Professional Documents
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Fotografias de Corrosion
Fotografias de Corrosion
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Services Overview Corrosion Photographs
Corrosion Control
Failure Analysis
Laboratory Testing ● bolt fracture surface ● boiler tube corrosion
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Environmental Services ● Intergranular fracture ● boiler tube corrosion (2)
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Special Corrosion Topics
Corrosion Photographs
Corrosion Glossary
Technical Newsletters
● turbine blade microstructure ductile iron micro
Failure Case Histories ●
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● turbine blade coating corrosion ● grain coarsening cracking
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● (2) turbine blade microstructure ● HE crack in 17-4PH
● dezincification (2)
● turbine hot corrosion
● hydrogen fracture
● bolt inclusions
● HE crack
● chloride SCC crack
● explosive decompression
● cleavage fracture
● graphitization
● polythionic acid SCC
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Services Overview SEM photograph of Hydrogen Embrittlement Fracture
Corrosion Control
Failure Analysis
Of A Fastener
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Fracture surface of a capscrew that failed due to hydrogen embrittlement. The intergranular fracture and
subsurface intergranular cracks are characteristic of fractures due to hydrogen embrittlement. The pitted
COMPANY
Contact surface was caused during cleaning to remove oxide from the fracture surface. 1000X
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Services Overview Hydrogen Embrittlement of Valve Capscrew Fasteners
Corrosion Control
Failure Analysis
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Technical Papers Body capscrews from a ball valve showing hydrogen embrittlement fracture. Exposed to atmospheric
Industry Standards conditions in a gulf coast environment, they corroded and fractured, separating the valve body. The left
RBI Procedure capscrew fractured due to hydrogen embrittlement cracking through the complete cross section. The right
capscrew initially fractured due to hydrogen embrittlement then propagated due to tensile overload. Both
COMPANY fractures started at the bottom of the photograph.
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Services Overview Hydrogen Attack Corrosion In A Boiler Tube
Corrosion Control
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Technical Papers Solids deposition and hydrogen attack corrosion at the ID weld in an 1800 psig carbon
Industry Standards steel boiler tube. The arrow marks the direction of flow. (~1X)
RBI Procedure
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Services Overview High-Temperature Hydrogen Attack In A Boiler Tube
Corrosion Control
Failure Analysis
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Technical Papers Hydrogen attack corrosion and cracking on the ID of an 1800 psig carbon steel boiler tube.
Industry Standards
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Services Overview Corrosion Of A Rene 80 Nickel Alloy Gas Turbine Blade
Corrosion Control
Failure Analysis
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Technical Papers Microstructure of a Rene 80 nickel allaoy blade from the 1st stage HP section of a gas
Industry Standards turbine. The blade suffered hot corrosion from exposure to molten sodium sulfate. The
RBI Procedure exfoliated, porous O.D. scale can be seen at the top of the photograph with sulfide
particles in the white layer underneath. The base metal contains unresolved brown gamma
COMPANY prime particles in the nickel alloy matrix. Electrolytic CrO3, 400 X.
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Services Overview Ductile Iron Microstructure
Corrosion Control
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Technical Papers Ductile iron microstructure of a reciprocating compressor body. The microstructure has
Industry Standards been heat transfered to transform all pearlite to carbide. The elongated, diamond shaped
RBI Procedure impressions are Knoop microhardness impressions. (100X)
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Services Overview Hot Corrosion Of Aluminide Coating On A Nickel Alloy Gas
Corrosion Control
Failure Analysis
Turbine Blade
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RBI Procedure SEM photograph of an aluminide coating on a gas turbine 2nd-stage HP nozzle showing
coating blisters caused by formation of corrosion products under the coating. 70X
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Services Overview 316 Stainless Steel Intergranular Cracking Photograph
Corrosion Control
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Technical Papers Grain boundary corrosion and intergranular cracking from excessive solution annealing
Industry Standards temperatures in a 316L stainless steel microstructure. Oxalic acid etch. (50X)
RBI Procedure
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Services Overview Hot Corrosion Of Aluminide Coating On A Nickel Alloy Gas
Corrosion Control
Failure Analysis
Turbine Blade
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RBI Procedure Microstructure of a Rene 80 blade from the 2nd stage high-pressure section of a gas
turbine that has experienced hot corrosion from molten sodium sulfate. Kallings Etch,
COMPANY 200X
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Services Overview Rene 80 Nickel Alloy Microstructure
Corrosion Control
Failure Analysis
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Technical Papers Microstructure of Rene 80 precipitation hardening nickel alloy showing intergranular
Industry Standards carbide particles (white irregular areas) and brown, gamma prime particles in the nickel
RBI Procedure alloy base metal. Kallings Etch, 400X
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Services Overview Corroded Gas Turbine HP 1st Stage Blade
Corrosion Control
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Convex side of a Rene 80 blade from the 1st stage HP section of a gas turbine. The
orange color represents the platinum-aluminide exterior coating. The green area has
experienced hot corrosion from molten sodium sulfate. The holes in the blade are trailing
edge cooling holes.
