2 Scope of work The Supplier performs all necessary calculations, selects equipment, fittings, pipelines, instrumentation and automated control systems devices, electrotechnical equipment required for operation of the installation of pyrohydrolysis. The Supplier performs complete delivery of the installation of pyrohydrolysis and spare Parts and accessories for two years of operation according to the design limit specified in the process flowsheet (see Fig. 1). Complete delivery of the installation of pyrohydrolysiscomprises process equipment, electrical equipment, instrumentation and automated control systems, metalwork (block-modular arrangement of equipment (items 17, see flowsheet in Fig. 1), thermal insulation of equipment and pipelines The Supplier shall develop the software, and provide equipment for the automated Process control system upper level (automated work station). The Supplier shall make complete the supplied equipment, reinforcements, control instrumentation units, including necessary drives, control cabinets, cabling etc The Supplier shall perform the works on supervised installation, reaching targeted indices, holding the training for the Customer's personnel, ‘The Supplier shall hand-over to the Customer the following documentation: + Diagrams and drawings on the following parts of the project: civil part (steel structures), process part, electric part, control instrumentation, and thermal insulation, including ~ Electric circuit diagrams, showing rated currents of the automatic circuit breakers, their rates (cutoff point); for input switches, breaker characteristics, and recommended settings must be indicated; - Connection diagrams; - Hardware complex structural diagram; - Process control diagram; ~ Electric circuit diagrams for instrument power supply; - Electric circuit breakers for measuring circuit, controlling circus, electric equipment surveillance and control circuits;- Emergency alarm electric circuit diagram; - Outside wiring connection diagram; - Outside wiring tie-in diagram; = Controller, and remote I/O stations — module location and connection diagrams (when controller is available); - Equipment layout, and cable routing diagrams; - Cable lists; - Cabinet and switchboard general arrangement, - Cabinet and switchboard specifications. Equipment, article, and material specification for the following project parts: civil (steel structures), process, electric, control instrumentation, and thermal insulation; + Explanatory notes with required calculations on the following project parts: civil part (steel structures), process part, electric part, control instrumentation, and thermal insulation; * Drawings for the equipment with dimensional and installation sizes, showing points ‘of equipment fixation, and loads, as well as the points for hardware and utility connection; Basic data for reinforced concrete structure development; * Utility demand (power, heat, fresh and recirculating water, compressed air, nitrogen, di * Process equipment and pipeline heat emissions; « Dimensional sizes, installation areas, and heat emissions for electrical cabinets and control instrumentation; Equipment noise rate; * Certificates / conformity declarations for supplied equipment according to the Technical regulations of the Customs Union «On machinery and equipment safety»; + Equipment technical data; «Packing list indicating dimensions and weight; Loading and unloading instruction; + Installation manual, and installation drawings; * Start-up and operational manuals; * Maintenance and repair manuals.2.1. Exclusions from the scope of works Reinforced concrete constructions, heating and ventilation, fire alarm system for the installation of pyrohydrolysis are designed and delivered by the Customer according to the initial data of the Supplier. 3. Requirements 3.1 Process part The installation of pyrohydrolysis is supposed to operate in a continuous mode. At that, considering trial character of operation, in the course of development of alumina production process frequent stops at emergencies or process violations are possible It is preferable to have the maximum extent of hydrolysis for complete regeneration of hydrochloric acid from chlorides of metals. There are no special requirements to a structure / grain sizing of pyrohydrolysis residue since it is production waste In the course of operation of the pyrohydrolysis installation with the use of absorption installation of its own running on water, concentration of hydrochloric acid obtained as a result of absorption should be as high as possible. Concentration of hydrogen chloride in waste gases after the absorption installation should be as low as possible and shouldn't exceed 30ppm To provide stable operation of the installation of pyrohydrolysis in acontinuous mode the flow of solution fed to the installation can be increased by increasing a share of recycled solution directed to pyrohydrolysis or for the account of process water (the increase in a flow fed to the installation of pyrohydrolysis should be agreed with the Customer). In case of impossibility / inexpediency to provide continuous operation of the installation of pyrohydrolysis due to low flow of solution, intermittent operation of the installation of pyrohydrolysis is possible according to the schedule proposed by the Supplier. At that, buffer tank of recycled solution will be delivered by the Customer on initial data of the Supplier (consumption tank (item11 (see Fig. 1) is delivered by the Supplier)The installation of pyrohydrolysis has to be equipped with the required quantity of shutoff and control valves, drainage and sampling devices The installation of pyrohydrolysis should be equipped with the required quantity of instrumentation and automated control systems ensuring automated functioning and remote control of the installation of pyrohydrolysis. The installation of pyrohydrolysis for the purpose of safe operation should be equipped the required number of safety valves / explosive plates. Withdrawal of vents from safety devices is carried out by the Supplier to design limit of the installation of pyrohydrolysis, the Customer in accordance with initial data of the Supplier carries out further withdrawal of vents Equipment and pipelines of the installation of pyrohydrolysis should be provided with thermal insulation in case if the temperature of surface exceeds 45 °C. The installation of pyrohydrolysis should be equipped with the required hoisting mechanisms to carry out remedial maintenance in case of fastening to the metalwork of the installation of pyrohydrolysis. If required, the Supplier will submit to the Customer initial data for designing external hoisting mechanisms for remedial maintenance. 