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Article in Transportation Research Record Journal of the Transportation Research Board · January 2003
DOI: 10.3141/1837-04
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Dan G. Zollinger
Texas A&M University
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TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 1
ABSTRACT
This paper presents an experimental study on the development of strength and modulus of
elasticity of cement-treated aggregate base (CTAB) materials. Unconfined uniaxial
compression tests were conducted with 189 samples in total for sixteen CTAB mixtures at
different ages. Two different aggregates, conventional crushed limestone base and recycled
concrete materials, were used in the test program. Based on the test results, equations were
proposed for estimating the development of compressive strength and modulus of elasticity of
CTAB materials with time. Test results indicated that the relationship between the compressive
strength and elastic modulus of CTAB materials could be expressed in a single equation
regardless of aggregate type and mixture proportions.
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 2
INTRODUCTION
Cement-treated aggregate base (CTAB) is defined as a mixture of aggregate material and
measured amount of portland cement and water that hardens after compaction and curing to
form a durable paving material (1). It is widely used as a base course for either flexible or rigid
pavements. Other descriptions, such as cement-treated base, cement-stabilized base or soil-
cement, are sometimes used for this type of application depending on the materials involved.
Compared to the other cement-treated or stabilized materials, CTAB generally involves higher
contents of cement and coarse aggregates, and therefore, higher strength and stiffness. As a
structural layer of pavements, CTAB shows elastic, slab-like response to loading and its
performance is influenced by the strength and modulus of the material. These properties are
also crucial for design procedures that consider the stress-strain relationship and fatigue
characteristics of the CTAB layer (2, 3).
By virtue of the simplicity of the test method, the unconfined compressive strength is
most commonly referred to as the mix design criteria for the construction of CTAB. Many
previous studies proposed empirical relationships between the compressive strength and
flexural or tensile strength of cement-treated materials that are useful for the structural design
of the layer. The flexural and split tensile strength of cement-treated materials were found to
be about 20-25% and 10-15% of the unconfined compressive strength, respectively (4). For the
design and analysis purposes, 10% of the compressive strength is generally regarded as an
acceptable estimate of the tensile strength of CTAB. It is noted that these relations are not
significantly different from the relationships proposed for normal concrete.
Methods to determine an appropriate elastic modulus of CTAB material are
complicated because of the difficulties associated with testing and interpreting the test results.
Because of these difficulties, it was recommended for design purposes to use a relationship
between the strength and modulus of elasticity of the material in lieu of testing. Many previous
studies have proposed relationships between the unconfined compressive strength and modulus
of elasticity of cement-treated materials (5-7). These studies suggest that different relationships
exist for different types of cement-treated materials depending on the quality of aggregates
used. For lean concrete and CTAB materials, Thompson (4) recommended use of the
relationship of normal concrete provided by the American Concrete Institute (ACI).
This study investigated the behavior of CTAB materials related to the development of
strength and elastic modulus under uniaxial compression. Methods of estimating those
properties were revisited and calibrated based on the CTAB data obtained in this study.
TEST PROGRAM
Materials
Two different aggregate base materials, which are currently used in practice for road base
construction in Harris County, Texas, were used in this study for mixing the CTAB test
samples. One is a conventional crushed limestone base material and the other is a recycled
concrete material. Both materials contain particles sized from 2 inches (50 mm) to –No.200
(75 µm) in accordance with the grading requirements of the Texas Department of
Transportation (TxDOT) Specification Item 276, Portland Cement Treated Base. Collected
aggregates were divided into seven different sizes (+3/4 in., 3/8 in., No.4, No.10, No.40,
No.200, and –No.200) and re-combined according to the aggregate proportions designed for the
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 3
test mixtures. The maximum aggregate size was limited to 3/4 inches (19 mm) throughout the
test program for fabricating the laboratory sized test samples.
Table 1 shows the specific gravity and absorption of the aggregates averaged from three
to five replications. The content of minus No.200 materials indicates the weight ratio relative
to the total weight of fine aggregates passing No.4 sieve. As indicated, the recycled concrete
material has higher absorption capacity and lower amount of the fines passing No.200 sieve
than the conventional crushed limestone base material. In addition to the aggregates, selected
amounts of Type I portland cement and water were added according to the mixture design of
the test samples.
