DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

DMS - 6100
EPOXIES AND ADHESIVES
EFFECTIVE DATE: JUNE 2014

6100.1. Description. This Specification details requirements for various types of epoxy and
adhesive materials suitable for highway use. These materials consist of a resin component and a
hardener component or a catalyzing agent mixed to produce the finished product.
All epoxies and adhesives must be resistant to the action of weathering, moisture, acids, alkalis,
and other environmental factors.
This Specification describes the following types of epoxies and adhesives.
• Type I (Classes A, B, and C)—precast concrete segment adhesive
• Type II—traffic marker adhesives
• Type III (Classes C, D, E, and F)—dowel, tie bar, and anchoring adhesives
• Type IV—bridge deck sealant and adhesive
• Types V and VII—concrete adhesives
• Type VIII (Classes A and B)—binder for producing grout or concrete
• Type IX—epoxy for crack injection
• Type X—epoxy coating for concrete

6100.2. Units of Measurements. The values given in parentheses (if provided) are not standard
and may not be exact mathematical conversions. Use each system of units separately. Combining
values from the two systems may result in nonconformance with the standard.

6100.3. Material Producer List (MPL). The Materials and Pavements Section of the
Construction Division (CST/M&P) maintains the Quality Monitoring Program (QMP) for
epoxies and adhesives, as outlined in DMS-6110. Materials listed on the MPL, entitled “Epoxies
and Adhesives,” do not require further testing, unless deemed necessary by the Engineer.
Products not currently listed on the MPL require project-specific testing and approval before use,
unless otherwise shown on the plans. Submit samples with a certified test report from an
independent laboratory with test data verifying that the material meets the requirements of this
Specification. Do not use the material until testing is complete.

6100.4. Sampling and Testing. The Department samples in accordance with Tex-734-I and
tests in accordance with Tex-614-J and other test procedures as stated.
Costs of sampling and testing are normally borne by the Department; however, the costs of
sampling and testing material that fails to conform to the requirements of this Specification are
borne by the Contractor or supplier. The Director of CST/M&P will assess the cost of sampling
and testing failing material at the time of testing. Amounts due to the Department for conducting
such tests will be deducted from monthly or final estimates on Contracts or from partial or final
payments on direct purchases by the State.

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DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

6100.5. Material Properties.

A. Type I—Precast Concrete Segment Adhesive.
1. Description. Type I adhesives are used for the joining of precast bridge segments. The
adhesive functions as a lubricant during the joining of the match cast segments and as a
durable, watertight bond at the joint. There are three epoxy classes.
a. Class A—Low Temperature. This formulation provides a fast reacting system for
placement when the concrete temperature is 40–60°F (4–16°C).
b. Class B—Medium Temperature. This formulation is suitable for placement when
the concrete temperature is 55–80°F (13–27°C).
c. Class C—High Temperature. This formulation is suitable for placement when the
concrete temperature is 77–105°F (25–41°C).
2. Physical Requirements. Table 1 describes the requirements for precast concrete
segment adhesive.
Table 1
Type I
Physical Property Test Method Requirements
The mixed adhesive must be sufficiently fluid to
Workability –
apply by spatula or trowel without any difficulty.
Gel Time, min.
Class A @ 60°F (16°C)
24 Min
Class B @ 80°F (27°C)
Class C @ 105°F (41°C)
Contact Time, min.
Class A @ 60°F (16°C)
60 Min
Class B @ 80°F (27°C)
Class C @ 105°F (41°C)
Tex-614-J
Thixotropy, in. (mm)
Class A @ 60°F (16°C)
0.2 (5.0) Max
Class B @ 80°F (27°C)
Class C @ 105°F (41°C)
Tensile Bond Strength @ 24 hr., psi (MPa)
Class A @ 40°F (4°C)
290 (2.00) Min
Class B @ 55°F (13°C)
Class C @ 77°F (25°C)
Compressive Strength @ 24 and 48 hr., psi (MPa)
Class A @ 40°F (4°C) At 24 hr.—2,000 (14.0) Min
Tex-614-J
Class B @ 55°F (13°C) At 48 hr.—6,000 (41.5) Min
Class C @ 77°F (25°C)
Hardness @ 120°F (49°C) ASTM D 2240 77 Min

