Hs80q co tne Conical Flaska, (NH 80 +gH,S05— L804 + 2MnSoy+ | aKIMnds + LOPES yt ho CNHs 205.4 SHO 5 Fe, C809 FA ig CAS ta, a easles of KMnu = 40 moles of ~ Re 2 xISeg of ¥MnOu o> 40 moles oF FAS —_ alc y oF Laninds = Looe ml aom FAS é io ve asoaras LOMFRS = gisg OF Kmnes if dom) x MPAS. = ie } it = 0.816% of KMndy \ ee = 9.816 X0-0S~ & = 0.01SE g. of Kind, ih do ml «x FAS zequits y ml oF KMnO, + Hence JY ml of Solution Contains Co, 81600033 OF Hide “4000 mi of KMndq will contain < 3162x1089 4 oft ul YA mn Fv Molowity of kMnQ, ~ Solution: 9216 % x190C0 5 | YXISR i | = Bey rr Isey : be atk Mm 3 ‘ “2. Expeement No. ke 4 Aim aed T peepate oi M standata salutton of Oxalic acid and to Find mnolattity of KiMnOn Solution by Heiating, ab agatnst Soluttor — OF oxaltc acid Approtus %—> 250 ml Velumel flask, beakeey gloss god, funnel, watch glass » busette, pipette , conical flask , busette — stancl ete Chernicols %— Oxalic acid 5 distiWed watet » KMnd, a ai > Soludtonin Folate of Kind, Solation = 2% M = 0,01logl' - 0O.0LM & Result t—> Molowity of KMnG@, Solutton: = Zv) Add kDnd, Galudion Eeam the Lukele tent 2 4 ‘ Cont flask ti | constan haking. till pevananent faint | and _p¥evian Steacling ftom he buvedtte (Thi is knanwn as carcttol Now Aitkate doml of Fitesh Solution. Buk at | . . [gol dap by dkep ath Constant shaking dill [EBS duuns point pink in Coleus. Nake this. Bending Fkom the bubitedt ll Repeat the Same _pkaceduke tm get Stat — | 7 ¢ hic tl ‘Me lotmest canstant eeading Sn the end _po'nt | —Ta ptepare OAM Stendakd Leolution of oxalic acid ond 4 ind molavidy af Kindy, lution by jbeiteating it against Standakd of | Oxalic _arcicl. Appatatu = 2.50 ral alumet ic Flasi. _heakets ais od _, Funnel caadtch als _bukette, | pipette conical Flask , bivette stand etc. | Che 1 so Oxalic acid » chet \led corcter, kMno, (Pota seitim petmang mates) Solution Theoky > Oxalic acid erick as H,C,O4.2H,O and 44 amolok miass ib 126. taco mL. of 41M Solution Bequite Ark OF c2xalte acid 2 to i Dia x Theoey > | Oxalic acid . extsh and its oF 4m Oxadic mola® mass as H,¢,04-2H,0 fs 126, joooml Solution tequikes i264 of acid Hence 260rn1 aim Yequite als g of oxalic a Solution acid willHequite gisg of oztalic acicl [Ptaceduwe i-—» A Preparation of Standa¥d solution of ,Orxal\ic acicl = lle: ; ; 15g) On wiadeh ala _— ue i oxalic acid in a alas hea key Mlalash the coakch gla dh¥ice every dime tuith ohouk 410ml of clistitled toate, and transfer oll the crashing iv) Lebo thy heaker Comtainine exalt Cid HYe the amixtuxe of mate’ anal Ovalic acid +n discalve the oxalic acid Completely in __tarbey Transfer thi Soludien Prors _peakes — icp 250 m1 Volumeteic Flask using funne inse the heake% @ times ith about ——_l| doml oF cnote ond deonsfee in doy Volumetkic Flask Add distilled — tacndet to VolumedxicFlast up da othe matk tn amake the flux 25% wml. Ai Close the flask (ith cate and shale dhe solution. This is 01m sdmndad —— olution ak axalic acicl 2) TH _dete¥ mine the Streng af gis/en Kind, salukion by using, stanclarcl eolution of oxalic eid Leoash oll the atatucs (ith coates [Rinse che buvette Coidd KMnO, solution. ou cots MnO salut tn Ze i). mark. fix the buxelte tn the stand Rinse the pipe bh “cot oxalic creict acid in a Clean Conical Flask. done dest tube oF olil, H, S04 to dhe Conical Flask v) Head oxalic acid _Solurtien about Bo -60" ot Add KMnQ, Solution ftom the huydbe dmirak each tHme. inte conical Flore G)ith Constant shaking AN petananent | Bain pink colbux ie obtained . Nate thtl Obeewvat on. | | | | ll ob. ] Volume OF |no |—— Pal) Lom! | 2. | dom) | 3. om) Lo! tom) _ |, Coleudakion s +7 z|| Wt of empt 2] Ot of -wadtch of oxalic wk. of oxalic | OF OF oxcdic Contto) teed! i | oxale o¢ id som” woubch gluss= 38-2369 - lass +oralic actd = 41.4859 atid tkansFeeed = 2. 9g aed preses Mn 260m! cl’ “B5144g. ‘n 2 Som! sol acid pecrend * Ger x1ee0 “44 250 > Bl49 x 1000 258 ee, ~ ES 36 9.if | { — TS 4 . : Malo‘ of oxalic aed soludic (rt me Oth Batt, S0g7 OK, SO4t 2M Soy v Flt,o 4 10CO, 2 moles of KMnOy 5 ymoled of oxalic add. rxisea of kKMnO, =looom) 5M oxalic odd 36g SF Kfind, 7 Looom\ 6M oxalic ack te, Loooml BM Hila, = 16 g of Kir Oq tom! * MH, G04 > 2iex loo. ie akMnd, +ShCeOu v ” loo0 XS 2 Bb 4 of KMnG, + SOO = 9. 0632.9 of kmno, = Lo ml —ond— | trating so p coodth ‘%ecatd the time equited When Céoss mark on dhe papets just becomes invicta} Lob exvali. fi ol Ha Onl No» 5203 i ta_ml Regdbi— Rate of Yeacton U/t) is diveotty Hrol 6 dhe Concrntration of sodtum thins ulntots Use ame pope’ cid — C¥ags matiAtami To _study the eFRect oF change ‘on the kate of eacdion bet” Soclinm thiasulphate ancl hy deachlaxi acid Theony ts The toate of a chernica) Yeaction depensle upon temperate At the temp Incteases the tote of __veaction. inckeases clie to inctease in _kinedic enekay of the amalecules The inctense af kinetic — en lok effective collisions between Heacting species. Appentas Mensuring cylindek_, conical Flask , [pape _Giith Ciao wmark , het mametex , toike gauze» —ttipad stand, shrpimctch ebe. Chemi “4ra study the effect of tompetatu te Change on “the tate of eactton between _ sodium thiosulphede and hyd chlo ic acid ‘ Theo y = The Hate of @ chernical clependsi Upon dempetaluze, Als the empeelute inCéease the tote of incteszes due de in¢éeaje in kinedte enetayy of the wolecwes . The incte. 2 OF Kinehic. enekay of molecules inckeases the rumbes of effete Lesh conde bet weac »cantcal Flosk Popes with s thetmometek 5 Gy gerze, ti podl Stand Stopwatch etc, O.4amM NA + Jas SO, , IMHO! Dyictitedl cowle® Expetment No.2 2 | | | i t \ {Leese = - I | Observed tor table | Yolume of O24 of 4LMHc! added , Volurre 9 oF ' a@hen Coss tft become invisible | | Gioph b> . ! Plot o geeph OF AA Chants yesges the temperatute — i Resulé >> { Rote of. Heacttgn beloeen 9.6 0; and Hot Ietende od deen peaduikeaf OF displacement The amon! of heat evolved o% absosbed tants ad indicabed by palonced chemical equation