8.

312
8.290

8.060
8.038

7.996
7.974

7.282
7.277
7.260
7.244
Parameter Set:#H1−QNP−34 (2008.11.19) TS1.3PL8.
NMR System: Bruker Avance DRX 400
Oper. MB/ Registry No.: 5992
User: R. Cioanca
DU \\Bruker−1−New\D\UTI−FChimInd\RCioanca Sample Changer Position:
data
USER BAO−AZO4
Sample name and description: BAO−AZO4 (spectru inregistrat la 55 grade C)
nmr
NAME h
EXPNO 1
PROCNO 1
Date_ 20090702
Time 17.18
INSTRUM spect
PROBHD 5 mm QNP 1H/29
PULPROG zg30
TD 57470
SOLVENT CDCl3
NS 16
DS 2
SWH 7183.908 Hz
FIDRES 0.125003 Hz
AQ 3.9999621 sec
RG 181
DW 69.600 usec
DE 6.00 usec
TE 328.2 K
D1 1.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 10.00 usec
PL1 −5.00 dB
SFO1 400.1328009 MHz
SI 32768
SF 400.1300227 MHz
WDW EM
SSB 0
LB 0.30 Hz
GB 0
PC 1.00
OFFSET 15.920 ppm
PH_mod pk

8.7 8.6 8.5 8.4 8.3 8.2 8.1 8.0 7.9 7.8 7.7 7.6 7.5 7.4 7.3 7.2 7.1 ppm
1.00

1.00

0.96

1.09