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Int J Fract (2007) 148:251–260

DOI 10.1007/s10704-008-9199-1

ORIGINAL PAPER

Cyclic loading and fracture mechanics of Ductal concrete


Ehab Shaheen · Nigel G. Shrive

Received: 13 November 2007 / Accepted: 19 March 2008 / Published online: 8 April 2008
© Springer Science+Business Media B.V. 2008

Abstract Reactive Powder Concrete (RPC) is a spe- 150 MPa [22 ksi] with metallic or organic fibres. All
cial type of ultra high strength, superplasticized, silica tests described here were performed on 40 × 40 ×
fume concrete, often fibre-reinforced, with improved 160 mm [1.6 × 1.6 × 6.3 in.] (Width (b) × Depth (d) ×
homogeneity because the traditional coarse and fine length (L)) prisms with Poly Vinyl Alcohol
aggregate are replaced by fine sand with particle sizes (PVA) fibres. Ductal is a family of RPC and micro-
in the range of 100–400 µm [4–16 thousandths of an defect-free concretes containing micro silica, silica
inch]. RPC properties are attractive because compres- fume, cement, Quartz sand, superplasticizer, and PVA
sive strengths up to 800 MPa [116 ksi] have been fibres. Mechanical and fracture parameters were inves-
recorded, but more typically in excess of 200 MPa tigated using four point bending. Low and high cyclic
[29 ksi]. Flexural strengths up to 141 MPa [20.4 ksi] fatigue tests were conducted in three stages, starting
and fracture energy of 40 kJ/m2 [kJ/in.2 ] have been from low to high strain cycles. Cracks generated by
reported—the latter achieved when steel or stainless cyclic fatigue tests were monitored periodically in order
steel fibres were included in the mix (Baché (1998) Pro- to evaluate the rate of crack propagation. Cracks were
ceedings of the 2nd international conference on superp- also investigated using a high magnification micro-
lasticizers in concrete, Ottawa, pp 35–41; Coppola et al. scope. Three pairs of specimens were tested, notched
L’Industria Ital Cemento 707:112–125 (1996); Blais and un-notched to evaluate fracture parameters. Four
and Couture PCI J 44(5):60–71 (1999); Richard and point bending was used again because determination
Cheyrezy (1994) Proceedings of V. Mohan Malhotra of the J-Integral (JI C ) requires the application of pure
symposium on concrete technology: past, present, and bending over a portion of the beam. Load was applied
future (SP 144). American Concrete Institute, Detroit, at the third points over a span (S) of 120 mm [4.7 in.],
pp 507–518; Richard and Cheyrezy Cement Concrete providing a span to depth ratio (S/d) of 3.0. Specimens
Res 25(7):1501–1511 (1995)). Ductal , a commer- were notched using a 1 mm [0.04 in.] thick diamond
cial RPC, has a compressive strength of approximately saw. The crack tip generated was circular and the crack
length (s) was approximately 10 mm [0.4 in.]. Tests on
the notched specimens included measurement of the
E. Shaheen (B) · N. G. Shrive crack mouth opening displacement (CMOD). Closed-
Department of Civil Engineering, University of Calgary,
2500 University Drive NW, Calgary,
loop testing was developed using a feed back signal
AB, Canada T2N 1N4 from the (CMOD) clip gauge attached to the notched
e-mail: eshaheen@ucalgary.ca specimens and from strain gauges attached to the un-
N. G. Shrive notched specimens. The weight (w) of each specimen
e-mail: ngshrive@ucalgary.ca was obtained prior to testing. Fracture parameters were

