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Article history: This paper demonstrates the operation of a smartphone based platform salinity sensor for accurate and
Received 8 April 2016 reliable monitoring of salinity level in oceanic water environment. To measure water salinity level using
Received in revised form 16 August 2016 the smartphone, two different approaches have been proposed and their sensing performances have
Accepted 18 August 2016
been compared. The first approach is based on Beer-Lambert principle where collimated light beam from
Available online 18 August 2016
an optical source while passing through the medium gets attenuated due to absorption by the medium
which can be detected and analyzed by the smartphone. The second approach is based on evanescent
Keywords:
field absorption from an uncladed U-bent sensing region of an optical fiber. Variation in salinity level
Smartphone
Salinity sensor
of the surrounding medium of the fiber sensing region affects the absorption of evanescent field and
Beer-Lambert principle this can be monitored by the smartphone. Two freely available android applications have been used for
Sensitivity detection and analysis of salinity level. The designed smartphone sensor has an ability to measure salinity
Ambient light sensor (ALS) level variation as low as 0.1 parts per thousand (ppt) with high accuracy and repeatability. We envision
that owing to its compact size, low-cost and truly user-friendly in nature, the sensing techniques could
emerge as potential alternative to existing salinity sensors that would be useful for different in-field
applications.
© 2016 Published by Elsevier B.V.
http://dx.doi.org/10.1016/j.snb.2016.08.102
0925-4005/© 2016 Published by Elsevier B.V.
I. Hussain et al. / Sensors and Actuators B 239 (2017) 1042–1050 1043
to do real time image processing, smartphone finds its applications 2. Working principle
in imaging, detection and analysis of different biological samples
[18–24]. In most of the smartphone based platform sensing sys- 2.1. Working principle of smartphone based direct transmission
tems, the CMOS image sensor of the phone has been explicitly used salinity sensor
for sensing of different chemical and biological samples.
The ambient light sensor (ALS) embedded in front panel of the Consider a collimated beam passes through an optical medium.
smartphone is meant for optimizing battery power consumption The beam gets attenuated due to absorption by the medium and
of the phone by controlling brightness of the display panel auto- the magnitude of absorption depends on the path length and the
matically in accordance with the surrounding environment. Almost concentration of the medium. According to Beer-Lambert principle
all branded smartphones contain Avago APDS-9930 or ams AG [31,32] the intensity of the transmitted light IT can be expressed as
(TAOS) TMD2771 integrated ambient light and proximity sensor
chip [25,26]. This integrated sensor assembly is composed of one IT = I0 exp (−εcl) (1)
low power infra-red (IR) LED and two photodiodes in which one where, I0 is the intensity of the incident light propagating through
is sensitive to both visible and infra-red light and the second pho- the absorbing medium of path length l, c is the concentration of the
todiode is sensitive primarily to IR light for proximity detection. solution and ε is the molar absorption co-efficient. From Eq. (1) it
The sensor module includes two built-in ADC for each photodi- can be inferred that for fixed optical path length, the intensity of
ode channel for conversion of photodiode current into a digital the transmitted light depends on concentration of the medium. In
value. The digital data is then transferred to a register and a built- the first sensing approach, we primarily exploit this principle for
in microprocessor reads the digital input signal. Thus, photodiode’s estimating the salinity level of water medium.