ake cor plete iq@ken no of goles of keacled fo foew the products te known ag peak of teacdion . The amount of heat eustved wher dt reste oF CuSO4 im Solukis canete A letely cotlt Solution teatis dornple 4 cot a \ chrmole of | Zn metal fs the heat of weaction fot H emery ef Cu by Zn Reaction 3-9 Cus0y +2n—> Zygon 4Cu AH = -Sakeal CUDRIT e Reguigemend — Thee rrormetes, 4 comical Flask 5 couk | cylindes /O2M Cugo,y solution,Result i> Rat. ak teacton ond HCl inctea se a tempe Bodie, imc¥ecseAim =* Te Jelebmine heat of displa cem: of Cu by ha Theory = The cmount of heat evolved o% absothed hen no. of male: of Yeacdants as jndinked foxy balanced Chemical equation abe completely steacted +a freon the products i Known a heal of Yeactions. The wrraunt of heat evolved ahen 4 mmol. of Cugoy in sol el (ith 1 amole of Cusoa in solution Beacde cornilaly nit 4male s£™ zn metals | heat of teactinn fo Sipe of Cu boy Zn Reaohon 1. _~ Cusow't7n Sao. s AH=z-s52.K cal CH2lt- + KT) rment —! Ghetmometeh, cofiical Plosk coh,t+ Obgetvadtons Lye WE. of Flow « Mg 2) Yolume Soluion (v= 'eom! i 3) Initol oF CuSo. golutton= ty ¢ : = RAB c ' 4 i 4)! Final temp. of Solutio + tec ‘ = 864 B) Rue in temp at~ct- 10% i Big Tc we sy t © Sp heat of Cuso, ~ solution = a), sps het of glass =O 2 ay) Density oF CuSO. soit \, | tx Colleuletion | | r 4 a . Heak evolved “ashen li | Yeat || Heat 7} | Loom). | 9.299 CuSO is }=) Gained by -|y ' goined by. Com plekey teacled| the solution, Conicad |! L L tL Flosk - Lvxd Xsp- heak AL |+ ; [rm %sp heat At} = L100KI x1 xg z+ bot 1P2.¢ "1B 6 ca my : LILO ~0.2 gig= ——-solukloé whe ny tdooml OM Cus with zn Wbetates complebiy teacted Oleg cod of heat 2m cugo, solution When ath zn tl) Whetate ‘ Loos mm! rep tetely tea cdes Dre pletely ‘ QAxlooo™% l > Ino X6-9 . [Ofe.6xX 10d Taty 0-2 ~ jJolez¢ ou = SO 54 ™%'O% cal 20) [ Sea) OSG '5? -a) “(FOSS x rok 107 VK ca), i (FT OSCK IBS KT Yas BUSOURT of heal » Heel of displacement ne. BH fob the weactlon Cu $04 +Zn —+ Zns0y - 201B4aky +) Result -2 e hea : Res Th 4 of displacmend of va : ‘3 Ze Zan) Poe sae eT of Co by Zn + Cui igt Reguiherments I- | Beakee cosom'd, corieal Flak fesom!), cglinde. (loam dhezmonretee, | , Hel C.591), NadH cas ) etc. 4 Theo > 3 Heat of neutedlizatton ig the amount of heal evolved when one geen equivalent ae gr acid ts neutsalized fT g a gd one om equivalent of a base in Jiube Solution, fox ste ong acids ond ste bases the Value of heat of Neutializafton iy con Stunt Thic it because the veachion hetween a skeona acid doa steorg ‘ ong and a st ong base metaly the mbiation of dmple oF Mand 4 " ° nd dt ymot x att “6 bet yn water NoOW cogs FHCH cay Alot C4 Gg AH =-19.4 cad Oras =-18 Re CSF 32R7 HHT ky 0 a 1 AH 2-18F keal ¢ TE 42K 5)Aim t— Ta _detetmine the heat of netutralizaton of ttong acid dnd Strong bore fs nis ¢—> Peaker (e356 mil), Conical flask osnni PLEA SUE Sho cs Mnder (loaml> themametes| Vubher coxle , Hel lo--m). NadH Co-m) this is be camre the eaction bettrcen