3.2. Electrical Part The Supplier completes equipment of the installation of pyrohydrolysis with the required electric drives, boxes/ control panels, cables, terminal blocks in borders of the installation of pyrohydrolysis The Supplier completes the installation of pyrohydrolysis with a system of electric lighting (working, emergency, maintenance) in borders of metalwork delivered completely. Lighting: toexecute LED. The required illuminance — 200 Ix Supply of electric power to the installation of pyrohydrolysis is carried out by the Customer on initial data of the Supplier. Power supply category is II (two incomers with switching breaker)Circuit rate - UH=380 V(+10%), FH=50 Hz (0,2 Hz) Motor rated voltage is 0,38 KV. Equipment resistivity to short circuit currents is no lower than 30 kA. Motor insulation grade F Grounding system TN-S. Input shall be arranged by the copper wire cables with the proper cross-section. Unit cabling is accepted with copper wires Electric equipment and lamps shall have protection degree no less than |P-64 Frequency converters (if used) shall be chemical resistant. At the inlet, radio filters must be envisioned; at the outlet, DU/DT filters must be installed. Cables coming out of the frequency converters to consumers shall have copper wires, and be screened For the motors power supplied by the frequency converters, winding protection from aging, winding temperature sensors, and non-conductive bearings should be provided 3.3 Instrumentation and PCS Equipment of the stage should be provided with the required blocking and alarm system in case of emergency situations (emergency shut-down of process equipment, deviation parameters of the process from set limits). For design of the automated process control system, the following needs to be envisioned: signal receiving from the sensors installed on equipment and pipelines, not included into pyrohydrolysis unit supply set, and interlocks wirth this equipment / sensors (the list of signals and need of interlocks to be determined at engineering stage). The following parameters are subject to obligatory monitoring - concentration of solution by HC! after absorber (item 5); - pressure and temperature of gases after reactor (item), cyclone (item.3), Venturi scrubber (item 4), absorbers (items 5 and 7), fan (item 6); - pressure, consumption and temperature of solution from pumps (items 9 and 12) - pressure and consumption of process water for installation of pyrohydrolysis (in tank item 13, in absorber item 5); - pH and electrical conductivity of solution after absorber (item 7);- pressure and consumption of solution after installation of pyrohydrolysis (from pumps item16); - pressure, temperature and consumption of fuel for installation of pyrohydrolysis; - level and temperature of solution in tanks (items 11, 13, 18, 17, 19); = level of pyrohydrolysis residue in bin (item 2); - temperature in the reactor of pyrohydrolysis (item 1); It is assumed to take the following key parameters being stabilized at operation of installation of pyrohydrolysis: - solution flow for pyrohydrolysis from pumps (item 12); - concentration of solution by HCI after absorber (item 5); - pH and electrical conductivity of solution after absorber (item 7), - temperature in the reactor of pyrohydrolysis (item 1) As key adjustable parameters of the installation of pyrohydrolysis are assumed: = consumption of process water in absorber (item §); - NaOH/NazS2Os consumption in absorber (item 7); - fuel consumption in the reactor of pyrohydrolysis (item 1); PCS should be carried out on the basis DeltaV systemby Emerson company. PCS has hierarchical two-level structure: - lower level (LL) of PCS; = top level (TL) of PCS Low level of PCS is presented by a complex of local control systems including control systems of equipment of process trains. Each local control system is presented by local control devices (sensors), operating mechanism for realization of controlling actions fixed on process control objects, programmable controllers (PLC) which perform control functions of the lower level, distributed 1/0 stations.Local control systems should ‘comprise operator panels (OP) intended for local visualization of process parameters, input of settings values, alteration in PCS operation. Interaction between controllers of LL PCS local automated control systems is carried out by through field network. Startup of equipmentshould be executed by the allowing signal of PCS. Operator information panel of control panel should provide:- information output by parameters of operation (operating hours, efficiency, amount of the unloaded material, etc.) and equipment conditions, - input and transfer of target values of process parameters; - input of information on realization of plan targets (Date, shift, etc.) TL PCS should be presented by WKS of operator and technological personnel. WKS software carries out receipt, processing and archiving of information from LL PCS to database of TL PCS. Interaction between LL PCS and server of TL PCS is carried out through Ethernet (TCP/IP) Control, operation conditions and functions of LL PCS: - support of automatic and manual (local) control mode of process equipment; - providing maintenance andpreventive mode of operation without shut down of principal processequipment and control units; - providing automatic serial switching on \switching off of process equipment; - providing automatic blocking and protection of equipmentfor regulated operation mode, start-up/ shut down and preventing development of emergency situations; - alteration and input (using the procedure of authentication, checking authenticity of values) values of settings of process parameters, alteration in the status ofequipment, alteration in control modes; - maintaining of process parameters according to the setting; - display of relevant process parameters, condition