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<0 C150/C150M - 18
TABLE 2 Optional Composition Requirements A
Cement Type Applicable Test I and IA II and IIA II{MH) and III and IV V Remarks
Method !I(MH1A li lA
Tricalcium aluminate {CSA)B, max, % See Annex AI 8 fo r moderate sulfate resistance
Tricalcium aluminate {C 3A)B , max, % See Annex AI 5 for high sulfate resistance
Equivalent alkalies (Na 2 0 + O.658K 2 0), max, % C114 D.BOc D.BOc 0.60 e O.BOc low-alkali cement
A These optional requirements apply on ly when specifically requested. Verify availabil ity before ordering. See Note 2.
B See Annex AI for calculation.
CSpecify this limit when the cement is to be used in concrete with aggregates that are potentially reactive and no other provisions have been made 10 protect the concrete
from deleteriously reactive aggregates. Refer to Specification C33 for information on potential reactivity of aggregates.
Au toclave expansion, max,% C15t 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80 0.80
report the amount used, expressed as a percentage of cement amounts used or greater and the total amount of organic
mass, along with the oxide composiLion of the processing processing add itions used shall not exceed 1.0 % by mass of
addition. See Note 4 . cement.
5.1.6 Air-entra ining addilion (for air-entraining portland
NOTE 4--These requirements are based on dam and recommendations
by Taylor. 3 cement on)y). The interground addition shall conform to the
requirements of Specification C226.
5.1.5 Organic Processing additions. They shall have been
shown to meet the requirements of Specificati on C465 in the ~. Chemical Composition
6.1 Portland cement of each of lhe ten types shown in
.l Taylor, P. , "Specifications and Protocols ror Acceptance Tests on Processing
Section 1 shall conform to the respective standard chemical
Additions in Cement Manufacturing." NCHRP Report 607, Transponation Research requiremen ts prescribed in Table 1. In addition, optional
3 Board, Washington. DC 20008, 96 pp. Available at www.trb .org. chemical requirements are shown in Table 2.
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• C150/C150M - 18
TABLE 4 Optional Physical Aequirements A
A pplicable
Cement Type
Test Method
I and II IA and IIA II[MHI II(MHIA II I iliA IV v
False sel, final pen etration , min, % C451 50 50 50 50 50 50 50 50
Heat of hydration:
Isothermal Cond uction Calorimetry:
3 days, max , kJlkg [caVgj C1702 255 (GOjS 255 [60]8 200 [50f
7 days, max, kJ/l<g [caVgJ 225 [55jC
Strength, not less than the values shown:
Compressive stre ngth , MPa {psi] Cl09/CI09M
28 days 28.0 22.0 28.0 22.0
[_01 [31901 [40601 131901
22.0B 18.0 B
NOTE 5-The li mi t on the sum. C)S + 4.75C3A, in Table I provi des 9. 1.9 Sulfate Resistance-Test M ethod C452 (sul fate expan-
contro l on the heal of hydration of the cement and is consistent with a T est sion).
Method C 1702 th ree~d ay heat of hydration limi t of 3J:i kJlkg [75 calls].
NOTE 6-Thcre are cases w her e performance of a cement is improved
9. 1.10 Time of Setting by Gillmore Needles- Test MeulOd
with SO) in excess of the Table I li mits in this specificati on . G uide C563 C266.
i s one o f several m ethods a manufacturer can use to evaluate the effect of 9. 1.11 Fineness by Turbidime ter·-Test Method C 115.
sulfate content on cement c haracteri stics. Whenever SO) content of a 9. J.12 Calcium Sulfate (Expansion of ) Mortar-Test
cement exceeds Tabl e 1 limits, Test Method C 1038 results provide Method C I 038.
evidence thm excessive ex pansion does nOl occur at lhis higher sul fate
con len t. 10. Inspection
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• C150/C150M -18
. air-entraining addition and of any processing addition used, an air-entraining lype, the words "air-entraining" shall be
and also, if requested, shall supply test data show ing compli- plain ly marked on each package. Similar information shall he
ance of such air-entraining addition with Specification C226 provided in the shipping documents accompanying the ship-
and of such processing additio n with Specification C465 , ment of packaged or bu lk cement. All packages shall be in
12.2 When iimeslOne is used, the manufacturer shall siale in good cond ition at the time of inspection.
writing the amou nt thereof and, if requested by the purchaser, Non; 9-Wi th the ch ange to SI units, it is desirable to establi sh a
shall supply comparative test data on chemical and physical standard Sf package for portland cem(!nts. To that end 42 kg [92.6 lb]
properties of the cernent with and without the lim esto ne (see provides a convenient, even-numbered mass reasonably similar lO the
trad itional 94-l b [42 .6-kg] package.
