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Wei Supplement May 2011:Layout 1 4/11/11 2:53 PM Page 95

Correlation of Microstructures and Process


Variables in FSW HSLA-65 Steel
Of the FSW process heat indexes investigated, heat input provided
the best correlation with post-friction stir weld microstructures

BY L. Y. WEI AND T. W. NELSON

ABSTRACT high-strength aluminum alloys that are steels are manufactured by thermo-
difficult to weld with conventional arc mechanical controlled processing (TMCP),
The present study focuses on devel- welding. The intense plastic deformation which produces uniform refined mi-
oping a relationship between process at elevated temperature produces a fine crostructures providing superior combina-
variables and postweld microstructure in equiaxed microstructure due to dynamic tion of high-strength and excellent tough-
friction stir welded HSLA-65 steel. Fully recrystallization (Refs. 3–5). As-welded ness (Ref. 16). In conventional arc welding
consolidated welds were produced in 7075Al-T651 shows a reduction in yield of HSLA steel, the heat-affected zone
HSLA-65 steel using a PCBN convex- and ultimate strengths in the weld nugget, (HAZ) is susceptible to hydrogen-assisted
scrolled-shoulder-step-spiral (CS4) tool which is associated with the coarsening of cracking (HAC). Moreover, significant loss
over a wide range of parameters. Mi- the very fine hardening precipitates (Refs. of strength and toughness in the HAZ can
crostructures in the nugget center (NC) 3, 4). Rapid implementation of FS welded seriously compromise the mechanical prop-
aluminum alloys into industry applications erties of the weld (Ref. 16).

WELDING RESEARCH
are governed by lath bainite and with
some polygonal/allotriomorphic grain has motivated its application to other non- Friction stir welding has offered dis-
boundary ferrite, which are highly de- ferrous materials, such as Mg (Ref. 6), Ti tinct advantages relative to the arc weld-
pendent on heat input. Friction stir (Refs. 7, 8), and Cu (Refs. 9, 10). ing of HSLA-type steels. Previous re-
welded dependent variables are related Although most FSW research has fo- search demonstrated the feasibility of
with FSW independent variables by non- cused on aluminum alloys, there is consid- FSW HSLA 65 (Ref. 17), and X80 and L80
linear relationship. Heat input is identi- erable interest in the application of this steels (Ref. 18), all of which exhibited sat-
fied as the best parameter index. With in- technology to steels. Several studies have isfactory mechanical properties. Softening
creasing heat input, the volume of bainite reported on FSW of carbon and stainless of the HAZ in HSLA 65 (Ref. 21) and X80
decreases and the ferrite grain and lath steels. Friction stir welded carbon and ul- (Ref. 18) weldments were reported. Post-
sizes increase. A linear relationship was trafine-grained plain low-carbon steels FSW microstructural analyses of HSLA
established between heat input and have shown increased strength in the stir 65 (Refs. 19–21), X80, and L80 (Ref. 18)
semiquantitative postweld microstruc- zone due to refined microstructures and were limited. In addition, the effect of
tures. the formation of martensite and bainite FSW parameters on postweld microstruc-
(Refs. 11–13). Similarly, FS welded 304L ture and properties in HSLA steels has not
stainless steel exhibits higher tensile prop- been thoroughly investigated.
erties than base metal (Ref. 14). It has also The influence of FSW parameters on
Introduction been reported that FSW significantly re- the microstructure and mechanical prop-
fines the grains in the stir zone of 2507 su- erties has been studied by a number of in-
Friction stir welding (FSW) is a solid-
perduplex stainless steel while maintain- vestigators in Al and Mg alloys. Querin
state technology that has attracted consid-
ing the 50/50 austenite/ferrite ratio in the (Ref. 22) and Rodrigues (Ref. 23) found
erable interest since it was invented at
weld (Ref. 15). higher rotation speed resulted in finer mi-
TWI in 1991. Friction stir welding utilizes
In recent years, there has been much crostructures in FSW AA2219-T87 and
a nonconsumable tool that is inserted into
interest in FSW of high-strength low-alloy AA6016-T4. Afrin (Ref. 24) and Cao (Ref.
the abutting edges of the base metal. The
(HSLA) type steel. High-strength low- 25) reported larger grain size and de-
rotating tool generates heat by friction
alloy type steels are relatively new struc- creasing tensile properties at lower weld-
and plastic deformation between itself and
tural steels for use in applications requir- ing speed in FSW AZ31B magnesium
the base plate complete the joining
ing high strength, ductility, and good alloy. Cui (Ref. 26) concluded the welding
process (Ref. 1).
weldability, such as shipbuilding, oil and speed strongly affected the total size of the
Friction stir welding has shown distinct
gas line pipe. High-strength low-alloy stir zone of A356 cast alloy. Pilchak (Ref.
advantages over traditional arc welding. Be-
27) showed the welding speed had an in-
cause there is no melting, FSW produces
significant effect on grain size of FSW Ti-
less distortion and defects associated with
6Al-4V alloy.
cooling from liquid phase, such as liquida-
KEYWORDS Most research to date has tried to es-
tion-related cracking and porosity (Ref. 2).
tablish correlations between FSW inde-
Additionally, FSW is a “green” technology
Friction Stir Welding pendent variables (travel speed, rotation
in that it produces no arc radiation, no
HSLA-65 Steel speed) with postweld properties. Re-
fumes, and no hazardous waste.
Nugget Center search is limited on the investigation of the
The FSW process can be used to join
Heat Indexes correlations between FSW dependent
L. Y. WEI (lingyun.wei@ssab.com) is with R & Ferrite Grain Size variables, e.g., power and heat input, and
D, SSAB Americas, Mascatine, Iowa, and T. W. Bainite Lath Size postweld characteristics. In traditional arc
NELSON is with Mechanical Engineering Dept., welding, it is common practice to correlate
Brigham Young University, Provo, Utah. welding process parameters and mi-

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Polygonal
ferrite

1
Upper bainite
island
3.500 Radius
Convex

Fig. 1 — Grain structures of the base metal. Fig. 2 — Geometry of CS4 tool used in the welding.

crostructures with weld heat input. Corre- Experiments torques were recorded during welding.
lations between HAZ grain size and width Trial experiments were conducted to
with process parameters have been well The chemical composition of the HSLA determine the working range of rotation
established in traditional fusion welding 65 (ASTM A945) used in this study is pro- and welding speeds. Feasible limits of the
(Refs. 28, 29). vided in Table 1. The base metal mi- parameters were chosen to ensure that the
In FSW, Nelson et. al (Ref. 30) reported crostructure consists of refined upper bai- FSW joints were free from any defects.
that peak temperatures in the HAZ and mi- nite islands randomly embedded in the Design of experiments (DOE) techniques
WELDING RESEARCH

crohardness increased with increasing heat polygonal fine-grained ferrite matrix, with were used to form the design matrix. Nine
input in FSW HSLA 65. However, the ex- the average grain size about 8 μm as shown experimental conditions are derived from
tent to which the dependent variables influ- in Fig. 1. full factorial experimental design matrix
enced the microstructural evolution of FSW Test plates were prepared from 9.5-mm- (32 = 9). The method of designing such a
HSLA 65 weld is yet unknown. No correla- thick rolled plate with dimensions of 762 matrix is presented elsewhere (Refs. 38,
tion between dependent variables and mi- mm in length and 203.2 mm in width. The 39). Table 2 shows the nine sets of FSW pa-
crostructures has been established. long axis of the test plate was parallel to the rameters used to form the design matrix.
The objective of this study was to estab- rolling direction. Each plate was lightly Fully consolidated welds were made at all
lish correlations between FSW process vari- ground on both sides to remove oxide and parameters summarized in this table. The
ables, both dependent and independent, surface scale prior to welding. Before weld- corresponding axial force and spindle
and postweld microstructures in HSLA 65 ing, the plates were degreased with torque are also shown in Table 2. The
steel. methanol. All welds were performed under recorded spindle torque increases with in-
a depth-controlled process. Partial penetra- creasing welding speed and decreasing ro-
tion welds were made parallel to the plate tation speed which is similar to that re-
Table 1 — Measured Chemical Composition rolling direction. Argon, at a flow rate of 1.1 ported by Cui (Ref. 26).
of HSLA-65 Steel (Ref. 16) m3/h, was used as shielding gas to protect Equations 1 and 2 were used to calculate
both the tool and the weld area from surface the power and heat input, respectively.
Element wt-% Element wt-%
oxidation.
( 2π ) ΩT
C 0.081 Cr 0.15 A convex-scrolled-shoulder-step-spiral P= (1)
Mn 1.43 Cu 0.26 (CS4) tool was used for all the welds. The 60
Si 0.2 N 0.009 shoulder and pin section of the tool are
P
S 0.003 V 0.055 manufactured from solid PCBN (polycrys- HI = (2 )
P 0.022 Ti 0.013 talline cubic boron nitride). The geometry v
Ni 0.35 Nb 0.021 of the CS4 tool is shown in Fig. 2. A 0.5-deg where P is power (kW); Ω is rotation
Mo 0.063 Al 0.018 head tilt was applied during plunge and speed (rev/min); T is recorded spindle
Fe Balance Boron <0.0005 torque by FSW machine (N.m); HI is heat
welding. All process parameters and

Table 2 — Average Heat Input Value for Each Process Parameter of HSLA-65 FSW (the bold parameters are selected to establish the correlations
with post-weld microstructures)

Rotation Welding Axial- Spindle Power Heat Advance per Pseudo Heat
Speed Speed Force Torque (kW) Input Revolution Index
(rev/min) (mm/min) (kg) (N.m) (kJ/mm) (mm/rev) (rev2/mm)

300 51 3410 90 2.8 3.33 0.17 1772


300 127 4297 119 3.8 1.77 0.42 709
300 203 4725 141 4.4 1.31 0.68 443
450 51 3144 71 3.3 3.93 0.11 3986
450 127 3769 85 4.1 1.91 0.28 1594
450 203 3740 98 4.6 1.37 0.45 997
600 51 3051 58 3.6 4.27 0.08 7087
600 127 4970 76 4.8 2.25 0.21 2835
600 203 3956 85 5.4 1.58 0.34 1772

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A B

C D

WELDING RESEARCH
Fig. 3 — A— PHI; B — APR; C — power; D — heat input vs. FSW process parameters.

input (J/mm); and ν is welding speed crease with increasing welding voltage and Ω2
(mm/min). current, and deceasing welding speed. PHI = ( 3)
v
In order to establish correlations be- Friction stir welding is substantially dif-
tween postweld microstructures and FSW ferent from arc welding. The independent v
APR = (4 )
process variables, four different welding variables in FSW include rotation speed, Ω
parameters (highlighted in bold text in welding speed, axial force, tool geometry,
Table 2) were chosen. The selected weld- and tool material. These variables can be di- Where Ω is rotation speed (rev/min), ν is
ing parameters covered the extreme and rectly controlled by the operator. Depend- welding speed (mm/min).
intermediate levels of power and heat ent process variables are heat input, power, These indexes do not take into account
input, based on the data in Table 2. and spindle torque. Unlike arc welding, the effect of spindle torque or capture the
Transverse samples were removed from power and heat input in FSW cannot be specific energy of the process. Given that
the welds for optical metallography analy- controlled directly by independent vari- postweld microstructures are strongly de-
sis. Each sample was ground and polished ables. Power is dependent on rotation speed pendent on heat input in traditional arc
successfully through 1-μm diamond paste. and spindle torque. Spindle torque is not a welding (Refs. 28, 29), it would seem neces-
Samples were etched with 2% Nital and an- controlled variable, but rather a response sary to capture the effect of the specific en-
alyzed optically at magnifications up to variable (Ref. 31). To complicate matters, ergy in FSW. Therefore, it is likely that
1000× using an Olympus GX51 microscope. spindle torque is a function of rotation power and heat input will exhibit better cor-
speed, welding speed, tool geometry, tool relation with postweld microstructures. The
Results and Discussions material, and tool depth/axial force. Thus, it comparison of these parameter indexes in
is difficult to develop simple relationships the following section provides additional
Relations between Independent and between independent and dependent vari evidence to identify the process index that
Dependent Variables in FSW ables in FSW. correlates best with postweld microstruc-
Early FSW machines did not have the tures.
In order to correlate postweld mi- ability to monitor or record spindle
crostructures with process variables, it is torque. As a result, earlier researchers at- Comparison of FSW Parameter Indexes
necessary to understand the relationship tempted to establish simple empirical re-
between FSW independent and dependent lationships between input variables and In order to illustrate the characteristics
variables. In traditional arc welding, those machine outputs. Pseudo heat index of PHI, APR, power, and HI (heat input),
relations have been well-established. Power (PHI) (Refs. 32–34) and advance per rev- comparisons of these parameter indexes
and heat input are controlled directly by the olution (APR) (Ref. 31) were developed are discussed below. Using the data in
independent variables, i.e., welding current, as parameter indexes to correlate with Table 2, PHI, APR, power, and HI are
voltage, and travel speed (Ref. 28). Power peak temperature and postmechanical plotted vs. FSW rotation speed and weld-
and heat input have a linear relationship properties. The PHI and APR are defined ing speed. These three-dimensional plots
with these independent variables, e.g., in- in Equations 3 and 4, respectively. are shown in Fig. 3.

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A B
WELDING RESEARCH

C D
Fig. 4 — Microstructures of weld nugget center (NC) at various heat inputs (500×).

The PHI exhibits a second-order linear 2024. The nonlinear relationships exist be- Figure 4 compares the microstructural
relationship with rotation speed and re- cause power and heat input are the func- features within the NC at various heat in-
ciprocal relationship with welding speed tion of spindle torque, and spindle torque, puts. The tool rotation speed (rev/min) and
as shown in Fig. 3A. The APR exhibits the as discussed earlier, is a response variable. welding speed (mm/min) are noted in the
linear relationship with welding speed and The nonlinearity suggests that single or upper right-hand corner of each micro-
a reciprocal relationship with rotation even two parameter investigations are inad- graph. Heat inputs are noted in the bottom
speed as shown in Fig. 3B. These charac- equate to develop correlation between left-hand corners. The symbols in these im-
teristics imply that APR is less compli- FSW process parameters and postweld mi- ages represent different transformation
cated parameter index, since it has a lower crostructure and properties. In this study, products: α represents polygonal ferrite;
order relationship than PHI. four parameters were chosen to investigate αgb represents grain boundary allotriomor-
Both PHI and APR are not unique in correlations between postweld microstruc- phic ferrite; B represents bainite; and αw
that multiple combinations of these in- tural characteristics and process parameters represents Widmanstätten ferrite. From
dexes may have the same heat input. For in FSW HSLA-65. The parameters used for these optical images, several microstruc-
example, in Fig. 3A, 600 rev/min-203 this aspect of the investigation are high- tural characteristics can be observed.
mm/min, and 300 rev/min-51 mm/min, lighted in bold in Table 2. There is no evidence of base metal
have the same PHI values, but these two (BM) microstructures shown in Fig. 4. The
parameters have different power and heat Effects of Process Variables on equiaxed grains in BM have completely
inputs. The APR has similar redundan- Microstructures in Nugget Center (NC) transformed to lath bainite with some
cies. For example, 600 rev/min-203 polygonal/grain boundary ferrite. This in-
mm/min has the same APR value as 300 Microstructures in NC dicates the weld nugget reached a peak
rev/min-102 mm/min, but these have dif- temperature in excess of the A3, even at
ferent heat inputs. Redundancies prevent In this section, some consideration is the lowest heat input 1.31 kJ/mm.
accurate correlations between parameters given to postweld microstructural changes It is well known that microstructural
and postweld microstructural features. in the friction stir weld nugget at different changes in the weld are primarily affected
Power and heat input display nonlinear heat inputs. The nugget center defined in by heating rate, peak temperature, and
relationships with rotation speed and this study is located at the vertical center- subsequent cooling (Ref. 36). Cooling rate
welding speed, as shown in Fig. 3C, D. line of the stir zone, which has equal dis- is associated with heat input, i.e., lower
This is similar to that reported by Pew tances between the top surface and bot- heat input produces faster cooling rate
(Ref. 35) in FSW Al Alloys 7075, 5083, and tom of HAZ in the weld. (Ref. 36). At the lowest heat input in Fig.

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Fig. 5 — Schematic diagram shows how the ferrite grain and bainite lath Fig. 6 — Bainite lath size vs. FSW process variables.
measurements were made. B represents bainite, α represents polygonal fer-
rite. The red lines show the length of the short and long axes in polygonal fer-
rite grains; the ferrite grain size is obtained by averaging the length of these two
axes.

4A, the microstructure is mainly lath bai- rate in FSW compared to arc welding. optical microscopy. Bainite lath size was
nite. The lath boundaries are relatively Faster cooling rates are the result of 1) measured using the line intercept ap-