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252 E. Shaheen, N. G. Shrive

calculated from the load–deflection curves obtained properties. Concretes in the chemically bonded ceram-
from the notched and un-notched specimens. ics (CBC) category can be divided into macro-defect-
free (MDF) and densified-with-small-particles (DSP)
Keywords Fracture mechanics · Reactive powder concretes. DSP materials include both ultra high perfor-
concrete · Poly vinyl alcohol (PVA) fibres · mance concrete (UHPC) and reactive powder concrete
Silica fume · Cyclic loading · Crack mouth opening (RPC) (Baché 1998; Blais and Couture 1999; Coppola
displacement (CMOD) · Fatigue et al. 1996; Richard and Cheyrezy 1994). These rela-
tively new materials are characterised by an extremely
Nomenclature dense microstructure, compressive strengths in the range
ac Critical effective crack length of 150–250 MPa [22–36 ksi] (UHPC), or 200–840 MPa
AT otal Total area under the load–deflection (P –δ) [29–122 ksi] (RPC) and superior durability performance.
curve Reactive powder concrete is a special type of ultra
Ac Area up to peak load (Pe ) high strength superplasticized silica fume concrete,
CMOD Crack mouth opening displacement often fibre-reinforced, with improved homogeneity
CTODc Critical crack tip opening displacement because traditional coarse and fine aggregate are
d Beam depth replaced by very fine sand with particle sizes in
δc Deflection corresponding to maximum the range of 100–400 µm [0.004–0.016 in.] (Blais and
load (Pc ) Couture 1999; Richard and Cheyrezy 1994, 1995). Com-
δe Deflection corresponding to maximum pressive strengths up to 800 MPa [116 Ksi] have been
load (Pe ) in the elastic region reported, but more typically strengths are around 200
δ150 S/150 MPa [29 ksi]. Flexural strengths are typically in the
E Modulus of elasticity of beam 20–30 MPa [2.9–4.4 ksi] range, but 141 MPa [20.4 ksi]
EC Plain strain modulus of elasticity of the was achieved when stainless steel fibres were included
imaginary beam including the effective in the mix (Dugat et al. 1996). Fibres are added to
elastic crack overcome the limited tensile capacity of concrete. The
g(ac ) Geometry function for stress intensity fibres alter the mechanical characteristics of the mate-
factor rial, especially after the matrix has cracked, by bridg-
GI c Critical energy release rate for mode-I ing across the cracks and providing some post-cracking
cracks ductility and fracture toughness. The bridging reduces
GF Fracture energy the stress intensity at the crack tip, and higher energy is
JIc Critical J -Integral required for crack extension. The amount of additional
KIc Critical stress intensity factor for mode-I energy required for crack extension depends mainly on
cracks the physical and material properties of the fibres and
Pc Maximum load reached in the the matrix (Dubey and Banthia 1998).
load–deflection curve (P –δ) For many structures the live load varies in a repeti-
Pe Maximum load reached in the elastic tive manner: forces developed by wind, waves, trains,
region vehicular traffic and the like are cyclic in nature, often
σb Flexural toughness factor inducing vibration. Thus the design of structures which
S Beam span have a significant live to dead load ratio requires knowl-
TJCI Absolute toughness, measured by the area edge of the behaviour of the building materials under
under the P –δ curve to a deflection of repetitive loading.
Span/150 The roof canopies of the Shawnessy light rail transit
ν Poisson’s ratio station in Calgary have been constructed with Ductal ,
w Beam width a commercial RPC. The thin, light weight shell cano-
pies constructed from this new concrete were pre-cast
1 Introduction and assembled on site (Adeeb et al. 2005). The exper-
imental investigation described here was performed to
Innovative Portland cement concretes are categorised investigate the fatigue behaviour and fracture parame-
according to their mechanical, chemical, and physical ters of this new material.

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Cyclic loading and fracture mechanics of Ductal concrete 253

2 Research significance LVDT

P/2 P/2
Most recent design codes require that ultimate and ser-
viceability limit states be considered in the design of
concrete and masonry structures. Serviceability limit
states use cracking criteria and crack initiation is usu- d a0
ally assumed to occur when the modulus of rupture or
S/3
cracking strength is exceeded (Reda Taha et al. 2002). S
Only a small amount of research has been performed
L
on the mechanical properties and fracture mechanics
of RPC. The mechanical properties of Ductal rein-
forced with 12 mm organic fibres (PVA) for corrosion Fig. 1 Specimen dimension parameters for cyclic fatigue and
four-point test set-up
free concrete were therefore investigated. Cracks were
examined to assess fibre bridging, pull-out or fracture
during crack propagation. The modes of failure under 3 mm thick carbide saw blade. The crack tip was semi-
monotonic and cyclic fatigue loading were compared. circular as shown in Fig. 3. Four point bending was used
as the determination of JI C requires the application of
zone of pure bending over the notched section of the
3 Experimental methods beam (Broek 1982; Shah et al. 1995; Rice et al. 1973).
Closed-loop testing was developed using a feed-
The compressive strength of the Ductal was deter- back signal from the CMOD clip gauge attached to
mined from 3 (50 mm [2 in.] diameter × 100 mm [4 in.] the notched specimens, or the strain gauge glued to
long) cylinders. Fracture toughness tests were the bottom of the un-notched specimens at their mid-
conducted to evaluate fracture parameters. Four point span. The feedback provided stable, controlled failure
bending tests were performed on three plain (un- of the samples. The CMOD and the applied load were
notched) and three notched 40 mm [1.6 in.] × 40 mm recorded using a data acquisition system sampling at
[1.6 in.] × 160 mm [6.3 in.] (width × depth × length) 5 Hz (5 readings/s). Loading was applied in displace-
beams over a span (S) of 120 mm [4.3 in.]. The results ment control (0.01 mm/s [0.0004 in./s]) using an MTS
obtained were used to evaluate different fracture param- machine. The machine was programmed to change the
eters. The method is that developed by Reda Taha et al. rate of loading from 0.01 mm/s [0.0004 in./s] to
(2002), with dimensions adjusted to suit the size of 0.00033 mm/s [13 µin./s] according to the CMOD feed-
specimens available. The span to depth ratio was 3.0 back signal, to provide a controlled rate of increment
for all specimens. Cyclic fatigue tests were performed of CMOD. For the un-notched (control) specimens,
on un-notched specimens of the same size, loaded in the mid-span tensile strain was the control parameter.
the same way over the same span. Three un-notched specimens were tested under mono-
tonic loading to obtain data for the fracture parameters.
Results from these specimens were also used to guide
3.1 Fracture mechanics tests the choice of fatigue strains to be applied to specimens
subject to fatigue loading.
The flexural performance of the fibre-reinforced con-
crete was evaluated in terms of fracture parameters
derived from areas under the load vs. mid-span deflec- 3.2 Cyclic fatigue
tion curves of beams loaded at their third points. Pairs
of notched and un-notched beams were tested in four The cyclic fatigue tests were conducted to measure the
point bending. The test arrangement was as per Fig. 1 number of cycles to failure (N) under different low,
but with space underneath the specimen to accommo- medium and high strain ranges. The four strain ranges
date a clip gauge to measure the crack mouth open- were:
ing displacement (CMOD) of the notched specimens – 170 µε between 70 and 240 µε (155 (mean) ± 85
as shown in Fig. 2. Specimens were notched using a (amp)).

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254 E. Shaheen, N. G. Shrive

Fig. 3 Crack geometry

recorded using a data acquisition system running at


5 Hz (5 readings/s).

4 Results and discussion

4.1 Physical and mechanical properties

4.1.1 Density, compressive strength and initial


modulus

The weight (w) of each specimen (notched and un-


notched) was obtained prior to testing. The densities of
the specimens were calculated and are given in Table 1.
The density ranged from 2,316 to 2,383 kg/m3 [145–
149 lb/ft3 ] with an average of 2,342 kg/m3 [146 lb/ft3 ].
These values are similar to those obtained for the carbon
fibre reinforced reactive powder concrete (CFRRPC)
density range reported by Shaheen and Shrive (2006)
(1,760–2,410 kg/m3 [110–150 lb/ft3 ]). The average
Fig. 2 Four-Point bending test: (a) notched and (b) un-notched compressive strength of the three cylinders was 136
(plain) specimens MPa [19.7 ksi]). The Young’s modulus determined for

– 150 µε between 100 and 250 µε (175 (mean) ±75 Table 1 Mass and density values (volume of 0.000256 m3
(amp)). (15.6 in.3 ))
– 320 µε between 80 and 400 µε (240 (mean) ± 160 Specimen Mass g (ounce) Density Kg/m3 (lb/ft3 )
(amp)).
– 470 µε between 80 and 550 µε (315 (mean) ± 235 UN1 601 (21.2) 2,348 (147)
UN2 599 (21.1) 2,340 (146)
(amp)). UN3 610 (21.5) 2,383 (149)
Closed-loop testing used a feed back signal from a N1 593 (20.9) 2,316 (145)
N2 599 (21.1) 2,340 (146)
strain gauge glued to the bottom centre of the test N3 595 (21.0) 2,324 (145)
prisms. The mid span strain and the applied load were

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Cyclic loading and fracture mechanics of Ductal concrete 255

Fig. 4 Load vs. deflection Deflection (in)


for notched and 0 0.01 0.02 0.03 0.04 0.05 0.06 0.07 0.08 0.09
non-notched specimens 20 2

18 1.8
Non-Notched
Notched
16 1.6

14 1.4

12 1.2

Load (Kips)
Load (kN)
10 1

8 0.8

6 0.6

4 0.4

2 0.2

0 0
0 1 2 3 4 5 6
Deflection (mm)

Table 2 Fracture toughness test values (40 mm [1.6 in.] × 40 mm [1.6 in.] × 160 mm [6.3 mm] beams with 10 mm [0.4 in.] notch depth
on tension side of beam)
Specimen Type Pc kN (Kip) δc mm (in.) Pe kN (Kip) δe mm (in.) Ac kN mm (Kip in.) ATotal kN mm (Kip in.)

UN-1 Un-notched 15.53 (3.5) 2.29 (0.09) 20.01 (4.5) 0.18 (0.007) 6.7 (0.06) 33.02 (0.3)
UN-2 Un-notched 17.83 (4) 2.03 (0.08) 20.61 (4.6) 0.11 (0.004) 7.2 (0.064) 31.41 (0.28)
UN-3 Un-notched 13.54 (3) 2.12 (0.08) 16.48 (3.7) 0.10 (0.004) 3.9 (0.035) 26.35 (0.23)
N-1 Notched 6.9 (1.6) 2.75 (0.11) 5.34 (1.2) 0.29 (0.011) 1.27 (0.011) 6.41 (0.06)
N-2 Notched 8.01 (1.8) 3 (0.12) 4.07 (0.9) 0.26 (0.01) 1.53 (0.014) 10.26 (0.09)
N-3 Notched 8.25 (1.9) 2.93 (0.12) 4.64 (1.0) 0.10 (0.004) 1.47 (0.013) 10.37 (0.09)

Ductal was 53.3 GPa [7.7 × 106 psi], which is lower integration (Adams 1995). For the notched specimen,
than the Young’s modulus reported for CFRRPC (85.5 the area under the curve up to the peak load was deter-
GPa [12.4×106 psi]) (Karihaloo and Nallathambi 1989; mined (AN ). For the un-notched specimen, the area
Mindess et al. 1977; Johnston 1982; Cox and Marshall under the curve up to the magnitude of the peak load
1994), but higher than values reported for OPC concrete of the notched specimen (AUN ) was first calculated,
and HPC (23 GPa and 30 GPa [3.3 and 4.3 × 106 psi], then the total area under the whole un-notched load
respectively). deflection curve (AT otal ). The parameters derived from
the experimental results are summarized in Table 2.
4.1.2 Fracture parameters of RPC The parameters in Table 2 were used to calculate sev-
eral fracture parameters using a MathCADTM program
Sets of different parameters were derived from the (Reda Taha et al. 2002) (Table 3). The critical notch
load–deflection curves obtained for the notched and depth (ac ) was calculated using the effective elastic
un-notched specimens (Fig. 4). These parameters crack model proposed by Karihaloo and Nallathambi
included the peak load (Pc ) and its corresponding (1989). The critical effective crack length (ac ) was
deflection (δc ), and the elastic load (Pe ) and its corre- assumed to correspond to the peak load (Pc ). The model
sponding deflection (δe ). Areas under each load– also determines the modulus of elasticity (E) using the
displacement curve were calculated using trapezoidal elastic load (Pe ) within the proportional limit and the