Experimental Design
Three test variables were selected to investigate the effects of the mixture components and their
proportions on the strength and stiffness of the CTAB mixture. Selected test variables are:
content of coarse aggregates (remaining No.4 sieve),
content of fines (passing No.200 sieve), and
cement content.
Content of each mix component is determined by the weight ratio of the component to total
aggregates. Two different application levels were selected for the respective mixture variables
as shown in Table 2. This two-level, three-variable factorial (23) design resulted in sixteen
different test mixtures in total; eight for each aggregate type, i.e., recycled concrete or crushed
limestone.
Table 3 shows the complete factorial of the test mixtures for each aggregate type. The
symbols (–) and (+) in the table indicate the low and high application levels of the mixing
variables, respectively. As shown, the test mixtures were identified by the numeric
identification code that represents the designated proportioning of the mixing variables. A two-
letter code, RC (recycled concrete) or CL (crushed limestone), was prefixed to the numeric
mixture ID for the identification of the aggregate type used in the respective mixtures. For
example, the identification ‘RC-1’ represents the test mixture that contains recycled concrete
material and all of the three mixture variables are combined at the low application levels.
Mixture Design
Aggregate gradations for the test mixtures were determined in accordance with the grading
requirements of the Grade 1 in the TxDOT Specifications Item 247, Flexible Base, and the
Type I-B in ASTM D 1241, Standard Specification for Materials for Soil-Aggregate Subbase,
Base, and Surface Courses. Table 4 shows the aggregate gradations of the test mixtures.
Corresponding gradation curves are presented in Figure 1. As can be seen, the aggregate
gradations are divided into two groups, fine mixtures (mixtures 1, 3, 5, 7) and coarse mixtures
(mixtures 2, 4, 6, 8), according to the contents of aggregates passing the No 4 (4.75 mm) sieve.
Mixtures in each group have the same aggregate proportioning except the content of fines
passing the No. 200 (0.075 mm) sieve. The crossed gradation curves in the lower corner of
Figure 1 represent the different application levels of the fines within the same mixture groups.
As previously indicated, the maximum aggregate size for test specimens was reduced to 3/4 in.
(19 mm). The proportioning of coarse aggregates was accordingly adjusted within the grading
requirements listed in Table 4. The portions required for the aggregates greater than 3/4 in. (19
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 4
mm) were evenly distributed to the portions of aggregates remaining 3/8 in. (9.5 mm) and No.4
(4.75 mm) sieves.
Molding moisture contents of the test mixtures were determined based on the optimum
moisture content (OMC) of the respective mixtures. The OMC of the each of sixteen test
mixtures was determined in accordance with ASTM D 558, Moisture-Density Relations of
Soil-Cement Mixtures. Table 5 shows the results of the OMC tests of the mixtures. It appears
from the results that the content of coarse aggregates is the most influencing factor for the
OMC and density of the CTAB mixtures, while the effects of other two mixing variables are
not considerable. Based on this observation, the OMC test results are decomposed into two
groups in average according to the content of coarse aggregates of the mixtures (Table 6). The
mixtures 1, 3, 5, 7 are designated as the fine mixes since they contain less amount of coarse
aggregates than the mixtures 2, 4, 6, 8, in which the coarse aggregates are mixed at the high
level of application.
Because of the higher absorption of recycled concrete materials, the OMC of the CTAB
mixtures containing the recycled concrete was higher than that of conventional crushed
limestone mixtures. Due to the very high absorption of the coarse particles of recycled
concrete materials, the coarse mixes containing the recycled concrete show higher water
demand for the OMC than the fine mixes, while the opposite is the case for the crushed
limestone mixtures. The maximum density does not show significant difference between the
fine and coarse mixes for a same aggregate source. As indicated in Table 6, the molding
moisture contents of the strength test samples were determined at the average OMC of the
respective mixture groups.
Test Methods
Unconfined compressive strength and modulus of elasticity of the test mixtures were
determined using 4×8 in. (100×200 mm) cylinder specimens in accordance with ASTM C 39,
Test Method for Compressive Strength of Cylindrical Concrete Specimen, and ASTM C 469,
Test Method for Static Modulus of Elasticity and Poisson’s Ratio of Concrete in Compression.
The specimens were fabricated in accordance with ASTM D 1632, Practice for Making and
Curing Soil-Cement Compression and Flexure Test Specimens in the Laboratory.