WELDING RESEARCH
straight and parallel. lower heat input, and 2) the large heat proach. The data presented represent an
With increasing heat input, two kinds sinking effect produced by the backing average of at least eight measurements
of microstructures are formed (shown in anvil. from each weld section. Although bainite
Fig. 4B, C): polygonal ferrite and upper Prior austenite grains (PAGs) are also lath sizes may only be semiquantitative at
bainite. Higher heat input produces a visible in these figures. However, most of best, they are repeatable and adequate for
slower cooling rate, and equiaxed polygo- the PAG boundaries are discontinuous. establishing the desired correlations.
nal ferrite starts to nucleate at the fer- The limited alloy addition in these type al- Figure 5 illustrates how the ferrite grain
rite/austenite boundaries and extend into loys result in limited segregation to the and bainite lath measurements are made to
untransformed austenite grain interiors PAG boundaries. As a result, etchants are acquire semiquantitative data. Bainite lath
(Ref. 37). unable to attack the prior austenite grain is measured by drawing a trace line (in
In Fig. 4D, the highest heat input at 4.3 boundaries (GBs) enough to produce suf- black) of known length perpendicular to the
kJ/mm, the primary microstructures are ficient contract to clearly identify them. lath boundaries, counting the numbers (N)
lath bainite along with dispersed particles Discontinuous PAG boundaries are high- of the lath intersections along this trace line,
at prior austenite grain boundaries coex- lighted by white curved lines in Fig. 5. then dividing the line length by the number
isting with some polygonal and allotri- Prior austenite grains are identified by the of intersections. Polygonal ferrite grains are
omorphic grain boundary ferrite. Allotri- existing boundaries with some estimation. easy to identify as shown in this figure. The
omorphic ferrite forms at a triple junction In order to investigate correlations be- measurements of ferrite grains were taken
of prior austenite grain boundaries (Ref. tween microstructures in the NC and FSW on every ferrite grain found in the optical
37). Long needle-shaped Widmanstätten process variables, quantitative grain/lath images by averaging the length of the long
ferrite is also observed in Fig. 4D. Pao size measurements are needed. Since the and short axes as shown in Fig. 5.
(Ref. 20) has reported similar structures in prior austenite grain boundaries are ab- The average grain/lath sizes are shown in
the stir zone of FSW HSLA-65. sent for the most part, PAG measurements Table 3. The ferrite grain size ranges from
In summary, additional polygonal/al- were not used in the present study for the about 10 to 25 μm as heat input increases
lotriomorphic grain boundary ferrite correlations made. In addition, bainite from 1.31 to 4.27 kJ/mm. Over this same
forms with increasing heat input. Al- lath size is difficult to quantify precisely by range, bainite lath size increases from 0.9 to
though higher-temperature transforma- optical microscopy even at higher magni- 2.25 μm. The authors believe the bainite
tion products (polygonal and allotriomor- fications (up to 1000×) because some bai- laths observed in these images consist of
phic grain boundary ferrite) are formed at nite lath structures are too fine to be dis- several thinner laths that are difficult to dis-
higher heat input, lath bainite is still the tinguished under optical microscope. tinguish by optical microscope. The lath
dominant microstructure in the FSW NC. Therefore, grain/lath size in the FSW NC sizes report may likely be larger than the ac-
This is due to the relatively fast cooling were measured as accurately as possible by tual value for reasons described previously.

Table 3 — Variation of Grain Size in the NC with Changing Power and Heat Input

Rotation Welding Power Heat Input Bainite Ferrite Width of


Speed Speed (kW) (kJ/mm) Lath Grain Size HAZ (mm)
(rev/min) (mm/min) (μm) (μm)

300 203.2 4.4 1.31 0.9 10 0.14


600 203.2 5.4 1.58 1.25 12.5 0.26
300 50.8 2.8 3.33 1.5 13 0.35
600 50.8 3.6 4.27 2.25 25 0.50

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A B

Fig. 7 — Variation of heat input vs. the following: A — Grain size; B — bainite lath size.
WELDING RESEARCH

Fig. 8 — Weld hardness contour map at 600 rev/min-203 mm/min (1583 J/mm) Fig. 9 — Width of HAZ vs. heat input
shows the hardness distribution. The black arrow indicates the HAZ. The white
lines indicate the measurement taken to obtain the average width of the HAZ. Red
arrows indicate the protruding spots in the HAZ.

