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2 Selective electron beam melting In a first step, a defocused electron beam scans the
Selective electron beam melting is, just like all the entire surface of the powder layer several times in order
other layer-based technologies, integrated into the to set the preheating temperature. Depending on the
process chain of additive manufacturing. This encom- utilised material, this varies from 300°C for pure copper
passes the elaboration of a three-dimensional virtual [6] right up to 1,100°C for some nickel-based alloys [7].
computer model of the component to be manufactured, This process step is extremely important for the process
the preliminary processing of this data by dividing it into stability. One challenge facing this procedure is the charge
individual layers with a constant layer thickness, the dissipation of the electrons via the powder bed. If this is
manufacturing and the post-processing. In the post-pro- not guaranteed, it results in the so-called “smoke“ phe-
cessing, the manufactured components are removed from nomenon with which the top powder layer, so to speak,
the powder bed by means of sandblasting with the same explodes because powder particles are thrown out of the
powder. The powder recovered in this way can be reused layer. This inevitably leads to the termination of the
for the process. Depending on the application of the com- process. Due to the slight sintering of the particles during
ponents, the surface can then be post-treated even fur- the preheating, it is possible to guarantee a sufficient elec-
ther, e.g. in order to reduce the roughness inherent in the trical conductivity. The inflow of helium up to 2 · 10-3 mbar
process. supports the stable process management. The helium
The possible material diversity of selective electron atoms are positively ionised by the electron beam and
beam melting is restricted to electrically conductive ma- can subsequently dissipate the negative charge from the
terials, i.e. metals. Since electrons interact with the at- powder bed. Furthermore, the entire powder bed supports
mosphere, the manufacturing takes place in a vacuum the component due to the sintering.
chamber which is usually regulated to a pressure in the In a second step, the regions belonging to the com-
range of 2 · 10-3 mbar using a controlled helium inflow. ponent geometry are melted completely with a focused
The electron beam gun with a typical power of up to 3 kW electron beam. Depending on the geometry, different
and an accelerating voltage of 60 kV is mounted on the process strategies which may be composed of a combi-
vacuum chamber. Beam diameters of 100 to 1,000 µm nation of contours and hatches at typical scanning speeds
are achieved depending on the quality and type of the of 4 m/s and 10 m/s are used here. In this respect, the
cathode and on the utilised power. Electromagnetic coils contours can optionally be processed in the so-called
can be used in order to move the electron beam at de- multibeam mode in which up to 100 contour positions
flection speeds of up to 10,000 m/s without any inertia. are melted completely in quasi-simultaneous operation.
Two powder tanks and one rake are installed in the inte- This is possible due to the high maximum deflection
rior of the vacuum chamber in order to apply the layers speed of the electron beam. A hatch describes an area
in the construction space with a mobile process platform. which is melted completely in a meandering shape with
The components of the vacuum chamber and the indi- certain line spacing, typically between 25 µm and 150 µm.
vidual process steps of the manufacturing are illustrated As standard, this scanning pattern is rotated by 90° in
on Fig. 1. each layer.
Fig. 1 • Process chain of selective electron beam melting: After the preheating of the entire powder layer with a defocused electron
beam (1), component regions are completely melted selectively according to the computer model (2). After the consolidation and
the solidification, the process platform is lowered by one layer thickness (3) and a new powder layer is applied (4); cf. [5].
3 Materials
Currently, there is just one manufacturer which com- IN718) and, to an increasing extent, titanium aluminides
mercially offers installations for selective electron beam are playing major roles nowadays.
melting (Arcam AB, Sweden). Therefore, the commercial The great advantage of the SEBM procedure is being
availability of materials which can be processed with shown with regard to the extension of the material range,
SEBM is still extremely restricted at present. However, in precisely for complex material systems, since the high lo-
the research field, a large number of alloys have already cal cooling rates result in very fine and homogeneous
been successfully processed into totally leak-tight com- structures. This leads to outstanding material properties.
ponents. In this respect, the number of available materials In this respect, the structural fineness may be two orders
and material systems is constantly increasing even further of magnitude below that of cast alloys [7]. Moreover, there
and is thus extending the potential application possibilities are approaches for using suitable beam manipulation
of this procedure. Table 1 gives an overview of the mate- strategies for the targeted setting of the structure according
rials already processed with SEBM today. to the requirements [17]. For example, the typically colum-
At the beginning of the introduction of the procedure nar structure in the building direction can be transformed
at the end of the 1990s, interest primarily centred on tool into an equiaxed structure by the intended formation of
steel, e.g. in order to implement casting shapes with cool- new nuclei, Fig. 7 (left).
ing operations close to the contours. Today, attention is In general, material properties which are the absolute
focusing on applications in medical technology or in avi- equal of or frequently even considerably better than those
ation. In association with these, the materials mainly of conventional manufacturing technologies can be
processed with SEBM have also been developed away achieved nowadays with the correct process strategy. The
from steels (316L and H13) towards Co alloys production of completely leak-tight components is a matter
(Co-Cr-Mo-C) and, above all, towards titanium (pure ti- of course in the meantime. The powder quality tends to
tanium and TiAl6V4). Moreover, nickel-based alloys (e.g. constitute a problem since gas pores introduced into the
powder by the atomisation process can be found in the coating. The reaction to be carried out in it is the release
component after the SEBM process. That explains a fre- of hydrogen from perhydro-N-ethylcarbazole, a liquid or-
quently arising residual porosity of max. approx. 0.5% which, ganic hydrogen carrier [24]. With regard to the heat trans-
however, can be removed, for example, by downstream hot port and the pressure loss, the structured reactor is far
isostatic pressing (HIP), in so far as this is necessary. superior to the classic powder bed reactor. Furthermore,
only additive manufacturing is feasible for reactor ele-
4 Applications ments such as the illustrated flue gas tube for the quick
One major advantage of additive manufacturing is the dissipation of the gaseous hydrogen or even integrated
almost unrestricted design freedom. This is particularly cooling ducts. The combination of the high thermal con-
great in the case of SEBM since the powder bed not only ductivity of pure copper with the design freedom due to
serves as a support for any overhangs but also has a high SEBM also makes it conceivable to manufacture complex
mechanical stability due to the slight initial sintering in heat exchangers which can be exactly oriented to an ex-
the preheating step, e.g. also in comparison with SLM. In isting heat transmission problem, Fig. 3 (right).
connection with the low inclination to distortion as a result The SEBM technology shows further advantages dur-
of the high preheating temperature, hardly any supporting ing the processing of high-temperature materials such as
structures are needed for SEBM and, apart from totally nickel-based alloys and titanium aluminides (TiAl). The
finished cavities (from which the powder can then no possibility of making the electron beam scan over the
longer be removed), there are unlimited freedoms with powder bed in a defocused mode at high deflection speeds
regard to the component designing. In this respect, the during the preheating permits a high energy input without
great variability of the electron beam permits the simul- melting the powder completely. Thus, the entire powder
taneous production of the geometry and the structure and bed can be constantly kept at temperatures above 1,000°C
thus the setting of the material properties. However, it is during the construction phase. With this strategy, residual
necessary to take account of the in-situ heat treatment stresses, particularly in thick-walled components, can be
due to the increased process temperature and its influ- reduced effectively and high-performance materials such
ence, for example, on precipitation processes. A few pos- as TiAl can be processed.
sible applications of SEBM are shown below. The use of TiAl for rotating parts, e.g. turbine blades
The SEBM procedure makes it possible to manufac- or turbocharger wheels, is particularly attractive as a result
ture cellular structures which could not be manufactured of the low density and the low moments of inertia. Until
in this way by conventional means, Fig. 2. Thus, hybrid now, more complex components made of TiAl have been
structures consisting of solid and porous regions are ap- manufactured almost exclusively by means of centrifugal
plied in medical technology today, e.g. as implants which casting. Selective electron beam melting constitutes an
are adapted to the patient and can be supplied in an ex- alternative with various advantages. The SEBM process
act-fitting form within just a few days on the basis of a works in a vacuum. Therefore, no contamination takes
scan of the patient’s bone structure. That increases the place in spite of the high affinity of the TiAl materials to
success of the treatment and reduces the operation stress reactions with other elements. Moreover, any reactions
for the patient. Moreover, metamaterials are easy to pro- of TiAl with the crucible material and thus any possible
duce with the SEBM procedure. These materials receive changes in the properties can be avoided since it is set up
their properties from their structures. For example, it is in the powder bed without any tools. The rapid solidifica-
possible to manufacture materials with negative Poisson’s tion leads to extremely fine microstructures and a homo-
ratios, so-called auxetic structures, or even materials with geneous distribution of the alloying elements. Any demix-
an acoustic band gap which completely eliminate me- ing processes are suppressed. In the case of electron beam
chanical oscillations in a certain frequency range. melting, supporting structures which turn out to be small
Moreover, cellular structures can be utilised in order in comparison with the casting residues in the centrifugal
to design structured reactors with adjusted reactions [23]. casting procedure are utilised in a targeted way for the
One example of this is illustrated on Fig. 3 (left). The re- formation of distortion-free components. In interplay with
actor was manufactured from TiAl6V4 with SEBM and the powder recycling after the manufacturing, this results
serves as the carrier material for a subsequent catalyst in good material utilisation.