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256 E. Shaheen, N. G. Shrive

Table 3 Fracture parameters for Ductal where S, beam span; w, beam width; d, beam depth;
Parameter Value δ150 , S/150. The fracture parameters calculated are
listed in Table 3. The flexural toughness factor calcu-
E GPa (×106 psi) 53.3 (7.7) lated for Ductal was slightly higher than the frac-
Ec GPa (×106 psi) 66.6 (9.6) ture toughness factor (6.4 MPa) reported by Dubey and
ac mm (in.) 10 (0.39)
KI C MPa m1/2 (Ksi in.1/2 ) 7.1 (6.4) Banthia (1998) for high performance steel fibre rein-
GI C N m/ m2 (lbf in./in.2 ) 229 (1.8) forced concrete with high reactivity Metakaolin and
CTODc µm (µin.) 28.8 (1,133) silica fume. This could be related to the bond strength
JI C N m/ m2 (lbf in./in.2 ) 1.3 × 104 (74.3) between the fibre and the matrix, which increases with
GF N m (lbf in.) 4.7 × 103 (26.9)
TJ CI N m (Kip in.) 31.9
an increase in matrix strength, but the rate of de-bond-
σb MPa (Kip) 7.4 ing following the peak load is much higher for high
performance matrices.

4.1.3 Cyclic fatigue


corresponding deflection (δe ). The elastic limit is usu-
ally defined as a proportion of the peak load. All the
No failure by complete separation of cracked surfaces
elastic loads chosen for analysis were about 65–75%
was obtained for any of the specimens tested in
within the linear region of the load–deflection curve.
fatigue—that is, no specimen broke into two pieces.
The LEFM parameters determined were the critical
The specimens certainly cracked and the cracks were
stress intensity factor KI C and critical energy release
bridged by fibres incorporated in the mix. For cements
rate GI C , using Eqs. 1 and 2 (Broek 1982):
reinforced with ductile (rubbery) fibres, a strong inter-

KI C = g(αc )σc π ac (1) face usually exists between the fibres and the cement
paste (Cox and Marshall 1994). For the specimen sub-
  jected to 70–240 µε, the test was terminated after 6 mil-
1 − ν2
GI C = KI2C (2) lion cycles; for the specimen subjected to 80–400 µε,
E
after 3.6 million cycles; the specimen subjected to 100–
where g(ac ), geometry function for stress intensity fac- 230 µε, after 4 million cycles; and finally, for the spec-
tor; ν, Poisson’s ratio. KI C was used to express the imen subjected to 80–550 µε, the test was terminated
fracture toughness of the concrete. KI C represents a after 6 million cycles.
measure of how much and how far the local stress Typical stress vs. load curves for cyclic fatigue speci-
field is altered (Broek 1982; Shrive and El-Rahaman mens are shown in Fig. 5. The cracks generated from the
1985; Gopalaratnam and Shah 1987). Finally, the frac- cyclic fatigue were investigated using a high magnifica-
ture energy GF was calculated. The fracture energy tion (300×) microscope. The high fatigue life was pro-
is calculated as the total energy absorbed to failure, vided by the organic fibres incorporated in mix, which
assuming that the energy absorption takes place only bridged the cracks. Of the fibres that appeared to remain
in the fracture zone and all deformation outside this bonded in the matrix, some appeared to be stretched
zone is purely elastic (Giaccio et al. 1993; Baalbaki below their elastic limit, and were buckled across the
et al. 1992). crack in the unloaded specimen (Fig. 6). One imagines
Toughness analysis was also conducted based on the that these fibres had partially pulled out of the matrix
JSCE method (Shaheen and Shrive 2006; JSCE-SF4 as the crack opened to the maximum tension of the
1994). JSCE flexural toughness parameters are based cyclic loading, and were now buckled across the shorter
on the total amount of energy required to deflect the crack width in the unloaded specimen. Other fibres
beam specimen by a specified amount. The absolute however, appeared to have experienced plastic defor-
toughness TJCI is defined as the area under the load– mation, clearly being subject to a permanent change in
deflection curve to a deflection of span/150. Another their cross-sectional area (similar to necking in ductile
parameter, called the flexural toughness factor σb , a metals) (Fig. 6). This seems feasible if these fibres did
measure of the equivalent flexural strength, defined as: not undergo any pull-out. Yet other fibres were bro-
TJCI · S ken (Fig. 6). Some fibres retained their geometry and
σb = (3) appeared straight with no signs of loading as can be
δ150 · w · d 2

