PRESENTATION OF RESULTS

FOR EXPERIMENT 6

ANALYSIS OF GROUP IIIA and IIIB CATIONS

PHARMACEUTICAL AND INORGANIC CHEMISTRY

GROUP 2

BALANDA, Alamir.

CANDELARIO, Danica

GARAS, Lea Mae

MABANSAG, Francheska Marie I.

MARQUEZ, Jemarine Kate Stephanie C.

MIGUEL, Sean Carlo R.

RAZON, Angela

.RIANZARES, Kate

ROVER, Allaine

SAEZ, Czarina Anne

VILLANUEVA, Randell Arjem

 EXPERIMENT NO. 6

Analysis of Group IIIA Cations

SUBSTANCE REAGENT RESULTS CONCLUSION

Centrifugate from exp. 5 3F HAc After adding 100 gtts The solution is acidic.
of 3F HAc, the blue
litmus paper turns red.
Solution 1 3F NH3 After adding 3 ggts of The solution is
3F NH3, the red ammoniacal.
litmus paper turns
blue.
Residue 1 Aluminon After adding the first Presence aluminum ions
drop of aluminon in indicated.
the solution turns red
right away.
Solution 2 3F NH3 After centrifuging the Presence of Aluminum ion
solution, red is CONFIRMED.
precipitate settles at
the bottom of the
solution.
Centrifugate 1 1F Ba(Ac)2 After adding 2 gtts of Presence of Ba CrO4 and
1F Ba(Ac)2 white BaSO4 indicated in the
precipitate forms residue.
immediately.
Residue 2 3F HCl After centrifuging the Presence of Chromium ion
solution with 10 gtts of indicated.
3F HCl, white
precipitate settles at
the bottom of the
solution.
Centrifugate 2 H2O2 After placing 2 drops Chromium ion is
of centrifugate 2 and ABSENT.
H2O2 in the filter
paper there is no blue
color the fades rapidly
appear.
Centrifugate 2 Thioacetamide After heating the Presence of Zinc ion is
solution solution in the boiling CONFIRMED.
water, white
precipitate formed
immediately.
PHOTO DOCUMENT:

After adding 100

gtts of 3F HAc

LITMUS PAPER:
BLUE-RED

After adding 3
gtts of 3F LITMUS PAPER:
AMMONIA RED-BLUE

After the RESIDUE with

CENTRIFUGE the washings
 After adding 3F
HCl, the residue
The RESIDUE dissolved

Adding
ALUMINON

After adding 5 gtts of

3F NH3, the solution
is ammoniacal.

After centriguging,
LITMUS PAPER: RED
RED-BLUE PRECIPITATE
settles at the bottom
 After 2 gtts of 1F
Ba(Ac)2

2 gtts of
CENTRIFUGATE + 2
gtts of H2O2

After adding 10 gtts After heating

of 3F HAc: BLUE- solution for 5 min,
RED litmus paper. white precipitate
formed.
: