08/09/19 PDN Scale Lab Scale

CNO (2hrs RXN) 50000 Kg 564.67 g

Esterification
PTSA 15 Bags 4.24 g
MeOH 5 KL 44.61 g
Trans-Esterification
Caustic Pearl Usage 0.0085 -
1st Rxn CP 80% - 3.84 g
1st Rxn Meoh 7100 L 63.34 g
2nd Rxn CP 20% - 0.96 g
2nd Rxn Meoh 3000 L 26.77 g
Wash 1 Water 5455 L 61.61 g
Wash 2 Water 5455 L 61.61 g
Wash 3 Water 5455 L 61.61 g
MeOH SG 0.79 - -
1st Rxn Drained SW
2nd Rxn Drained SW
W1 Drained Water
W2 Drained Water
W3 Drained Water
% Yield
 RO for Blending 50000 Kg 1900 g
Trans-Esterification
Caustic Pearl Usage 0.65% -
1st Rxn CP 80% - 9.88 g
1st Rxn Meoh 80%(25) L 380.00 g
2nd Rxn CP 20% - 2.47 g
2nd Rxn Meoh 20%(25) L 95.00 g
Wash 1 Water 5123.00 Kg 194.67 g
Wash 2 Water 5123.00 Kg 194.67 g
Wash 3 Water 5123.00 Kg 194.67 g
MeOH SG - -
1st Rxn Drained SW
2nd Rxn Drained SW
W1 Drained Water
W2 Drained Water
W3 Drained Water
% Yield
 CME WIP - Good AO (T12)
Date Completed: 1/9/2020
 12/20/2019 2:15:00 PM PDN Scale Lab Scale
CNO N/A Kg 502.94 g
Citric Acid Purity (%) 6.0
Addition of Citric Acid (Qty) 1.24
Gum QTY
Addition of Lye (Qty) 40.85
Addition of Wash Water (Qty) 25.99
Drained Wash Water (g)
Drying Weight Before
Drying Weight After
% Yield