DAILY CONTROL TESTS

Steam Ships (32-60 Bar MPSG) Control and Dosage Chart Standard Treatment with DREWPLEX® OX Corrosion Inhibitor
Read MSDS before running these tests. Before testing, samples must be cooled to 25°C (77°F) by collecting through a sample refiltered through the same filter paper since the filter becomes more retentive on the second filtration.
cooler for safety and to prevent flashing which concentrates the sample.
If the sample is colored or turbid, filter before testing. If the sample remains cloudy after the first filtering, the sample should be
DEHA DAILY TEST PROCEDURES
1. Fill the sample cup to the 25-ml mark with feedwater sample. (Fig. 1).
2. Add 2 drops of Activator Solution. Stir gently with tip of an ampoule from the DREWPLEX OX 1 2 3 4 5 6
corrosion inhibitor Ampoule Test Kit to mix the contents of the sample cup (Fig. 2).
ml

4
25
20
3. Immediately snap the tip of the ampoule by pressing the ampoule against the side of the
sample cup. The sample will fill the ampoule and begin to mix with the reagent, leaving a
15
10
ml
25
20
10 : 0 0
5
small bubble to facilitate the mixing (Fig. 3).
15
10
5

4. Remove the ampoule from the cup. Mix the contents of the ampoule by inverting it several
times, allowing the small bubble to travel from end to end each time (Fig. 4). MEANS OF ADJUSTMENT DOSAGE INFORMATION
5. Wipe all liquid from the exterior of the ampoule and WAIT EXACTLY 10 MINUTES for full • DREWPLEX® OX corrosion inhibitor LESS THAN 0.2 PPM – INCREASE BY 25%
color development (Fig. 5). • Continuous Dosage 0.2 - 0.5 PPM – SATISFACTORY - NO CHANGE
6. Place the DREWPLEX OX corrosion inhibitor ampoule, flat end downward into center tube GREATER THAN 0.5 PPM – DECREASE BY 25%
of comparator. Direct the comparator toward a source of bright white light while viewing from
Initial dosage* is 100-300 ml/day. Increase dosage by 50-100ml/day until the DEHA control range is reached.
bottom. Hold comparator in a nearly horizontal position and rotate it until the color standard
below the DREWPLEX OX corrosion inhibitor ampoule shows the closest match (Fig. 6). Feed continuously with DREWPLEX AT boiler water treatment. (*When starting up a new system or one that
has been down for some reason).
7. Record the result and adjust dosage as necessary.
PHOSPHATE – Filter sample before running test DAILY TEST PROCEDURES
1. Fill sample cup to the 25-ml mark with cooled, filtered boiler water (Fig. 1). 1 2 3 4 5
2. Place phosphate VACU-VIALS1 ampoule in sample cup. Snap tip by pressing ampoule ml

against side of the cup. Ampoule will fill, leaving a small bubble to facilitate mixing (Fig. 2).
25
20 4
05 : 0 0
3. Mix the contents by inverting the ampoule, allowing the bubble to travel from end to end. 15
10
Wipe all liquid from the exterior. WAIT 5 MINUTES (Fig. 3). 5

4. Press ON. When the display shows “---”, the photometer is ready (Fig. 4).
5. Zero photometer by inserting VACU-VIALS blank ampoule into cell compartment, aligning
vertical line on ampoule with water droplet on photometer. Cover ampoule with light shield. MEANS OF ADJUSTMENT DOSAGE INFORMATION
Press ZERO button. Display will show “S1P” momentarily, then it will read “-0.0-” (Fig. 5). • ADJUNCT® B phosphate boiler 0 - 10 ppm — 30 grams per ton of water in the boiler system
6. After the 5 minute wait required in step 3, insert the phosphate VACU-VIALS ampoule with water treatment 10 - 20 ppm — 15 grams per ton of water in the boiler system
proper cell alignment into the cell compartment. Cover the ampoule with the light shield. 20 - 40 ppm — SATISFACTORY - NO CHANGE
Press the READ button. The meter will show “S1P” momentarily, then it will display the test 40+ ppm — HIGH, BLOWDOWN REDUCE DOSAGE
result in ppm ortho phosphate as PO4. Record the result and adjust dosage as necessary. INTIAL DOSAGE: 30 grams per ton of water in the boiler system
P & T ALKALINITY DAILY TEST PROCEDURES
PHENOLPHTHALEIN (“P”) ALKALINITY
1&2 3 5&6 7 8&9
1. Collect 50-ml cooled boiler water sample (Fig. 1 & 2).
2. Pour into evaporating dish (Fig. 1 & 2).
3. Add 4 drops phenolphthalein (Fig. 3).
4. Pink color - Alkaline. No Color - “P” alkalinity zero.
5. Add sulfuric acid N/10 drop by drop until pink color disappears (Fig. 5 & 6).
6. Note level of acid in buret. Convert ml to ppm using chart at right and record result in ppm as MEANS OF ADJUSTMENT DOSAGE INFORMATION
“P” alkalinity. Keep sample for “T” alkalinity test. Record result & adjust dosage as necessary. • GCTM concentrated alkaline liquid ML SULFURIC ACID N/10 PPM DOSAGE ADJUSTMENT
TOTAL (“T”) ALKALINITY 0 - 0.2 0 - 20 0.15 liter per ton of water in the boiler system
0.3 - 0.5 30 - 50 0.10 liter per ton of water in the boiler system
7. Add 3 drops Total Alkalinity Indicator-GP (Fig. 7). 0.6 - 0.8 60 - 80 0.05 liter per ton of water in the boiler system
8. Add sulfuric acid N/10 until pink color develops (Fig. 8 & 9). 0.9 - 1.3 90 - 130 SATISFACTORY
9. Note the level of acid in buret. Convert ml to ppm using chart at right and record result in ppm 1.3+ 130+ BLOWDOWN — REDUCE DOSAGE
as “Total Alkalinity”. Record the result & adjust dosage as necessary. TOTAL ALKALINITY TEST RESULT MUST BE IF NOT, DOSE 1 LITER OF GC REGARDLESS
LESS THAN TWICE THE “P” ALKALINITY. OF THE “P” ALKALINITY. TEST AGAIN IN 2 HRS.
©2012 Drew Marine • ®Registered trademark, TMTrademark, Drew Marine • 1Registered trademark of CHEMetrics Inc. – 1 – SS_BWT_STD_OX_CS
 CHLORIDE TEST DAILY TEST PROCEDURES
1. Measure 10-ml cooled boiler water sample into plastic vial (Fig. 1).
1 2 4
2. Add 3 drops phenolphthalein (Fig. 2). 3 N/10
Sulfuric
Acid
3. Add N/10 Sulfuric Acid dropwise until pink color disappears. Add 1 more drop (Fig. 3).
4. Add 6 drops Potassium Chromate. Sample will be yellow.
5. Add N/10 Silver Nitrate dropwise until the sample turns orange. 10 mil
6. Drops N/10 Silver Nitrate X 10 = ppm chloride.
7. Record the result and refer to chart at right for blowdown adjustment (Fig. 4). SATISFACTORY
MEANS OF ADJUSTMENT BLOWDOWN
• BLOWDOWN
NO BLOWDOWN
Silver Nitrate Drops N/10 1 2 3 4 5 6 7 8 9 10
PPM Chloride 10 20 30 40 50 60 70 80 90 100

