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Journal of Manufacturing Processes 30 (2017) 374–384

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Journal of Manufacturing Processes


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Full length article

A new approach for manufacturing copper-clad aluminum bimetallic


tubes by friction stir welding (FSW)
Ahmad Tavassolimanesh, Ali Alavi Nia ∗
Department of Mechanical Engineering, Bu-Ali Sina University, Hamedan, Iran

a r t i c l e i n f o a b s t r a c t

Article history: A new method is developed for manufacturing bimetallic tubes from pure Copper and 6061-T6 Aluminum
Received 1 June 2017 tubes by Friction Stir Welding (FSW). The tubes were successfully joined by this new method. Then, the
Received in revised form effect of welding parameters such as rotational speed and traverse speed on surface quality, hardness
26 September 2017
profile, macro and micro-structure and shear strength of the samples was investigated. Experimental
Accepted 6 October 2017
Available online 14 October 2017
results showed that copper and aluminum to be blend much better when bimetallic tubes are manu-
factured by FSW compared to other methods such as Severe Plastic Deformation (SPD). Furthermore,
incorporating high rotational speeds during welding results in generation of excess heat, thus reducing
Keywords:
Copper-aluminum bimetallic tube weld surface quality and strength of copper and aluminum tube joints. According to the results, samples
FSW welded at rotational speed of 710 rpm and traverse speed of 60 mm/min presented the highest shear
Tube welding strength.
Mechanical properties © 2017 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.
Microstructure

1. Introduction welding of copper and aluminum [4] do not seem to be acceptable


due to formation of brittle and hard intermetallic phases (IMC) with
Copper and its alloys are extensively used for their electrical weak mechanical properties.
properties, thermal conductivity, corrosion resistance, easy fab- Friction Stir Welding (FSW) was introduced in 1991 by The
rication and acceptable fatigue resistance [1]. Although copper Welding Institute in Britain as a technique for solid state joining
offers high electrical conductivity, its high density hinders its appli- of aluminum alloys [5]. In this type of welding the temperature
cation in light-weight designing. Additionally, its relatively high does not exceed melting temperature of the materials, hence heat
price results in high costs. Therefore, it has been attempted to use input and consequently formation of intermetallic phases can be
aluminum, a cheaper and less dense metal of similar electrical prop- controlled, thus improving the mechanical properties. Many exper-
erties, instead [2]. Bimetallic copper and aluminum structures are imental studies addressed joining copper and aluminum by FSW
advantageous solutions to replace copper. These structures pro- in butt joints [6–10] and lap joints [11–18]. Saeid et al. [11] stud-
vide lower weight and cost for the structure on the one hand, ied the effect of welding speed on the quality of 1060 aluminum
and incorporate intrinsic characteristics of copper on the other. and pure copper lap joints. Their results showed Al4 Cu9 and Al2 Cu
Bimetallic tube is a type of double-layer copper-aluminum struc- intermetallic phases and cracks to exist near copper-aluminum
tures. Bimetallic tubes can be adequate replacements for tubes interface. They also showed that the cracks can be reduced by
fabricated from copper and its alloys. Copper alloy tubes are exten- increasing welding speed. Elrefaey et al. [12] showed that by incor-
sively used for drinking water distribution in buildings, chemical porating a zinc (Zn) interlayer in friction stir welding of 1100H24 Al
industries, refineries, hydraulic lines, air conditioning, and heat and copper in a lap joint, strength increases threefold, intermetal-
exchangers and also in food industries [1]. Given their different lic phases were limited and scattered in a wider area. Xue et al.
physical, mechanical and chemical properties, and also formation [13] successfully performed friction stir welding of 1060 Aluminum
of intermetallic phases, joining copper to aluminum by common and pure copper at a relatively low rotational speed (600 rpm) and
welding methods such as laser welding [2] is very difficult. More- welding speed of (50 mm/min) using a tool with 8 mm pin. Akbari
over, joining methods such as cold roll bonding [3] and friction et al. [14] addressed the effect of material positioning on heat gen-
erated as a result of friction stir welding in a 1070 Aluminum and
pure copper lap joint. Their results suggest the maximum strength
is achieved when aluminum is placed above copper. Bisadi et al.
∗ Corresponding author.
[15] performed friction stir welding for AA5083 Aluminum and
E-mail addresses: alavi1338@yahoo.com, alavi495@basu.ac.ir (A. Alavi Nia).

https://doi.org/10.1016/j.jmapro.2017.10.010
1526-6125/© 2017 The Society of Manufacturing Engineers. Published by Elsevier Ltd. All rights reserved.
A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384 375

Fig. 1. Schematic view of FSW system for welding tubes in lap joints.

Fig. 2. a) Welding system designed for joining tubes before and after FSW procedure; b) a sample bimetallic tube fabricated with two weld lines after FSW.

pure copper lap joints at various rotational and traverse speeds method offers lower maximum welding temperature and a shorter
and examined the mechanical and microstructural properties of thermal cycle, hence enhanced mechanical quality of the junction.
the junction. They achieved maximum tensile shear strength by In recent years, there have been a number of studies on tube
welding at a rotational speed of 825 rpm and traverse speed of butt joints made by FSW. Packer and Matsunaga [19] designed a
32 mm/min. Galvão et al. [16] addressed the effect of aluminum machine for welding X65 pipes by FSW. Peterson et al. [20] devel-
alloy type on copper and alloy lap joint welding. Friction stir weld- oped a new system and method for welding pipes of small diameter
ing was performed using 1 mm-thick copper sheet and 6mm-thick by FSW. Moreover, some researches have been made concerning
sheets of AA 5083-H111 aluminum (without heat treatment capa- aluminum tube butt joints [21–25]. Chen et al. [26] have recently
bility) and AA 6082-T6 aluminum (with heat treatment capability). presented a new FSW welding method for Al3003 aluminum and
Their results showed the copper and AA 5083 sheets to offer a weld pure copper pipes of low diameter and thin wall (diameter of the
with excellent surface quality while the inside is faulty and lacks copper tube was 1 mm and that of the aluminum tube was 1.5 mm).
interaction of base materials. On the contrary, welding AA 6082 alu- According to their results, there are a number of challenges in fric-
minum alloy and copper resulted in a low quality surface but strong tion stir welding of copper and aluminum tubes, namely: 1) the big
bonding of the base materials. Kuang et al. [17] joined copper and difference in mechanical properties of copper and aluminum tubes,
1A99 aluminum sheets using a pin-less tool configuration and 0.2 such as the 400◦ K difference of their melting temperatures; 2) very
mm-thick zinc foil by friction stir welding. Experimental evidence different material flow on the surfaces of tube curves compared to
suggests the interlayer thickness to decrease as rotational speed flat conditions; and 3) demand for precise control of the welding
of the tool is increased and welding progress is slowed down, with procedure given the thin wall of the tubes.
rotational speed playing a more effective role. In order to control the Moreover, attempts have been made to fabricate copper and
heat generated during friction stir welding of 6061-T6 aluminum aluminum bimetallic tubes by rolling [27] and severe plastic defor-
and pure copper, Zhang et al. [18] tried underwater welding. This mation [28] to provide replacements for pure copper tubes and
376 A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384

Fig. 4. A schematic view of tools and tubes configuration.