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Cyclic loading and fracture mechanics of Ductal concrete 257

Fig. 5 Stress–strain curve (u in)


(low cycle fatigue) 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000
20 3

18
2.5
16

14
2

Stress (MPa)
12

(Ksi)
10 1.5

8
1
6

4
0.5

0 0
0 50 100 150 200 250 300
Strain (ue)

Fig. 6 Fibre failure


Fibre break

Plastic
Deformation

Elastic
Deformation

seen in Fig. 7: these we assume had de-bonded and multiple cracking was noticed around the crack tip,
pulled out at one end. Finally, some fibres split (Fig. 8), as shown in Fig. 9a, b. Such crack branching would
which we attribute to shear in these fibres because of increase the energy demand for further crack prop-
their angle relative to the crack. In specimens subjected agation, thereby increasing local fracture toughness.
to low cycle and medium cycle fatigue, fibre splitting The multiple crack formation may be due to the pres-
was observed and fibres with elastic and plastic defor- ence of flaws near the crack tip. Flaws such as air
mations. However, in the specimen subjected to the voids, micro cracks, etc. are inherent in the concrete
high strain range (550 µε), all forms of fibre defor- as shown in Fig. 10, even though the RPC tested
mation and failure were present. Given that we did here is typically very dense with low porosity and
not actually break a specimen with the fatigue load- permeability.
ing applied—even up to 6 million cycles, it is clear that Fibre failure is expected to precede matrix crack
the fibres are able to provide sufficient tensile rein- growth (Cox and Marshall 1994). There was no actual
forcement across the cracks, and have sufficient fatigue crack propagation rate versus number of cycles
resistance themselves to stabilize the response of the recorded in order to construct a fatigue compliance
specimen under these loading conditions. Additionally, curve. The rate of crack growth was estimated by

123
258 E. Shaheen, N. G. Shrive

Fig. 7 Fibre de-bonding

Fig. 8 Fibre splitting

attempting to measure the crack length and noting the


associated number of cycles. Fatigue generated cracks
were initiated approximately after 1,380 cycles for the Fig. 9 Crack branching (a) and (b)
specimen subjected to 80–400 µε, with an initial crack
length of 0.6 mm [0.02 in.]. Subsequent readings are
listed below and shown in graphically Fig. 11: at the contact points between the test specimens and
top and bottom rollers. A picture of the material loss
– 3,050 cycles, crack length 10 mm [0.39 in.]
due to support contact fretting is shown in Fig. 12.
– 3,150 cycles, crack length 13.5 mm [0.53 in.]
Ductal is also manufactured with steel fibres which
– 3,260 cycles, crack length 21.5 mm [0.85 in.]
would potentially produce different results because of
– 36,490 cycles, crack length 31 mm [1.22 in.]
the different fibre properties. However the basic mecha-
The rate of crack growth was fast initially but the rate nisms involved in increasing the toughness of the con-
slowed down as more and more fibres were brought crete with fibres would remain—fibre pull-out, fibre
into action bridging the crack. The curve is opposite in yield and fibre fracture. The fatigue properties of steel
sense to what would be expected from the Paris equa- would be different to those of the organic fibres used
tion, which describes crack growth in metals. in the mix tested here, but a similar high resistance to
Some fretting-like behaviour was observed on all fatigue failure would be expected based on the work of
fatigue test samples. Gradual material loss was noticed Richard and Cheyrezy (1995). Mild steel fibres might

