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Article history: This study explores the influence of olive waste ash (OWA) on the performance of concrete exposed to
Received 18 March 2008 elevated temperatures in the range from 400 to 600 1C. The performance of concrete to elevated
Received in revised form temperature was evaluated using compressive strength and electrical charge of concrete. Three OWA
16 August 2008
levels were used in the study: 7%, 15%, and 22% by weight of cement. The other experimental parameters
Accepted 25 August 2008
investigated in the study were elevated temperature (400 and 600 1C), aggregate type (crushed basalt
Available online 18 October 2008
and volcanic tuff), w/c ratio (0.5 and 0.7), and air content (non-air and air entrained). After the initial
Keywords: moist curing period of 90 days, concrete specimens were exposed to elevated temperatures for a period
Olive waste ash of 2 h using an electric furnace.
Elevated temperatures
The study showed that the performance of OWA concrete to elevated temperatures is higher than
Concrete
that of the control concrete. Additionally, the performance of OWA concrete to elevated temperature
Compressive strength
Electrical charge increased when the OWA content was increased. The resistance of OWA concrete containing tuff
aggregate to elevated temperatures was observed higher compared to OWA concrete containing basalt
aggregate. The OWA concrete at w/c ratio of 0.5 was found to be more resistant to elevated temperatures
than that of OWA concrete at w/c ratio of 0.7. The performance of the air entrained OWA concrete to
elevated temperature was observed higher compared to the non-air entrained OWA concrete.
& 2008 Elsevier Ltd. All rights reserved.
0379-7112/$ - see front matter & 2008 Elsevier Ltd. All rights reserved.
doi:10.1016/j.firesaf.2008.08.006
ARTICLE IN PRESS
2. Experimental program
2.1. Materials
Table 4
Proportions of concrete mixture (kg/m3) used in the study
Mix OWA (%) w/c Cement (kg) OWA (kg) W (kg) CA (kg) FA (kg) Aggregate SP (%) AE (%)
SP: superplasticizer, AE: air entraining admixture, CA: coarse aggregate, FA: fine aggregate.
Dosages of SP and AE admixtures are reported as percent by weight of cement.
Table 5 800
Compressive strength (MPa) of the concrete mixtures used after 90 days of curing 400 C
type and cured in a water tank for an initial moist curing period of
90 days. Three concrete specimens (cubes and cylinder slices) 200
were prepared and tested in the study for each test condition
to obtain average values. Table 5 shows the compressive
strength of the concrete mixtures used in the study after 90 days 0
of moist curing. 0 2 4 6 8 10 12 14 16 18 20 22
Time (hour)
2.4. Test procedures
Fig. 2. A schematic diagram for the thermal treatment used in the study.
Residual Compressive Strength (%) N.M. Al-Akhras et al. / Fire Safety Journal 44 (2009) 370–375 373
100 100
80 80
60 60
40 40
20 20
0 0
0 7 15 22 0% at 400 C 15% at 400 C 0% at 600 C 15% at 600 C
OWA Content (%) Percent OWA at Exposed Temperature
Fig. 3. Effect of OWA content on the residual compressive strength of OWA Fig. 5. Effect of aggregate type on the residual compressive strength of plain and
concrete exposed to elevated temperatures. OWA concrete exposed to elevated temperatures.
10000 to 600 1C decreased from 8600 C for control concrete to 3400 C for
400 C 600 C the 22% OWA concrete.
Electrical Charge (Coulomb)
10000 10000
Basalt Tuff w/c = 0.5
Electrical Charge (Coulomb)
6000 6000
4000 4000
2000 2000
0 0
0% at 400 C 15% at 400 C 0% at 600 C 15% at 600 C 400 600
Percent OWA at Exposed Temperature Exposed Temperature (C)
Fig. 6. Effect of aggregate type on the electrical charge passed through plain and Fig. 8. Effect of w/c ratio on the electrical charge passed through OWA concrete
OWA concrete exposed to elevated temperatures. exposed to elevated temperatures.
100 100
w/c = 0.5 Non-Air Entrained
80 w/c = 0.7 80 Air Entrained
60 60
40 40
20 20
0 0
400 600 400 600
Exposed Temperature (C) Exposed Temperature (C)
Fig. 7. Effect of w/c ratio on the residual compressive strength of OWA concrete Fig. 9. Effect of air content on the residual compressive strength of OWA concrete
exposed to elevated temperatures. exposed to elevated temperatures.
The increase in the performance of OWA concrete including charge (indicating more resistance at elevated temperatures) than
tuff aggregate to elevated temperatures compared to OWA that of OWA concrete at w/c ratio of 0.7. The electrical charge
concrete including basalt aggregate is attributed to the low unit decreased significantly for OWA concrete at w/c ratio of 0.5
weight and specific gravity of the tuff aggregate compared to that compared to OWA concrete at w/c ratio of 0.7. The percent
of the basalt aggregate. Therefore, the porosity of the tuff decrease in the electrical charge was 58% and 52% for OWA
aggregate is higher than that of basalt aggregate. Upon exposing concrete exposed to elevated temperature of 400, and 600 1C,
concrete including tuff aggregate to elevated temperatures, the respectively.
vapor pressure built up will escape to the pores of the tuff The increase in the performance of OWA concrete exposed
aggregate and relieving the pressure induced in the concrete. to elevated temperatures at w/c ratio of 0.5 compared to the
OWA concrete at w/c ratio of 0.7 is explained that the OWA
concrete at w/c ratio of 0.7 had large capillary pores that filled
3.3. Water to cement ratio
with water compared to OWA concrete at w/c ratio of 0.5. Thus,
the vapor pressure induced in the OWA concrete at w/c ratio of 0.7
The study investigated the effect of two w/c ratios (0.5 and 0.7)
was increased significantly compared to OWA concrete at w/c
on the resistance of OWA concrete to elevated temperatures. The
ratio of 0.5.
effect of w/c ratio on the RCS of OWA concrete exposed to elevated
temperatures is shown in Fig. 7.
The OWA concrete at w/c ratio of 0.5 showed higher 3.4. Air entrainment
performance to elevated temperature than that of OWA concrete
at w/c ratio of 0.7. The RCS of OWA concrete exposed to elevated The study investigated the effect of two air contents (non-air
temperatures at w/c ratio of 0.5 increased significantly compared entrained and air entrained) on the resistance of OWA concrete to
to OWA concrete at w/c ratio of 0.7. The RCS of OWA concrete elevated temperatures. The effect of air content on the RCS of OWA
exposed to 600 1C decreased from 36% for OWA concrete at w/c concrete exposed to elevated temperatures is shown in Fig. 9.
ratio of 0.5–19% for OWA concrete at w/c ratio of 0.7. The air entrained OWA concrete showed higher performance to
Fig. 8 shows the effect of w/c ratio on the electrical charge elevated temperature than the non-air entrained OWA concrete.
passed through OWA concrete exposed to elevated temperatures. The RCS of the air entrained OWA concrete increased significantly
The OWA concrete at w/c ratio of 0.5 showed lower electrical compared to the non-air entrained OWA concrete. The RCS of OWA
ARTICLE IN PRESS
Air Entrained
8000
peratures. Nevertheless, the incorporation of other supplementary
cementing materials such as silica fume and metakaolin reduced
6000 the resistance of concrete exposed to elevated temperatures.
Based on the outcomes obtained from this study, the following
4000
conclusions may be drawn: