Method: Cu 060618 P7G17 R2 Page 1 Date: 6/6/2018 10:43:07 AM

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Analysis Begun

Start Time: 6/6/2018 10:15:56 AM Plasma On Time: 6/6/2018 10:15:28 AM

Logged In Analyst: Perkin Elmer Technique: ICP Continuous
Spectrometer: Optima 7000 Autosampler: S10

Sample Information File: C:\Documents and Settings\All Users\PerkinElmer\ICP\Data\Sample Information\

Cu 060618 P7G17 R2.sif
Batch ID:
Results Data Set:
Results Library:

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Method Loaded
Method Name: Cu 060618 P7G17 R2 Method Last Saved: 6/6/2018 9:51:29 AM
IEC File: MSF File:
Method Description:
Initialize Optics completed successfully

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Sequence No.: 1 Autosampler Location: 1
Sample ID: Calib Blank 1 Date Collected: 6/6/2018 10:21:10 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time:

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Replicate Data: Calib Blank 1
Net Corrected Calib. Analysis
Repl# Analyte Intensity Intensity Conc. Units Time
1 Cu 327.393 -609.5 -609.5 [0.00] mg/L 10:22:21 AM
2 Cu 327.393 -753.7 -753.7 [0.00] mg/L 10:22:28 AM
3 Cu 327.393 -602.1 -602.1 [0.00] mg/L 10:22:34 AM

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Mean Data: Calib Blank 1
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Cu 327.393 -655.1 85.50 13.05% [0.00] mg/L

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Sequence No.: 2 Autosampler Location: 2
Sample ID: Cu 2ppm Date Collected: 6/6/2018 10:23:18 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time: 30 Auto Dilution Factor: 1

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Replicate Data: Cu 2ppm
Net Corrected Calib. Analysis
Repl# Analyte Intensity Intensity Conc. Units Time
1 Cu 327.393 1165462.0 1166117.1 [2] mg/L 10:24:26 AM
2 Cu 327.393 1234696.3 1235351.4 [2] mg/L 10:24:29 AM
3 Cu 327.393 1180586.5 1181241.6 [2] mg/L 10:24:31 AM

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Mean Data: Cu 2ppm
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Cu 327.393 1194236.7 36400.59 3.05% [2] mg/L

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Sequence No.: 3 Autosampler Location: 3
Sample ID: Cu 4ppm Date Collected: 6/6/2018 10:25:11 AM
Analyst: Data Type: Original
Method: Cu 060618 P7G17 R2 Page 2 Date: 6/6/2018 10:43:07 AM

Initial Sample Wt: Initial Sample Vol:

Dilution: Sample Prep Vol:
Wash Time: 30 Auto Dilution Factor: 1

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Replicate Data: Cu 4ppm
Net Corrected Calib. Analysis
Repl# Analyte Intensity Intensity Conc. Units Time
1 Cu 327.393 1227144.6 1227799.7 [4] mg/L 10:26:19 AM
2 Cu 327.393 1190761.3 1191416.4 [4] mg/L 10:26:22 AM
3 Cu 327.393 1211208.6 1211863.7 [4] mg/L 10:26:24 AM

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Mean Data: Cu 4ppm
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Cu 327.393 1210359.9 18238.20 1.51% [4] mg/L

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Sequence No.: 4 Autosampler Location: 4
Sample ID: Cu 6ppm Date Collected: 6/6/2018 10:27:04 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time: 30 Auto Dilution Factor: 1

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Replicate Data: Cu 6ppm
Net Corrected Calib. Analysis
Repl# Analyte Intensity Intensity Conc. Units Time
1 Cu 327.393 3661934.4 3662589.5 [6] mg/L 10:28:13 AM
2 Cu 327.393 3747579.2 3748234.3 [6] mg/L 10:28:15 AM
3 Cu 327.393 3725727.0 3726382.1 [6] mg/L 10:28:18 AM

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Mean Data: Cu 6ppm
Mean Corrected Calib
Analyte Intensity Std.Dev. RSD Conc. Units
Cu 327.393 3712402.0 44501.00 1.20% [6] mg/L