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DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

3. General Requirements. The adhesive has a low sensitivity to damp conditions during
application.
After curing, the adhesive exhibits high bonding strength to cured concrete, good water
resistivity (resistance), and low creep characteristics.
B. Type II—Traffic Marker Adhesive.
1. Description. Type II adhesive is designed for machine application and is suitable for
bonding ceramic, plastic, or metal markers to concrete pavements.
Include the following information with every shipment:
• proper type of dispensing equipment to be used and
• weather conditions, during application, that are detrimental to material
performance.
2. Physical Requirements. Table 2 describes the requirements for traffic marker
adhesive.
Table 2
Type II
Physical Property Test Requirement
Method
Gel Time, min. 7 Min
Tensile Bond @ 2 hr., psi (MPa) 200 (1.40) Min
Stability, % increase 20 Max
Increase in Viscosity after 14-day heat
aging @ 120°F (49°C)
Difference in Viscosity Between the 2 15 Max
Components, % Tex-614-J

Tensile Shear Strength, psi (MPa) 1,800 (12.40) Min

Impact Strength, ft.-lb. (N-m) 6-1/2 (9.0) Min
Wet Strength, psi (MPa) 270 (1.85) Min
Thixotropy @ 120°F (49°C) (sag on test 0.2 (5.0) Max
panel), in. (mm)

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DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

Table 3 indicates the approximate set time for field conditions for traffic marker
adhesive.
Table 3
Approximate Set Time for Type II Epoxy
Pavement Temperature Set Time (Hr.)
115°F (46°C) 0.5
95°F (35°C) 1.0
77°F (25°C) 2.0
60°F (16°C) 4.0
50°F (10°C) 7.0

3. General Requirements. The ratio of the epoxy adhesive resin to hardener components
is 1:1 by volume.
The producer must not use alumina or hard abrasive materials that might abrade or
damage the application equipment as fillers.
The producer must distinctly pigment each component of adhesive to produce a third
color similar to concrete when properly mixed.
C. Type III—Dowel, Tie Bar, and Anchoring Adhesive.
1. Description. Type III adhesives are used to anchor dowels and tie bars in concrete and
are suitable to bond steel to hardened concrete. There are four classes.
a. Class C. This formulation is a standard cure cartridge-dispensed material or a bulk
material for machine application only. Class C is used for either horizontal or
vertical down application of dowel and tie bars. (See NOTE.)
b. Class D. This formulation is a fast cure cartridge-dispensed material or a bulk
material for machine application only. Class D is used for either horizontal or
vertical down applications of dowel and tie bars. This adhesive can be used in cold
weather conditions. (See NOTE.)
c. Class E. This formulation is a standard cure cartridge-dispensed material for use in
anchoring applications where the anchor is placed in either horizontal or vertical
down applications. (See NOTE.)
d. Class F. This formulation is a fast cure cartridge-dispensed material for use in
anchoring applications where the anchor is placed in either horizontal or vertical
down applications. This adhesive can be used in cold weather conditions. (See
NOTE.)

NOTE: Vertical overhead applications are not allowed.

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DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

2. Physical Requirements.
a. Class C and Class D. Table 4 describes the requirements for Class C and Class D
dowel and tie bar adhesives.
Table 4
Type III, Class C and Class D
Physical Property Test Requirements
Method
Class C Class D
1
Gel Time 6 min. Min 2 hr. Max at 40°F
Tensile Bond @ 6 hr., 200 (1.40) Min 200 (1.40) Min
psi (MPa)
Tensile Bond @ 120°F 400 (2.8) Min 400 (2.8) Min
(49°C), psi (MPa) Tex-614-J
Thixotropy @ 120°F 30 (0.75) Min 30 (0.75) Min
(49°C), mils (mm)
Wet Pullout1 Strength, 4,500 (20) Min 4,500 (20) Min
lbf. (kN)
1. For Class D, perform gel time at 40°F and perform pullout at 4 hr. under dry
conditions.

