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ABSTRACT: Experimental design technique is applied to optimize shaking table and dry high intensity magnetic
separation processes on recovery of cassiterite from Igla Placer ore of Eastern Desert of Egypt. It could
investigate the effects of individual operating parameters and their interactions for both shaking table and dry
high intensity magnetic separation processes. Applying the optimum conditions for both separation techniques
showed that in case of shaking table separation concentrate containing 13.2% SnO2 and recovery of 86.2% by
weight SnO2 was obtained from a feed containing about 0.048 % SnO2. Cleaning of this concentrate by using dry
high intensity magnetic separation a final concentrate with 90.67% SnO2 and operational recovery of 96.7% SnO2
by weight was obtained.
Keywords: Cassiterite, shaking table, dry high intensity magnetic separation, Box-Behnken design, statistical experimental design
response surface [23]. Analysis of variance separation processes. Table 3 illustrates the factorial
(ANOVA) was used to estimate the statistical design, recovery and grade of cassiterite for both
parameters. The extent of fitting the experimental shaking table and magnetic separation processes.
results to the polynomial model equation was
expressed by the determination coefficient, R2. F-test Table 2. Test levels of parameters for both shaking
was used to estimate the significance of all terms in table and dry high intensity magnetic separation
the polynomial equation within 95% confidence Dry High Intensity Magnetic
Shaking Table Separation
interval. "Adeq Precision" measures the signal to Separation
noise ratio, a ratio greater than 4 is desirable and Symbol (-) (0) (+) Symbol (-) (0) (+)
indicates an adequate signal. α 3 4 5 ε 70 75 80
β 2 2.5 3 δ 50 75 100
Table 2 represents the operating parameters for both γ 100 250 400 ϕ 500 750 1000
shaking table and dry high intensity magnetic λ 15 20 25
Table 3. Factorial design for shaking table and dry magnetic separation
Run Shaking Table Separation Dry Magnetic Separation
α β γ λ ρ η ε δ ϕ μ σ
1 4 3 400 20 7.37 81.4 75 75 750 90.6 96.7
2 5 2.5 400 20 6.87 84 80 75 500 62.5 96.4
3 4 2 100 20 10.6 76.8 80 100 750 58.7 95.6
4 4 2.5 100 25 8.94 82 75 100 1000 77.1 91.2
5 4 3 100 20 5.7 80 75 75 750 90.6 96.7
6 4 3 250 25 7.95 83 75 50 500 81.3 94.6
7 5 2.5 100 20 6.2 81.9 70 50 750 74.6 87.6
8 4 3 250 15 7.46 79.8 70 75 1000 73.2 88.1
9 3 3 250 20 5.79 79.2 75 75 750 90.6 96.7
10 4 2.5 400 25 12.47 83.4 75 75 750 90.6 96.7
11 3 2.5 400 20 9 82.6 80 50 750 61.3 95.7
12 4 2.5 100 15 8.5 81 75 50 1000 79 92.3
13 5 2 250 20 4 74.5 80 75 1000 64.2 96.1
14 3 2.5 100 20 8.2 81.4 75 75 750 90.6 96.7
15 3 2.5 250 15 7.95 80.8 70 100 750 78.6 85.8
16 4 2.5 250 20 13.2 84.9 70 75 500 72.4 89.3
17 4 2.5 250 20 13.2 84.9 75 100 500 78.2 91.7
18 4 2.5 250 20 13.19 84.9
19 5 2.5 250 15 4.5 76.4
20 3 2 250 20 8.8 80.4
21 5 3 250 20 3.4 77.5
22 4 2.5 400 15 9.4 79.4
23 4 2.5 250 20 13.21 84.9
24 4 2 400 20 11.5 77.9
25 4 2 250 25 11.9 80
26 3 2.5 250 25 10 82
27 4 2.5 250 20 13.2 84.9
28 4 2 250 15 9.4 78.4
29 5 2.5 250 25 8.7 88.6
Table 4. Complete chemical analysis of Igla original 3.2. Size Analysis of Original Igla Placer
placer tin ore Cassiterite Ore
Constituent Assay %
Figure 4 shows the grain size analysis of the
SnO2 0.048 cassiterite ore. It is shown that the ore passed 100 %
SiO2 58.6 from 22 mm sieve size. The d80 and d50 of the ore are
Al2 O3 12.01 14 mm and 6.8 mm respectively. It is seen that the
SnO2 % increases with decreasing the size. The
MgO 8.26 distribution percentage of the SnO2 reaches its