The specimens were cured at a controlled temperature of 77°F (25°C) and 100 %
relative humidity until the designated ages of testing. The tests were conducted at the ages of
1, 3, 7 and 28 days. Therefore, 64 different test conditions were considered in this test program
by the combination of 2 different aggregate types, 8 different mixture proportions, and 4
different testing ages. Three samples were prepared for the respective test cases.
Uniaxial compressive load was applied to the specimen by a servo-hydraulic MTS
testing system at a constant rate of 0.05 in./min. (1.25 mm/min.). The axial deformation of the
specimen was traced during the test by three linear variable differential transformers (LVDTs)
installed at the middle of the cylinder at 4 in. (100 mm) gage lengths. Figure 2 shows the test
configuration.
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 5
t
f c (t ) = f c (28) (1)
a + b⋅t
where, fc(t) = compressive strength at time t,
fc(28) = reference 28-day compressive strength, and
a, b = experimental coefficients.
Calibration of the ACI model to the CTAB test data resulted in a new set of coefficients
of a=2.5 and b=0.9. This new set of coefficients is expected to be applicable for any CTAB
mixtures regardless of aggregate type and mixture proportioning. Figure 5 shows the strength
prediction curves of the test mixtures projected over the average test data of the mixture groups
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 6
of low (4%) and high (8%) cement contents. As shown, the ACI model and the calibrated
model produce close estimations to each other, yet the ACI model gives some conservative
estimation for the strength of CTAB mixtures in early ages.
Modulus of Elasticity
The development of elastic modulus of CTAB materials was investigated using the stress-strain
relationships of the mixtures identified from the strength tests. Modulus of elasticity is
determined as the initial secant modulus at 25 percent of the ultimate stress. Figure 6 shows
typical stress-strain relationships obtained in this study for the two types of CTAB mixtures at
different ages. It is noted that high strength mixtures follow the typical stress-strain behavior of
brittle materials like concrete, while the response of low strength mixtures shows some yielding
plateau, which is a typical behavior of unbound materials.
Table 8 shows the average modulus of elasticity of the test mixtures at different ages.
Same as the results of strength measurements, the elastic modulus of recycled concrete
mixtures are 20 to 30 percent lower than that of crushed limestone mixtures. The effects of
mixing variables on the development of the modulus of elasticity were also found not much
different from the result of strength tests. Again, for a given aggregate type used, applied
cement content appears to be the most governing factor for the development of stiffness or
modulus of elasticity. The ratio of elastic modulus of high cement (8%) to low cement (4%)
mixtures reaches over 2.0 at the early ages, while it generally ranges from 1.3 to 1.7 for the
mixtures aged more than 7 days.
It is noted that the development of elastic modulus may be inferred from the
characteristics of strength development. Use of ACI model shown in Equation 2 has been
generally accepted for the estimation of elastic modulus of CTAB materials. However, it
should be noted that the ACI model was proposed for concrete applications and it may not be
relevant to CTAB materials. In this regard, relationship between the measured compressive
strength and modulus of elasticity of CTAB test mixtures was investigated. The empirical
coefficient and exponents in Equation 2 were calibrated for the CTAB data obtained in this
study. The calibration resulted in Equation 3 that can be used for the prediction of elastic
modulus of CTAB materials. The time-dependent strength, fc(t), can be estimated by Equation
1. Therefore, when the 28-day compressive strength is known, the time-dependent strength and
elastic modulus of CTAB materials can be estimated by using Equations 1 and 3.
Figure 7 shows the relationships between the compressive strength and elastic modulus
of CTAB mixtures projected over the scatter plot of test data obtained in this study. As can be
seen, the proposed model (Equation 3) provides a good agreement at high correlation with the
test data. The ACI model shows shifted overestimations of the modulus of CTAB mixtures.
Supposedly, the ACI model was developed based on the concrete data having strength ranges
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 7
above 2000 psi. The ACI model then may not be useful even for concrete at lower strength or
early-age concrete. The proposed equation covers all the data for the mixtures of the two
different aggregate types at a wide range of strength from 200 to 2000 psi (1.4 to 13.8 MPa).
