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Laboratory Evaluation of Workability and Moisture Susceptibility of Warm-Mix Asphalt Mixtures Containing Recycled Asphalt Pavements
Laboratory Evaluation of Workability and Moisture Susceptibility of Warm-Mix Asphalt Mixtures Containing Recycled Asphalt Pavements
Abstract: Warm mix asphalt (WMA) and recycled asphalt pavements (RAP) are two popularly used sustainable technologies in pavement
industry. Because RAP materials contain aged binder, its use is limited to a certain percentage in hot mix asphalt (HMA) as it may affect the
workability and, fatigue and thermal cracking performance. Higher percentages of RAP can be incorporated into HMA with softer asphalt
binder or in combination with softening agent. However, the combination of WMA and RAP may allow for greater percentages of RAP
without modifying the original HMA job mix formula. The objective of this study was to explore the use of higher percentage of RAP, using
two different WMA technologies—Evotherm additive and foamed asphalt—to study the workability and moisture sensitivity of WMA-RAP
asphalt mixtures. The study found that the use of WMA technologies can eliminate the need for a softer grade binder in high RAP mixtures.
DOI: 10.1061/(ASCE)MT.1943-5533.0001825. © 2016 American Society of Civil Engineers.
Author keywords: Warm mix asphalt; Reclaimed asphalt pavement (RAP); Tensile strength ratio (TSR); Moisture susceptibility;
Workability.
two WMA technologies (use of Evotherm and foamed asphalt) HMA and WMA mixtures. For 40% RAP mixtures, PG 58-28
containing different RAP contents, in comparison to a control binder was used in addition to PG 64-22 to investigate the possibil-
HMA mixture. Additionally, the effectiveness of Evotherm as ity of eliminating the need for using a softer grade binder when
an antistrip additive was also evaluated. Three different RAP WMA technology is used. Ignition Oven tests were conducted
percentages—0, 20, and 40% were used. The specific research to determine the binder content and aggregate gradation for the
objectives of the study were to: (1) characterize and compare RAP material (AASHTO 2007, 2013a)
the mixtures based on workability using the % Gmm evolution
curves; (2) evaluate moisture susceptibility of the mixtures using Volumetric Properties of Various Mixtures Used
TSR test; and (3) assess effectiveness of Evotherm additive as an
antistrip additive using TSR test. Optimum design asphalt content was determined for the HMA
mixtures with 0, 20, and 40% RAP material. Superpave gyratory
compactor (SGC) was used to compact the mixtures to 65 gyrations
Materials Used and Sample Preparation Procedure (N design ) as per the 9.5B mixture specifications. The optimum as-
phalt contents for the HMA mixtures with 0, 20, and 40% RAP
Granite aggregate, PG 64-22 and PG 58-28 binders were used in
contents were used to prepare WMA samples and their volumetric
this study. Mixtures were designed for 9.5B (12.5 mm NMSA) sur-
properties were verified. The volumetric property requirements for
face course mix. RAP material for mixture was obtained from a
the WMA mixtures for all RAP percentages were satisfied when
single local source and stockpile to maintain uniformity. In addition
optimum asphalt content values, corresponding to that of HMA
to the aggregates, pond fines passing 75 μm sieve size at 1.5% by
mixtures were used to prepare the WMA mixtures. Optimum as-
weight of aggregates was also used. The aggregate gradation used
phalt contents were determined to be 6.0, 5.9, and 5.8%, respec-
is shown in Fig. 1. PG 58-28 binder was also used in addition to PG
tively for 0, 20, and 40% RAP content (for both PG 64-22; and
64-22 to check for the need of the use of a softer binder for WMA
PG 58-22 binder grade in case of 40% RAP use in mixtures).
mixtures when high RAP (40%) content was used. Three different
The volumetric properties of the mixtures are shown in Table 1
RAP contents—0, 20, and 40% were used in this study. An antistrip
and it may be noted that these properties are satisfied based on
additive, AD-here LOF 6500, was added to the binder at 0.75% by
Superpave mix design specification limits for all mixtures.
weight of binder.
Two WMA technologies were used in this study—
MeadWestvaco’s Evotherm 3G additive and The PTI Foamer Workability of Mixtures
device. The former is a chemical based and latter is water based
technology. Evotherm was added to the asphalt binder at a rate Following the NCAT (Leiva-Villacorta 2007), workability of the
of 0.5% by weight of total binder in the mixture. Two percent water mixtures was compared in terms of compactness of the mixtures.