o—sttavig acid and_a__steang bare ic woevaly Me combination of imole af H* and 4 male of OH" to fem suite= - | 7 | Obsesvations + eae | 1y Temp: of Hci solution ive 28. catytion <4 2 16:6 i »| Texnp oF NadH so ution = T © § | | Ada} Le . hats | D) Aretage Mia Temp FE | ¢ | = 28626 | . i te 22.6% i : vO Final time. of omiaduze = tle = BS" i | | Rise | D> Tota volume of -mixtute (Umitd- lootloo VU Q@etght ” d spy heak \ Den sity t Actas ot | | the: scleebtan temp Abe (ky tye 2 (aS ~ 2663" > 2.9%, 2 ¥ oom) “oF contcad Flask 2110 of glass -o 2 ‘ ci | oF so'ution Cy) >! | oF sglubion = 1 i i i goined bs Heat geired | +| by canton | Flask | LNaQHcagict HCleagi——— Nate Cl+H, Os Ates 13% K cal (os 82K) OH 4H* ——>5 0 aH =~/3t Keal —SPL.O2 |T Aeaulé im Heat of #eaky trong acid » Wcl a trong, base NoOH CAH) = - 58.05 KT. sie esLJ +E Msp. heat vat]| a [ite 0.2% 2-34 | Loo me! oeST HC! or Complete neud oe section! evolves Q col. OF heat 4 2M wc on com plete neubtalisation CHAR xtolod x} (9m ~O. C408 .f = 3.8498 | 2498103 ca) _ = 8498x107 io? Kea) C498 RK cad = (8.498 GLAVKT oF heat. > BROLKT of heat weak of neu tilteatin of He! by NadHean) | { =SB09 KY Ceovll -§ Hed OF teadtalroudean of Stkary 4 ce y tong € iS, He’ by @ Stang. base Aut ia -s5.o9Ky,Noaheds Given -~CooH qeur b) Substance 4 Tallen’s * fea! Lebli ngs solution g Febling’s salusion r- Sub stance CPehling Solr A & d pine £ & hea! Result ya! Valtsrnes) Geoy pph. o% sWee mistot ‘3 Obtained Red ppt of Cu,0 | ce OF iy cooH JEP acal ge f Coca de> pe trnce is peesent aolution condain _ Tale ence i Ico soup is | | present \ +7 CHO geeup is——. Test | ohse Substance + ! Erfewence of |= Sool —gvoup Il NaH Cog soln CO. _ig__p¥esent Result => Given Solution camtain _—cnoH gtoup— is __pie ent 9)ll Test fox =CHO _g¥olin. Test | obsckvation “Cnfevence Q) || Tollen’s teagent | tesbt-» Substance Gkay ppb ov CHO aroup + Tollen’ sengent Silvek amib¥ok ie present end to0%m is _obbained byl Pehl solution dest s> Substance = + ebling's solukisn _Cu,0 1_ptesentpoe caly oF Ca. ws | : a | | Resulé = a | {i Giver Solufton A Contain coo quar! 8 pet sent 4) Test Fox “-NH. gtoup Test obseeuats ton | Snfetence _ |_gubstance +dil Hal} O#enge "eed [eros grou LL +NoNOz soln cool} dye 1S present | band of thre sol | | +s 90!" of 4 |B nepthars! im Naot ‘ Fr ctuiasbemaipibcdincesieipteerestitienepanlonts i | —e co . ' jBesut > Giver Se!" 1B contain yy, arur I is peesenk.9) || Test foe —caoH ¥ ——— gee Test | Ob sexvation | Thkerence liquid soln + [ECPetence OF |=coott -gyeoup | MaHco, soln_| co is_pitesent __4)|| Test fat NH geoup— Test | ob se¥-vation | TnFerence. ubstance + pvange ed NHL Soug Lif Hel +N NG dy {is pesent oln cool and Habis gal” i olitton oF A Diapthemol_in Natt: Resulhi-> Given solution & contain ~NH jf asep pases| obsetvakton i Tnfetence. gubstonce + Rive oe Geen phenol =oK " ates 4 Vow violet ater ts " peesent Neubsed Fetl, 0 Colou ¥atton Result = Guyen solution ¢ contain phenolic | | - eit i eset