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    14 views2 pages

    C 113

    Uploaded by

    sushmabindu
    astm

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    © All Rights Reserved
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    iy Designation: C 113 - 93 Standard Test Method for ‘re Ree Praga, Pot pte von aaa oo AS Sr, apy AST intitedmbwcurert coved ek spe nme eek Reheat Change of Refractory Brick’ “This standard i sed unde the fred designation C 113 the wemer immediately flowing the designation indicts the year af ‘nig! adoption ti he cate of revo, th ea fat ein. A umber pentose Indes he ya oat eaRpva. A ‘Supererp epon (indicts an eit huage sine the ast ein o approval This sander has been approved fr use by agencies ofthe Deparment of Defense. Const ihe BoD Index of Sprifeaion ond Standards forthe speci ear of sue which has ben adopted by he Departmen of Defense 1, Scope 1.1 This test method covers the determination of the permanent linear change of refractory brick when heated under prescribed conditions. 1.2 The values stated in inch-pound units are to be regarded asthe standard, The values given in parentheses are for information only. [Note {—Test methods incorporating additional provisions pertinent to specific refractory materials are given inthe following Test Methods: C179, C210, C436, and C605. 1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this stardard to establish appro- Driate safely and health practices and determine the applica- bility of regulatory limitations prior to use. 2, Referenced Documents 2.1 ASTM Standards: C 134 Test Methods for Size and Bulk Density of Refrac- tory Brick and Insulating Firebrick? C179 Test Method for Drying and Firing Linear Change of Refractory Plastic and Ramming Mix Specimens? €210 Test Method for Reheat Change of Insulating Firebrick? C436 Test Method for Reheat Change of Carbon Refrac- tory Brick and Shapes* ‘C605 Test Method for Reheat Change of Fireclay Nozzles and Sleeves? £230 Temperature-Electromotive Force (EMF) Tables for Standardized Thermocouples? 3. Significance and Use 3.1. Refractory brick and shapes of different compositions exhibit unique permanent linear changes after heating or reheating. This test method provides a standard procedure for heating various classes of refractories with appropriate heating schedules. 3.2 Linear rebeat changes obtained by this test method are suitable for use in research and development, also often used to establish written specifitations between producers and consumers. test method ie under the juratiction of ASTM Commitee C4 on Refractories andthe det respoasbity of Subeommltee CUBIS on Pysca ‘Teas ‘Cures edition approved March 15, 1993. Publihed May 193. Orally ublhed as C1134. Las previous ediion C113 17 2 annual Book of ASTM Standards, Vol 130 3 annual Book of ASTM Standards, Vol 14.03, 3.3. Care should be exercised in selecting samples that are representative of the product being tested and that the schedule selected is appropriate to the product. 4. Apparatus 4.1 Kiln, of such design that the specified heating schedule and atmosphere can be maintained throughout the heating zone. 4.2 Linear Measuring Device, capable of being read to 0.02 in, (0.$ mm) over a span of 10 in, (254 mm). A hook-nule, as specified in Test Methods C 134, a vernier caliper, of a dial gage device may be used. 4.3 Gas Sampling and Analysis Equipment, capable of determining the percent free oxygen and total combustibles in the atmosphere of the test chamber. 5. Tesi Specimens 5.1 For each test use three rectangular specimens mea- suring 9 by 4% by 2% or 3 in. (228 by 114 by 64 or 76 mm) in size, or, if smaller, shapes approaching these dimensions as, closely as possible, These may be commercial brick of the specified size or test pieces cut out of larger shapes. 5.2 Using ceramic paint or crayon, label each specimen, and make a reference mark at each end on the center line of a broad face to indicate the exact position where the measurement is made, Measure the length on each of the three test specimens to the nearest 0.02 in. (0.5 mm). 6, Procedure 6.1 Placing Specimens in Kiln—Place the test specimens in the kiln go that each rests edgewise, that is, ona 9 by 2 or 3.in, (228 by 64 or 76-mm)} face and set only one course high. Place each specimen upon the corresponding face of supporting brick that is from the same lot as the test specimen or at least of equal refractoriness. Place between the test specimen and the supporting brick a layer of suitable refractory material, that is non-teactive under the test conditions and passing an ASTM No. 16 (1.18-mm) sieve (equivalent to a 14-mesh Tyler Standard Series) and retained ‘on an ASTM No. 40 (42541m) sieve (equivalent to 35-mesh Tyler Standard Series). Place each specimen so that it is not less than 1/4 in, (38 mm) from other test specimens ‘or from the furnace wall. 6.2 Temperature Measurement—Measure the tempers- ture within the kiln by means of an appropriate calibrated thermocouple. Refer to E230 Tables 1 and 2 for the tolerances and upper temperature limits for use of various thermocouples. At higher temperatures, the thermocouple may be withdrawn and a calibrated optical or radiation Gh 113 ‘TABLE 1 Heating Schedule for Reheat of Various Types of Retractoriee gate ioumenl ‘Temperature of Test Spacivan, °F (°C) (Th highest erperature in each chad sha be maria fx 8) tom Stat of reting." ‘Schools A Schule ScheduaG Schakle Schade E Schade © Schade Sched H 7 ‘son Teed aa) THO GED Tw (950) reosTeTE) SOO I) TORR 10 GED TAO RD 2 25 (4) 2or0 (1700) 2470 7300 25701900) 2280(128) — zz30 (12a zarO THEME) 297090 7070 1500) 3 Seto 21901200) 2560 (1400) 2608 (1475) 2as0 (1960) ZaHOLTZN BEKO (L4G) 26N (1478) 2685 (479) 4 365, 2845 (1585) ‘ran H600) 2645 1666) 2848 (1868) 3 365) 2510 1600) 2o10 (160 2910 1600) é #65) zero (183 29701690) e888) 5000 1680) 3000 1880) ; re) 3008 1688) 565) ‘3070 (1660) 1565, 3090 (700) TABLE 2. Precision of Interiaboratory Test Reaults \Nore—Relaveprecksen does no pp shoe vans pass tough th pot oz, ‘Shoals 8 Soedue Sheaae Pooled 2550°F 210 ‘00 Presion waoay 73, 3 oa 70% 30%, 70% 2m Freauy ——_Alzuna Feacey Aumina___Abmona___——Auming Alara Teor Garge ‘owage§ on 078 nos +209 +018 3 083 Praser Repestaniy 032 ome 03s 036 018 oss oa 096 eprod Sy Ie Ose ore oat 086 02s 078 oa 080 pyrometer can be used. Place the hot junction of the thermocouple or sight the pyrometer so as to register the ‘temperature of the test specimens. Make temperature read- ings at intervals not greater than 15 min, Check the kiln periodically by thermocouples, pyrometers or pyrometric cones to ensure that temperatures over the hearth do not differ by more than 25°F (14°C) or one-half cone. 6.3 Test Atmosphere—At all temperatures above 1470°F (800°C) the furnace atmosphere shall contain a minimum of 0.5 % oxygen and 0% combustibles. Take gasanalysis ‘samples from the furnace chamber proper. 64 Tes Temperature ScheduleOpeate the kiln 0 sto conform to the appropriate heating schedule for the class of | refractory being tested as shown in Table 1. Adjust the firing

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