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Lv Sy kom Am Om [5/18 > aamEnER. O Dak AD INTERNATIONAL ISO STANDARD 9717 Third edition 2017-09, Metallic and other inorganic coatings — Phosphate conversion coating of metals Revétements métalliques et autres revétements inorganiques — Couches de conversion au phosphate sur métaux 5 & ——— Reference number, 180 9717:2017(E © 180 2017 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q Dak AT 1SO 9717:2017(E) Contents Page Foreword. iv Introduction. v 1 Scope x 2 Normative references. 1 3 Terms and definitions 1 4 Information to be supplied by the purchaser to the processor. 1 5 Coating types and their importance. 2 5.1 Coating types. 2 5.2 Designation of conversion coating. 2 6 Requirements. 3 61 Appearance 3 6.2 Coating mass per unit area 3 63 Post treatments. 3 64 Correlation of coating thickness and area-related mass. 4 7 Heat treatment. 4 Annex A (normative) Determination of phosphate conversion coating resistance to neutral salt spray test 5 Annex B (informative) General information. 8 Annex C (informative) Identification of phosphate conversion coating 41 liography 13 > m2 ee 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q Dak AD ISO 9717:2017(E) Foreword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. 180 collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives). Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www.iso.org/patents). Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement. For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISO's adherence to the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following URL: www.iso.org/iso/foreword.html. This document was prepared by Technical Committee ISO/TC 107, Metallic and other inorganic coatings, Subcommittee SC 8, Chemical conversion coatings. This third edition cancels and replaces the second edition (ISO 9717:2010), which has been technically revised. The following changes have been made: — the Scope has been clarified; — the Normative references have been updated; — the Terms and definitions have been replaced by a reference to ISO 2080; — Glause 4 has been revised; — the terms in Clause 5 have been revised; — requirements for the phosphate layer have been revised; — statements on corrosion resistance have been shifted toa new Annex.A; — Annex on salt spray testing has been revised; — Annex. to the properties of the phosphate layers has been revised. > m2 ee 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q Dak AD iv (@1SO 2017 — All rights reserved REIBA Pepe 1S0 9717:2017(E) Introduction Phosphate conversion coatings are applied to ferrous metals, aluminium, zincand their alloys (including zinc- and zinc-alloy-plated steel, cadmium and their alloys) either as an end finish or as an interme layer for other coatings. They are intended to — impart corrosion resistance, — improve adhesion to paints and other organic finishes, — facilitate cold-forming operations, such as wire drawing, tube drawing and extrusion, and — modify surface frictional properties so as to facilitate sliding. Phosphate conversion coatings are produced by treatment with solutions, the main constituents of which are the appropriate dihydrogen orthophosphates. These coatings are applied principally to ferrous materials and zinc, and differ in coating mass per unit area and apparent density, depending on — the construction material and surface condition of the components, — previous mechanical and chemical treatment of the components, and — processing conditions for phosphating. All phosphate conversion coatings are more or less porous but can be sealed substantially by subsequent sealant processes. > m2 ee Lv Sy kom Am Om [5/18 > aamEnER. O Dak AD © 150 2017 ~ All rights reserved v > m2 ee Lv Sy kom Am Om [5/18 > aamEnER. O Dak AD INTERNATIONAL STANDARD 1S0 9717:2017(E) Metallic and other inorganic coatings — Phosphate conversion coating of metals WARNING — This document calls for the use of substances and/or procedures that could be injurious to health ifadequate safety measures are not taken. This document does notaddressany health hazards, safety or environmental matters associated with its use. It is the responsibility of the producers, purchasers and/or users of this document to establish appropriate health, safety and environmentally acceptable practices and take appropriate actions. 