Patent Tahun Judul

US 9,284,289 B2 2016 Method for producing tetrahydrofuran

US 7,465,816 B2 2016 Production of tetrahydrofuran from 1,4 butanediol

US 7,465,816 B2 2008 Production of tetrahydrofuran from 1,4 butanediol

Bahan Baku Fase Metode Reaktor Tekanan Temperatur Laju alir
1,4-Butanediol Liquid Cyclodehydration Fix Bed Reactor

Fix Bed Tubular

1,4 Butanediol Gas Dehydration Reactor 1 150-350 3-10
Liquid Reactor + Separator 1 150-350 5

1,4 Butanediol Dehydration

e
Katalis Konversi Kelebihan
Acid Katalis

catalyst having a high-efficiency reaction activity

Zirconium Sulfat 99.5 selectivity and has an excellent catalyst stability.
Zirconium Sulfat 99.5
Acidic Alumina 76.1
TPA 83.4
Silica Alumina 73.2
Zirconium Sulfat
Kekurangan

However, the above process has problems that inorganic acid is dangerous to
handle and the reactor is corroded by the inorganic acid.