100
90
80
70
Percent Passing
60
50
40
30
20
Control Points
10
Sieve Sizes
Fig. 1. Federal highway 0.45 power gradation chart showing aggregate gradation
NCHRP Report 691 proposed the use of number of gyrations re- Table 2. N92 Values for All Mixtures Used
quired to reach 92%Gmm , to evaluate workability of asphalt mix- Mixture technology
tures (Bonaquist 2011). Laboratory experiments (Hanz 2012;
RAP HMA EVO Foamer
Faheem and Bahia 2007); and field calibrations (Leiva-Villacorta
2007; Bonaquist 2011) have indicated that N92 (number of gyra- 0% 17 15 16
tions to 92 percent Gmm ) and compaction force index (CFI) are sen- 20% 18 17 16
40% PG 64-22 23 19 16
sitive to WMA additives and the compaction temperatures. It was 40% PG 58-28 16 20 18
also determined that the area under the curve from N ini to 92 per-
cent Gmm , can be used to rank the mixtures based on their work-
ability. In this study the N92 parameter was used to determine
workability. As per a recommendation in the draft appendix to Table 3. Percentage Change in N92 Values for Mixtures With Respect To
HMA Mix with 0% RAP
AASHTO R 35, WMA is more sensitive to compaction tempera-
ture than HMA if the increase in number of gyrations to 92% rel- Mixture technology
ative density (92%Gmm ) exceeds 25% when the compaction RAP HMA (%) EVO (%) Foamer (%)
temperature of WMA is decreased by 30°C (54°F) (AASHTO
0% Control −12 −6
2015). This measure was found to be sensitive to the compaction 20% 6 0 −6
temperature, the WMA process, and the presence of RAP in the 40% PG 64-22 35 12 −6
mixture (Bonaquist 2011; Hanz 2012). Hanz et al. have used this 40% PG 58-28 −6 18 6
as a limiting value in determining the WMA compaction temper-
ature during their proposed mix design process (Hanz 2012).
In this study, for all mixture specimens compacted, the develop-
ment %Gmm curves were determined as a function of number of Workability of Mixtures Compared with that of HMA
gyrations. For 40% RAP content, mixtures prepared with both PG Mixture with 0% RAP (Control Mixture)
64-22 and PG 58-28 were compared. The effect of changing RAP The N92 value of the HMA mixture with 0% RAP was considered
content and mix production technology on compactness was also as the control value. The N92 values and the percentage change in
determined. The number of gyrations to reach 92% Gmm , N92, was N92 values of the mixtures with respect to the control HMA mix
determined for all the mixtures. An average N92 value of three with 0% RAP are shown in Tables 2 and 3. Fig. 2 shows graphical
specimens was used for compactness comparison for each mixture. representation of the N92 values for all the mixtures. From Table 3
Increase in N92 value for a mixture suggests a decrease in work- it is observed that only the HMA mixture with 40% RAP and PG
ability of the mixture. 64-22 binder exceeds the 25% limit on the increase in N92 values
The N92 values of all mixtures were compared with that of compared with HMA mixture with 0% RAP.
an HMA mixture with 0% RAP (control mixture); the effect Therefore, it is concluded that workability of the HMA mixture
of RAP content on workability was studied; and the effect of mix- with 40% RAP and PG 64-22 binder is much lower than the work-
ture technology on workability for different RAP contents was ability of the HMA mixture with 0% RAP. This observation also
evaluated. validates the fact that most agencies require using a softer binder
Decreasing Workability
22
N92
18
14
10
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Mix Type
when high RAP contents are used. It is also observed that when WMA mix from that of the HMA mix was calculated for each
WMA technologies are used, it is not necessary to use a softer RAP content. For 40% RAP mixtures, the HMA mixture with
binder (change in binder grade). PG 64-22 binder was designed as control, i.e., the percentage
change in N92 values of WMA mix with PG 64-22 binder and
Effect of RAP Content on Workability PG 58-28 binder, and HMA mix with PG 58-28 binder was calcu-
lated with respect to the HMA mix with 40% RAP and PG 64-22
To measure the effect of RAP content on workability, the percent- binder. Figs. 4(a–c) show the workability for different mixture tech-
age change in the N92 value with increase in RAP content as nologies for each RAP content used. Table 5 shows the percentage
compared with the respective 0% RAP mixture was calculated change in N92 values attributable to different mixture technologies
for all three mixture technologies. The %Gmm evolution curves used for different RAP contents.
for HMA and WMA mixtures with different RAP contents are For all three RAP contents, the workability of mixtures in-
shown in Figs. 3(a–c). Table 4 shows the percentage change in creased when WMA technology was used. For 40% RAP mixtures
N92 values with increase in RAP content with respect to the respec- with PG 64-22 binder, the Foamer mixture has much higher work-
tive 0% RAP mixture. ability compared with the HMA mixture. HMA, Evotherm and
From Table 4, it is evident that the increase in RAP content has Foamer mixtures with 40% RAP and PG 58-28 all have better
very little effect on the workability of foamed mixture. However, workability than the HMA mix with 40% RAP and PG 64-22
the increase in RAP content in HMA reduces the workability. For binder.