1 Scope This document specifies a process for the confirmation of requirements for phosphate coatings which are usually destined for application on ferrous materials, zinc, cadmium and their alloys (see Annex B). 2 Normative references ‘The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 2080, Metallic and other inorganic coatings — Surface treatment, metallic and other inorganic coatings — Vocabulary ISO 3892, Conversion coatings on metallic materials — Determination of coating mass per unit area — Gravimetric methods ISO 4519, Electradeposited metallic coatings and related finishes — Sampling procedures for inspection by attributes ISO 9227, Corrosion tests in artificial atmospheres — Salt spray tests 3 Terms and definitions For the purposes of this document, the terms and definitions given in ISO 2080 apply. > 180 and IEC maintain terminological databases for use in standardization at the following addresses: gy — IEC Blectropedia: available at http://wwwelectropedia.org/ — 180 Online browsing platform: available at http://www.iso.org/obp 8 A 4 Information to be supplied by the purchaser to the processor ‘The following information shall be provided by the purchaser. Sip ») kom mh KH <5 18 > eum. 2 Dak AD In cases of phosphating steel parts with tensile strength 2 1 000 MPa, possibly also locally restricted, e.g. for case-hardened or cold-formed structures or in weld seam areas, the safety against brittle fracture (hydrogen embrittlement) is of primary importance. The phosphatising process shall be carried out in such a manner that any damage caused by hydrogen-induced brittleness is excluded. Technical measures to minimize the risk of hydrogen-induced brittleness shall be defined by the user and provided by the supplier/customer. Heat treatment in accordance © 150 2017 - Allvights reserved 1 180 9717:2017(E) with any recommendations cannot guarantee full freedom from hydrogen embrittlement. The performance of the heat treatment shall be demonstrated by the supplier. ) The sampling procedure, the acceptable quality limit or any other requirements and tests that deviate from 10 4519. d) The surface treatment or phosphating. ©) The appearance of the surface. f) The corrosion resistance. ) The quality, appearance and condition of basis metal, if any of these properties affect the usability and/or appearance of coatings. h) Where applicable, technical measures to minimize the risk of hydrogen induced brittleness as defined by the user. 5 Coating types and their importance 5.1. Coating types The conversion coating shall be declared according to Table 1. Table 1 — Declaration of conversion coatings [ Elements detected Coating type Iron (II) Feph Manganese Mnph Zine (no Caleium) Znph Zine and Calcium ZnCaph There are other coating types of zine phosphate that are altered because of the buildin of iron and/or nickel and/or manganese. This altered metal is usually present as a double salt, such as gy Zn2ME(PO4)2 x 4 H20, whereby ME can be Fe(II), Ni or Mn. Zn will continue to be the main metal element of those coatings, which do not have separate markings in order to avoid confusion. It should also be noted that metal taken from the basis material is included in the conversion coating, a Information for coating characteristics can be found in Annex B and the identification methods can be found in Annex C. 5.2 Designation of conversion coating 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q Dak AD a) number of this document, i.e. ISO 9717, and the designation “phosphate coating” b) followed by a hyphen; ©) designation of basis material: by means of the material chemical symbol (or the symbol of the primary alloy components); d) followed by a solidus(/); ©) asymbol describing the type of coat f) followed by a solidus (/}; 2 © 150 2017- Allrights reserved 1SO 9717:2017(E) g)_asymbol, which indicates the function of the conversion coating as follows: y 2) = simplification of cold forming; adhesion promoter and/or corrosion protection; 3) g= reduction of friction; 4) e= electrical insulation; h) followed by a solidus (/); i) a number, which indicates the surface-related mass per square metre with a measurement uncertainty of +30 %. If the phosphate coating receives a supplementary treatment, the following information shall be added to the designation: i) solidus (/) k)_asymbol, which defines the supplementary treatment (see Table 2). Repeat this process if necessary. Solidi (/) shall be used to separate data fields in the designation corresponding to the different ‘sequential processing steps. Double separators or solidi indicate that a step in the process is either not required or has been omitted (see ISO 27830). 