b. Class E. An approved building code evaluation service must evaluate Class E

adhesives in accordance with AC308 prior to pre-qualification. Approved code
evaluation services include International Code Council Evaluation Service
(ICC-ES), the International Association of Plumbing and Mechanical Officials
(IAPMO), or any other service accredited by ANSI in accordance with
ISO/IEC Guide 65. Refer to DMS-6110 for pre-qualification requirements.
Class E adhesives also have the following properties.
• Maximum cure time of 24 hr. at 77°F
• Minimum gel time of 25 min. at 77°F
c. Class F. An approved building code evaluation service must evaluate Class F
adhesives in accordance with AC308 prior to pre-qualification. Approved code
evaluation services include International Code Council Evaluation Service
(ICC-ES), the International Association of Plumbing and Mechanical Officials
(IAPMO), or any other service accredited by ANSI in accordance with
ISO/IEC Guide 65. Refer to DMS-6110 for pre-qualification requirements.
Class F adhesives also have the following properties.
• Maximum cure time of 2 hr. at 77°F
• Maximum gel time of 2 hr. at 40°F
D. Type IV—Bridge Deck Sealant and Adhesive.
1. Description. Type IV adhesive is a low viscosity epoxy intended for use in sealing
cracks in concrete and restoring its structural integrity.

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DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

2. Physical Requirements. Table 5 describes the requirements for bridge deck epoxy.
Table 5
Type IV
Physical Property Test Method Requirement
Viscosity of Mixed Components, 125 (0.125) Max
centipoise (Pa-s)
Gel Time, min. 25 Min
Tex-614-J
Compressive Stress, @ 5% strain after 5,000 (34.5) Min
48-hr. cure @ 77°F (25ºC), psi (MPa)
Wet Strength, psi (MPa) 350 (2.4) Min
Track-Free Time, @ 77°F (25ºC), hr. ASTM C 679 5 Min
40 mil thickness 8 Max

3. General Requirements. The consistency of epoxy allows for the filling of voids in
concrete by gravity flow.
The epoxy has the capability of bonding to damp surfaces without shrinking, swelling,
or cracking during or after its curing process.
E. Type V and Type VII—Concrete Adhesives.
1. Description. Type V and Type VII adhesives are used to bond fresh concrete to
existing concrete and to bond hardened concrete to hardened concrete.
a. Type V. This formulation is suitable for sealing the surface of fine cracks in
concrete or for waterproofing applications and designed for applying to horizontal
and vertical surfaces.
b. Type VII. This formulation is a high-viscosity epoxy for vertical wall and
overhead application where a high build-up is required. Type VII is also suitable
for sealing the surface of cracks in concrete.
2. Physical Requirements. Table 6 describes the requirements for concrete adhesives.
Table 6
Type V and Type VII
Physical Property Test Method Requirements
Type V Type VII
Gel Time, min. 30 Min 30 Min
Tex-614-J
Tensile Bond @ 6 hr., psi (MPa) 200 (1.40) Min 200 (1.40) Min
Viscosity of Mixed Components, poise
400 (40) Max 1,200 (120) Min
(Pa-s)
Stability, % increase
Increase in Viscosity after 14-day heat Tex-614-J 20 Max 20 Max
aging @ 120°F (49°C)
Bond Strength of fresh concrete to cured
350 (2.4) Min 300 (2.10) Min
concrete, psi (MPa)

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DEPARTMENTAL MATERIALS SPECIFICATION EPOXIES AND ADHESIVES

3. General Requirements. The ratio of resin and hardener components is either 1:1 or
2:1 by volume.
The concrete adhesive must not contain volatile solvents.
F. Type VIII—Binder for Producing Grout or Concrete.
1. Description. Type VIII epoxies are binder materials mixed with select aggregates to
form a quick-setting epoxy for use in concrete repair. There are two classes.
a. Class A. This formulation is a low-modulus epoxy grout used to repair spalls,
chipped areas, and other defects in precast concrete.
b. Class B. This formulation is a high strength epoxy grout used to repair potholes,
cracks or spalls, and other defects in concrete.
2. Physical Requirements. Table 7 describes the requirements for binder components of
the epoxy grout without aggregate.
Table 7
Type VIII (Binder)
Physical Property Test Method Requirement
Class A Class B
Gel Time, min. 30 Min 30 Min
Stability, % increase 20 Max 20 Max
Increase in Viscosity after 14-day
heat aging @ 120°F (49°C)
Tex-614-J
Tensile Bond @ 24 hr. for Class 200 (1.40) Min 200 (1.40) Min
A and 6 hr. for Class B, psi
(MPa)
Water Gain, % 0.5 Max -
Elongation, % Tex-618-J 40 Min -