Correlate Postweld Microstructures with linearly with increasing heat input. With lath/ferrite grain sizes and heat input were
Process Variables an increase in heat input of 2.27 kJ/mm, established. Since the peak temperature
ferrite grain size and lath sizes increased and cooling rate are governed by the heat
In this section, correlations between 150% and 150%, respectively. input in the FSW nugget center, higher
FSW process variables and postweld mi- The width of the HAZ in a friction stir heat input produces the following: 1)
crostructures are investigated. Using the weld provides additional evidence of heat higher peak temperature above A3 in the
data in Table 3, the bainite lath size is plot- input dependence. The width measurement NC, and 2) slower cooling rate. Peak tem-
ted against PHI, APR, P, and HI to iden- was obtained from a Vickers hardness map perature strongly affects prior austenite
tify which FSW process index exhibits the of the weld as shown in Fig. 8. The weld con- grain size, i.e., higher peak temperature
best correlation with postweld microstruc- tour map clearly displays the HAZ as indi- produces coarser austenite grains. This in
tures. The weld indexes were scaled to fit cated by the black arrow in the map. The turn would produce coarser microstruc-
on the same plot as shown in Fig. 6. range of 200 to 205 Hv was selected as the tures at the same cooling rate since larger
The PHI is not a unique FSW heat value of hardness at which the HAZ width PAG size provides fewer nucleation sites
index. Both the 600 rev/min and 203 was measured. The region adjacent to the (Ref. 39). This combined with slower cool-
mm/min, and the 300 rev/min and 51 weld is the HAZ, which turns a light blue ing rate prompt the formation of larger
mm/min (circled in Fig. 6) have the same color in the hardness map. The HAZ width grain/lath structures with increasing heat
PHI but a 17% difference in bainite lath was measured at ten different locations as input.
size. Contrary to most heat indexes, APR shown by the white lines drawn in Fig. 8 to In the present study, linear correlations
exhibits a nonlinear inverse relationship obtain the average measurement. Some between heat input and postweld mi-
with bainite lath size, e.g., bainite lath size protruding spots (as indicated with red ar- crostructures in the FSW nugget center
increases with decreasing APR. Addition- rows in Fig. 8) in the HAZ do not represent (NC) are established. Although the fit is
ally, power exhibits essentially no rela- the actual HAZ, which is HAZ with some good, the accuracy would likely improve if
tionship with bainite lath size. Bainite lath softening spots in the base metal or bad quantitative microstructural data were ob-
size correlates best with HI, exhibiting a hardness points. So measurements of the tained. These efforts are currently under
nearly linear increase with increasing HI. HAZ widths were not made at those pro- investigation.
Additionally, HI is a unique heat index, truding spots. In addition, the measure-
capturing all elements of the process that ments were not taken at the bottom of the Conclusions
contribute to the specific energy. The HI weld as the heat transfer was likely different
will be used as the FSW heat index at that location. The HAZ width as a func- The following conclusions can be made
through the remainder of this paper. tion of HI is plotted and shown in Fig. 9. from this investigation:
Using the data in Table 3, bainite lath Similar to traditional arc welding (Refs. 28, 1. Of the FSW process heat indexes in-
and ferrite grain sizes were plotted against 29), the width of the HAZ increases linearly vestigated, heat input provided the best cor-
heat input — Fig. 7. Ferrite grain size (Fig. with increasing heat input in FSW. relation with post-friction stir weld mi-
7A) and bainite lath size (Fig. 7B) increase The linear relationship between bainite crostructures. Heat input exhibits a linear

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relationship with ferrite grain size and bai- neering A 429: pp. 50–57. rotation speed and welding speed on material
nite lath size. 14. Posada, M., Deloach, J., Reynolds, A. P., flow and stir zone formation during FSW/P. Fric-
2. Other process indexes (APR, PHI, Skinner, M., and Halpin, J. P. 2001. Friction stir tion Stir Welding and Processing V, TMS Annual
and power) exhibit nonlinear relationships weld evaluation of HH-36 and stainless steel Conference, pp. 125–133.
weldment. Friction Stir Welding and Processing, 27. Adam, L., Pilchak, Z., Li, T., Fisher, J. J.,
with postweld microstructures. The APR
Indianapolis, Ind., Nov. 4–8. pp. 159–171. Reynolds, A. P., Juhas, M. C., and Williams, J. C.
and PHI are not unique: e.g., different weld 15. Sato, Y. S., Nelson, T. W., Sterling, C. J., 2007. The relationship between friction stir
parameters can have the same index value. Steel, R. J., and Pettersson, C. O. 2005. Mi- process (FSP) parameters and microstructure in
3. Ferrite grain size and bainite lath size crostructure and mechanical properties of fric- investment cast Ti-6Al-4V. Friction Stir Welding
both increased 150% with an increase in tion stir welded SAF 2507 superduplex stainless and Processing IV, pp. 419–428.
heat input of 2.27 kJ/mm. steel. Materials Science & Engineering A 397: pp. 28. Gunaraj, V., and Murugan, N. 1999. Pre-
376–384. diction and comparison of the area of the heat-
16. Sampath, K. 2006. An understanding of affected zone for the bead-on-plate and bead-on-
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