Lampiran A Perhitungan

A.1 Perhitungan Neraca Massa

Sampel input = 150 ml
Sampel output = 85 ml
Over flow output = 65 ml
Total input =150 ml
Total output = sampel output +over flow output
= 85 ml + 65 ml
= 150 ml
A.2 Perhitungan Neraca Panas

 Panas dibawa air pendingin (T3)

m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔

Cp1 = 4,2 Kj/kgK

TFT 17°C = 290K

 Panas dibawa air pendingin = FT. Cp1. TFT

= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 69°C = 342 K

 Panas dari Heater = FT. Cp1. TFT

=10-3 kg. 4,2 Kj/kgK. 342K
=1,4364 kj
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
 =(65 ml. 0,6548 gr/ml).2,26 J/grC. 32 C
= 3078,0838 J
= 3,0780 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,4364 kj – (3,0780 kj + 1,2180 kj )
Qloss =1,4364 kj-4,296 kj
Qloss = -2,8596 kj

Perhitungan untuk t = 5 menit

Sampel input = 150 ml

Sampel output = 127,5 ml
Over flow output = 22,5 ml
Total input =150 ml
Total output = sampel output +over flow output
= 127,5 ml + 22,5 ml
= 150 ml

 Panas dibawa air pendingin (T3)

m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 17°C = 290K

 Panas dibawa air pendingin = FT. Cp1. TFT

= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 72°C = 345 K
  Panas dari Heater = FT. Cp1. TFT
=10-3 kg. 4,2 Kj/kgK. 345K
=1,449 kj
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
=(22,5 ml. 0,6548 gr/ml).2,26 J/grC. 32 C
= 1627,2 J
= 1,6272 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,449 kj – (1,6272 kj + 1,2180 kj )
Qloss =1,449 kj-2,8452 kj
Qloss = -1,3962 kj

Perhitungan untuk t = 10 menit

Sampel input = 150 ml

Sampel output = 138 ml
Over flow output = 12 ml
Total input =150 ml
Total output = sampel output +over flow output
= 138 ml + 12 ml
= 150 ml

 Panas dibawa air pendingin (T3)

m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 17°C = 290K

 Panas dibawa air pendingin = FT. Cp1. TFT

= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
 = 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 69°C = 342 K

 Panas dari Heater = FT. Cp1. TFT

=10-3 kg. 4,2 Kj/kgK. 342K
=1,4364 kj
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
=(12 ml. 0,6548 gr/ml).2,26 J/grC. 33 C
= 586,0198 J
= 0,5860 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,4364 kj – (0,5860 kj + 1,2180 kj )
Qloss =1,4364 kj- 1,804 kj
Qloss = -0,3676 kj

Perhitungan untuk t = 15 menit

Sampel input = 150 ml
Sampel output = 105,5 ml
Over flow output = 11 ml
Total input =150 ml
Total output = sampel output +over flow output
= 139 ml + 11 ml
= 150 ml

 Panas dibawa air pendingin (T3)

m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1
𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 17°C = 290K

 Panas dibawa air pendingin = FT. Cp1. TFT

= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
 m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 70°C = 343 K

 Panas dari Heater = FT. Cp1. TFT

=10-3 kg. 4,2 Kj/kgK. 343K
=1,4406 kj
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
=(11 ml. 0,6548 gr/ml).2,26 J/grC. 31 C
= 504,6281 J
= 0,5046 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,4406 kj – (0,5046 kj + 1,2180 kj )
Qloss =1,4406 kj-1,7226 kj
Qloss = -0,282 kj

Perhitungan untuk t = 20 menit

Sampel input = 150 ml
Sampel output = 141,3 ml
Over flow output = 8,7 ml
Total input =150 ml
Total output = sampel output +over flow output
= 141,3 ml + 8,7 ml
= 150 ml

 Panas dibawa air pendingin (T3)

m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 17°C = 290K
  Panas dibawa air pendingin = FT. Cp1. TFT
= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 69°C = 342 K

 Panas dari Heater = FT. Cp1. TFT

=10-3 kg. 4,2 Kj/kgK. 342K
=1,4364 kj
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
=(11 ml. 0,6548 gr/ml).2,26 J/grC. 31,5 C
= 512,7673 J
= 0,5127 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,4364 kj – (0,5127 kj + 1,2180 kj )
Qloss =1,4364 kj-1,7307 kj
Qloss = -0,2943 kj

Perhitungan untuk t = 25 menit

Sampel input = 150 ml
Sampel output = 140,2 ml
Over flow output = 9,8 ml
Total input =150 ml
Total output = sampel output +over flow output
= 140,2 ml + 9,8 ml
= 150 ml

 Panas dibawa air pendingin (T3)

m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
 = 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 17°C = 290K

 Panas dibawa air pendingin = FT. Cp1. TFT

= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 61°C = 334 K

 Panas dari Heater = FT. Cp1. TFT

=10-3 kg. 4,2 Kj/kgK. 334K
=1,4028 kj
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
=(9,8 ml. 0,6548 gr/ml).2,26 J/grC. 31 C
= 449,5778 J
= 0,4495 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,4028 kj – (0,4495 kj + 1,2180 kj )
Qloss =1,4028 kj-1,6675 kj
Qloss = -0,2467 kj

Perhitungan untuk t = 30 menit

Sampel input = 150 ml
Sampel output = 145 ml
Over flow output = 5 ml
Total input =150 ml
Total output = sampel output +over flow output
= 145 ml + 5 ml
= 150 ml
  Panas dibawa air pendingin (T3)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 17°C = 290K

 Panas dibawa air pendingin = FT. Cp1. TFT

= 10-3 kg . 4,2 Kj/kgK. 290K
= 1,2180 kj
 Panas dari Heater (T1)
m3
FT = 1 L x 10−3 L
= 10−3 𝑚3
𝑘𝑔
= (10−3 𝑚3) x 1𝑚3
= 10−3 𝑘𝑔
Cp1 = 4,2 Kj/kgK
TFT 70°C = 343 K

 Panas dari Heater = FT. Cp1. TFT

=10-3 kg. 4,2 Kj/kgK. 343K
=1,4406 kg
Panas dibawa oleh over flow (T2)
Panas dibawa oleh overflow = D. Cp1. TFT
=(5 ml. 0,6548 gr/ml).2,26 J/grC. 30 C
= 221,9772 J
= 0,2219 Kj
Qloss = Qheater – (Qoverflow + Qwatercooler)
Qloss = 1,4406 kj – (0,2219 kj + 1,2180 kj )
Qloss =1,4406 kj-1,4399 kj
Qloss = -0,0007 kj

Massa jenis ekstrak minyak atsiri =

𝑏𝑒𝑟𝑎𝑡 𝑝𝑖𝑘𝑛𝑜𝑚𝑒𝑡𝑒𝑟 𝑏𝑒𝑟𝑖𝑠𝑖 𝑒𝑘𝑠𝑡𝑟𝑎𝑘 − 𝑏𝑒𝑟𝑎𝑡 𝑝𝑖𝑘𝑛𝑜𝑚𝑜𝑒𝑡𝑒𝑟 𝑘𝑜𝑠𝑜𝑛𝑔
𝑣𝑜𝑙𝑢𝑚𝑒 𝑝𝑖𝑘𝑛𝑜𝑚𝑒𝑡𝑒𝑟
13,13 𝑔𝑟−9,7 𝑔𝑟
= 0,72 gr/ml
5𝑚𝑙
𝑔𝑟 𝑔𝑟
0,8 −0,72
𝑚𝑙 𝑚𝑙
% efisiensi evaporator = 𝑔𝑟 x 100 %
0,8
𝑚𝑙

= 10 %
Lampiran B Rangkaian Alat