6 Requirements 6.1 Appearance Zinc phosphate, zinc calcium phosphate and manganese phosphate coatings shall evenly cover th@) metal surface and shall not show any white stains, corrosion products or fingerprints. NoTE ight fluctuations in the appearance of phosphate coatings because of contact with frames, properties of the base material or through minor contact inside the drum do not constitute any reason for claim, a 6.2. Coating mass per unit area A The coating mass is measured in accordance with the procedures speci in ISO 3892. 63 Post treatments 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q DaSk AD effect a temporary protection. Table 2 shows the symbols when post-treatments are required. Table 2 — Symbols for post after-treatments Symbol ‘Type of treatment ‘Application of varnishes or organic coatings Tt | Application ofinorganic ur nom flor forming organic sealants ‘T2__ [Application of inorganic or organic sealants 73 [Dyeing T4 [Application of grease or oil or other lubricants TS __ [Application of wax 76 [Application of soap © 150 2017 ~ All rights reserved 3 ISO 9717:2017(E) The corrosion resistance of the after-treated components shall be verified in accordance with the corrosion test specified by the customer. If there is no test method prescribed, the components shall be tested according to the neutral salt spray (NSS) test described in ISO 9227 NSS test and Annex A. The test duration shall be agreed between the contractual parties. The minimum testing periods specified by the customer shall be reached before the first appearance of corrosion effect. A coating of zincphosphate type Znph, which has been applied on a ferrous material to prevent corrosion, with an area related mass of 3 g/m? + 0,9 g/m? and an after-treatment with a sealing (T2) and a painting (T1), has the following designation: Phosphate coating ISO 9717 — Fe/Znph/r/3/T2/T1 64 Correlation of coating thickness and area-related mass The thickness and the related mass in gram per square metre can be measured according to the following methods: — magnetic inductive, according to ISO 2178; — dissolving method, according to ISO 2177; — xray according to ISO 3497. 7 Heat treatment Heat treatment after the phosphating is not recommended, because the phosphate layer will be damaged ata temperature higher than 120°C. > m2 ee 2h sy kee MA A A B <5 se > ese. Dak AD 4 © 150 2017- Allrights reserved RARE, VF POMS C ES a 1 1S0 9717:2017(E) Annex A (normative) Determination of phosphate conversion coating resistance to neutral salt spray test A.1_ Determination of corrosion resistance A neutral salt spray (NSS) test in accordance with ISO 9227 NSS is the standard test for determining corrosion resistance. If required, other test methods may be agreed between the contracting parties. The test should be performed with original components. Where it is not possible to carry out the test on the actual item, special test panels can be used. If special test specimens are used to represent the coated articles in a test, the specimens shall be of the same nature, same surface condition, and same material and in the same metallurgical condition as the article they represent, and shall be placed in the same production lot of, and be processed along with, the coated article they represent. Original components or test plates can be used either for testing the coating systems. 5 The salt spray test provides a means of controlling for the quality and continuity of coating. The test panels shall measure 150 mm x 100 mm (see Figure A.1), Two holes of diameter 5 mm anf lightly countersunk on each side shall be drilled at 6 mm from each edge near adjacent corners at th ends ofa 100 mm side, to enable the specimens to be suspended vertically during the test. All cut edge and corners shall be lightly rounded off and smoothed. A Dimensions in millimetres oe Sno kom Axe 6 QO 150 50 1 | 50 | 100. 