of process equipment in local operator panels; - display of information on condition of PCS equipment (power supply units, controllers, modules of analog and discrete signals etc.) in local operator panels; - signaling of excess in values of set process parameters or equipment protection, Funetions of TL PCS: - receipt of information from LL PCS - parameters of process, condition of process equipment and devices of control system; - processing of parameters values (averaging, summation, etc.) by various time frames, - maintaining data archive; - creation of technological, emergency and system messages with transfer to LL PCS archiving thereof. - differentiation of access to TL PCS using the procedure of authentication;= information output by parameters of operation and state of processing equipment; - visualization of process state in the form of mnemonic diagrams (for the whole process train, with possibility of displaying separate units); = information output on condition of PCS equipment (power supply units, controllers, modules of analog and discrete signals etc); = recording of confirmations (acknowledgment) of messages (date, confirming user, message) - input and transfer of values on parameters of process to LL PCS; - review of archive data in graphic and text modes with the use of reference and user documents; = administration of users access rights to functions and resources of TL PCS (parameter, screen forms, etc.); - export of PCS data to other standard software for processing and display of data (MS Excel, MS Access, etc.); - to provide possibility to integrate pyrohydrolysis PCS with high level of area Pcs. Degree of protection of instrumentation boxes and automated control systems not lower than IP-64, Besides above listed,delivery set comprises cable production with terminal blocks and installation materials to it, and software, 3.4 Construction Part Installation of pyrohydrolysis is placed in a heated building of the pilot plant of alumochioride process. The Supplier performs complete delivery of metalwork of pyrohydrolysis installation for arrangement of equipment (items . 1+7) (see flowsheet in Fig. 1), including pipeline supports, elements of cables fastening, protection enclosures of working platforms. Metalwork should be provided with anticorrosive protection considering operation conditions, Other equipment of the installation of pyrohydrolysis (items 8*20) is placed at elevation 0,000 near the module delivered completely according to basic engineering of the SupplierThe Supplier provides initial data for designing of the bases of the installation ofpyrohydrolysis (bases for module delivered completely for equipment (items 1+7), stand-alone bases for equipment (items 8+20), supports of pipelines and so forth). The Supplier gives recommendations on design, material, anticorrosive protection of floors, trays, bases, metalwork for the installation of pyrohydrolysis. The Supplier specifies places of working passes in the installation of pyrohydrolysis for designing by the Customer of flights of stair and transitional bridges for joining working platforms of the installation of pyrohydrolysis with working platforms of the Pilot plantof alumochioride process. 3.5 Sanitary part The Supplier shall make available to the Customer the heat emissions from the pyrohydrolysis unit, in order to develop the project on heating and ventilation of the ‘experimental and industrial area on alumochloride process. Emergency shower / eye shower are designed outside the desorption unit. Blowing residue from the safety devices and aspiration suction are designed and handled by the Supplier within the limits of the pyrohydrolysisunit. The blowing residue and aspiration suction are removed from the pyrohydrolysisunit to the traps by the Customer based on the Supplier's initial data The Supplier shall provide compressed air, water and nitrogen to the equipment within the limits of the pyrohydrolysisunit. The Customer shall provide compressed air, water, and nitrogen to desorption unit based on the Supplier's initial data Effluent discharge from the work grounds of the pyrohydrolysisunit down to 0,000 elevation is provided by the Supplier. Effluent discharge from the pyrohydrolysisunit at 0,000 elevation is carried out by the Customer based on the Supplier's initial data. 3.6 Documentation Documentation is executed in the Russian and English languages in MS Office and PDF. Format for drawings — dwg and paf. 3D models of equipment and drawings in dwg, step, inventor. Units of measure for drawings and documentation — in Si-system. 3.7 Terms of performance of work Terms of submitting technical and commercial offer is September, 30 2018,Terms of submitting documentation required for designingisSeptember, 30 2018 for installation drawings. Term of delivery isthe minimum possible (determined by the Supplier), the approximate start date of construction is 2020. Duration of installation supervisionisdetermined by the Supplier Duration of reaching target parametersisdetermined by the Supplier. Duration of training of personnel of the Customerisdetermined by the Supplier. 3.8 Check tests and accepting Acceptance of equipment is carried out by the commission in several stages: = external inspection; — quality control of assembly and completeness of equipment; — leakproofness and strength test; = inspection of the bodies and control systems, compliance of equipment with safety requirements; — idle test (for machines, mechanisms and vehicles with a drive) ~ final acceptance of the equipment is carried out by testing under production conditions under load with achievernent of the declared design parameters. After that the Acceptance Certificate "On acceptance of equipment after individual testing” is issued. 3.9 Principal conditions of agreement The recommended payment terms are 100% within 60 calendar days after the signing of the acceptance certificate. 3.10. Warranty liability Not less than 18 months. 3.11. Technical and commercial offer validity Recommended period of validity is 1 year. 4 Process parameters The Supplier selects parameters of theprocess providing maximal degree of hydrolysis of chlorides of metals contained in recycle solution yielding regenerated hydrochloric acid of maximum possible concentration