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Services Overview Dezincification Corrosion of Admiralty Brass
Corrosion Control
Failure Analysis
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Technical Papers Dezincification corrosion of an Admiralty brass exchanger tube in cooling water service.
Industry Standards
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Services Overview Hydrogen Embrittlement Crack In AISI 9623 Low Alloy Steel
Corrosion Control
Failure Analysis
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Technical Papers Hydrogen embrittlement crack initiated by corrosion of a AISI 9623 alloy in downhole
Industry Standards service. The microstructure is unetched, case hardened, quenched and tempered
RBI Procedure martensite at HRC 29. 2% Nital Etch, 50X
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Services Overview 304 Stainless Steel White Water Filter Screen Corrosion
Corrosion Control
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Tunneling corrosion of a 304 stainless steel screen wire in a papermill white stock water
Industry Links service thought to be influenced by microbiologically induced corrosion (MIC).
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Services Overview Quench Cracking in AISI 4140 Low Alloy Steel Fastener
Corrosion Control
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Technical Papers Quench cracking along a line of aluminum oxide dross particles in a hex head capscrew. The aluminum
Industry Standards oxide particles were probably added as a "killing" agent in the steeling practice. The gray material in the
RBI Procedure crack interior is high-temperature oxide formed during tempering. The microstructure is 44 HRC quench
and tempered martensite. 2% Nital Etch, 200X
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Services Overview Carburization of a HP-40 Stainless Steel
Corrosion Control
Failure Analysis
Ethylene Furnace Tube
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Industry Links HP-40 stainless steel ethylene furnace tube sample I.D. carburization after etching with
nitric and hydrofluoric acid.
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Services Overview Corrosion Of Galvanized Potable Water Piping
Corrosion Control
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Technical Papers I.D. of a galvanized carbon steel nipple from the cold water inlet connection of a residential
Industry Standards water heater. Tubercles have formed on the I.D. in low flow conditions. Underneath the
RBI Procedure tubercles are deep corrosion pits. The cold water chemistry exhibited a Langelier Index of -
0.31 and contained 8 ppm of dissolved oxygen.
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Services Overview Fretting Fatigue Striations On The Fracture Surface Of An
Corrosion Control
Failure Analysis
Aluminum Gasket
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Industry Links Fretting fatigue striations on the fracture surface of an aluminum head gasket from a
reciprocating gas compressor.
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Services Overview Corrosion Fatigue Cracks In AISI 1020 Steel In Oil And Gas
Corrosion Control
Failure Analysis
Downhole Service
Laboratory Testing
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RBI Procedure Multiple corrosion fatigue cracks at the I.D. of a AISI 1020 carbon steel downhole tool. The
tool was rotating with the I.D. exposed to a water based drilling fluid. 2% Nital Etch, 50X
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Services Overview Fatigue Cracking In A Pipeline Sample
Corrosion Control
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Industry Standards Fatigue cracks at the O.D. of an underwater pipe fracture surface resulting from a repair
RBI Procedure attempt.
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Services Overview Non-Metallic Inclusions In The Thread Of A SAE J429 Gr. 8 Bolt
Corrosion Control
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Technical Papers Longitudinal view of the microstructure of a Gr. 8 bolt showing entrapped foreign material
Industry Standards in a thread crest. The material is probably scale trapped during thread rolling. 2% Nital
RBI Procedure Etch, 100X
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Services Overview Fastener Hydrogen Embrittlement Fracture Surface
Corrosion Control
Failure Analysis
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Industry Standards Hydrogen embrittlement fracture surface of a bolt showing multiple initiation sites. The
RBI Procedure fastener was one of eight body bolts in a high pressure pump that failed after years in
atmospheric service
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Services Overview Fatigue Fracture Of A Grade 8 Bolt
Corrosion Control
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Technical Papers Fracture surface of a Grade 8 bolt showing multiple rotating-bending fatigue origin
Industry Standards features.