0 Key 1 seratches Figure A.1 — Test panel © 150 2017 ~ All rights reserved ISO 9717:2017(E) A.2. Determination of resistance of phosphate conversion coatings to neutral salt spray test without supplementary treatments or organic coatings Use the neutral salt spray test method (see ISO 9227) to provide a means of controlling the quality and continuity of the phosphate conversion coatings by a continuous moving moisture film. The test duration shall be specified by the user or purchaser. A3_ Determination of resistance of phosphate conversion coatings, which have been subsequently treated with corrosion-preventing mediums, to neutral salt spray test A3.1 Principle Phosphated test pieces are treated with an appropriate corrosion-protecting medium (e.g. oil) under specified conditions and these treated test pieces are subjected to the neutral salt spray test (see ISO 9227). The test may be used either to evaluate a specific corrosion-protecting system or for comparative testing of a range of phosphate conversion coatings in conjunction with a specific corrosion-preventing medium. A.3.2, Supplementary treatment AL 1 Specific treatment Immerse the phosphated component or test panel in the corrosion-protecting medium under examination, carefully following the appropriate instructions and ensuring that the liquid, semi-solid or waxy film which forms on the phosphated surface is free from air bubbles and discontinuities. Before testing, suspend the test pieces for at least 24 h at a temperature of 23 °C + 5 °C and a relative humidity not exceeding 65 %, in a dust and draught-free atmosphere, so as to allow the surplus of oil to drip off and the solvents to evaporate. < 15 \/18 > ew. Dak AD > m2 ee 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q Dak AD Suspend the phosphated test pieces (previously dried at a temperature of between 100 °C and 120 °C and cooled to room temperature) from suitable plastic hooks or plastic-coated steel hooks and immerse them vertically in the oil for 1 min at a temperature of 25 °C + 2 °C. During this time, move the test panels gently to and fro and then withdraw them gradually from the oil in about 30 s. The oil film that forms on the phosphated surface shall be free from air bubbles and discontinuities. Suspend the test panels for at least 24 h at a temperature of 23 °C + 5 °C and a relative humidity not exceeding 65 %, in a dust and draught-free atmosphere, prior to testing. A3.3 Procedure Subject the oil-treated components or test panels (see A.3.2) to the neutral salt spray test (see ISO 9227). This test determines the exposure times attainable by a specific corrosion-protecting system before the first evidence of corrosion of metal becomes visible. For this purpose, take test pieces from the test chamber at predetermined intervals and examine them visually (with corrected vision if necessary) for evidence of corrosion. Whether or not the after- treatment film (or layer) is to be removed before visually examining the components or test panels is subject to agreement. For a specific phosphate coating, considerable scatter occurs in the exposure times up to the first occurrence of corrosion, depending on the composition of the supplementary treatment medium and the coating level. Therefore, minimum exposure times for supplementary-treated phosphate conversion coatings shall always be referred to a specific product from the category of corrosion-preventing 6 © 150 2017- Allrights reserved 1S0 9717:2017(E) oils, greases and waxes, of known coating level, in grams per square metre, as determined by mass difference. > m2 ee Lv Sy kom Am Om [5/18 > aamEnER. O Dak AD © 150 2017 ~ All rights reserved 7 Mike, RAMS SSH fue, wes, meee neweene! 1S0 9717:2017(E) Annex B (informative) General information B.1 General Phosphate conversion coatings are produced by treatment with solutions, the main constituents of which are specified in Table B.1. These coatings are usually applied on ferrous material, al zinc and cadmium. They differ in the surface related mass and the apparent density depending on the following: a) the raw material and surface quality of the component; b) the mechanical and chemical pre-treatment of the component; > m2 ee )_ the working conditions of phosphating. Phosphate coatings are more or less porous, but they can be compacted with an appropriate retreatment ‘Table RA — Charactertetice of phoenlinte coatings Lv Sy kom Am Om [5/18 > aamEnER. O Dak AT : coating - ain cae vor ents of phosphat-| ing-type appearance ingbath | producea | Y™bol_ | “Sfeoating | Fe al zn ca a Zine a Light greyto | 44, : S antiP0)2 | gydag | tmp | MBBEREEY ET 14030 | 0:30 10 1020 Z(HePO) 2 |zineceateium| zacanp, | biehterevto| 16539 | — | ao | — Ca(tizP04)2 | Phosphate ph | Garkegrey Manganese Dark greyto | 49 ~ Mn(H2P0d)2 | MADEEPESS | Mnph Kereyto | rtoao | — = Amorphous Phosphate coatings of of treated about 0,1 g/ crete (bins mito me iridescent, e.. Me(i(Hi2Po.) 2 | (SOF | eph — |"Yetlowish to'| O2t015| <05 | 0202; — cathof bluish grey ferrous Coatings over materials) about 1 g/m? rey 3 _Me(I) denotes a cation of alkali metal or (Wiig B.2 Surface preparations Components need to be removed from scale, grease, oil and corrosion products by using a suitable pretreatment. Phosphating is usually characterized by dipping the components (if necessary in moving fluids), flooding or spraying with a phosphating solution. In cases of handling with tape material, it is possible to use the roll application process. 8 © 150.2017 Allrights reserved 1S0 9717:2017(E) B.3 Application of phosphate coatings B.3.1 Cold forming Zinc phosphate conversion coatings are preferred to assist with cold forming. Guidance on the coating mass per unit area for various intended use is given in Table B.2. The deformation rate is achieved by using an adequate lubricant. Table B.2 — Zinc-phosphate-conversion-coating mass per unit area to assist cold forming (Coating mass per unit area Intended use g/m? > Drawing of steel wire 5 tos Drawing of welded steel tubes 3t010 & Drawing of steel precision tubes 2t010 a [Cold heading and cold extrusion 5t020 Deep drawing without wall-thickness reduction 20S “ Deep drawing with wall-thickness reduction 5to1S B32 wection B <5 se > ese. DaSk AD tht 87D kom mA A A coating masses per unit area for various end-uses. ‘The factors listed below should also be taken into con: jeration, a) Although manganese phosphate coatings are generally preferred, other types of coatings, for example zinc phosphate, are also suitable, particularly at lower coating levels. The type of coating selected will depend on the stresses in the coating involved for the intended end-use. b)_ The coating level used depends on the dimensional tolerances of the coated components in the assembled unit. Such coatings are normally used in conjunction with a suitable lubricant. Table B.3 — Manganese-phosphate-conversion-coating mass per unit area to influence tribological properties Coating mass per unit Intended use area Notes g/m? IGoinpenents wich enall ceatonees ep suas coating ot maliipmenganere pistons of refrigerator compressors [phosphate [Components with large clearances, e.g. gears, crown wheels and pinions of gear units and 5to20 differentials |Coating of manganese iron | phosphates (iron present in bath) B.3.3. Application of phosphate conversion coatings to improve corrosion resistance Table B4 reviews the significance of coating mass per unit area of phosphate conversion coatings regarding their application, © 150 2017 ~ All rights reserved 9 ISO 9717:2017(E) Table B.4 — Use of phosphate conversion coatings to improve corrosion resistance Phosphate coating Preferred | Coatingmass| supplementary ‘Typical applications Basismetal / “typeof | Perunitarea covers and end-uses treatment xi? 4 >5,but 5 Znph Mmph | eeterably Corrosion protection in transit and/or Feph TD [protective oils or {storage. Ferrous waxes, as required, materials iter dyeingotthe |oFFosion eppection ary ‘1 1 . Fathi environment (no condensation). znCaph S * ‘Temporary protection outdoors 5 with overhead cover. % Ferrous materials, zinc, Motor-vehicle bodies, refrigerator and aluminium, AmphZataph.) a.t000) ‘washing-machine cabinets. 8 jeadmium lOrganic coatings A varnishes and Motor-vehicle bodies, sheets and related coatings _| strips that are formed after zine Znph 151045 application of organic coatings and, in particular, where flexing of an B <5 se > ese. Dak AD 2h sy kee MA A A Ferrous Feph 020015 |non ‘environment (no condensation). materials ‘Znph 15to45 [None ‘Short-term, in-plant storage of | machine components (< 24 hi. 10 © 1S0 2017 ~ All rights reserved 1S 9717:2017(E) Annex C (informative) Identification of phosphate conversion coating > & a C1 General A This annex describes methods for identifying the type of phosphate conversion coating. The methods are applicable to coatings containing phosphorus, iron, manganese, zinc and calcium. They are not applicable to the detection of iron or zinc if these metals are present in the basis material. Lv Sy kom Am Om [5/18 > aamEnER. O Dak AD 2.1 Principle Removal of the phosphate conversion coating froma test specimen by treatment with sodium hydroxide solution, Detection of the elements present in the solution by any suitable instrumental analytical technique, e.g. atomic absorption spectrometry. 