signal intensity converts into corresponding digital output which
can be displayed in the monitor of the smartphone by using suit-
2.2. Working principle of smartphone based evanescent field
able smartphone applications. Since the digitally converted output
absorption salinity sensor
is proportional to the photocurrent generated in the photodiode
of the smartphone, this easily readable output can be exploited
In the second sensing scheme, the exponentially decaying
for various photo-sensitive measurements. Freely available appli-
evanescent field from the fiber core-air interface of an uncladded
cations such as ‘Light meter app’ for photo-detection and ‘stanXY
U-shaped optical fiber has been utilized for development of the
app’ [27,28] for calibrations and data analysis for android platform
smartphone salinity sensor. Evanescent wave absorption in an
smartphones can be a used for direct sensing or measurement of
external medium is obtained by removing a certain region of the
various parameters. Using the ‘Light meter app’ a large dynamic
cladding of an optical fiber and then bent it to form a U-shaped
range 0–20,000 LUX of the smartphone ALS sensor can be recorded
fiber probe [33]. If the refractive index of the absorbing medium is
which eventually can be utilized for intensity modulation based
less than the refractive index of the core then the evanescent wave
sensing investigations. Again, using the existing mobile network
penetrates a short distance into the low index medium when total
facility it is possible to transfer data from remote location to any-
internal reflection occurs at a dielectric interface. The penetration
where in the world and real time data analysis can be performed
depth dp is the perpendicular distance from the interface at which
from the central laboratory. Very recently, we have demonstrated
the electric field amplitude E, deceases by 1/e of its value, E0 in the
that using ALS sensor of the smartphone and by using the above
interface [34]. We can write
applications, turbidity in drinking water and different environmen-
tal water bodies can be estimated reliably [29]. Using the integrated z
flash lamp and the ALS of the smartphone, an optical set-up can be E = E0 exp − (2)
dp
designed by which one can easily monitor the presence of chemical
and other toxic elements in water sample [30]. In the present work, The transmitted power P, of the optical fiber in which the
we primarily exploit the embedded flash lamp and the ALS of the cladding of length l is locally replaced by an absorbing medium
smartphone for salinity level detection and analysis of sea water. and is given by
In order to estimate the salinity level in sea water we propose two
smartphone optical set-up approaches. While the first technique P = P0 exp (−cl) (3)
is based on Beer-Lambert principle where the intensity of the col- where, P0 is the power transmitted without the absorbing medium,
limated light beam after passing through the saline medium gets is the evanescent wave absorption co-efficient and c is the
attenuated due to absorption by the medium and the intensity of concentration of the medium. The evanescent field absorption
the transmitted beam depends on salinity level (or concentration) co-efficient for a ray making an angle with the normal to the
of the medium which can be measured accurately and reliably by core-cladding interface is given by [35]
the smartphone sensor. The other approach is based on evanes-
cent field absorption from a U-shaped fiber optic sensor which is εn2 CosCot
␥= 1/2 (4)
coupled to the flash lamp and the ALS of the smartphone. The per- 2n21 cos2 c sin2 − sin2 c
formances of both the techniques have been compared in terms of
its sensitivity, reproducibility, and its dynamic range. Further, the where, ε is the bulk absorption co-efficient of the absorbing mate-
experimental data of the sensor responses have been compared rial, is the wavelength of light source, is the radius of the fiber
with the standard conductivity meter often used for such purpose. core, n1 and n2 are the refractive index of core and cladding,
For both the schemes, the experimentally obtained data have been is the incident angle at the core-cladding interface and c is the
analysed in the phone itself using freely available applications. critical angle of incidence. Since the bulk absorption co-efficient ε
Owing to its compact size, relatively inexpensive for development is proportional to the concentration of the medium therefore for
of the sensor, user friendly apps for handling of the sensing systems a controlled launching condition the evanescent wave absorption
and ability to share in-field data through the existing mobile net- co-efficient can be related to the concentration of the absorbing
work, we envision that the proposed techniques could emerge as a medium. If the sensing region of the optical fiber is bend to a U-
potential alternative tool over the existing commercially available shaped probe then the bending decreases the incident angle of
Salinometers in the market. the ray with the normal to the interface and the incident angle
approaches closer to the critical angle. Thus, from Eqs. (3) and (4)
1044 I. Hussain et al. / Sensors and Actuators B 239 (2017) 1042–1050
Fig 1. (a) Schematic of smartphone based direct transmission salinity sensor, (b) photo image of the proposed sensor.
it can be seen that using a U shaped probe the sensitivity of the 4.2. Experimental design of smartphone based evanescent field
evanescent field absorption can be enhanced significantly [33]. absorption salinity sensor
Fig. 2. (a) Schematic of smartphone based evanescent field absorption salinity sensor, (b) photo image of the designed sensor.
calibration curve and from the plotted data, the salinity value of a signal, the response of the designed sensor is found to be more sen-
medium has been estimated. Thus, using simple optical set-up and sitive for 635 nm incident light signal. This is attributed to the peak
two free applications, the salinity of any unknown samples can be spectral response of the embedded photo detector of the ALS of the
estimated easily with both of the designed sensing set-ups. smartphone, which is found to be highest in the wavelength range
600–700 nm and a 635 nm incident radiation overlaps fairly with
the peak spectral response of the embedded photo-detector. This
6. Results and discussion
preliminary investigation infers that a 635 nm incident radiation
would be suitable for the present sensing studies.