Figure 8 shows the scattered comparisons of measured and estimated elastic moduli of the
CTAB test mixtures. The proposed model was used in these comparisons. The coefficient of
determination shown in the figure just represents how well the measured and estimated values
correlate linearly. This may indicate the soundness of the estimation using the proposed model.
The proposed model is expected to be applicable for the estimation of elastic modulus of any
CTAB mixtures regardless of aggregate type and mixture proportioning.
SUMMARY
The behavior of CTAB materials was experimentally investigated with respect to the
development of strength and elastic modulus of the material. Findings of the study may be
summarized as follows.
1. CTAB containing recycled concrete materials develops lower strength and modulus than
the mixtures with conventional aggregate base materials having the same mix proportioning
and age. This might be caused by the higher moisture requirements of recycled concrete
materials.
2. For a given aggregate type, the developments of strength and modulus of CTAB mixtures
are mostly governed by the applied cement content. Other mixing variables, such as
contents of coarse aggregate and fines, are found to be compounded each other, and their
overall effect is less significant compared to the effect of cement content.
3. The development of compressive strength of CTAB mixtures can be estimated by using
Equation 1 regardless of the aggregate types used. Experimental coefficients of the
equation are calibrated for CTAB materials.
4. The ACI equation proposed for the estimation of elastic modulus of normal concrete is
found to overestimate the modulus of CTAB. The equation is refined for CTAB
applications based on the test data obtained in this study.
5. The relationship between the compressive strength and modulus of elasticity is proposed for
CTAB materials (Equation 3). The proposed relationship is expected to cover any types of
CTAB materials having the strength in the range of 200 to 2000 psi (1.4 to 13.8 MPa).
ACKNOWLEDGMENTS
This paper was prepared from a study conducted in Texas Transportation Institute under the
research project 4954, “Use of Recycled Portland Cement Concrete Fines in TxDOT
Applications,” sponsored by Texas Department of Transportation.
REFERENCES
1. PCA. Cement-Treated Aggregate Base. Report SR221.01S. Portland Cement Association,
1979.
2. PCA. Thickness Design for Soil-Cement Pavements. Bulletin EB068.01S, Portland Cement
Association, 1970.
3. George, K. P. Characterization and Structural Design of Cement Treated Base. In
Transportation Research Record 1288, TRB, National Research Council, Washington,
D.C., 1990, pp. 78-87.
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 8
4. Thompson, M.R. Mechanistic Design Concept for Stabilized Base Pavements. Civil
Engineering Studies, Transportation Engineering Series No.46, University of Illinois,
Urbana, IL, 1986.
5. Lilley, A. A., and R. I. T. Williams. Cement-Stabilized Materials in Great Britain. In
Highway Research Record, HRB, National Research Council, Washington, D.C., 1973, pp.
70-82.
6. Larsen, T. J., and P. J. Nassbaum. Fatigue of Soil-Cement. Bulletin D119, Portland Cement
Association, 1967.
7. Williams, R. I. T. Cement Treated Pavements: Materials, Design and Construction.
Elsevier Publishers, London, UK, 1986.
8. Scullion, T., S. Sebesta, and J. P. Harris. A Balanced Approach to Selecting the Optimal
Cement Content for Soil-Cement Bases. Research Report 404611-1, Texas Transportation
Institute, Texas A&M University, College Station, TX, 2000.
9. ACI Committee 230. State-of-the-Art Report on Soil Cement. Committee Report ACI
230.1R-90, ACI Manual of Concrete Practice: Part I, 1998.
10. ACI Committee 209. Prediction of Creep, Shrinkage, and Temperature Effects in Concrete
Structures. Committee Report ACI 209R-92, ACI Manual of Concrete Practice: Part I,
1998.