Note 7). The comparative tes ts do not supersede the normal
testing to confirm that the cement meets chemi cal and physical 14, Storage
requirements of this standard. The amount of limt!stone in
cement shall be determined in accordance with Annex A2. 14.1 The cement shall be slored in such a manner as to
permit easy access for proper inspection and identification of
NOTE 7-Comparative test data may be from qualification lests per- eac h shipment, and in a suitable weather-tight building that
formed by the manufacturer during formula tion of the cement wi th
will protcct the cement from dampness and minimize ware-
limestone.
house sel.
12.3 At the request of the purchaser, the manufacturer shall
report the chl oride content as determined using Test Methods 15. Manufacturer's Certification
C 11 4 , in percent by mass of the cement, in the manufacturer's
15. 1 U pon request of the purchaser in the contract or order,
report (see Note 8).
a manufacturer's report shall be furnished at the time of
Nan; &-Chlo rides in concrete come from multiple ingredients and shipment stati ng the resulLS of tesL') made on samp les of the
cement chloride content may be required to estimate concrete chloride material taken during production or transfer and certifying that
content. Requirements for concrete ch lOii de content are provided in
building codes and other documents.
lhe cement co nforms to applicable requirements of thi s speci-
fication.
13, Packaging and Package Marking
NmE I O-Ouidance on preparing the manufac turer's report is provided
13 .1 When the cement is de livered in packages, the words in Appendix X I.
"Portland Cement," the type of cement, the name and brand of
the manufacturer, and the mass of the cement contained therein 16, Keywords
shall be plainly marked on eac h package. W he n the cement is 16.1 h ydraulic cement; portland cement; specification
ANNEXES
(Mandatory Information)
AI.I All values calculated as described in this annex shall within the precision of the analytical methods, even when the methods are
be rounded according to Practice E29 . When evaluating properly qualilied under the requirements of Test Methods C114.
confOimance to a specification, round va lues to the same A 1.3 When the rati o 01' percentages of aluminu m oxide to
number of places as the corresponding table entry before ferric oxide is 0.64 o r more, the percentages of tricalcium
making compari sons. The expressi ng of chemical limitations silicate, dicalcium sili cate, tricalciu m aluminate, and letracal-
by means of calculated assumed phases does not necessarily cium alumino ferrite shall be calculated from the chemical
mean that the oxides arc actually or entirely present as such analysis as follows:
phases. Tricalcium silicate (CaS) ,. (4.071 x % CaD) - (7.600 x % Si0 2 )
- (6.718 x % AI 2 0 a) - (1.430 x % Fe~P3) - (2.852 x % 503 )
A 1.2 When expressing phases, C; CaO, S; SiO"
(A l. 1)
A; AI,O" F; Fe,O,. For example, C,A; 3CaO-AI,o,. Ti-
Dicalclum silicate (C 2 S) '" (2.867 x % Si0 2 ) - (O.7544 x % C 3 S)
tanium dioxide and phosphoru s pentoxide (TiO, and P,O,)
shall not be included with the AI,O, contenl. See Note AL I. (A 1.2)
NOTE A I. I-When comparing oxide analyses and calcu lated phases Tricalcium aluminate (C 3A) '" (2.650 x % A1 2 0 3) - (1.692 x % Fe 2 D 3 )
from di fferent sources or from differen t historic times, be aware that they (A 1.3)
may not have been reported on exactly the same basis. Chemical data
Tetracalcium aluminoferrite (C 4 AF) '" 3.043 )( % Fe 2 0 3
obtained by Reference and Alternale Test Methods of Test Methods C 114
(wet chemistry) may include titania and phosphorus as alumina unless (A l. 4)
proper correction has been made (see Test Methods C 114), while data
obtained by rapid instrumental methods usually do not. T his can result in AIJ.l When the alumina-ferric oxide ratio is less than 0.64,
small dilf(!renccs in the calcu lated phases. Such di llcrences are usually a calcium aluminoferri lc so lid solu tion (ex pressed as
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• C150/C150M - 18
. ss(C,AF + C2F» is formed. No tricalcium aluminate will be L the percentage by mass of limestone ,
present in cements o f thi s composi t ion. Dicalcium silicate shall P ;; the percentage by mass of inorgani c processing
be calculated as in Eq A 1.2. Conlents of this so lid solution and addition, and
of tricalcium silicate shall be calculated by the fo llowing Xf = the percentage by mass of C, S, C, S, C, A , or C.AF in
fonnulas: the fini shed cement.
ss(C4AF + C2F) :;= (2,100 x % A1 20 3) + (1.702 x % Fe203)
The adj us ted va lues for the fini shed cement sha ll be reported
(A I .5) on the manufac turer's report.
