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Static and Cyclic Properties of Clay Subgrade Stabilised With Rice Husk Ash and Portland Slag Cement PDF
Static and Cyclic Properties of Clay Subgrade Stabilised With Rice Husk Ash and Portland Slag Cement PDF
To cite this article: Argaw Asha Ashango & Nihar Ranjan Patra (2014) Static and cyclic properties
of clay subgrade stabilised with rice husk ash and Portland slag cement, International Journal of
Pavement Engineering, 15:10, 906-916, DOI: 10.1080/10298436.2014.893323
Download by: [Universidad Del Norte] Date: 20 February 2017, At: 12:26
International Journal of Pavement Engineering, 2014
Vol. 15, No. 10, 906–916, http://dx.doi.org/10.1080/10298436.2014.893323
Static and cyclic properties of clay subgrade stabilised with rice husk ash
and Portland slag cement
Argaw Asha Ashango1 and Nihar Ranjan Patra*
Geotechnical Engineering Division, Department of Civil Engineering, IIT Kanpur, Kanpur 208016, India
(Received 3 July 2013; accepted 19 January 2014)
In the present study, clay soil collected from new Banda, Uttar Pradesh, India has been treated with rice husk ash (RHA)
and Portland slag cement (PSC). Based on unconfined compressive strength test results, the optimum mix obtained is of
82.5%Soil þ 7.5%PSC þ 10%RHA. The increase in strength of the optimum mix is about 29.8%, 37.2% and 48.55%
for a curing period of 7, 14 and 30 days, respectively. The soaked California bearing ratio (CBR) test gives about
91.75% higher values as compared to unsoaked CBR test for a curing period of 30 days. Strain-controlled cyclic
triaxial tests were conducted to study the variation of degradation index, shear modulus and damping ratio of the
optimum mix with number of cycles for strain amplitudes of 0.4%, 0.6%, 0.8% and 1% and for frequencies of 0.2 and
1 Hz at an effective confining pressure of 100 kPa. It is observed that the degradation index decreases at a fast rate for
the first 25 – 50 cycles. From the study, it is concluded that the aforementioned mix may be suitable for pavement
subgrade material.
Keywords: clay subgrade; rice husk ash; Portland slag cement; California bearing ratio; cyclic tests; degradation index
List of notations
1. Introduction
Expansive soils are found in the arid and semi-arid regions
AASHTO: American Association of State Highway and and formed due to poor drainage and hot climatic
Transportation Officials condition, and its colour varies from grey to deep black
ASTM: American Society for Testing and Materials and rarely reddish or yellowish and the thickness also
ASTM D: American Society for Testing and Materials varies from 30 cm to 15 m (Rao 2000). Twenty percent of
Designation the total land in India is covered by expansive soils and
CAH: calcium aluminates hydrate generally it is called black cotton soil (Rao 2000). In
CBR: California bearing ratio addition to India, this black cotton soil is available in many
CH: highly expansive clay soil parts of the world such as Africa, Australia, Ethiopia,
CSH: calcium silicate hydrate Israel, Jordan, the USA, and so on (Rao 2000). The annual
D: damping ratio damage to civil engineering structure due to this soil are
G: shear modulus estimated to be around billion dollars in the world and
Hz: Hertz particularly 1 billion dollars in the USA and 150 million
IS: Indian Standard dollars in the UK (Gourley et al. 1993, Sabat and
JCPDs: Joint Committee on Powder Diffraction Nanda 2011).
Standards Rice husk ash (RHA) is a waste material obtained from
MDD: maximum dry density controlled burning of rice husks at a temperature of 6008C
OMC: optimum moisture content (Della et al. 2002) and 20% of rice husk are ash. RHA is
PSC: Portland slag cement classified as a pozzolanic material [American Society for
RHA: rice husk ash Testing Materials (ASTM) C618 2012a], which is
UCS: unconfined compressive strength siliceous and aluminous by composition. This material is
UCSC: Unified Soil Classification System in bulk amount in major rice producing countries such as
XRD: X-ray diffraction India and China (Ramakrishna and Pradeep 2008) and its
XRF: X-ray fluorescence fineness and low density make it to fly over the air, which
d: degradation index contributes to environmental issues and in addition to that
g: strain amplitude storage has claimed for land proclamation (Rahman 1987).
