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Designation: F 150 – 98

Standard Test Method for


Electrical Resistance of Conductive and Static Dissipative
Resilient Flooring1
This standard is issued under the fixed designation F 150; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

This standard has been approved for use by agencies of the Department of Defense.

1. Scope 3. Terminology
1.1 This test method covers the determination of electrical 3.1 Definitions:
conductance or resistance of resilient flooring either in tile or 3.1.1 conductive flooring—resilient tile or sheet which,
sheet form, for applications such as hospitals, computer rooms, when tested in accordance with 8.1.1 or 8.2.1 shall have an
clean rooms, access flooring, munition plants, or any other average resistance greater that 25 000 V (2.5 3 104V) and less
environment concerning personnel-generated static electricity. than 1 000 000 V (1.0 3 106 V). When tested in accordance
1.2 This standard does not purport to address all of the with 8.2.2 the average value shall be no less than 25 000 V (2.5
safety concerns, if any, associated with its use. It is the 3 104V) with no individual measurement’s value less than 10
responsibility of the user of this standard to establish appro- 000 V.
priate safety and health practices and determine the applica- 3.1.2 static dissipative flooring—resilient tile or sheet
bility of regulatory limitations prior to use. which, when tested in accordance with 8.1.2 or 8.2.2 shall have
an average resistance greater that 1 000 000 V (1.0 3 106V)
2. Referenced Documents and less than or equal to 1 000 000 000 V (1.0 3 109 V). When
2.1 ASTM Standards: tested in accordance with 8.2.2 the average value shall be no
D 2240 Test Method for Rubber Property–Durometer Hard- less than 1 000 000 V (1.0 3 106V) and less than or equal to
ness2 1 000 000 000 V (1.0 3 109V).
E 177 Practice for Use of the Terms Precision and Bias in
ASTM Test Methods3 4. Significance and Use
E 691 Practice for Conducting an Interlaboratory Study to 4.1 Conductive and static dissipative floors (static control
Determine the Precision of a Test Method3 flooring) serve as a convenient means of electrically connect-
2.2 Other Standards: ing persons and objects together to prevent the accumulation of
EOS/ESD-SD7.1 Flooring Materials—Resistive Character- electrostatic charges. A static control floor is specified on the
ization of Materials4 basis of controlled resistance values. The surface of the floor
NFPA 99-1990 Health Care Facilities5 provides a path of moderate electrical conductivity between all
Federal Test Method Std. No. 501a, Method 8311— persons and equipment making contact with the floor to
Electrical Conductance6 prevent the accumulation of dangerous electrostatic charges.
Mono #11 Conductive Flooring for Hospital Operating Static control footwear will need to be used in conjunction with
Rooms7 the floor for the floor to perform effectively with personnel.
4.2 The resistance of some flooring materials change with
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age. Floors of such materials should have an initial resistance
This test method is under the jurisdiction of ASTM Committee F-6 on Resilient low enough or high enough to permit increase or decrease in
Floor Coverings and is the direct responsibility of Subcommittee F06.20 on Test
Methods—Products Construction/Materials. resistance with age without exceeding the limits prescribed in
Current edition approved Oct. 10, 1998. Published January 1999. Originally the product specifications (see Federal Test Method No. 501a,
published as F 150-72. Discontinued February 1998 and reinstated as F 150-98. Method 8311).
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Annual Book of ASTM Standards, Vol 09.01.
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Annual Book of ASTM Standards, Vol 14.02. 5. Apparatus
4
Available from the Electrical Overstress/Electrostatic Discharge Association,
Inc., Rome, NY. 5.1 Self-Contained Resistance Meter (such as a megohm
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Available from National Fire Protection Association, Batterymarch Park, meter) or power supplies and current meters in the appropriate
Quincy, MA 02269.
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Available from Standardization Documents Order Desk, Bldg. 4, Section D,
configuration for resistance measurement with 6 10 % accu-
700 Robbins Ave., Philadelphia, PA 19111-5094, Attn: NPODS. racy. For safety all power supplies used herein should be
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Available from National Bureau of Standards, Dept. of Commerce, Washing- current limited, usually below 5.0 mA. This apparatus shall be
ton, DC, March 1960.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.

