3.

6 Density

Volume piknometer = 25 mL

Berat piknometer (a1) = 33,5020 gram

Berat piknometer + CU 0,1% (b1) = 57,0406 gram

Suhu (T1) = 27,1oC

ρ1 = b1-a1 = 57,0406-33,5020 = 23,5386 = 0,9415 gr/cm3

V 25 25

Density (dC1) = ρ1 x density air

= 0,9415 x 0,99654

= 0,9382

Berat piknometer (a2) = 33,3785 gram

Berat piknometer + CU 0,2% (b2) = 56,7842 gram

Suhu (T2) = 27oC

ρ2 = b2-a2 = 56,7842-33,3785 = 23,4057 = 0,9362 gr/cm3

V 25 25

Density (dC2) = ρ2 x density air

= 0,9362 x 0,99654

= 0,9329

Berat piknometer (a3) = 40,9013 gram

Berat piknometer + CU 0,3% (b3) = 66,2032 gram

Suhu (T3) = 27,2oC

ρ3 = b3-a3 = 66,2032-40,9013 = 25,3019 = 1,0120 gr/cm3

V 25 25
Density (dC3) = ρ3 x density air

= 1,0120 x 0,99654

= 1,0084

Berat piknometer (a4) = 41,4774 gram

Berat piknometer + air (b4) = 66,7638 gram

Suhu (T4) = 27oC

ρ4 = b4-a4 = 66,7638-41,4774 = 25,2864 = 1,0116 gr/cm3

V 25 25

Density (dC4) = ρ4 x density air

= 1,0116 x 0,99654

= 1,0080

3.7 Viskositas

Waktu alir (detik)

Air Contoh uji 0,1% Contoh uji 0,2% Contoh uji 0,3%

26,29 27,65 27,60 28,48

25,43 27,16 26,96 28,67

24,94 27,09 27,43 28,40

25,40 27,85 27,68 28,69

25,83 26,99 27,39 28,75

25,49 26,29 27,04 28,18

26,21 26,78 27,49 28,05

25,79 27,44 27,86 28,12

24,72 26,33 28,05 28,05

 25,77 26,49 27,30 28,03

Rata-rata 25,58 27,004 27,48 28,32

η contoh = dC x tC x ηs
ds x ts

keterangan :

dC = density contoh

tC = waktu alir contoh

ds = density air (lihat tabel)

ts = waktu alir air

ηs = lihat tabel

η contoh (0,1%) = 0,9382 x 27,04 x 0,8545 = 21,6777 = 0,8503 cp

0,99654 x 25,58 25,4914
η contoh (0,2%) = 0,9329 x 27,48 x 0,8545 = 21,9060 = 0,8593 cp
0,99654 x 25,58 25,4914
η contoh (0,3%) = 1,0084 x 28,32 x 0,8545 = 24,4027 = 0,9572 cp
0,99654 x 25,58 25,4914

3.8 Tegangan Permukaan/Daya Basah

No. Konsentrasi Banyak Contoh Uji Berat Benang Waktu

1. 0,2 % 50 mL 5,034 gram 186 detik

2. 0,3 % 75 mL 5,730 gram 108 detik

3. 0,4 % 100 mL 5,629 gram 120 detik

4. 0,5 % 125 mL 5,072 gram 139 detik

5. 0,6 % 150 mL 5,568 gram 97 detik

 6. 0,6 % 150 mL 5,673 gram 63 detik

7. 0,7 % 175 mL 5,519 gram >240 detik

Grafik hubungan antara Konsentrasi ZAP dan waktu

300

250

200

150
Waktu (Detik)
100

50

0
0.1 0.2 0.3 0.4 0.5 0.6 0.6 0.7

Konsentrasi ZAP (%)

3.9 Metylene Blue Active Subtances (MBAS)

No. x y (A) x.y x2

1. 0 -0,061 0 0

2. 0,3 0,002 0,0006 0,9

3. 0,5 0,006 0,003 0,25

 4. 1 0,007 0,007 1

5. 1,5 0,032 0,048 2,25

6. 2 0,496 0,992 4

∑ 5,3 0,482 1,0506 7,59

Keterangan : x = konsentrasi

y = absorbansi

grafik hubungan antara konsentrasi dan absorbansi

Y = absorbansi
0.6
0.5
0.4
0.3
0.2
0.1
0
-0.1 0 0.3 0.5 1 1.5 2 X = Konsentrasi (%)

∑x = 5,3

(∑x)2 = 28,09

𝑛.(∑𝐱𝐲)− (∑𝐱).(∑𝐲) (∑𝐲).(∑𝐱 𝟐 )− (∑𝐱).(∑𝐲)

a= b=
𝑛.(∑𝐱 𝟐 )− (∑𝐱)𝟐 𝑛.(∑𝐱 𝟐 )− (∑𝐱)𝟐

a = 6 x 1,0506 – (5,3 x 0,482) b = 0,482 x 7,59 – 5,3 x 0,482

6 x 7,59 – 28,09 6 x 7,59 – 28,09
a = 6,3036 – 2,5546 b = 3,6583 – 2,5546
45,54 – 28,09 45,54 – 28,09
a = 3,749 = 0,2148 b = 1,1037 = 0,063
17,45 17,45

y = ax + b
0,482 = 0,2148x + 0,063
0,482 – 0,063 = 0,2148x
0,419 = 0,2148x
x = 0,512