CaO 4.90 maximum at size less than 11.3 mm. It is noticed that
Na2O 4.05 the size fraction larger than 11.3 mm represents
K2O 1.79 about 30 % by weight from the cassiterite ore and
contains only about 0.017 % SnO2. Therefore the ore
TiO2 0.53
is screened on the sieve 11.3 mm for preparing a feed
Fe2O3 6.16 for the recovery process. The oversize is discarded
ZrSO4 0.01 and the undersize fraction is used for the recovery
Cl 0.20 process. Table 5 represents the size analysis and
P 2O5 0.11 distribution percentage of SnO2 of the undersize of
the sieve 11.3 mm. The size fraction from 11.3 mm
SO3 0.046 to 0.125 mm represents about 95 % by weight with
L .O. I 3.00 0.061 SnO2 % and 95 % distribution of cassiteriate.
It was crushed and grinding using rod mill in closed
circuit with screen 0.125 mm to prepare a feed for
shaking table.
18 100 0.10
Cum. Wt% passing
16
SnO2 % ( ±0.0005)
14 80 SnO2 Distribution % 0.08
Cumulative Weight % Passing
SnO2 Distribution %
12
60 0.06
SnO2 %
10
8
40 0.04
6
4 20 0.02
2
0 0 0.00
10 100 1000 10000
Size, micron
Figure 4. The relation between the size (micron) of the original sample and cumulative weight %, SnO2 %, and
distribution percentage of the SnO2
Table 5. Size analysis and distribution of the
fine fraction less than 80 micron was taken for falcon
undersize fraction of sieve 11.3 mm separation technique.
Weight SnO2 % Distribution
Size, mm Table 6. Grinding and screening
% (±0.0005) %
-11.3 + 0.9 81.52 0.061 80.80 Size fraction, Weight SnO2 % Distribution
-0.9 + 0.4 7.39 0.060 7.17 (mm) % (±0.0005) %
-0.4 + 0.125 6.60 0.064 6.83 -0.125 + 0.080 45 0.0580 42.08
-11.3 to 0.125 95.51 0.0611 94.8 - 0.080 55 0.0653 57.92
-0.125 + 0.08 1.88 0.060 1.82 Total 100 0.062 100
-0.08 2.61 0.080 3.37
Total 100.00 0.062 100.00 3.4. Relation between Recovery of Cassiterite and
Different Experimental Parameters
3.3. Preparation of Feed for Shaking Table The Design-Expert 6.0 software program was used
The results of grinding and screening of size fraction to analyze each response to the regression model of
less than 11.3 mm are presented in table 6. It has the parameters listed in table 3. Table 3 represents
been noticed that the size fraction -0.125 +0.08 mm groups of experimental data and it could establish the
represent about 45 % by weight with 0.058 % SnO2 multinomial model of the relation between recovery
and 42 distribution percentage of cassiterite . The of cassiterite and the operating parameters. It can be
M. A. Youssef, M.K. Abd El-Rahman, N.H. Helal, M. M. El- Rabiei, S. R. Elsaidy / The Journal of ORE DRESSING ® 2009 5
expressed as equations 2 and 3 for both shaking table separation (λ, α2, β2, αλ) are more significant terms
separation and dry high intensity magnetic and the terms in case dry magnetic separation
separation. The analysis of variance of the ( ε,δ,ϕ,ε2, δ2, ϕ2) are more significant terms. The
multinomial model is given in tables 7 and 8. The values greater than 0.1000 indicate model terms are
model F-value (χ) for both shaking table separation not significant. Table 8 represents the “ANOVA”
and dry magnetic separation represents 5.26 and statistical analysis for both shaking table and dry high
100.79 respectively and it indicates that the model is intensity magnetic separation. The values in that table
significant. There is only 0.19 % and 0.01 % chance indicate the will fitting of the experimental results to
for shaking table and dry magnetic separation that a the polynomial model equations for both shaking
"Model F-Value" this large could occur due to noise. table and dry magnetic separation and hence accuracy
Values of "Prob > F" less than 0.0500 indicate model of these models.
terms are significant. The terms in case shaking table
η Recovery = _7.43 _ 2.48 * α + 77.38 * β + 7.76 * γ _ 0.68 * λ _1.8 * α2 _ 17.42 * β2 _ 6.63* γ2 _ 0.045* λ 2 + 2.1* αβ +
1.5* αγ + 0.55* αλ + 1.0* βγ + 0.16* β λ + 1.0* γλ (2)
σ Recovery = -585.05 +16.94* ε + 0.33* δ + 0.014* ϕ - 0.11* ε2 - 4.44* δ2 - 2.36* ϕ2 + 3.40 * εδ + 1.80* εϕ + 7.20*
δϕ (3)
Table 8. ANOVA for response surface quadratic model for the shaking table separation and dry high intensity
magnetic separation
Shaking Table Separation Dry Magnetic Separation
The statistical parameters ρ (Grade %) η (Recovery % μ (Grade %) σ (Recovery %
The standard deviation 0.85 1.77 2.24 0.50
R-squared 0.9575 0.8402 0.9820 0.9923
Adequate precision 15.631 7.879 18.017 28.811
78.4849
different values of the studied factors. In figure 5a it
is noticed that with increasing both splitter 76.325
3.00
Desirability
0.295 0.417
0.417 0.540
85.9647 0.540
84.4923
83.0198 2.75
Recovery %
81.5474
Predicti 0.91
2.50
25.00
400.00
22.50
325.00
2.25 0.786
20.00
250.00
water flow rate (l/min) 17.50 175.00
Feed rate (gm/min) 0.540
15.00 100.00 0.540
0.663
0.417
Figure 5b. Response surfaces for the shaking table 2.00
concentrate recovery as a function of different factors 3.00 3.50 4.00 4.50 5.00
(a)
97.212
100.00
Desirability
94.0903 0.381
0.381
90.9685
Recovery %
87.8468
87.50
0.536
84.725
0.536
Belt speed (rpm)
0.690 0.690
75.00
Predicti 1.00
100.00
80.00
87.50
77.50
75.00
75.00 62.50
Belt speed (rpm) 62.50 72.50
Splitter inclination (degree)
50.00 70.00
50.00
Figure 6a. Response surfaces for the dry magnetic 70.00 72.50 75.00 77.50 80.00
separation concentrate recovery as a function of (feed
rate 500gm/min.) Splitter inclination (degree)
(b)
Figure 7. Optimum parameters for shaking table and
98.2563 dry high ıntensity magnetic separation
95.1641
88.9797
Table 10. Shaking table and dry high ıntensity magnetic separation cassiterite concentrates at optimum
parameters
Shaking Table Separation
Fraction Weight % SnO2 % Recovery %
Concentrate 0.314 13.2 86.2
tail 99.686 0.0066 13.8
Total 100 0.048 100
Cleaning of Shaking Table Concentrate using Dry High Intensity Magnetic Separation
Fraction Weight % SnO2 % Recovery %
Operational Overall Operational Overall
Non magnetic 14.5 0.046 90.67 96.7 83.36
Magnetic 85.5 0.268 0.51 3.3 2.84
Total 100 0.314 13.2 100 86.20
grade for both shaking table and dry magnetic accumulations in the ESCAP region, Berlin,
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experimental design. The best combination desirable
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Herz, N. eds, Concise encyclopedia of mineral
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