Portland slag cement (PSC) is made by inter-grinding different strain amplitudes of 0.4%, 0.6%, 0.8% and 1% and
of high quality of clinker, slag and gypsum. Clinker used effective confining pressure of 100 kPa at a frequency of 0.2
for the production of slag cement contains highly reactive and 1 Hz. Based on static and cyclic test results on stabilised
tri-calcium silicates (3CaO·SiO2) that facilitate good clay, conclusions have been drawn for the material mix and
reactivity and strength development in the cement. its applicability for pavement subgrade.
Granulated blast furnace slag containing high glass
content (more than 90%) is obtained by rapid quenching
or chilling of molten slag generated from blast furnace 2. Experimental programme
during steel making. Gypsum (CaSO4·H2O) is added to the The experimental programme was divided into four parts.
clinker and slag to manufacture PSC and it should be in In the first part, the geotechnical properties of the soil, RHA
amounts such that the sulphur trioxide (SO3) in the cement and PSC were determined. In the second part, the optimum
produced does not exceed the limit of 3%. It is a mix for stabilisation of the soil sample was determined. In
cementitious material consisting of lime (CaO), silicon the third part, unsoaked and soaked CBR tests, unconfined
dioxide (SiO2), aluminum oxide (Al2O3) and magnesium compression test and durability tests were carried out. In the
oxide (MgO). The high amount of lime(CaO), 50.85%, fourth part, cyclic tests have been conducted to determine
present in PSC makes it a suitable binding material for degradation index, shear modulus and damping ratio of the
mixing it with silicon dioxide (SiO2) that exist in RHA. optimum mix. The detailed experimental programme of the
The PSC does not contain carbon and it does not cause present study is given in Table 1.
instability in the entrained air content.
Aubert et al. (2006) have reported that reusing the waste
material in environmentally friendly and economically 3. Materials
sustainable ways are important topics on which authorities The three materials are used in this study and explained in
and researchers are working on. Apart from this, the detail in the next section. The samples of each material are
demand of construction material and its cost increases day shown in Figure 1.
by day and this leads to scarcity of raw materials and
increase in price of energy. The improvement in strength of
the clay soil is due to the presence of cementitious materials 3.1 Soil sample
in soil –cement matrix (Stavridakis 2005, Kamruzzamn The soil (black cotton) used in the present study was
et al. 2006). The cementitious materials are formed by the collected from new Banda site, Uttar Pradesh, India. The
reaction between hydrated lime from cement and the silica geotechnical properties of the soil are shown in Table 2,
and alumina from RHA and clay minerals and that leads to and the particle size distribution is shown in Figure 2. The
formation of calcium silicate hydrate and calcium soil was classified as highly expansive soil according to
aluminates hydrate (Rahman et al. 2010). Unified Soil Classification System and A-7-6 according to
The heavy traffic loading, railway, earthquake, etc. can American Association of State Highway and Transpor-
affect the dynamic property of soils (Thammathiwat and tation Officials (AASHTO) classification system. The soil
Chim-oye 2004). This dynamic property of soils such as has approximately 98% particles passing U.S. No 200
shear modulus and damping ratio depends on the cyclic sieve. The silt and clay fractions are about 52% and 46%,
frequency and strain amplitude (Zhou and Gong 2001, respectively.
Jiang et al. 2010). The cyclic loading affects the
chemically mixed soils (Hoyos et al. 2004, Shafiee et al.
2004). Few cyclic triaxial test results of stabilised clay soil 3.2 Rice husk ash
have been reported by Ashango and Patra (2013). Clay soil Rice husk is milled at circulating fluidised bed boiler at
stabilised with RHA and PSC in terms of strength, 4708C temperature and Lancashire boiler at 6708C and
durability and California bearing ratio (CBR) are limited. collected from locally available resources. The chemical
In the present study, black cotton clay soil collected analysis has shown that the RHA consists of 81.9% SiO2,
from new Banda, Uttar Pradesh, India has been mixed with 0.9% Al2O3, 0.4% Fe2O3, 0.8% CaO, 0.5% MgO,0.4%
RHA and PSC to determine the optimum mix. The Na2O, 1.3% K2O, 0.1% MnO2, 4% C and 4% loss of
unconfined compressive strength (UCS) of the optimum ignition. The physical properties of RHA are shown in
mix has been carried out for different curing periods. The Table 3.