Tricalcium silicate (e 3 s) = (4.071 x % CaO) - (7.600 x % Si0 2 )
- (4.479 x % A1 20 3) - (2.859 x % Fe203) - (2.B52 x % S03)
NmE Al.2-Where the ox ide analysis of the fini shed cement, the
(A 1.6 ) limestone, and inorganic processing addition , are known along with the
mass percentage of limestone (L) an d m ass percentage of inorgan ic
AlA If no limestone or inorganic processing additions are processing addilion (P) , o ne method of determi ning the base cement oxide
used in the cement, or in the absence of information on composition is to use the following equati on:
limesto ne or inorganic processing additions use in the cemen t,
phases shall be calculated osing procedures in Eq A l.l-A 1.6
without adjustment. where:
A 1.5 In absence of infonna tion on limes tone or inorganic Oh lhe b ase cemen t ox ide content (% by mass of base cement) ,
Of the fini shed cement ox ide content (% by mass of fi nished
processing additions content, results shall note that no adjust- cement),
ment has been made for possibl e use of limestone or inorganic OJ the li mestone oxide conten! (% by mass of limestone), and
processing addition s. Op the inorganic processing addition oxide content (% by mass of
inorganic processing addition).
A I. 6 When inorgan ic processing additions or limes tone or T he base cement phase composition can be determi ned using these
both are used with the base ceme nt (portland ceme nt clinker values of oxide unalyses in equations &t A I.I -AI.6 . Eq A L7 is uscd to
an d any added calciu m sulfate). the contents of C,S, C 2S, C, A, calculate the adjusted phase composition.
and C.AF, shall be adjusted as fo llows: NaTE A l .3-F or ex ample:
Where the cement inc ludes 3.5 % limestone and 3.0 % of an inorganic
A1.6.1 The percentage of C 3 S, C 2S, C, A , and C.AF in the processing addition and the base cement has 60 % C 3S, 15 % C 1S, 7 %
base cement (see Note A1.2) shall be determ ined based on C)A, and 10 % C4 AF, the adju sted phase composition is:
chemi cal analyses using methods in Test M ethods C I1 4 and
60 X (100 - 3.5 -- 3.0)
using Eq AI.l-A I. 6 as appropriate. The con tenls of each of C,Sf = 100 ~ 56 %
these phases shall be adjusted to account for the use of
limes to ne or in organic process ing additions as follows: 15 X (100 - 3.5 -- 3.0)
C,Sf = 100 ~ 14%
A2. 1 When limestone is u sed, the limestone content in Non; A2.1-For example:
portland cement shall be deri ved from the determination of Where the determined CO 2 content in [he fin ish ed cem ent = 1.5 % and
the CO 2 content of the limeston e = 43 % (CaC0 3 in limestone ;; 98 %)
CO, in the fin ished cement. Analysis of CO2 shall be based on
Then:
methods described in Test Methods C l1 4. The percent lime-
stone in the cement is calculated from the CO 2 analysis based 1.5
43 x 100 = 3.5 % limestone conl en t in cem em
on the CO2 con tent of the limestone used.
The manufac turer shall include the CO 2 content and calcu -
A2.2 This specification requires that the limestone to be
lated limestone content of the cement on the Mill Test Report.
used musr contain a minimum of 70 % CaC03 . The manufac-
Th e limestone con tent of the cement is calcul ated as fo llows:
turer shall include the CaC03 content of the limestone on the
% CO 2 in me cemenl . . manufacturer's report. Calculate the CaCO:l content of the
% CO in the limestone X 100 = % hmestone 1ft cem ent limestone as foll ows: % CaCO, = 2.274 x % CO2 .
2
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• C150/C150M -18
NOTE A2.2-For verification of limestone conte nt of cement, the
purchaser must analyze for CO 2 content and make a cOlTeclion for the
content of CueD} in the limestone in order for the data to be comparable
to the manufacturer's report.
APPENDIX
(Nonmandatory Information)
X I . I To pro vide uniformity for reporting the resu lts of tests mall y performed on cemcnts meeting Specification el sa.
perfo rmed on cemen ts under thi s specification , as required by Purchaser reporting req uirements shou ld govern if different
Section I S of Specification elsa en ti tled "Manufactu rer's from norm al reponing by the ma.nufacturer or fro m those
Certi fi cation," an example Mill Test Report is shown in Fig. recommended here.
XI.I.