eter inside the tubes for bearing the vertical load applied by the
tool. Fig. 3, shows the mold used inside the tube and the schematic
model.
The mold can be used for tubes of various inner diameters. Plac-
ing the mold inside the tube and fastening its screw, the mold
expands and provides the support of tube walls against the pressure
applied by the tool. After welding, the mold can be removed from
the tube easily as it is unscrewed to a smaller size. Tubes of suitable
Fig. 3. Mold inside the tubes a) schematic b) fabricated model.
lengths and diameters that fitted inside one another in a tangen-
tial compliance configurations were prepared and installed on the
consequently reducing costs and total weight of tubing. Examining fixture to be welded. Although all the tubes surface can be welded
copper-aluminum bimetallic tubes, Sajuri et al. [29] realized that no by proper rotational and horizontal motion of the tubes in a spiral
blending had taken place at copper-aluminum interface, with only course producing a double-walled tube by FSW method with the
a thin layer of intermetallic phases formed. Additionally, fatigue pin exit hole being located at the end of the tube and hence omit-
resistance of these pipes is 55% of the pure copper tubes. ted, in order to be able to prepare shear test samples and examine
Reviewing previous researches on methods of fabricating its mechanical properties, the tubes were welded in a peripheral
copper-aluminum bimetallic tubes, it was found that FSW has not line all the way to 360◦ . FSW was performed according to parame-
been ever applied to copper and aluminum bimetallic tube lap ters presented in Table 2 and the effects of different rotational and
joints. This research, proposes a novel method for joining 6061-T6 travel speeds were studied on the mechanical and microstructural
aluminum and pure copper tubes in lap joint in order to fabri- properties of the weld.
cate bimetallic aluminum tubes with copper cover. Furthermore, For briefness, samples welded at 710 rpm were named Lrs (Low
microstructural and mechanical properties of the joint were stud- Rotational Speed) and samples welded at 1000 rpm were named
ied at various rotational and traverse speeds. Hrs (High Rotational Speed).
In order to examine shear strength of the weld, three spec-
2. Methodology imens of 15 mm width and 70 mm length (Fig. 2b) with similar
welding conditions, taken normal to weld direction were prepared
6061 aluminum alloy and annealed pure copper tubes were used and tested and their average shear force was calculated. Shear test-
in this study. The outer diameter of the 150 mm-long aluminum ing was carried out at the rate of 2 mm/min using STM150 test rig
and copper tubes were 54 and 58 mm, and their wall thicknesses and failure force and location was recorded for each specimen. Due
3 and 2 mm, respectively. Chemical composition of the aluminum to the difference in the thickness of the shear test specimens, the
and copper tubes is presented in Table 1. stress calculated for the weakest part of each specimen was con-
Three specimens were prepared from each base material for sidered for comparing their shear strength. Moreover, specimens
tensile testing, based on ASTM-E8 M standard and the mechani- were prepared for macro/microstructural investigation and hard-
cal properties of the base materials were obtained by averaging the ness measurement. Hardness measurement tests were performed
results. The Ultimate Tensile Strength (UTS) of the aluminum and using a micro-hardness tester along two parallel lines for both cop-
copper were found to be 339 and 192 MPa, respectively. per and aluminum (0.05 kg for 15 s). A stereo optical microscope
An H13 steel FSW tool with concave shoulder of 10◦ and right- was employed for imaging. The specimens were etched at the weld
hand-threaded cylindrical pin was used for welding. Shoulder area by two steps. First Keller solution was used to reveal aluminum
diameter was 16 mm, pin diameter 5 mm and pin length was 3 mm. grains, then HCl, FeCl3 , H2 O solution was used to reveal copper
A schematic view of the welding system is presented in Fig. 1. grains in compliance with ASTM E407-99 standard. Additionally,
The system, while producing bimetallic tubes, and a sample fabri- a VEGA TESCAN-XMU scanning electron microscope was used for
cated bimetallic tube with two weld lines are shown in Fig. 2a and imaging and Energy Dispersive Spectroscopy (EDS) analysis.
b, respectively.
A fixture composed of three major parts was designed for weld- 3. Results and discussion
ing pipes in lap joints: a) the set of motor, gearbox, and inverter for
precisely providing rotation and torque required for turning the Using the designed welding system (Fig. 1), 6061-T6 aluminum
pipes, b) tube to motor coupling, and c) mold with variable diam- and pure copper tubes were welded in a lap joint. Weld surface,
A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384 377

Table 1
Chemical compositions of 6061-T6 aluminum and pure copper (%Wt.).

Material Al Si Fe Cu Mn Mg Cr Ni Zn

Al alloy Balance 0.66 0.6 0.40 0.11 0.93 0.05 0.02 0.07
Cu Trace <0.005 <0.005 䊐99.9 Trace – Trace <0.005 <0.01

Table 2 study suggest high rotational speed of the welding tool to result in
Parameters considered for welding each sample.
excess heat input leading to aggregation of aluminum particles on
Sample Rotational speed Welding speed advancing side, reduced thickness of copper and lower quality and
(rev/min) (mm/min) strength of the weld (Fig. 5a). But, a weld surface of reasonable
Lrs1 710 30 quality can be achieved in cases with lower rotational speeds and
Lrs2 710 45 a heat input enough for acceptable material flow (Fig. 5b).
Lrs3 710 60
Hrs1 1000 30
Hrs2 1000 45 3.2. Microstructure of the welding zone
Hrs3 1000 60
In order to examine the effect of rotational speed of the tool on
the microstructure of the weld, SEM images of weld nuggets cor-
macro/microstructure and its mechanical properties were exam- responding to samples Lrs1 and Hrs1 are presented in Fig. 6 along
ined to understand the characteristics of this welding method and with some of their microstructural properties. According to Fig. 6b,
the effect of different welding parameters. the weld structure incorporates dark areas indicating the presence
of voids. Insufficient material flow in the stir zone can be acknowl-
3.1. Material flow and weld surface edged as the reason for the formation of these voids that are starting
points for fracture. Penetration of copper lamellas into aluminum
Fig.4 schematically shows the position of the tubes and FSW (Fig. 6a) indicates that the pressure applied by the shoulder has
tools and their configuration with respect on one another. Accord- successfully driven copper flow down into aluminum thus creat-
ing to Fig. 4, in order to achieve what is known as “tilt angle” in FSW, ing a proper mixture of copper and aluminum particles. Figures 6b
the equipment start penetrating tube walls with an offset (1.7 mm) and d shows a hook-like structure and crack on the retreating side
relative to the centerline of the tubes. which continues to advancing side. This defect often exists when
A fundamental difference between FSW lap-joints for tubes and welding heterogeneous soft and hard metals and when pin pene-
sheets is the shoulder diameter of the tools used. On the one hand, tration is high [13]. Carlone et al. [31] have also observed this defect
given the high curvature of the tubes, tools with large shoulder when using FSW to join copper and aluminum in butt joints. Pre-
diameter cannot be made use of since their shoulder have a smaller vious studies [32,33], too, attribute the hook defect (which makes
contact area with the tube walls and result in an incomplete forg- the top sheet thinner and the weakens the weld) to the upward
ing of the material flow from top to bottom, and consequently, motion of the material on one side of the lap joint weld. Moreover,
defects such as tunnels. On the other hand, using tools with small given the manners of material flow in FSW, some of the material is
shoulder diameter reduce heat generation required for metal flow transported from the retreating to the advancing side behind the
thus producing a defective weld. Moreover, tube diameters and pin where the weld was formed and due to movement of the pin,
wall thickness are determining parameters when selecting correct resulting in hook-like faults in the weld nuggets [34].
FSW tools and must fit shoulder diameter and the pin length. For Investigating the weld structure around hook defects (Figures
instance, if tubes with a small diameter and large thickness are 6-b and d) it find that the hook zone has a dull edge and better mix-
used, the high curvature does not allow the use of tools with large ture of copper and intermetallic copper-aluminum phases around
shoulder diameter required for more heat generation, and the large it for the sample with the lower rotational speed (Lsr1). However,
thickness limits heat transfer and material flow. According to the hook edge is sharper in the sample with higher rotational speed
tests performed, in lap-joints of copper and aluminum tubes, the (Hrs3) and metallic phases around this zone predominantly consist
rotational speed of the tools is also very effective on material flow of the copper particles. The reason for this is probably that increas-
and the final quality of the surface. After welding with the earlier ing rotational speed of the tool and therefore generating more heat,
mentioned parameters, two distinct weld surface qualities were increase the fluidity of the metal and decrease cohesion of metal-
obtained for the samples. Fig. 5 shows two welded samples with lic particles together and to the tool. Therefore, the concentration
different qualities. The surface obtained from welding sample Hrs2 of intermetallic phases is less on sides and more in the middle
at rotational speed of 1000 rpm and traverse speed of 45 mm/min of the weld. Needless to say, a sharper hook defect facilitates the
is shown in Fig. 5a and surface of Lrs3, welded at 710 rpm and separation of copper and aluminum interlayers. A magnified view
60 mm/min is shown in Fig. 5b. of a hole-containing region in Hrs3 is shown in Fig. 6c. Nandan
In lap joints, the vertical flow of material (from bottom to the et al. [34] showed that holes are mostly formed on the advanc-
top, and vice versa) is essential for metals to blend. Thus, a threaded ing side which can be attributed to sudden microstructural shift
pin was employed in this study to provide better material flow. from a highly refined zone in the nugget to TMAZ while the tran-
It seems that upward flow of aluminum and downward flow of sition takes place gradually on the almost defect-free retreating
copper takes place at a faster pace when a higher rotational speed side [34]. The difference in grain size of Heat Affected Zone (HAZ)
is applied, which can be attributed to the higher heat generation and Thermo-Mechanically Affected Zone (TMAZ) can be clearly
thus higher welding zone temperature and better material flow. observed in Fig. 6a, where grains have a smaller size in a constant
Although reducing welding temperature and heat input results in radial distance, compared to further regions. For better comparison,
lower mixture of the metals in FSW [30], previous studies [26] have quantitative values of grain sizes in the TMAZ (Fig. 7b) and HAZ of
shown the fixture used for welding tubes to provide limited heat sample Lrs1 are presented.
dissipation during welding which is further decreased as heat input According to Fig. 7, grain size in the HAZ and TMAZ are 15.27 and
is increased. Therefore, heat is gradually accumulated and increases 4.7 ␮m, respectively. Therefore, it is safe to say that the grain size
maximum temperature during welding. Similarly, the results of this in the TMAZ is almost 31% of that in HAZ, which provides higher
378 A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384