unsoaked and soaked CBR tests have been carried out for
the mixture for different curing periods. The durability test
is carried out for the optimum mix. Strain-controlled cyclic 3.3 Portland slag cement
triaxial tests have been conducted to study the variation of The PSC was collected from the locally available market
degradation index, d, shear modulus, G and damping ratio, (Gujarat, India). PSC is made by inter-grinding of high
D of the optimum mix of soil with number of cycles for quality clinker, slag and gypsum. It is a cementitious
908 A.A. Ashango and N.R. Patra
Mix proportion (%) Curing days Uncuried Curing days D/W days Strain amplitude (%) Strain amplitude (%)
100 0 0 X X
90 0 10 X X X X X X X X
92.5 2.5 5 X
87.5 2.5 10 X X X X X
82.5 2.5 15 X
77.5 2.5 20 X
90 5 5 X
85 5 10 X X X X X X
80 5 15 X
75 5 20 X
87.5 7.5 5 X
82.5 7.5 10 X X X X X X X X X X X X X X X X X
77.5 7.5 15 X
72.5 7.5 20 X
Note: X, test conducted; D/W, drying and wetting.
Values
Soil properties Clay Optimum mix
Grain size distribution
Gravel (. 4.75 mm) 0 0
Sand (4.75 to 0.075 mm) 2 0.7
Silt (0.075 to 0.002 mm) 52 98.05
Clay (, 0.002 mm) 46 1.25
Specific gravity 2.69 2.47
Atterberg limit
Liquid limit (%) 53 51.5
Plastic limit (%) 20 41.28
Plasticity index (%) 33 10.22
Shrinkage limit (%) 11 46.32
Proctor compaction
MDD (kN/m3) 16.12 14.79
OMC (%) 22 25.25
Compressive strength (kN/m2) 193 835
CBR (%)
Unsoaked 8.27 15.8 Figure 2. Particle size distribution of the clay soil and optimum
mix (82.5%Soil þ 7.5%PSC þ 10%RHA).
International Journal of Pavement Engineering 909
Table 3. Physical properties of RHA. completes the wetting and drying for one cycle. The
same procedure was repeated for 12 cycles. The sample
Property Value
that existed for 12 cycles was tested for UCS test in
Colour Black grey accordance with ASTM 559.
Bulk density 3.2 kN/m3
Moisture 1.6%
Specific gravity 2.308 4.2 X-ray diffraction analysis
PH 8.4
X-ray diffraction (XRD) analysis was carried out for clay
soil, RHA, optimum mix after static test and optimum mix
material that consists of lime (CaO), silicon dioxide after cyclic test using SIETRONICS XRD SCAN
(SiO2), aluminum oxide (Al2O3) and magnesium oxide instrument. XRD patterns were obtained using a Cu, Ka
(MgO). X-ray fluorescence was carried out by ZFX Primus (l ¼ 1.541841 Å) with continuous scan mode over a range
II RIGAKU machine with 36.58C internal temperature and of 5– 7082u with a 0.028 step and a 2 s per step count time.
3 kV power for the PSC to find the oxide contents. The The analysis was performed by comparing or matching the
chemical analysis shows that the PSC consists of 50.8% Joint Committee on Powder Diffraction Standards data
CaO, 27.7% SiO2, 11.2% Al2O3, 2.9% Fe2O3, 2.8% SO3, and the scanned XRD data for different minerals such as
2.5% MgO, 0.6% Na2O and 0.5% K2O. The high amount montmorillonite, kaolinite, illite, quartz, feldspar and
of lime (CaO) in PSC reflects it as a binder material. calcite. The minerals contents in samples of clay soil,
RHA, optimum mix after static test and optimum mix after
cyclic test are shown in Figures 3– 6, respectively.
4. Testing procedures
4.1 Static tests 4.3 Cyclic tests
The geotechnical laboratory tests were carried out on clay The optimum mix samples (Soil-PSC-RHA) were
soil for the classification of the expansive soil. The RHA prepared having 50 mm diameter and 100 mm height
varies from 5% to 20% with increment of 5% and the PSC mould and compacted with 98% of MDD. Strain-
varies from 2.5% to 7.5% with increment of 2.5% of dry controlled cyclic triaxial test was conducted in accordance
unit soil which were mixed thoroughly and kept for with ASTM 3999 up to 300 number of cycles with
10 min. The maximum dry density (MDD) and the different strain amplitudes of g ¼ 0.4%, 0.6%, 0.8% and
optimum moisture content (OMC) for various mixtures 1%, frequency of 0.2 and 1 Hz at an effective confine
were determined by standard proctor method in accord- pressure of 100 kPa.