HMA mixtures, when 40% RAP is added and the same binder In conclusion, the use of WMA technology increases the work-
grade is used, the workability is much lower based on the criteria ability of mixtures compared with the HMA mixture for all RAP
given in the draft appendix of AASHTO R 35. This decrease in contents for the same design binder grade.
workability can be overcome by using a softer grade binder, PG
58-28, which increases the workability of the HMA mixture with
40% RAP. Similarly, the addition of RAP decreases the workability Moisture Susceptibility
for Evotherm mixtures. From Table 4 for Evotherm mixtures, when
40% RAP is added and the same binder grade is used, the increase Modified AASHTO T 283 (AASHTO 2014), “Standard method
in N92 values is more than 25%. Using a softer binder grade does of test for resistance of compacted hot mix asphalt (HMA) to
not help improve the workability as seen in Table 4. However, the moisture-induced damage” as followed by the North Carolina
decrease in workability of Evotherm mixture with 40% RAP with Department of Transportation (NCDOT) was used to evaluate
respect to the control HMA mixture with 0% RAP is within the the mixtures’ moisture susceptibility using the tensile strength ratio
25% limit (12%) as shown previously. (TSR). TSR tests were conducted to evaluate moisture susceptibil-
In conclusion, the workability of HMA and Evotherm mixtures ity of asphalt mixtures with varying RAP content, and produced
decreases noticeably with increase in amount of RAP used. How- using the WMA technologies used in this study. For all mixtures,
ever, increase in RAP content has little effect on workability of a liquid antistrip additive LOF 6500, in the amount of 0.75%
foamed mixtures. Use of softer binder grade increases workability by weight of total binder was used, including the mixture with
in HMA mixture when 40% RAP was used, but it had less effect on Evotherm WMA additive.
the workability of Evotherm and foamed mixtures with 40% RAP. The TSR test specimens were prepared as per the standard spec-
ifications and were compacted to a target air void content of
7 0.5% with specimen dimension of 150 mm diameter and
Effect of Mixture Technology on Workability for
95 5 mm height using the Superpave gyratory compactor. The
Different RAP Contents
specimens were prepared using the same aggregate gradation that
To evaluate the effect of mixture technology on workability for dif- was used for mix design, and the optimum asphalt content deter-
ferent RAP contents, the percentage change in N92 values of a mined during the Superpave mix design are presented in Table 1.
% Gmm
H40R PG 58-22
92.0
90.0
88.0
N initial = 7 N design = 65
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86.0
1 10 100
98.0
E0R PG 64-22
96.0 E20R PG 64-22
E40R PG 64-22
94.0
E40R PG 58-22
% Gmm
92.0
90.0
88.0
N initial = 7 N design = 65
86.0
1 10 100
(b) No. of Gyrations
98.0
F40R PG 58-22
96.0 F40R PG 64-22
F20R PG 64-22
94.0
% Gmm
F0R PG 64-22
92.0
90.0
88.0
N initial = 7 N design = 65
86.0
1 10 100
Fig. 3. %Gmm evolution curves for HMA, Evotherm and Foamer mixtures with different RAP contents: (a) HMA; (b) Evotherm; (c) Foamer
Table 4. Percentage Change in N92 Values with Increase in RAP (163°C for HMA and 136°C for WMA). The specimens were
Content as Compared with the Respective 0% RAP Mixture for All then cooled for 2 h and cured at 60°C (140°F) for 16 h. After
Three Mixture Technologies curing, the mixtures were heated for 2 h to their respective
Mixture 40% RAP w/ 40% RAP w/ compaction temperatures (149°C for HMA and 120°C for WMA)
technology 20% RAP PG 64-22 binder PG 58-28 binder and then compacted to a height of 95 5 mm using the Superpave
HMA 6 35 −6 gyratory compactor.