Fig. 5. Comparing weld surfaces obtained by welding a) at rotational speed of 1000 rpm and traverse speed of 45 mm/min (Hrs2) b) at 710 rpm and 60 mm/min (Lrs3).

Fig. 6. SEM images a) magnified images of TMAZ and HAZ and b) nugget zone of Lrs1 c) a closer look at the hole created on the surface of Hrs3 weld and d) Hrs3 nugget zone.

hardness and improved mechanical properties of the weld. The dif- Fig. 7-c and d shows the nuggets to contain dark and grey
ference in grain size, is due to the effect of rotational movement areas, suggesting different chemical compositions. Furthermore,
of the pin on deformation, restoration and modification of grain the atomic ratio of copper and aluminum on the aforementioned
structures in the TMAZ of the weld. spots in both samples are presented in Table 3.
In order to examine the type of intermetallic phases formed in As shown in the Figs. 6 a, 7 c and stated by numerical results
the stir zone when a lower rotational speed is used to perform FSW of microstructural examination, in Lrs1, most of the composite
on the tubes, a few spots were selected (Fig. 7-c) for EDS analysis. zone is occupied by copper particles which are seen in silver and
Moreover, in order to investigate the impact of rotational speed of have layered structures. Light grey areas (A and B) contain Al4 Cu9
the tool on the type of intermetallic phases formed in the weld, and Al3 Cu4 intermetallic phases, respectively. Contrary to what is
Hrs3 was analyzed by EDS on the spots shown in Fig. 7-d. Fig. 8 expected based on its color, point D marks aluminum phase with
shows the diagram for atomic contents of aluminum and copper trace amounts of the Al2 Cu. Based on Fig. 7-c and EDS analysis, it
for these points in Lrs1. can be concluded that Al2 Cu consists the largest volume of inter-
A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384 379

Fig. 7. Grain size for a) TMAZ, b) HAZ in Lrs1, spots selected for EDS analysis in c) Lrs1 and d) Hrs3 samples.

Table 3
EDS results (at%) for the points shown in Fig.7-c and d.

Lrs1 Hrs3

Position A B C D A B C D

Al (K) 47.28 21.63 66.23 95.67 0.01 23.22 66.48 96.93


Cu (K) 52.72 78.37 33.77 4.33 99.99 76.78 33.52 3.07
Possible phases Al3 Cu4 Al4 Cu9 Al2 Cu (Al) + Al2 Cu Cu Al4 Cu9 Al2 Cu Al

metallic phases in the nugget being more dispersed close to the tional speeds, which are associated with a higher boiling point,
aluminum side below the stir zone. The abundance of intermetallic intermetallic phases containing more Cu are formed. This is impor-
phases of the Al2 Cu type is due to sufficient amount of aluminum tant given that the type of intermetallic phases and their dispersion
in the nugget in contrast to copper particles in this zone promot- in the weld is very influential on the mechanical properties of the
ing the formation of intermetallic phases with a higher content of Cu/Al joint.
the aluminum. Comparing pictures 6-b and d, 7-d and consider- Hrs3 weld nugget is shown in Fig. 9 for a better examination.
ing EDS results in Table 3, it is found that the weld area in Hrs3 According to this Figure, a composite structure of copper and inter-
contains Al2 Cu and Al4 Cu9 intermetallic phases. Unlike the Lrs1 metallic phases was formed in the nugget zone with grey and
weld which contains considerable amounts of Al, the Hrs3 pre- layered structures. Moreover, copper particles can be seen as they
dominantly consists of pure Cu particles and Al4 Cu9 compounds. are dispersed in intermetallic phases. Based on the Fig. 9, only cop-
This shows the fact that due to welding samples at high rotational per particles were scattered in the aluminum matrix.
speed and therefore generating more heat, softening of copper par- Zhang et al. [18] have mentioned two reasons for this phe-
ticles more happened, increasing their concentration in the weld nomenon, one being that melting temperature of copper is higher
and changing the structure of the intermetallic phases in this zone. than aluminum. Therefore, aluminum softens to a larger degree
Therefore, the intermetallic phases in specimens welded at lower compared to the copper at the same temperature, meaning that
rotational speeds contain more Al and those welded at higher rota- viscosity of the aluminum is lower than the copper. Therefore, dis-
380 A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384