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Calibration Summary

Analyte Stds. Equation Intercept Slope Curvature Corr. Coef. Reslope

Cu 327.393 3 Lin, Calc Int -143749.7 557700 0.00000 0.921877

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Sequence No.: 5 Autosampler Location: 9
Sample ID: Cu 1 Date Collected: 6/6/2018 10:28:59 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time: 30 Auto Dilution Factor: 1

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Replicate Data: Cu 1
Net Corrected Calib. Sample Analysis
Repl# Analyte Intensity Intensity Conc. Units Conc. Units Time
1 Cu 327.393 2511173.8 2511828.9 4.762 mg/L 4.762 mg/L 10:30:07 AM
2 Cu 327.393 2568078.8 2568733.9 4.864 mg/L 4.864 mg/L 10:30:10 AM
3 Cu 327.393 2579930.5 2580585.6 4.885 mg/L 4.885 mg/L 10:30:12 AM

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Mean Data: Cu 1
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Cu 327.393 2553716.2 4.837 mg/L 0.0659 4.837 mg/L 0.0659 1.36%

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Method: Cu 060618 P7G17 R2 Page 3 Date: 6/6/2018 10:43:07 AM

Sequence No.: 6 Autosampler Location: 10

Sample ID: Cu 2 Date Collected: 6/6/2018 10:32:23 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time: 120 Auto Dilution Factor: 1

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Replicate Data: Cu 2
Net Corrected Calib. Sample Analysis
Repl# Analyte Intensity Intensity Conc. Units Conc. Units Time
1 Cu 327.393 3213761.8 3214416.9 6.022 mg/L 6.022 mg/L 10:33:32 AM
2 Cu 327.393 3176272.2 3176927.3 5.955 mg/L 5.955 mg/L 10:33:34 AM
3 Cu 327.393 3225642.9 3226298.0 6.043 mg/L 6.043 mg/L 10:33:36 AM

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Mean Data: Cu 2
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Cu 327.393 3205880.7 6.007 mg/L 0.0462 6.007 mg/L 0.0462 0.77%

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Sequence No.: 7 Autosampler Location: 11
Sample ID: Cu 3 Date Collected: 6/6/2018 10:35:47 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time: 120 Auto Dilution Factor: 1

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Replicate Data: Cu 3
Net Corrected Calib. Sample Analysis
Repl# Analyte Intensity Intensity Conc. Units Conc. Units Time
1 Cu 327.393 5544343.7 5544998.8 10.20 mg/L 10.20 mg/L 10:36:56 AM
2 Cu 327.393 5587862.3 5588517.4 10.28 mg/L 10.28 mg/L 10:36:59 AM
3 Cu 327.393 5637369.6 5638024.7 10.37 mg/L 10.37 mg/L 10:37:01 AM

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Mean Data: Cu 3
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Cu 327.393 5590513.6 10.28 mg/L 0.083 10.28 mg/L 0.083 0.81%

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Sequence No.: 8 Autosampler Location: 12
Sample ID: Cu 4 Date Collected: 6/6/2018 10:39:13 AM
Analyst: Data Type: Original
Initial Sample Wt: Initial Sample Vol:
Dilution: Sample Prep Vol:
Wash Time: 120 Auto Dilution Factor: 1

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Replicate Data: Cu 4
Net Corrected Calib. Sample Analysis
Repl# Analyte Intensity Intensity Conc. Units Conc. Units Time
1 Cu 327.393 7475470.1 7476125.2 13.66 mg/L 13.66 mg/L 10:40:22 AM
2 Cu 327.393 7486669.9 7487325.0 13.68 mg/L 13.68 mg/L 10:40:25 AM
3 Cu 327.393 7545645.9 7546301.0 13.79 mg/L 13.79 mg/L 10:40:27 AM

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Mean Data: Cu 4
Mean Corrected Calib. Sample
Analyte Intensity Conc. Units Std.Dev. Conc. Units Std.Dev. RSD
Cu 327.393 7503250.4 13.71 mg/L 0.068 13.71 mg/L 0.068 0.49%