Fig. 5 • Essential physical phenomena during selective electron beam melting. Representation of the powder bed (blue), the elec-
tron beam (red) and the molten pool (temperature distribution from white to red) including the molten pool dynamics (arrows) [5].
the heat conduction, the energy input by the electron crystalline structure is to result from the formation of new
beam or the heat loss caused, for example, by heat radia- grains on the bottom of the molten pool. However, it is
tion or evaporation. Furthermore, a lot of material pa- unexplained why this does not coincide with the classic
rameters are temperature-dependent and thus sensitive model for CET (columnar-to-equiaxed transition). On Fig.
to correct modelling. The complete melting of the material 7 (right), the solidification rates at the solidification front
results in a molten pool whose dynamics are essentially are illustrated over the temperature gradient from data in
determined by capillarity, evaporation pressures, wetting the numerical simulation for two different sets of param-
effects, Marangoni flows and gravitation. During the so- eters. These results contradict the CET in two aspects.
lidification, the temperature gradient and the solidification Firstly, the formation of new grains would be expected at
rate have decisive influences on the occurring microstruc- the end of the solidification of the molten pool on the
ture unless this is destroyed once again by solid phase basis of the results whereas new grains form at the bottom
transformations. of the molten pool. Secondly, the assignment of colum-
By applying numerical simulation [25...27], it was pos- nar-crystalline and polycrystalline structures should be
sible to explain different phenomena arising during the precisely opposite to the process parameters on the basis
SEBM process. One such phenomenon is, for example, of the solidification conditions [29]. These contradictions
the characteristic of tunnel porosity. Any kind of porosity could be revealed with the aid of numerical simulation
should be minimised in order to achieve good mechanical and are currently the subject of the research into the mod-
properties. The porosity structures for an experiment (top elling of the texture characteristic, especially the formation
left) and a simulation (top right) with existing tunnel of new grains, during selective electron beam melting.
porosity are illustrated on Fig. 6. It is possible to explain
this phenomenon by considering the development of an 6 Concluding remarks
imperfection over many layers in the simulation (bottom). Selective electron beam melting is suitable for manu-
Due to the low power of the electron beam and the sto- facturing technically sophisticated products and offers
chastically unfavourable positions of the particles in the the possibility of processing high-performance alloys. In
powder bed, the molten pool can be divided into two this respect, additive building-up permits complex geo-
smaller ones. The surface tension curves both molten metrical shapes which are subject to hardly any restric-
pools at the separating point and establishes a small im- tions. These possibilities are reflected in the diversity of
perfection. Since the melting depth with the electron beam the technological applications. Nevertheless, the further
is not sufficient in order to melt this defect completely, industrial success of this procedure needs continuous re-
the molten pool is now separated at this defect time and search into new materials, better process observation and
time again and both parts are drawn to the sides of the process control as well as understanding for process and
defect by capillary forces. Thus, the imperfection may per- component optimisation measures.
sist over many layers and the tunnel porosity occurs [28]. At present, a wide material range of the most diverse
By choosing suitable parameters, though, it is possible material systems is the subject of the research. In this re-
to manufacture compact and leak-tight components spect, the complexity of the materials and the require-
which no longer differ in the transverse sections. However, ments on the processing are increasing continuously. Out
both columnar-crystalline and polycrystalline structures, of numerous application possibilities as individual com-
as illustrated on Fig. 7, can be recognised on EBSD (elec- ponents and small-scale series, reactors as a combination
tron backscatter diffraction) orientation maps. One aim of cellular and solid structures and turbine blades with
during the manufacturing is to be able to set this structure internal cooling ducts were described here.
freely in order to exert targeted influences on material In addition to applications of this procedure, simula-
properties in a component. Experimental results show tion is an important pillar for better understanding of the
that the solidification direction of the molten pool plays process. The development of the tunnel porosity or the
an essential role in this respect. The greater the deviations texture characteristic was specified as an example but
from the building direction are, the more likely a poly- many other subject fields such as alterations in the alloy
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Closing date for editiorial contributions: 14 July 2017 Closing date for editiorial contributions: 12 September 2017
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