RBI Procedure
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Services Overview Creep (Stress Rupture) Voids In A 304ss Stainless Steel Furnace
Corrosion Control
Failure Analysis
Tube
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Industry Links Cast 304 stainless steel shock bank tube in an ethylene cracking furnace showing stress
rupture (creep) voids and cracking. 100X
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Services Overview Chloride Stress Corrosion Cracking Photograph
Corrosion Control
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Technical Papers Chloride stress corrosion cracking (SCC) on the cooling water side of a 316L stainless
Industry Standards steel exchanger tube. The cooling water contained approximately 400 ppm chlorides had
RBI Procedure been blocked in with the 350F shellside process still flowing. The black stringers are
sulfide inclusions. 100X
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Services Overview Hydrogen Embrittlement Crack
Corrosion Control
Failure Analysis
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Subsurface hydrogen embrittlement crack initiated at a non-metallic inclusion. 100X
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Services Overview Stress Corrosion Cracking Fracture Of A Carbon Steel Weld
Corrosion Control
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Technical Papers Cleavage fracture surface of a carbon steel weld from an emergency relief valve pipe.
Industry Standards Fracture was believed to be due to C0-CO2-h30 stress corrosion cracking. (~250X)
RBI Procedure
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Services Overview Explosive Decompression Blistering of Viton B
Corrosion Control
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Technical Papers Viton B elastomer showing blisters resulting from explosive decompression failure.
Industry Standards
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Services Overview Polythionic Acid Stress Corrosion Cracking Of 310 Stainless
Corrosion Control
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Steel
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RBI Procedure Polythionic acid stress corrosion cracking of type 310 stainless steel. The item was
exposed to sulfur containing natural gas in a continuous flare. (100X)
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Services Overview Graphitization Of A Carbon Steel Furnace Tube
Corrosion Control
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Industry Standards Graphitization of a carbon steel furnace tube due to long term overheating and coking in
RBI Procedure rich oil service.
See Case History 011.
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Services Overview Fatigue Fracture Of A Compressor Connecting Rod
Corrosion Control
Failure Analysis
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Technical Papers Fatigue fracture of a compressor connecting rod. The fatigue crack initiated at the left in
Industry Standards the phoograph. (~0.6X)
RBI Procedure
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Services Overview Metal Dusting Photograph -
Corrosion Control
Failure Analysis
Graphitization Of A Carbon Steel Furnace Tube
Laboratory Testing
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Industry Standards
Pitting due to metal dusting in a carbon steel furnace tube in gas treating rich oil service.
RBI Procedure
See Case History 011
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Services Overview Creep Voids in RA-330 Stainless Steel Photograph
Corrosion Control
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Technical Papers Creep voids in an RA-330 stainless steel alloy as shown by Nomarski interference contrast
Industry Standards illumination. (200X)
RBI Procedure
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Services Overview Gear Tooth Fatigue Pit
Corrosion Control
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Technical Papers Progressive pit on the loaded surface of a case hardened pinion gear tooth due to surface
Industry Standards contact fatigue.
RBI Procedure See Case History 012.
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Services Overview Nickel Alloy Weld Metal Corrosion In Hydrochloric Acid Vapors
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Technical Papers Preferential weld metal corrosion of a high nickel (C-22) alloy in dilute hydrochloric acid
Industry Standards vapors.
RBI Procedure
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Services Overview Gear Tooth White Etching Area
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Technical Papers White etching area (WEA) at the surface of a case hardened pinion gear tooth.
Industry Standards
RBI Procedure See Case History 012.
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Services Overview Caustic Cracking of 304 Stainless Steel Photograph
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Technical Papers Caustic cracking in a 304L stainless steel pipe in methanol reforming service - oxalic acid etch. (50X)
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Services Overview Gear Tooth Rolling Contact Fatigue Crack
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Technical Papers Subsurface rolling contact fatigue crack eminating from inclusions in a case hardened
Industry Standards pinion gear tooth.
RBI Procedure
See Case History 012.
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