EVO 13 27 33 The unconditioned specimens were tested at room temperature,
FOAM 0 0 13 i.e., 25°C (77°F). The saturated specimens were moisture
conditioned before testing as per the modified AASHTO T283
(AASHTO 2014) procedure according to the NCDOT specifica-
For WMA mixtures that used Evotherm, 0.5% dosage by weight of tions. After the conditioning, they were cooled for 2 h in a water
binder content was used. bath at 25°C (77°F). The specimens were then tested for their indi-
In accordance with AASHTO T283 (AASHTO 2014), the loose rect tensile strength (ITS) values. The tensile strength ratio (TSR)
mixtures were prepared at their respective mixing temperatures was determined for all mixtures as a percentage of the conditioned
% Gmm
92.00
90.00
88.00
N initial = 7 N design = 65
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86.00
1 10 100
(a) No. of Gyrations
98.00
H20R PG 64-22
96.00 E20R PG 64-22
92.00
90.00
88.00
N initial = 7 N design = 65
86.00
1 10 100
(b) No. of Gyrations
98
H40R PG 64-22
96 E40R PG 64-22
94 F40R PG 64-22
% Gmm
H40R PG 58-28
92
E40R PG 58-28
90
F40R PG 58-28
88
N initial = 7 N design = 65
86
1 10 100
(c) No. of Gyrations
Fig. 4. %Gmm evolution curves for 0, 20, and 40% RAP mixtures: (a) 0% RAP; (b) 20% RAP; (c) 40% RAP
Table 5. Percentage Change in N92 Values Attributable to Different It is observed from Table 7 that (1) generally, with a couple of
Mixture Technologies for Different RAP Technologies exceptions, the addition of RAP materials increases the ITS in both
Mixtures 0% RAP (%) 20% RAP (%) 40% RAP (%) conditioned and unconditioned state; that is expected because RAP
materials contain harder asphalt (oxidized); (2) in general, the TSR
Evotherm with PG 64-22 −12 −6 −17
Foamer with PG 64-22 −6 −11 −30
ratio decreases with increasing RAP content; and (3) except for
HMA with PG 58-28 — — −30 Foamed mixtures with 40% RAP, all mixtures pass the NCDOT
Evotherm with PG 58-28 — — −13 acceptance criterion of 85% retained TSR. It is noted that all mix-
Foamer with PG 58-28 — — −22 tures contain an LOF 6500 antistrip additive. It is interesting to note
that Evotherm WMA with 40% RAP material barely meets the 85%
acceptance criterion even though in addition to the mix containing
Evotherm, which can also act as an antistrip agent, and LOF 6500
to unconditioned ITS ratio. The required minimum passing ratio by antistrip additive. A previous NCDOT study using similar base ma-
NCDOT is 85%. A summary of the number of specimens tested for terials noted that doubling the amount of antistrip additive from
each mixture in the TSR test is given in Table 6. The results of the 0.75% did not improve the performance of virgin WMA (Malladi
TSR tests for all mixtures are presented in Table 7. et al. 2015). Therefore, samples with an additional amount more
One anomaly in the results is that the 40% RAP Foamer mix- Table 8. The TSR ratio for mixtures with only Evotherm is 88%
tures exhibited very low TSR values. This is probably caused by the that passes the minimum required TSR value of 85% as specified
high ITS values exhibited by the unconditioned set of specimens by NCDOT; and, therefore, for the mix under consideration,
with 40% RAP foamed mixture. The ITS values for all mixtures Evotherm can be used not only as a WMA additive but also as
increased with increase in RAP content. However, for HMA an antistrip additive.
mixtures the ITS values decreased when the RAP content was in- However, it is emphasized that when RAP is used with the mix,
creased from 20 to 40%. This may be because of the use of a softer especially higher contents, it may be necessary to either increase
binder, PG 58-28, for HMA mixtures with 40% RAP instead of PG the Evotherm dosage or add an additional antistrip additive such
64-22 which was used for the remaining mixtures. This also ex- as LOF 6500 as used in this study. This observation is based on
plains why Evotherm and Foamer mixtures with 40% RAP exhib- Table 7 results that show a 85% TSR ratio for the mix with
ited higher conditioned and unconditioned ITS values than HMA 40% RAP but containing 0.5% Evotherm and 0.75% LOF 6500
mixtures with 40% RAP and PG 58-28 binder. Fig. 5 shows the by weight of asphalt.
2500 120%
Indirect Tensile Strength (kPa)
100%
2000
Tensile Strength Ratio
80%
1500
60%
1000
40%
500
20%
0 0%
HMA 0% EVO 0% FOAM 0% HMA 20% EVO 20% FOAM 20% HMA 40% EVO 40% FOAM 40%
RAP RAP RAP RAP RAP RAP RAP PG58- RAP RAP
28
Mixture Type
Fig. 5. ITS values of conditioned and unconditioned samples and tensile strength ratio