123
Cyclic loading and fracture mechanics of Ductal concrete 259

Fig. 10 Microscopic picture of fracture surface. Air voids and Fig. 12 Fretting of the concrete at the contact support
reinforcing fibres are visible

cant improvements to a number of properties. When


be expected to corrode, although corrosion of such investigating the fatigue properties of a material simi-
fibres would be very slow in the high density mixes lar in many respects to Ductal (CARDIFFRC), Far-
achieved, because of the very low permeability and hat et al. (2007) had similar difficulty in failing the
porosity. However mild steel fibres exposed in a crack specimens. A couple of specimens were tested up to
might corrode locally. Obviously, stainless steel fibres 20 million cycles, 10–85% of the ultimate flexural
would not create this risk. The concrete tested here strength.
will also have excellent durability to corrosive environ-
ments, due to the use of polymer based fibres. With fur-
ther knowledge of the behaviours of RPC, RPC mixes 5 Summary and conclusions
using steel or other fibres could potentially be opti-
mised for certain attributes. The results obtained in The density of Ductal was in the range of (2,316–
the tests described here show the material has con- 2,383) Kg/m3 [145–149 lb/ft3 ]), Young’s modulus cal-
siderable potential to provide concretes with signifi- culated for Ductal was 53.3 GPa [7.7 × 106 psi]. The

Fig. 11 Crack length vs. Crack Length (in) (a)


number of cycles for loading 0 0.2 0.4 0.6 0.8 1 1.2 1.4
40000 40000
between 80 and 400 µε

35000 35000

30000 30000
Number of Cycles (N)

Number of Cycles (N)

25000 25000

20000 20000

15000 15000

10000 10000

5000 5000

0 0
0 5 10 15 20 25 30 35
Crack Length (mm) (a)

123
260 E. Shaheen, N. G. Shrive

fracture parameters indicate that the material is tougher Dugat J, Roux N, Bernier G (1996) Mechanical properties of
than other concretes. The results of the tests reported reactive powder concretes. Mater Struct 29(188):233–240
here also show that Ductal clearly possesses excel-
Farhat FA, Nicolaides D, Kanellopoulos A, Karihaloo
BL (2007) High performance fibre-reinforced cementitoi-
lent resistance to low and high cyclic fatigue load, us composite (CARDIFRC)—performance and application
even in the presence of a crack. The material is thus to retrofitting. Eng Fract Mech 74(1–2):151–167
an excellent candidate for many structural elements Giaccio G, Rocco C, Zerbino R (1993) The fracture energy (GF )
of high-strength concretes. Mater Struct 26(7):381–386
and structures that are subjected to high and low cycle Gopalaratnam VS, Shah SP (1987) Failure mechanisms and frac-
fatigue. ture of fibre reinforced concrete. In: Shah SP, Batson GB
(eds) ACI SP-105. Fiber reinforced concrete properties and
Acknowledgements We are grateful to Lafarge North America applications. Oslo, Norway, pp 1–25
for supplying the specimens, and the technical staff of the Depart- Johnston CD (1982) Definition and measurement of flexural
ment of Civil Engineering for their help in the testing. The finan- toughness parameters for fibre reinforced concrete. Cement
cial aid of the Natural Sciences and Engineering Research Coun- Concrete Aggregates 4(2):53–60
cil of Canada is gratefully acknowledged. JSCE-SF4 (1994) Standard for flexural strength and flexural
toughness, method of tests for steel fiber reinforced con-
crete. Concrete Library of JSCE, No. 3, June Japan Concrete
Institute (JCI), pp 58–66
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