Fig. 8. EDS results for some point in Lrs1.

Fig. 9. Optical microscopy images from Hrs3 weld zone.


A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384 381

Fig. 10. a) the right half of the weld in Hrs3 along with b and c) enlargement of the defects.

persion of the copper particles in the aluminum matrix takes place 3.3. Mechanical properties
easier. The second reason is that density of the copper is more than
the aluminum, so when the copper is placed above the aluminum Fig. 11 shows micro-hardness along two parallel lines on the
(as in this research), the Cu particles are easily dispersed in Al by copper and aluminum for samples welded at 710 rpm (Fig. 11a) and
gravity. at 1000 rpm (Fig. 11b). According to these Figures, the hardness is
Another defect resulted from high rotational speed and heat greater at the center of the weld compared to other parts. The high-
generation in FSW of tubes is the formation of porosity in the weld. est copper tube hardness at the center was found to be 165.4 HV for
Fig. 10 shows an enlarged image of the right half of Hrs3 sample samples welded at rotational speed of 710 rpm and traverse speed
along with porous defects and a non-uniform layer of the inter- of 30 mm/min, and 142.6 HV for the samples welded at 1000 rpm
metallic phases formed. and 30 mm/min. Similarly for the aluminum tubes, hardness was
The porosities, seen as microscale voids, reduce the strength measured to be 120.1 HV (710 rpm and 30 mm/min) and 109.4 HV
of this zone and result in growth and propagation of defects such (1000 rpm and 60 mm/min) that are significant.
as voids and cracks. Mehta et al. [35] attributed the porosities to The lowest hardness for the copper and aluminum tubes was
absorption of the atmospheric Hydrogen by the aluminum and found at HAZ on the advancing side. Bisadi et al. [15] attributed this
copper oxides. to the excess heat input on the advancing side and the consequent
Employing severe plastic deformation method, Lapovok et al. enlargement of grains which leads to lower hardness. Hardness was
[28] produced bimetallic copper and aluminum tubes. They measured 105.4 and 101 HV for the copper tube and 74.5 and 70.8
attached the tubes by simultaneously applying hydrostatic pres- HV for the aluminum tube at rotational speeds of 710 and 1000 rpm,
sure and high shearing force to the inner tube, resulting in respectively. Examining hardness profiles during FSW on Al6065-
expansion and residual stresses in the tube. Their tests showed T5 alloy, Sato et al. [36] found FSW to significantly reduce hardness
the size of the interdiffusion zone at the interface of Cu and Al, of the solid solution. Their experiments also showed that aging
is typically of the order of 40–50 nm includes a thin layer of brittle, samples for 2 h at 175 ◦ C increases the concentration of strengthen-
hard intermetallic particles, while FSW results for welding copper ing precipitates thus increasing hardness in precipitate-dissolved
and aluminum show blending of metals to be around 1.5–2 mm. region. Comparing the experimental results of this study with those
Drawing on test results and considering the optimum conditions reported by Sato et al. [36] it is deduced that transportation of the
obtained in this study for lap-joint FSW of tubes in a spiral course heat that is generated and accumulated during welding from the
from the start to the end of the tubes, double-walled tubes of copper to the aluminum results in growth of strengthening precip-
great quality can be produced which shows the superiority of FSW itates in the aluminum, cancelling the reducing effect of FSW on
method for the manufacture of double-walled copper-aluminum hardness. Previous studies suggest the intermetallic phases of the
tubes. copper and aluminum to be much harder than any of the two base
382 A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384

