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Research Problem Discussed by Researcher
Research Problem Discussed by Researcher
ANALYSISOF
Finding/Results of Experiments
It was found from weight loss method that by increasing inhibitor concentration IE increases and at
15 V/v the extract have have high efficiencyb82.26% in hydrochloric acid, which showed that TN
plant leaves would give good corrosion inhibitor..From Scanning electron microscopy (SEM) data
collected the results obtained were concluded that because of the formation of good protective film of
TN leaves extract on mild steel surface improvement in which was seen in surface morphology is
responsible for inhibition for corrosion
Critical Analysis
Introduction To Topic:
For prevention corrosion in mild steel a lot of study and research has been carried out. Corrosion is
very common problem especially in the acidic environment which directly affects cost as well as
safety. There is numerous methods and techniques used in the industries in order to remove scales
and rust from the mild steel I,e some methods like some acidic chemical used for removal of
rust,Pickling,Etching (chemical or electrochemical) ,sometime the rust is washed with certain acids
these techniques are expensive also hazardous, On the other side some organic corrosion inhibitors
have certain advantages as compared to above discussed methods these inhibitors are considered to
be cost effective and also do not disturb the eco system of our planet. These inhibitors mostly derived
from natural resources i,e plants which contains sulfur,nitrogen and oxygen atoms by using different
mechanism and techniques the atoms can remove rust and corrosion.
Key Findings :
It was found from weight loss method that by increasing inhibitor concentration IE increases and at
15 V/v the extract have have high efficiencyb82.26% in hydrochloric acid, which showed that TN
plant leaves would give good corrosion inhibitor. The data collected from potentiodynamic
polarization confirmed that by decreasing I corr values with increasing in the concentration of the
leaves extract,we can get % at 15 v/v The maximum inhibition efficiency of 92.77, which is the
optimum concentration of the inhibitor decreasing the oxidation of metal and forming on the metal
surface protective film .From Scanning electron microscopy (SEM) data collected the results obtained
were concluded that because of the formation of good protective film of TN leaves extract on mild
steel surface improvement in which was seen in surface morphology is responsible for inhibition for
corrosion
Methodology and Parameter analysis:
In order to carried out the research first of all a Specimen of mild steel ( 4 cm x 2 cm x 0.1cm)
were made.than the mild steel were polished using emery paper. Than TN plant leaves were dried
and grinded. Than the specimen were dipped in HCL solution and weight loss was measured. Than by
using Bruker ALPHA 8400S spectrophotometer FTIR spectra were recorded ,Through Potentiodynamic
polarization methods ,polarization measurements for the evaluation of corrosion potential,
corrosion current and Tafel slope were carried out. For the assessment of qualitative chemical
composition of various samples of plant phytochemical screening were made,than after Mild steel
were immersed in the inhibitor solution upto 24 hours speciemen was removed dried rinsed in
distilled water and then by using JEOL Method surface morphology of Mild speciemen was
measured.
Importance Conclsion:
The author concluded that TN leaves is an effective corrosion pickling inhibitor for mild steel in 1 N
HCl acid. By using TN plants as an inhibitors for corrosion its non toxic eco-friendly, cost economical
and also TN leaves can found easily. Extraction of TN Leaves that there is 84.26% at optimum
concentration of 15 v/v by immersing one at room temperature.These leaves extraction prove to be a
mixed type inhibitor on the metal surface.The electrochemical tests results shows that weight loss
measurements are consistent