2.2. Reagents During the analysis, use only reagents of recognized analytical grade and distilled water, or water of equivalent purity. 2.2.1 Sodium hydroxide solution, 50 2/1. 2.3. Apparatus Use ordinary laboratory apparatus and any appropriate instrument suitably equipped for the detection of phosphorus, manganese, zinc and calcium, e.g. an atomic absorption spectrometer for metals. C24 Test specimen Use a test specimen having a total coated surface area of approximately 100 cm2, C.2.5 Procedure Immerse the test specimen (C,2.4) in 100 ml of the sodium hydroxide solution (C.2.2.1) maintained at a temperature of 80 °C to 90 °C, until the coating has been removed or has at least undergone obvious attack. If necessary, remove the coating by rubbing with a rubber squeegee. Using the appropriate analytical instrument (C.2.3), detect which of the elements, phosphorus, manganese, zinc and calcium, are present in the test solution, C.3 Method 2 As an alternative to method 1 (C.2), a scanning electron microscope equipped for energy dispersive spectroscopy (EDS) may be used for the direct detection of metal elements in the coating. C4 Interpretation of results Taking account of the elements detected, identify the types of coating in accordance with Table C.1 © 150 2017 ~ All rights reserved 1 ISO 9717:2017(E) Table C.1 — Identification of type of phosphate conversion coating For ferrous basis materials, the absence of manganese or zinc in the conversion coating indicates almost certainly that the coating consists of iron(II) phosphate (Feph). Elements detected Coating type Phosphorus Phosphate 5 Manganese Mnph nc (no calcium) ‘Znph & Zine and calcium ZnCaph a a NOTE The presence ofa satisfactory coating can be deduced by ‘a) rubbing the treated surface with fine steel wool; untreated steel chows a bright burnished appearance, or 2h sy kee MA A A < (18 )/18 > eaprmtariR. Q Dak AD scraping small area with a sharp knife; coated surfaces yield a light grey powder. ‘Test methods b) and c) may not give very marked indications, 12 © 180 2017 - All rights reserved 1SO 9717:2017(E) Bibliography 5 [1] 1s0 2177, Metallic coatings — Measurement of coating thickness — Coulometric method by anod dissolution a [2] 1SO 2178, Non-magnetic coatings on magnetic substrates — Measurement of coating thickness — Magnetic method A [3] 180 3497, Metallic coatings — Measurement of coating thickness — X-ray spectrometric methods [4] 180.4536, Metallic and non-organic coatings on metallic substrates — Saline droplets corrosion test tht SiH 15} [6] (71 [8] 19] [10] fu] kom pho KH <5 18 > eum. 2 Dak AD ISO 10289, Methods Jor corrosion testing of metallic and other inorganic coatings on metallic substrates — Rating of test specimens and manufactured articles subjected to corrosion tests ISO 10587, Metallic and other inorganic coatings — Test for residual embrittlement in both metallic- coated and uncoated externally-threaded articles and rods — Inclined wedge method ISO 27830, Metallic and other inorganic coatings — Guidelines for specifying metallic and inorganic coatings ASTM E527, Standard practice for numbering metals and alloys in the Unified Numbering System (UNS). Available from ASTM International, 100 Barr Harbor Drive, West Conshohocken, Pennsylvania, USA ASTM B117, Standard practice for operating salt spray (fog) — Apparatus Defence Standard 03-11, Phosphate treatment of iron and steel, UK Defence Standardization, Kentigern House, 65 Brown Street, Glasgow G2 8EX, Scotland Rav G.P. Thickness testing of electroplated and related coatings, 2nd edition, 1993, Electrochemical Publications Ltd, Isle of Man, ISBN 0 901150 27 4 13 © 150 2017 ~ All rights reserved SUAROER, MR TAALESES B rso0m Epos RE-RI METREDORTA, > m2 ee BBP METRY LH 8p kom MAR A Ei ISO DIS CENRHRIN) JSAITS GEAR) 150 TR. 196503-2019_K 1571-2010 9705-2-2001 aErie mR RFRA ab xa | ER anes DARD Fem BHF Bae) porn RETR < [as |/18 > cee) ISO CERI) LEC 2425-1-1987 61754-7-2-2019 ERA] sees cmos 1010821118 eam. Q Dak AT cee) UEC ERM) TEC EAE) G17547-2-2017 —60695-1-40-2013 12952-2-2C wes REINEARS > m2 ee

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