oH gveup fs pe rtSubstance + esp Mates + ov Violet Meutval FeCl, | Colouration ptesent soln | _l | Result => Given solution ¢ Contain phenolic oH -geaup is peesent—_—__| | CO, , 5°” o¢ No;' | May be present | cogt may be a) Coloue and odeut Coloutless & of the gos | odoutless gos is| present. evolved with | buick, eheteeen | b) Gas is posed lime wotez | cog* a5 lime ake tutne milky. Cont ao [ae 2) Podee+ di HNO, Pet. is D- ger aagey | Ago, soln obtained he cr, Bytes T | iT 95 be peesent | a) Colove, GF ppd. Curdy white CIT! present | b) Solubility of ppt! i Pes in excels of Soluable CV may be péecent NH.OH. | ' Yellow ppt CI $5 conFiemes) ) Chromsg chlonide te fowdet, + sold k,C49, + fee A‘eops of Conc. Hy $04 ond aNAnalysis of Acid __tadicals. Test obseevatton Pomder +dilHCl Gas is evalued! t— Colout and odau colouless —Or oF the ga is evolved | ama he & | coz may be waith beisk | ig thkough lime _-tiens to» _ Con Pitame amily |ee | Ie | | Above Naou | Coln t lead acetals \ Result > Given Known powder Following acid ‘tadicles Te to Bois = Cogt ptesent Tr ID- stoup— ian present vu containsTest Ob seevation Tnfevence. CO chitornyl chlonide. Aes Pocndes + | Vollows Ppk. | ci” may be | slid KaCe.Oy + | contitvened | Fe ca d#op oF \ Cone _H, SO, and! heated evolved. bYoun L ue Seo = 1 Nool soln Above NoOH soln + dead acetate. Result i—> | GrivenKnoson _posade _conbains fo Heng on td li e.. Lectin DU coe Giz.n \ ft wae . Linaly a fo-sdl — Tianewence, i. Test for yop Pesdes tdi! + No 4 is evalved: TT g¥eup ts obsent 1& Cot, B04 »S* os NOP Th Beep AS absent ven CVE or; ate absent ~ Test foe Of e# : j Yodicles 0) Test fox SO. 1) Dissae the prod White pp is 504” wmey be o do HCL oe Obtained pees wate + Bal, se’ : — v Lahite ppt + PRL ots 80% ic ere Sol uoble conf? med ~ Dark - is dg IS powdes U4 g c : ' 3 on fi eee Pane Ac : —_—enAnalysis of acid tadicles__ Pogide —_is__un Knowon | Test | obsetvation | Imnfetence. 4)|| Test “fae x! Qkoup = parades No ger_is [aot gaup is pol LHC) evolve d. lobsent if cogs | Soph ise Noy 9) || Tesh oat - fet is Thy soups ‘ pos Jet-tcli ined -obsent Le a Be oe Fake tRgNO Soln ace || Test fb | L Othe eodicler a)||test Foe Soyer! MWiDictalve Ha fit opt is S072 snnay des indi) | obtnined be Het o& coke’. ' +RaCl soln ali tlhit ppb + _ppk- is gopt ue Cocn. HCl insoulah le conFivemed byiITest foe. NOM Ring, tes bi Diss olve, poude| ect ft etennton itfec dtops of | use layers Gene 4,80, ond | i cool + Fece tf deat « Lube ; | . I : | 7 7 i | ea Result o> | Give i ) ok and ' aban i wp NO 4 | oo1 — _ | Test absexvation “Tn ference i bl. Tes) fox. NOW tron lays _NOP is \! Ring Teh” Lis obtained — ConcFlemed . acid vadteles S0-% nel, Nog| | nRevente- ote sex yad ior | , { | ole sesyal ion reese’ | est fox Tgt up No ges rs “ Powdeg + atl He! evolved 2. Tesh foe gtoup Dissolved the PPE is obtained, T- geoup kadicles | Powder in dil Hnio, QE BE oe ode +Ag NO, tesent soln Obseve Colouk PPE is YellowshBeorsmeoy be | jof Ppt ‘and ity white ed | | Seluability in prtriblea_ | Meag. 4: | | NH,O# | 'Loye Test t- ‘Powder +4/1HN0, Otonge ed BUA te + fee d¥ops of heavy Joye, Confit med cone. HNO, & is Obtained 1. Warm Hii Colouk chenges cool Diluate +Obsexvation | nfewence. | “Teg fix TL group “pee {s_ohtainel TE p | Missdlve dhe | wedide cx, | Jpocades ia cil HAO) Tyas | OX. Obset ve B | of_ppk. and ise | cobite piserent | Solubility ia |_Enselubble NHq OH loyer. egk $— poiniet tdi 1 Unb Cea wed Be" te + Pea dyogs of “heavy Lager jconblemedd Con HNO, A. warm \9 Ob tnined 4M ower Coo) cl iluate i+: and add im! of | CC1. shake and obsre cotows of heavy Layer,Ta Ob setevation "CCl, Shake ond obsetve Colout | Trfevence OF heavy fenpet | @ Teh fo other Yodkcles | 5) Jeet fot So? ‘ 1 i) Disselve the | white pet | S04? raay Powder indi! ig chhdned | be ptesent i Hel o& water | Bath. ‘sol |. )) @hite PPA + | per is - Gone HO | nsolualte Fecenaa | ; Reut i | Given — powdet — Containe ~ follocgin | powder ) vy eo Be WY $04 * | hk,“Test “Terk Foe othe’ Sadicles a) 05%! ‘ 3)/nrdlytic of acid eadicles | t A #. Test oF LY pocdes. fe rafesence | _ Test. \_ | nm A) Tesh Rurgtoup Togtoup is | ; 3 | Pocodde + oft JHC) we | Gos ig evolved | Peeserd CO | ne [ dil 4,80... ' ; GO," $08 | Noy may be| | - Present . | | i | ay Colouke and odou¥|Colourler: & cost ama j 1 oF the gos lodourless with be peess | bEck bfferveccence} b) Gas 8" passed lime code co is throug lime cootek | Hutns milky Confit red! 9) Fea, ake mileut kof oo I 2y | Test fee geoup . r- Atoup \s | Ditcolve the prods PPt fe obtained pesent.” je in JITHNOn + Agog, Tellesssh ter c17 WE gL may! Solve” celeus he | be p Yesent Obceducolout of | boas PRte. ord its “tetas BR nlm Solus lta n NH,0H ha prowge Layee egt.t G Powder, tdi! HNO, 4 feu d¥ops of Conc. HNIg dnd} | |2° | Test i Obsetvation [ Tn tet fevence. i Ay Test fax Tegtoup Gas is [apts Sitouip is) | powdeb dillicl evolved. ipkesent Coy, sce! ow dil Wy S04 No2 ek Nor ray b i Pecdenk. el Colouk ond oda Coloutless & Coz" may he—| of the gas. clousle. covth present betel ef feuvescone + byl Gis 18__paseed. Lr dake Cog i : Cokes 1 i 2)|| Teat fp Te geoup! Tie group is_purs eu Ipiasolve th LPPt.is obtaimed ie. Cl Seine To jpotadebin oiling gel levaich in___may be puetend| be soln Colous & inealuble i Layers Test i= iirl _excese Lea cope af’ ellnaich | he | cone. HNOg& coat Coleuh 1x obtained ptetea te —— | | Wal calaux Cool! ond diluct ib |took a! Olowr charges | voiled OF purple Te iy coo! Diluade it heavy ge J Conf hy wed. ond add Lim! of| obtained cel, shake ond | Obeseeve Colouy| of heavy oe | ) Result . i Given poudat Fellowsing acd Radltcles |) cg & | yy or i 1 “Beh. | obser vation | Inkeeenc, | \—" sai1 foe ard panicles | Test | Oh seevatton | Tn fetence. Test fate Tguoup No qe is_tregtoup ia oheal Powder +d HCl evolved lie coe, soz” | | Noy en be i absent. . 2) || Test | i i Soln Ql Tect foe otek tacicles o> ‘ 1 | Paces ow conteh Pocl Sol. y ' i ‘ sot, «Bat methine: _Confixmed —E ~ =i He Coote abe cetake) 2—> coloub Se id __con + Popode'e, + wakes +Nedtad eCsd On ode “Feat foe 2 Powe ees — i Topeenvakion _|Tnfeeence Test 2) Test Bet eyeou pt No gps is evolved |\T-g #0up ic Powder tg HCl | 4 al | - OS™ FOP NG; pMmay be abset 2) Tect for D- gee’ PY Dissolve the po - (No ppt ts De -gtoup dete indil HNO, 08) obtained. absent ie wober + Ag NO, soln (CI Re, £7 roy bese: 3) Test Poe othe | ‘tadicles I~ o)| Test for SOQ* 1 i) | DissoWe the poroder| Cohite pps © 505 may in dil HCl of wuleet $6 Obbutned, Present” BaCl, soln. 1) Oshite pe t PPL. is nsoluakle cod may Cone. HC! i Shee! ) be Oo7 ) BY | . - Bleed sed CHgcoo™ 1s Col , a Pousel ‘ Slows us Confie ms ° Obtained Neutsal Fetls somhheaty. Test Obsetvation “TnFekence. : ‘of col, chake | vbilek oe 0 rts and Ghekvebve purpl ecw: Gonflimied. iI | Colour oF Nyt o i loyen | * obtnined / Q ssctone Chiven. poco jis. Fstloe ing acid tadicles. Ul tm, is5 " n ) Result 8 Given tadicles cote and 7 CH, Coan 0% — pow de't Contains — follow; "yResult 2 oi Te tadtcle | Soh andl -CH,cOo. rafap Ee jobion | Inference 4) Test for T-gtovp, gos is evolved |- geoup es fowodee + dil HCl ob | jpeesent: he cof H, $04 i SO, , STIARND | io ay Be Pkestent 9) Coleus and odout Colourless & wor may be | Of the gas oboutlers gas peesent | evolved ith, _belsk effeevescene Coe is lime octet Confiymned datas amilky ; b) Gas is passed thyough —[vmes ates 2) Test forT-gtoup No eph ta TE geoup u Powder tdi! HNO,+ Obtuned absent ie cir, AgNO; soln Ro ase may be obsent 3) Test fax. 0) STect Fa | \ | S027 aay ¢ oF net ‘d obtained | obsensTastee 4 poradet “Test | obseevalion |_ Th fetence. 4) Test Fos Tegtoug Gar re evobied| T= g¥aup cy | icles tcl HCl piesentis. cds F ow 1, 80, | ots o% NO Colout and Coloukless & w ‘ ladouk of the obouteless gai __| p#esenf. gos |; evolved caita | bist efCetscen i b) Gos—ispassed, Lime _goates | Co% is Hthxaugh. time deen mil My aed =I \ ftuell a oe waket, Bal ele . . | P|!Jel Wer o% 3)' Test foe Oy + ” ‘Pocddent @Daters | Conc nidwcoctd4 ‘orn montium m9 Jyb dale Result Giver powda No blood ted | -GHycoo’ | zs Coloue "absent is 3- yellow ppt Po, is 1 obtained + Con Fiterited \ fonkain « oF Abel RD) a Son tah So Poe a dese : follocaing eocl! cles.Obsee vation | Tnteefevence, ("_tp)l{ “Teed fine Noes | \ Ring Text 2 t ; : hn in dif Heloy é Confined. || eo aber -} Fear d¢opsof @nc HS, cindl_ Coo) fe $0. sal" along the sides oF the _c) gnpees Aundlysis _of Powde's NOe Basic. Rad icalg Coleus a blue ‘ di! Hc! Solubility J ‘ TTT ~ pi aes NHP” fee absent. ___Obsesvation | ote Retenc. 