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F 150 – 98
capable of open circuit voltages of 500 6 10 VDC or 100 6 10 100 VDC) and take a reading 5 s after the application of
VDC, or both. Test leads should be isolated from ground. voltage or once the reading has reached equilibrium.
5.2 Electrodes—Either style A or style B electrode may be
NOTE 1—The voltage applied should be determined by the use of the
used, but the same style shall be used together as a set. floor. The conductive resistance range tested at 500 VDC generally should
5.2.1 Style A—Two metal electrodes with terminals for be used in areas where explosive gases, chemicals, or munitions are used
making connection to the ohmmeter. Each electrode shall or stored.
weigh 5 lb 6 1 oz (2.27 kg 6 28 g) and shall have a dry, flat
circular contact area 2.5 6 0.062 in. (63.5 6 1.58 mm) in 8.1.2 Surface to Ground Test—Attach the positive electrode
diameter. or the positive wire from the megohm meter to the ground
5.2.2 Style B—Two cylindrical 5 lb 6 1 oz (2.27 kg 6 28 g) connection and place the negative electrode on the surface of
metal electrodes shall have a diameter of 2.3 6 0.062 in. (63.5 the flooring material. The negative electrode should be over 6
6 1.58 mm) each having contacts of electrically conductive in. (152.4 mm) from the ground connection and over 6 in.
material with a Shore-A (IRHD) durometer hardness of 50–70 (152.4 mm) from any metal ground strip embedded in the
(Test Method D 2240). The resistance between the electrodes adhesive. Apply the prescribed voltage (either 500 VDC or 100
shall be less than 1 Kohms when measured at 10 V or less on VDC) and take a reading 5 s after the application of voltage or
a metallic surface. once the reading has reached equilibrium.
5.3 Preparation of Electrode Style A—Place a piece of 8.2 Installed Testing—Lightly wipe the area to be tested
aluminum or tin foil 0.0005 to 0.0010 in. (0.0127 to 0.0254 with a lint-free cloth to remove any foreign material prior to
mm) thick on a flat, hard, smooth surface. On top of the foil placing of the electrodes. The surfaces of the electrodes, prior
place a layer of rubber 21⁄2 in. (64 mm) in diameter, 1⁄4 in. (6.4 to placing, should be cleaned with a minimum 70 %
mm) thick and having a Shore-A(IRHD) durometer hardness of isopropanol-water solution using a clean low linting cloth.
50–70 (Test Method D 2440). Place the electrode on top of the Allow to dry. Follow the manufacturer’s recommendation as to
rubber pad, draw the foil up around the rubber layer and the time after installation prior to testing.
electrode. Secure the foil with a rubber band or pressure- 8.2.1 Surface to Surface Test—Place the electrodes 1 in.
sensitive tape. Repeat procedure for second electrode. (25.4 mm) in from an edge of the specimen and 36 in. (914.4
mm) apart. Apply the prescribed voltage (either 500 VDC or
6. Test Specimen 100 VDC) and take a reading 5 s after the application of
voltage or once the reading has reached equilibrium.
6.1 Qualification Testing—When mounting specimen, use
insulative support material (1⁄4 in. tempered hardboard is 8.2.2 Surface to Ground—Place the electrodes 36 in. (914.4
recommended). Use manufacturer’s recommended procedures, mm) apart and at least 36 in. (914.4 mm) from any ground
adhesives, and grounding method to install the sample floor. connection or grounded object resting on the floor. Attach the
The specimen shall consist of a portion of floor covering 48 by positive electrode or the positive wire from the megohm meter
48 in. (1.22 by 1.22 m) in area. If a qualification test is to the ground connection and place the negative electrode on
required, one specimen shall be tested unless otherwise speci- the surface of the flooring material. Apply the prescribed
fied. Unless otherwise specified, make five measurements on voltage (either 500 VDC or 100 VDC) and take a reading 5 s
the specimen with electrodes at different locations for each after the application of voltage or once the reading has reached
measurement and record the value to two significant figures. equilibrium.
6.2 When the following is to be tested after jobsite instal- 8.3 On an installed floor, perform a minimum of 5 tests per
lation, the specimen shall be a portion of the floor not floor surface material or a minimum of 5 tests per 5000 ft2
exceeding 20 by 20 ft (6 by 6 m) in dimensions. (46.5 m2) of floor material, whichever is greater. A minimum of
three of the five tests should be conducted in those areas that
7. Conditioning are subject to wear or have chemical or water spillage or that
are visibly dirty.
7.1 Whenever possible, condition the test specimen at least
8.3.1 Areas that have lower ambient relative humidity could
24 h at 73.4 6 1.8°F (23 6 1°C) and 50 6 5 % relative
have resistance readings that vary from reading at higher
humidity, and test in the same environment.
ambient relative humidity.
8. Procedure NOTE 2—The ESD Association, ESD 7.1 uses 100 V. Underwriters
Laboratories certifies static control flooring using 500 V.
8.1 Qualification Testing—Place the installed specimen as
described in 6.1 on a nonconductive surface, and lightly wipe 9. Report
with a lint-free cloth to remove any foreign material prior to
placing of the electrodes. The surfaces of the electrodes, prior 9.1 Qualification Testing—The report shall include the fol-
to placing, should be cleaned with a minimum 70 % lowing:
isopropanol-water solution using a clean low linting cloth. 9.1.1 Number of square feet comprising test area, date, and
Allow to dry. Follow the manufacturer’s recommendation as to number of tests performed.
the time after installation prior to testing. 9.1.2 Average, minimum, and maximum values of measure-
8.1.1 Surface to Surface Test—Place the electrodes 1 in. ments in ohms and voltage.
(25.4 mm) in from an edge of the specimen and 36 in. (914.4 9.2 Installed Testing—The report shall include the follow-
mm) apart. Apply the prescribed voltage (either 500 VDC or ing:

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F 150 – 98
9.2.1 Number of square feet comprising test area, date and NOTE 3—Refer to the Appendix X1 for further information on the
number of test performed. studies performed.
9.2.2 Average, minimum, and maximum values of measure- 10.2 Precision and bias testing is being rerun by interlabo-
ments in ohms and voltage. ratory round robin in strict compliance with Practice E 691 and
the directive from ASTM’s Committee on Standards. The
10. Precision and Bias testing is proposed to be completed by March 1999.
10.1 Even though there is some degree of correlation within
and between laboratories for the same spot tested, variations 11. Keywords
within the sample limits the ability to provide a statistically 11.1 conductive; electrodes; electrostatic charge; flooring;
significant precision and bias statement for the test method. ground; megohm meter; resistance; static dissipative

APPENDIX

(Nonmandatory Information)

X1. INTRA- AND INTERLABORATORY STUDIES

X1.1 A variation study was conducted in one laboratory taken between different specified locations. Each of the five
with two operators and two instruments on a single test readings is treated as an individual test result.
specimen. Repeated test determinations were taken across five
points. X1.4 The repeatability standard deviation, 5 s, is therefore
the standard deviation for individual readings taken in one
X1.2 The average repeatability of measurements in this laboratory, by one operator, at different locations on the single
laboratory were found (1) without lifting the instrument test specimen. Tests were conducted dry surface-to-surface
(possibly representing variation in instrument readings) and (2) (dry SS), dry surface-to-ground (dry SG), wet surface-to-
lifting the instrument and repeating the measurement. The surface (wet SS), and wet surface-to-ground (wet SG).
means and repeatability standard deviations follow: Condition Test Range 95 % limit
Avg Std Dev Avg Std Dev
Repeatability Reproducability
Operator Instrument Average Not Lifted Lifted
Dry SS 0.44-1.62 1.15 1.60
A A 1.174 0.033 0.300
Dry SG 0.14-0.54 0.33 0.43
B 2.242 0.084 0.482
Wet SS 0.15-0.60 0.53 0.63
Wet SG 0.053-0.174 0.076 0.123
B A 1.646 0.045 0.233
B 1.554 0.069 0.239
X1.5 The terms repeatability limit and reproducibility limit
X1.3 An interlaboratory study was conducted on a single are used as specified in Practice E 177. The respective standard
test specimen consisting of 16 12 by 12 in. tiles mounted to a deviations among test results may be obtained by dividing the
plywood surface. In each of ten laboratories, five readings were numbers in columns 3 and 4 by 2.8.

ADDITIONAL MATERIAL

(1) Navships 0901-690-0002, Naval Ships Technical Manual, Chapter Underwriters Laboratories, July 1985.
9690, Electrical Measuring and Test Instruments, Part 7, Accuracy 3 (5) Department of Defense Military Handbook, MIL-HDBK 253, Guid-
percent of scale @ 25°C, Naval Sea Systems Command, Crystal City, ance for the Design and Test of Systems Protected Against the Effects
VA. of Electromagnetic Energy, Section 09675, Conductive Flooring,
(2) Army Material Command, 20315 – 385-224 Section 7, Static Elec- December 1988.
tricity, Washington, DC, June 4, 1964. (6) Department of Defense Contractor’s Safety Manual for Ammunition
(3) Bureau of Mines Bulletin #520, Static Electricity in Hospital Operat- and Explosives 4145.26-M, March 1986.
ing Suites, Direct and Related Hazards and Pertinent Remedies, (7) Department of Defense Military Handbook, DOD-HDBK-263 and
Superintendent of Documents, Government Printing Office, Washing- Military Standard DOD-STD-1686, Electrostatic Discharge Control
ton, DC. Program for Protection of Electrical and Electronic Parts, Assemblies
(4) UL-779, Standard for Electrically Conductive Flooring, Fifth Edition, and Equipment (Excluding Electrically Initiated Explosive Devices).

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F 150 – 98
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