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 9
LIST OF TABLES
LIST OF FIGURES
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 10
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 11
TABLE 2 Test Variables and Application Levels for the CTAB Test Mix Design
Application Levels
Test Variables Designation
Low (–) High (+)
Cement Content C 4% 8%
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 12
1 – – –
2 + – –
3 – + –
4 + + –
5 – – +
6 + – +
7 – + +
8 + + +
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 13
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 14
TABLE 5 Optimum Moisture Content (OMC) and Maximum Dry Density (γd-max) of the
Test Mixtures
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 15
TABLE 6 Determination of the Molding Moisture Contents for the Test Mixtures
Max. Dry Density Molding
OMC (%)
Aggregate Mixture (lb/ft3) Moisture
Type Group Content
Mean SD (a) Mean SD (%)
Fine Mixes
Recycled 10.75 0.058 121.5 0.418 10.5
(Mix 1,3,5,7)
Concrete
(RC) Coarse Mixes
11.18 0.096 121.3 0.479 11.0
(Mix 2,4,6,8)
Fine Mixes
Crushed 7.23 0.096 134.8 0.312 7.0
(Mix 1,3,5,7)
Limestone
(CL) Coarse Mixes
6.65 0.173 133.7 0.417 6.5
(Mix 2,4,6,8)
(a) Standard Deviation
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 16
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 17
TABLE 8 Modulus of Elasticity of the CTAB Test Mixtures at Different Curing Times
Modulus of Elasticity (×106psi)
Aggregate Mix ID
1 day 3 days 7 days 28 days
1 0.464 0.377 0.628 0.847 (1)
2 0.289 0.391 0.807 0.858 (1)
3 0.380 0.515 0.864 0.996 (1)
Recycled 4 0.322 0.727 (2) 0.804 0.944 (3)
Concrete
(RC) 5 0.475 0.861 1.057 (4) 1.426
6 0.584 0.945 1.298 1.312
7 0.551 – 1.111 1.243
8 0.727 1.110 (5) 1.200 1.276
1 0.561 0.657 0.872 1.050
2 0.760 0.823 0.842 0.878
(6)
3 0.764 0.837 0.843 1.198 (7)
Crushed 4 0.516 0.905 (5) 0.917 1.200 (8)
Limestone
(CL) 5 1.039 1.466 1.744 1.780
6 1.038 1.454 1.614 1.545
7 0.840 1.405 1.786 (4) 1.910
8 1.080 1.463 (5) 1.446 1.678
(1) Tested at 34 days; (2) Tested at 5 days; (3) Tested at 33 days; (4) Tested at 8 days
(5) Tested at 4 days; (6) Tested at 2 days; (7) Tested at 29 days; (8) Tested at 30 days
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 18
100
Gradation limits
Fine Mixtures: 1, 3, 5, 7
80
Coarse Mixtures: 2, 4, 6, 8
Percent Passing
60
40
20
0
0.01 0.1 1 10 100
Sieve Size (mm)
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 19
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Lim and Zollinger 20
1200
Low Content
800
600
400
200
0
A (+No.4) F (-No.200) C (Cement)
Test Variables
1600
Low Content
1400
Compressive Strength (psi)
High Content
1200
1000
800
600
400
200
0
A (+No.4) F (-No.200) C (Cement)
Test Variables
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 21
2500
RA, 4% Cement
28-day Compressive Strength (psi)
RA, 8% Cement
2000 CL, 4% Cement
CL, 8% Cement High Cement
Mixtures
1500 R2=0.561
1000
FIGURE 4 Scatter Plot of the 28-Day Compressive Strength and Maximum Dry
Density of Test Mixtures
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 22
2000
0
0 10 20 30 40
Time (day)
2000
Compressive Strength (psi)
1500
4% Cement
1000 8% Cement
ACI 209
This Study
500
0
0 10 20 30
Time (day)
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 23
1000
28day
Stress (psi) 750
7day
500
3day
250
0
0 0.0005 0.001 0.0015 0.002 0.0025
Strain (in/in)
2500
2000
28day
Stress (psi)
1500
7day
1000
3day
500
0
0 0.0005 0.001 0.0015 0.002 0.0025
Strain (in/in)
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 24
3.0
Test Data - RC
Test Data - CL
2.5 ACI 209 (Eq.2)
Modulus of Elasticity, E (10 psi)
2.0
1.5
1.0
0.5
0.0
0 500 1000 1500 2000 2500
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.
Lim and Zollinger 25
2.0
Test Data
Line of Equality
1.5
Estimated (10 psi)
6
1.0
0.5
R2 = 93.6%
0.0
0.0 0.5 1.0 1.5 2.0
6
Measured (10 psi)
2.5
Test Data
1.5
1.0
0.5
R2 = 94.3%
0.0
0.0 0.5 1.0 1.5 2.0 2.5
6
M easured (10 psi)
TRB 2003 Annual Meeting CD-ROM Paper revised from original submittal.