Fig. 11. Hardness diagram for a) samples welded at rotational speed of 710 rpm and b) samples welded at 1000 rpm.

metals reaching up to 760 HV. Therefore, in addition to the heat- in HAZ and its vicinity. Further examinations showed thickness of
induced growth of strengthening precipitates in the aluminum, the copper sheet in Lrs2 to be significantly reduced during the weld-
growth of intermetallic phases can be counted as a hardening factor ing which is the reason for failure from this part. But in Lrs1 and
in the weld zone. Furthermore, hardness diagrams for both groups Lrs3 failure starts near HAZ in aluminum on the advancing side
show the rotational speed to be the factor determining hardness which shows the negative effect of excess heat input resulting in
while traverse speed is less effective on hardness results. grain growth in HAZ and reduction of strength. Samples welded at
In order to investigate the shear strength of the Cu/Al joint, 1000 rpm have all been subject to failure from stir zone. This shows
specimens that were separated from the weld cross-section were the significance of controlling heat generation during welding cop-
shear tested. The fracture location and failure load are presented in per and aluminum.
Table 4. Examining images of fractures in Table 4, it is figured that Another important difference of FSW for copper-aluminum
samples connected at low rotational speed, offer higher failure load sheets and tubes is the different effect of material flow and heat
compared to samples welded at similar traverse speed but higher transfer resulting from the movement of the pin inside the metal
rotational speed. Previous studies show that growth of intermetal- in either of those. When welding tubes, given the geometry of the
lic phases results in weak mechanical properties since the growth tubes and the inner mold, the generated heat in the first stage pre-
takes place at the interface of metals or in the nugget, especially heats the material prior to welding. If the heat generated in the first
at high rotational speeds [11,12,37]. Therefore, the lower strength stages of welding is sufficient and controlled, pre-heating enhances
of samples welded at higher rotational speeds can be attributed to material flow and weld strength, but if the heat is generated exces-
growth of intermetallic phases in the stir zone. According to the sively due to high rotational speed of the tool and its accumulation
Table 4, location of fracture in the samples welded at 710 rpm was in the mold inside the tubes, excess metal softening and conse-
A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384 383

Table 4
Fractures images and failure load for each sample.

Sample Failure location image Failure load (N) Place of fracture

Lrs1 2711.3 In Al and between stir zone And HAZ

Lrs2 2203.6 Cu HAZ

Lrs3 3373.4 Al HAZ

Hrs1 1813.7 Stir zone

Hrs2 1633.4 Stir zone

Hrs3 2439 Stir zone

quently defects and low strength are to follow, diminishing weld microstructural and mechanical properties of the joint were exam-
quality to a large extent. In fact, mechanisms must be made to cool ined as different welding parameters were incorporated. The most
the tubes when welding or the maximum temperature in the weld notable results of this study can be summarized as follows:
zone must be controlled by low rotational speed or high traverse
speed.
Results show increasing traverse speed to 45 mm/min reduces
shearing force; further increasing traverse speed to 60 mm/min, 1. A new method for production of bimetallic copper and aluminum
failure load is enhanced which suggests a critical traverse speed tubes by FSW was presented and components needed for man-
when welding of copper and aluminum in lap joints. The failure ufacturing were designed and fabricated.
load was obtained for Lrs3 sample at 3373.4 N which is higher than 2. Despite challenges in welding copper and aluminum tubes in
the other samples. Additionally, weld shear strength in this sample lap joints compared to sheets, and considering microstructural
was higher since the sample failure took place in aluminum. Results examinations, an acceptable mixture was achieved between
prove the high quality of the weld in this study. copper and aluminum. Copper and aluminum tubes were con-
nected with much better blending compared to previously
proposed methods for fabrication of bimetallic tubes.
4. Conclusion 3. Examining hardness diagrams of the samples showed the weld
between copper and aluminum to cancel the reducing effect of
A bimetallic copper and 6061-T6 aluminum tube was fabri- FSW on hardness of 6061-T6 aluminum and even to increase its
cated by Friction Stir Welding. Surface quality of the weld, and hardness to values above the base material.
384 A. Tavassolimanesh, A. Alavi Nia / Journal of Manufacturing Processes 30 (2017) 374–384

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