Table 8 describes requirements for the complete epoxy grout (binder and aggregate).
Table 8
Type VIII (Grout)
Physical Property Test Method Requirement
Class A Class B
Compressive Strength, psi (MPa) 500 (3.4) Min 5,000 (34.5) Min
Tex-618-J
Resilience, % 70 Min -
Old concrete to new grout mix, 200 (1.4) Min 290 (2.0) Min
psi (MPa)
Tex-614-J
Thixotropy (sag on test panel), in. 0.2 (5.0) Max 0.2 (5.0) Max
(mm)

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DEPARTMENTAL MATERIALS SPECIFICATION

3. General Requirements. The manufacturer must include the suitable mixing ratio on
the label of every container for the resin, hardener, and the aggregate mix by volume.
The manufacturer must specify the type and gradation of aggregate in the
binder/aggregate mixture.
G. Type IX—Epoxy for Crack Injection.
1. Description. Type IX epoxy is a low viscosity epoxy adhesive to be pressure-injected
into cracks in concrete to restore its structural integrity.
2. Physical Requirements. Table 9 describes the requirements for epoxy for crack
injection.
Table 9
Type IX
Physical Property Test Method Requirement
Gel Time, min. 20 Min
Viscosity of Mixed Components, 1,000 (1.0) Max
Tex-614-J
centipoise (Pa-s)
Wet Strength, psi (MPa) 250 (1.7) Min

3. General Requirements. Type IX epoxy is capable of bonding to damp surfaces.

The pigment of the mixed adhesive is gray in color with no streaks.
H. Type X—Epoxy Coating for Concrete.
1. Description. Type X epoxy is a high-solids epoxy coating designed mainly as a
coating for pier caps and the interior walls of rest areas.
2. Physical Requirements. Table 10 describes the requirements for the resin component
of epoxy coating for concrete.
Table 10
Type X (Resin Component)
Physical Property Test Method Requirement
Grind (Fineness of Dispersion), Tex-614-J 4 Min
Hegman

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DEPARTMENTAL MATERIALS SPECIFICATION

Table 11 describes the requirements for the mixed resin and hardener components of
epoxy coating for concrete.
Table 11
Type X (Mixed Resin and Hardener Components)
Physical Property Test Method Requirement
Gel Time, min. 80 Min, 160 Max
Thixotropy, mil (mm) 8 (0.20) Min
Thickness retained from a Tex-614-J
coating of 10 mil (0.25 mm)
Hiding Power (contrast ratio) 0.80 Min

6100.6. Packaging and Labeling. Package components in airtight containers and protect from
light and moisture. Include detailed instructions for the application of the material and all safety
information and warnings regarding contact with the components.
The label must include the following:
• resin or hardener components;
• brand name;
• name of manufacturer;
• lot or batch number;
• temperature range for storage;
• date of manufacture;
• expiration date; and
• quantity contained therein.

6100.7. Storage. Store the epoxy and adhesive components at temperatures recommended by
the manufacturer. Do not use damaged or previously opened containers and any material that
shows evidence of crystallization, lumps, skinning, extreme thickening, or settling of pigments
that cannot be readily dispersed with normal agitation.

6100.8. Environmental Requirements. Follow sound environmental practices when disposing

of epoxy and adhesive wastes. Dispose of all empty containers separately.
Dispose of individual components by mixing according to manufacturers' instruction and
allowing the mixed adhesive to cure before disposal.
Dispose of epoxy adhesive provided in prepackaged containers by completely emptying and
mixing the epoxy before disposal.

6100.9. Archived Versions. Archived versions are available.

TEXAS DEPARTMENT OF TRANSPORTATION 9–9 EFFECTIVE DATE: JUNE 2014