NEUTRALIZED CONDUCTIVITY DAILY TEST PROCEDURES

1. Connect the Conductivity Electrode-ATC to the meter. Press the power button to power up 2 3
the meter.
2. Add 2 drops of phenolphthalein indicator to the cooled boiler water sample and stir. If the
sample turns pink, add Gallic Acid while stirring until the pink color disappears. This
neutralizes the sample (Fig. 2).
3. Place electrode into sample and take care to ensure that the liquid level is above its upper
steel band. Stir the electrode gently in the sample to create a homogenous sample (Fig. 3).
MEANS OF ADJUSTMENT DOSAGE INFORMATION
4. Allow time for the reading to stabilize. Note the reading on the display.
5. Record the result and refer to chart at right for blowdown adjustment. • BLOWDOWN Up to 700 µS/cm - Satisfactory Above 700 µS/cm
NORMAL MAINTENANCE BLOWDOWN INCREASE BLOWDOWN FREQUENCY
Blowdown should be carried out as per boiler manufacturer’s instructions. Blowdown is necessary to reduce
dissolved and suspended solids. If suspended solids are noticed in boiler water samples, blowdown regardless
of conductivity test results. Increase flash bottom blowdown for the first 4-6 months after treatment startup to
remove any transported oxides coming back from the steam system.

CONDENSATE pH TEST - Test immediately after drawing sample. DAILY TEST PROCEDURES
1. Collect 50-ml cooled condensate sample and pour into evaporating dish (Fig. 1).
1 2 3 4
2. Add 3 drops phenolphthalein. Sample should turn pink (Fig. 2).
3. Add sulfuric acid N/10 drop by drop until pink color disappears (Fig. 3).
4. Record the result and adjust dosage as necessary (Fig. 4).

MEANS OF ADJUSTMENT DOSAGE INFORMATION

• SLCC-ATM condensate corrosion
inhibitor
• Continuous Dosage
LIQUID COAGULANTTM Boiler Sludge Conditioner - No Test Required (For Oil Contamination Only)
Daily dosage 28-ml (1.0 oz.) per day for each ton of water capacity to condition suspended solids (oil and sludge) for removal by
bottom blowdown. Flash bottom blow and scum blow several times at 20 minute intervals after dosing the LIQUID COAGULANT
APPARATUS
Storage: Water Treatment Test Cabinet: PCN 1AA0016 (220 Volt) or 1AA2148 (110 Volt)
DEHA: DREWPLEX OX corrosion inhibitor AmpouleTest Kit: PCN 0387-01-0 includes: Sample Cup, Comparator,
30 Ampoules, 1 x 10 ml Activator Solution. The Activator Solution is also supplied separately under
PCN 0387036 (6 x 7 ml). Ampoules are also supplied separately under PCN 0387-02-8
Alkalinity/Chloride: Alkalinity/Chloride Reagent Set: PCN 0301-02-8 includes:
1 bottle Phenolphthalein, 1 bottle Total Alkalinity Indicator GP, 2 bottles Sulfuric Acid N/10, 2 Chloride LMP
Test Kits Alkalinity/Glassware Set PCN 0201-02-0 includes: LP Titration Assembly, Evaporating Dish (140ml),
Graduated Cylinder (50ml, plastic), 30ml Dropper Bottle for Total Alkalinity indicator GP,
30ml Dropper Bottle for Phenolphthalein, 3 Plastic Stirring Rods (150mm)
©2012 Drew Marine • ®Registered trademark, TMTrademark, Drew Marine • 1Registered trademark of CHEMetrics Inc.
NO PINK WITH PHENOLPHTHALEIN – INCREASE BY 25%
PINK COLOR – 1-2 DROPS N/10 ACID TO CLARIFY– SATISFACTORY NO CHANGE
PINK COLOR – 3 OR MORE – DROPS N/10 ACID TO CLARIFY– DECREASE BY 25%
INITIAL DOSAGE: 0.15 liter per ton of WATER IN THE boiler system
boiler sludge conditioner. Dose for two weeks or until oil removal is complete. If severe contamination persists, the possibility of
continuing oil leakage should be investigated and eliminated.
Conductivity: Conductivity Meter Kit Complete: PCN 0173062 includes Meter and Electrode, Case, Stand,
Rubber Armor, Gallic Acid, Brass Spoon, Plastic Beaker, 2 x 4 AAA Batteries and Manual
Standards are supplied separately under PCN 6968-03-8 (84µs) and PCN 6968-02-0 (1413 µs)
Phosphate: Phosphate Vacu-Vials1 Test Kit: 1AA5850
Filter Paper: PCN 0225-01-2, Box of 100
Funnel: PCN 0221-01-0
– 2 – SS_BWT_STD_OX_CS