Prior to start of the investigation, the performance of the smart-
phone ALS sensor has been evaluated for different incident light
wavelength. Three different optical filters with optical pass wave- 6.1. Evaluation of sensor performance for both the sensor
length of 460 nm, 540 nm and 635 nm have been placed one by modules
one in the optical set-up of Fig. 1.We then introduce 10 samples
of different salinity level in the range 0–100 ppt in the optical path Upon confirming the incident radiation wavelength suitable for
of the set-up and the sensor responses have been recorded. Fig. 4 the present sensing investigation the sensor performances have
describes the sensor response curves for the three different inci- been evaluated for both the schemes described in Figs. 1 and 2.
dent wavelengths recorded by the designed sensing system for all Fig. 5 describes the sensor responses measured by the smartphone
the considered samples. These experimental data clearly indicate for both approaches for the considered samples. We observe sim-
that as compared to 460 nm and 540 nm incident wavelength light ilar trend in sensor responses for both the schemes. Compared to
Fig. 3. Workflow of the smartphone applications for salinity measurement of water samples.
1046 I. Hussain et al. / Sensors and Actuators B 239 (2017) 1042–1050
responses for both the schemes for media with salinity value rang-
ing from 0 to 1 ppt. Clearly, as compared to direct coupling scheme,
with U-bent fiber sensing probe a higher sensitivity (which is the
ratio of the change in sensor response to change in salinity level) has
been observed. The higher sensitivity for the U-shaped fiber probe
is attributed to the enhanced evanescent light signal coupling from
the sensing region to the surrounding absorbing medium. Further,
among the two designed schemes, the linearity in sensor response
for U-shaped fiber probe is found to better (with correlation coef-
ficient r ∼ 0.99386) than the first scheme (correlation coefficient
r ∼ 0.93608) in the salinity range 0–1 ppt. The error bars shown
in this figure represents the standard deviations for 5 consecutive
measurements of each sample.
Fig. 4. The response characteristic curve of smartphone ALS for different wave- 6.2. Evaluation of sensor characteristics for both the proposed
length. sensing schemes
direct transmission scheme, the sensitivity for the U-bent optical The evaluation of sensor characteristics for both the sensor mod-
fiber probe is however found to be higher. The responses of the ules have been carried out and corresponding sensor parameters
sensors are found to be piece-wise linear for both the schemes. The has been compared. The Detailed analysis of all the necessary sens-
inset in the same figure shows the zoom-in view of the sensors ing parameters has been discussed in the sub-sections given below:
Fig. 5. Response curve for both the sensor module for salinity range 0 ppt–100 ppt.
I. Hussain et al. / Sensors and Actuators B 239 (2017) 1042–1050 1047
Fig. 6. Uncertainty in measurement for both the sensing module for the salinity Fig. 7. Stability measurement data of solution with salinity of 35 ppt for both the
range 0 ppt–1 ppt. sensor module.
Table 1
Comparison of different sensing parameters for both the sensor module.
Sensor parameters direct light coupling salinity sensor U-shaped fiber probe salinity sensor
where, and s are the residual standard deviation (RSD) of the solutions of random salinity value using artificial sea salt have been
response and slope of the calibration curve. To measure the DL for prepared in the laboratory and the salinity level of the prepared
both the sensors, we consider the calibration curve shown in Fig. 5 samples has been initially measured with the standard conductivity
in the range 0–1 ppt. The RSD and slope has been evaluated from meter (3540 Bench conductivity meter, Bibby Scientific) in s/cm
this curve and the DL of the designed sensor is estimated using the and then converted the value into corresponding salinity ppt units
Eq. (6). The DL for the direct transmission salinity sensor is found [38]. The salinity of the prepared samples were then measured by
to be 0.13 ppt while for the U-shaped fiber optic probe this value is our designed sensing systems. Fig. 9 describes the histogram repre-
estimated to be 0.04 ppt. sentation of the experimental sensor data for the two smartphone
platform sensors and the standard tool. These data again clearly
indicate that almost similar sensor response have been observed
6.2.6. Evaluation of sensing range for both the sensor modules for all the three situations. For direct light coupling scheme, the
The evaluation of uncertainty in measurements signifies that error associated with the experimental data is found to be high in
with direct transmission based sensing scheme, a higher measure- low level of saline medium. This is attributed to low absorbance
ment error is obtained in the range 0–1 ppt with co-efficient of of the medium for low salinity level due to which a relatively high
determination R2 = 0.90322. It shows piece-wise linear trend for intensity of light signal is being received by the smartphone ALS.
higher salinity values. The sensing range for this specific scheme is This may cause fluctuations in the sensor readings. On the other
observed to be sensitive in the range 1–100 ppt. The uncertainty in hand, with fiber optic sensing set-up we observe fairly linear and
measurement for U-shaped fiber sensing probe is however found comparable data as that of the standard tool-conductivity meter
to be much less than the direct light coupling sensing scheme with used for the present work.
co-efficient of determination R2 = 0.98488 in the salinity range of The proposed two smartphone sensing schemes are useful in
0–1 ppt. This indicates that the sensing range for the former scheme transmitting the in-field experimental data from remote location
could be suitable for 0–100 ppt. to the central laboratory or anywhere in the world through the
Important sensing parameters such as sensitivity, residual stan- existing mobile network facility. Owing to the involvement of rel-
dard deviation, uncertainty, sensing range and DL have been atively low cost components and relatively simple optical set-up
evaluated for both the designed sensors. Table 1 summarizes the we envision that the designed sensing system could emerge as an
performance comparison for these parameters as yielded by both inexpensive alternative to its commercially available counterparts
the schemes. with added advantages of having ability to monitor and analyze
Finally, the performances of both the sensing schemes have in-field sensing data from the central laboratory. Fluctuations of
been compared with the laboratory grade conductivity meter usu- temperature and pressure may affect the measurement data, since
ally used for estimating the salinity level of sea water. Saline
Fig. 9. Histogram representation of comparison of salinity measurement of prepared water samples by the standard conductivity meter and by our smartphone salinity
sensing module.
I. Hussain et al. / Sensors and Actuators B 239 (2017) 1042–1050 1049
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Biographies Pabitra Nath received the M.Sc degree in Physics from Tezpur University, Napaam,
India, and the Ph.D. degree in electronics science from Gauhati University, Guwahati,
India, in 2000 and 2009, respectively. He is currently an Associate Professor with the
Iftak Hussain received the M.Sc degree in Physics from Tezpur University, Napaam, Department of Physics, Tezpur University. He has visited Micro and Nano Tech-
India, and currently pursuing his PhD degree from Tezpur University. His current nology Laboratory (MNTL), Department of Electrical and Computer Engineering,
research interests include design and development of smartphone integrated sen- University of Illinois at Urbana Champaign, Urbana, through BOYSCAST fellowship
sors for water quality monitoring and fiber optic sensor design. program 2010–2011 sponsored by the Department of Science and Technology, Gov-
ernment of India. His current research interests include fiber optics sensors and
Munmun Das has completed her master of science (M.Sc) in Physics from Tezpur system, Smartphone platform sensing systems, SERS and optical bio-sensing sys-
University, in 2016. Her current research interests include fiber optic sensors, Smart- tems.
phone platform sensing systems and optical devices.
Kamal Uddin Ahamad received B. Tech degree from NIT Bhopal M. Tech and PhD
degree both from IIT Guwahati. He is currently an Assistant Professor with the
Department of Civil Engineering, Tezpur University. His current research interests
include Water treatment, Low-cost treatment Technology, Water Quality, Waste
management.