ance with ASTM 698. UCS test was conducted on sample
having a dimension of 38 mm diameter and 76 mm height
prepared with their respective mix of MDD and OMC in 5. Test results and discussions
accordance with ASTM 2166 for three samples. The 5.1 XRD analysis
average of them was taken as the UCS value. This sample The XRD analyses are shown in Figures 3 – 6 for clay soil,
was tested after 0, 7, 14 and 30 days of curing in a room RHA, optimum mix after static test and optimum mix
maintained at 90 – 100% relative humidity and temperature
of 32– 358C with a strain rate 0.625 mm/min.
Test specimens were prepared at OMC with their
respective mix for CBR test in accordance with ASTM
1883. The CBR tests were conducted for unsoaked and
soaked conditions. The sample was soaked for 4 days after
cured in a room maintained at 90 –100% relative humidity
and temperature of 32 –358C for 0, 7, 14 and 30 days.
Then, the sample was tested at a strain rate of 1.25 mm/
min. The durability test was conducted for three samples
prepared for UCS tests in two steps: wetting and drying.
In the wetting case, the samples after 7 days of curing were
immersed in water for 5 h. Then, their weight and height
were recorded. In the drying case, the samples were dried
after 5 h of immersion in water. Then, their weight and
height were measured. These samples were oven-dried for Figure 3. XRD of clay soil sample. 1, illite (Al2Si3(OH)2); 2,
42 h at a temperature of 808C and were cooled for 1 h. kaolinite (Al2Si2O5 (OH)4); 3, montmorillonite (Al2O34SiO2·H2O);
Then their weight and height were measured. This 4, quartz; 5, calcite (CaCO3).
910 A.A. Ashango and N.R. Patra
Figure 4. XRD of RHA sample. 1, montorillonite Figure 6. XRD of optimum mix (82.5%Soil þ 7.5%
(Al2O34SiO2·H2O); 2, kaolinite (Al2Si2O5(OH)4); 3, illite PSC þ 10%RHA) sample after cyclic triaxial test. 1, illite
(Al2Si3(OH)2); 4, quartz; 5, calcite (CaCO3). (Al2Si3 (OH)2); 2, kaolinite (Al2Si2O5 (OH)4); 3, montmorillonite
(Al2O34SiO2·H2O); 4, quartz; 5, calcite (CaCO3).
Figure 16. Variation of deviatoric stress with mean normal Figure 18. Variation of shear modulus with number of cycles
effective stress for optimum mix (0.2 Hz). for optimum mix (0.2 Hz).
914 A.A. Ashango and N.R. Patra
Figure 19. Variation of shear modulus with number of cycles Figure 21. Variation of damping ratio with number of cycles for
for optimum mix (1 Hz). optimum mix (1 Hz).
Figure 20. Variation of damping ratio with number of cycles for Figure 23. Variation of degradation index with number of
optimum mix (0.2 Hz). cycles for optimum mix (1 Hz).
International Journal of Pavement Engineering 915
secant modulus in the Nth cycle to secant modulus in the The degradation index decreases at a fast rate for
first cycle. first 25– 50 cycles and then it is almost constant or
The degradation index decreases at a fast rate for first the decrease is negligible. The percentage
25 –50 cycles and then it is almost constant or the decrease decrease in degradation index is about 33% for
is negligible. The degradation index decreases from 1% to strain amplitude varying from 0.4% to 1% at
0.51%, 1% to 0.47%, 1% to 0.37% and 1% to 0.34% with 0.2 Hz frequency.
increase in the number of cycle at strain amplitudes of (4) Based on dry density, strength, durability and CBR
0.4%, 0.6%, 0.8% and 1%, respectively, at a frequency of values, the stabilised subgrade material is suitable
0.2 Hz. In the same way, the degradation index decreases for subgrade of flexible pavement.
from 1% to 0.26%, 1% to 0.25% and 1% to 0.24% with
increase in the number of cycles at strain amplitudes of
0.4%, 0.8% and 1%, respectively, at a frequency of 1 Hz.
The percentage decrease in degradation index is about Note
33% and 7.7% for strain amplitude varying from 0.4% to 1. Email: argaw97@gmail.com
1% at a frequency of 0.2 and 1 Hz, respectively.
6. Conclusions References
Based on the study, the following conclusions are drawn:
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