UNKNOWNSAMPLE

TESTTUBE1 TESTTUBE2
+3dropsunknownsample
+5dr opsAgHCsol
uti
on +Remai ni
ngunknownsampl e
acidifywi
th3MHNO³ +slowwi thsti
rri
ng,satur
ated
AgAcsolutionuntil
ppt
completesti
rthroughl
ythen
NO centr
ifuge

Preci
pit
atecolorfr
om white
t
hroughposi
ofyell
ow,or
ti
vecolorchanges
angeandbrownt o
-Thi
osul
fat
e
fi
nalcolorbl
ack

YES

+Thi
osul
fat
e

CENTRI
FUGATE PRECI
PITATE
END

WashPPTthroughH²Ocontai
ningf
ewdr opsoft
hreeFHNO³
di
scar
dwashagai nwi
thout3M HNO³greatwashpreci
pit
ate
10dropsAgNO³sti
rthr
oughoutendcentr
if
uge

Di
scar
d

CENTRI
FUGATE RESI
DUE

+1dr
opof3M HCI
+1dropof1M
+3M HNO³unt
ilsol
uti
oni
sdesi
del
yaci
d
FeCl
³

WHITE For
mati
onofred
PRECI
PITATE col
orat
ion

YES

+SCNi
ons
NO

YES NO -SCNi
ons

+CLi
ons -Cl
ions
END END