4) Pomde& +NadH soln No Snell of | ond woemed NH gas \ i 2) 0.8. +d't Het No ppt [7 gteup Fe absent, 8), Above Soln—wattrred PPL ig obtained |= ates ts MHS gos and Filtered a PPE ANOS aolh PPE ts Insoluble. b), Golous of ppt Riock be peesent FPL SIR HNG) ond PRL is Solvable. *Cu' may be pre heated above sol—~ Deep blue colouta-|Cu% i “pie cen} Cooled +excess of Avow Ton | Above Soln* acetic, Chocolate Cat $5 ConPem so'n +" blue Glouzed ppt dis appeaved 4 pee: i » Fexsocunde soln 0 O PM walle fof deaeas ; " d a Me Pet I-#K geet pit absent fay 4 bated te vomowe| Analysis oF Baste Riadicles i Poorcles No. 2 4 i Colon tht e Solubi Listy £—= Cold dil Hel Test Lol Vatt { %: )/[Preaclors + Noo soln! Alo smell of Nuit ts and aio mned NHe. gas absent MI! O.g td FHCL Nd pp Ti gteup st ahseut! Lftbove soln cootmed PPE + I = gpualips Ls yi HHS ga Cond Palsetal Obtninect Pisesenks | puesent ! p)Calouk of ppt Black hoe bgt saat | ! he 36f senb f | _ollpek + tatinin, and | peLis alusable! Cuttenay he 1 heated above sol"! teen blue _Pwesent e Hi Lc a erent | 4 | Filbtnke of TT gqaoup lo ppt. ThA geoup is ——] boiled bs Semove. ,Has gor t Cone HNO Lond balled - cooled" ; goln~"bo' led +0 temove Hyg. Volume uced hy bat ling 1 Cooled aNHacl texcess i fu, 0: ' oF NH,O44/NH, \ Cog Soln 7) Above solution +cotisr! Phosphate Result 3 hadi No’ PY: ae Btoup ic ow senk No pp ’ = % geoup ie abd No ‘pp= a gemup @ absent. @hite ppe “gtoup! te peers Given powdes Contain's “RE [rast te con Fier! ia : Fallows basié= [ey aT 7 ee a | Test |_obseevakion | Tntebefekence. || Hs gasacone HIND, Nop. ln pitoup te | andl_tboiled cooled + absent. AY Ac] Caotid)texcese | | of NH,OH Hil soln z mel! oF NH ty afkeh anntacing | + i a ola +H ges + |lReeubt 3 M hast o x e i Cu2* and w ar 3 aMeld HCl od the r fone. rrouth of he 4: 2 0.6 +d:'4C! golf Gov a ond 4 4) oiled the Filter of agtoup +3 tems g Conc. HN'D, ond ed “onledtNu.c! Gokd)+ excess oF NHLCH Aull seln giver srre!! OF NH, akek Mining 0 of et nas Sod- dipped DENSE eadicals Basic 7 No. rght_gzeen “Gok ott HEL jayton op white furred . | | I- gkoup is obser ie Pa Seg aL. gtoup Vs obser Raddich b¥oun’ BD -gteup “may PRE fs obtain be ptesert. te fe e223" aye*( Analysis. oF Basic _tadicals } a Powdes No. 222 4 Colou% =» Night a ¥een. ! il © || eatutaitity to Hot dit Het. | $ Test [phattualion | Tiotekence—f 4 est: fat. NHS | i tl Pee Jobs| Sve of omnisat_aoay le — Land ect \_ga |ptesents § “2 Hold _gos— od| Dense white | NH, is Iippled toca Furnes | canblemed wet at dre | | rmoauth. of the bal \ od tla.g tot) HCl flo ppt it puoup a ‘ jeu ie | [I pow nf gat] NOs _ppt clam. phous lmed +H,s ges ' iIbovlec! the _Raddish Alteved of at4 opt u do keme\e He gtt_conc— uno’ ond belle Cooled +NHt4eee zs — _ | CoS our _of Jisthbeoon fife? | Test Observation blue | Dissolve the ppt. Deep in dil HCI+KPe@ny Coloutation So” 34 n) pel -+dit Her + Blood ed fe5* | is Arn thiocyanate Colouat ion Gonbieetd # Result ss Given powder. Contains FoNe using: basicoH ere ee i | ‘Test Dh servation “Interference, csolid\ texcegs @ | of NH,oH 441 cela y, \, [of NH afles | }}omining. i | Dissolve the ppl meep blue | fet jo dil Ye _caloutatte n cantlemed, KeaPeCcny«s soll Rlond ted fet wy tl PPL-tdil Melel ealousotioan confltmed " a | ; Gluten poudet _contrine Bellauing _borlea sadicler 2—» {t\ NH.t and i) fet ele