X I.S Cemen ts may be shi pped prior to later-age tcst data
X 1. 2 The identity information given shou ld unambiguously being available. In such cases, the test value may be len blank.
identify the cement production represented by the Mill Test Alternati vely, the manufacturer can generally provide esti-
Report and may vary depending upon the man ufacture r's mates based on hi storical productio n data. The report should
designation and purchaser's requirements. indicate if such esti mates arc provided.
XI. 3 The Manufacturer' s Certification statement may vary
depending upon the manufacturer's procureme nt order, or legal X 1.6 In re porting limits fro m the tables in Specificati on
requi rements, but should certify that the cement shipped is CIS0 o n the Mill Test Report, onl y those limits speci fically
represented by the certificate and that the cement' conforms to app li cable should be listed. In so me cases, Specification eISO
appli cable requirement" of the specification at the time it was table limits are superceded by other provisions.
tested (or retested) or shipped.
XI.? When limestone or inorganic processing auditions or
X 1.4 The sample Mill Test Report has heen developed to both arc used in the cement, additional data are reported by the
refl ect the chemical and phys ical requirements of this specifi- manufac rurer. An exampl e addilional data report is shown in
cation and recommends reporting all analyses and tests nor- Fig. X1.2.
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dOli., C150/C150M - 18
'W
ABC Portland Cement Company
Qualitytown, N.J.
STANDARD REQUIREMENTS
ASTM C1S0 Tables 1 and 3
CHEMICAL PHYSICAL
Item Spec. Test Item Spec. Test
Limit Result Limit Result
A
5iO:<. (%) 20.6 Air content of mortar (volume "!o) 12 max 8
AI,203 (%) 6.0 max 4.4 Blaine fineness (m2/kg) 260 min 377
Fe 2 0 3 (%) 6.0 max 3.3 430 max
A 0.80 max 0.04
CaO{%) 62.9 Autoclave expansion ("!o)
MgO{%) 6.0 max 2.2 Compressive strength (MPa) min:
A
50 3 (%) 3.0 max 3.2 1 day
Ignition loss ("!o) 3.5 max 2.7 3 days 7.0 23.4
A 12.0 29.8
Na,20(%) 0.19 7 days
A A
K:<.O (%) 0.50 28 days
Insoluble residue (%) 1.5 max 0.27 Time of setting (minutes) (Vicat)
A Initial Not less than 45 124
CO 2 {''Io) 1.2
limestone (%) 5.0 max 3.5 Not more than 375
CaC0 3 in limestone ("!o) 70 min 79 Heat of hydration (kJ/kg) (ASTM C1702)
B
Inorganic processing addition 3 days 245
(ground. granulated blastfurnace slag) 5.0 max 3.0 Test Method C1038 Mortar Bar Expansion (%) o O.010 E
Potential phase composition (%)C
A
C,S 59
A 10
C,S
C,A 8 max 5
A
C4 AF 10
C4 AF + 2(C 3A) 20
CaS + 4.75C aA 100 max 83
A Not applicable.
B Test result represents most recent value and is provided for information only.
C Adjusted per A1.6 .
o Required only if percent 80 3 exceeds Ihe limit in Table 1 , in which case the Test Method C1038 expansion shall not exceed 0.020 % at 14 days.
E Test result for this production period not available. Most recent test result provided.
OPTIONAL REQUIREMENTS
ASTM C150 Tables 2 and 4
CHEMtCAL PHYSICAL
Item Spec. Test lIem Spec. Test
FUmit not specified by purchaser. Test result provided for information only.
arest result for this production period not yet available.
We certify that the above described cement, at the time of shipment, meets the chemical and
physical requirements of the ASTM Cl 50 - XX or (other) specification.
Signature' _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ __ Title: _ __ _ _ _ _ _ _ _ __ _ _ __
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• C150/C150M - 18
ABC Portland Cement Company
Qua!i\ylown, N.J.
Plant: Example Cement~ Dale: March 9 20xx
Additional Data
We certify Ihallhe above described data represents the materials used in the cement manufactured during the production period indicated.
Signature: _ _ _ _ __ _ _ _ _ __ _ __ __ Tille: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ __
SUMMARY OF CHANGES
Committee COl has identified the location of selected changes to this standard since the last issue
(C I50/C150M - 17) that may impact the usc of this standard. (Approved Apri l I, 20 18.)
(I) Removed references to Test Method C 186 throughout. (3) Revised 12.3 and Note 8.
(2) Revised Table 4.
Committee CO 1 has identified the location of selected changes to this standard since the last issue
(C150/Cl 50M - 16") that may impact the use of this standard. (Approved April I, 2017.)
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