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? sean Aly Designation: C 133 - 97 (Reapproved 2003) Standard Test Methods for Cold Crushing Strength and Modulus of Rupture of Refractories’ ‘This sina sine under he fed design C 133; the eurnber imumedieyfllowing the designation indicts the year of txigial adoption ox ne case of ison, the year of las evision. A numer inpaeahecs few the your oft eappevl, A super eailon (© Incas an etal ehange sce the last revision o eappeora ‘his andar has bean epprved for use by agencies of the Departmen of Defense 1, Scope 1.1 These test methods cover the determination of the cold crushing strength and the modulus of rupture (MOR) of dried of fired refractory shapes of all types. 1.2 The test methods appear in the following sections: Test Metnad Sectors (oo Crushing Svengt 409 Mosul of Fugue row is 1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use, It is the responsibility of the user of this standard to establish appro- priate safety and health practices and determine the applica: bility of regulacory limitations prior to use. 2. Referenced Documents 2.1 ASTM Standards C862 Practice for Preparing Refractory Concrete Speci- mens by Casting? © 1054 Practice for Pressing and Drying Refractory Plastic and Ramming Mix Specimens? 4 Practices for Force Verification of Testing Machines? 3. Significance and Use 3.1. The cold strength of a refractory material is an indica- tion of its suitability for use in refractory construction. (Itis not measure of performance at elevated temperatures.) 3.2 These test methods are for determining the room tem- perature flexural sitength in 3-point bending (cold modulus of Fupture) or compressive strength (cold crushing strength), ot both, for al refractory products ‘these tat metods are under the juritision of ASTM Commitee C08 08 Refactor and ar he divec respons of Sobcommites C08. os Steg ‘Care edon approve Apel 10, 2003. Pablihed Joly 2003 Ogi spyroved in 1937, Las previous ition approved in 1997 ae C133 97, 4 Annual Boot of ASTM Sendai, Vo 180 * annual Baok a ASTM Senda, Vo (3.01. ‘oprah @ AST ea, 69 Bar Mar Ce, PO Box C0, Wie Consens, PA 18262080, ed Se 32 3.3 Considerable care must be used to compare the results of different determinations of the cold crushing strength or ‘modulus of rupture. The specimen size and shape, the nature of the specimen faces (thet is, a-formed, sawed, or ground), the orientation of those faces during testing, the loading geometry, andthe rate of load application, may all significantly affect the numerical zesults obtained. Comparisons ofthe results between sfferent determinations should not be made if one or more of these parameters differ between the two determinations. 3.4 The relative ratio of the lirgest grain size to the smallest specimen dimension may significantly affect the mumericel results. For example, smaller, cut specimens containing large grains may present different results than the bricks from whieh they were cut. Under no eircumstances should 6- by I- by L-in. (4152. by 25- by 25-mm) specimens be prepared and tested for materials containing grains with a maximum grain dimension exceeding 0.25 in. (64 mm). 3.5 This test method is useful for research and development, engineering application and: design, manufacturing process control, and for developing purchasing specifications. COLD CRUSHING STRENGTH 4. Apparatus 4.1 Testing Machine—Any form of standard mechanical ot hydraulic compression testing machine conforming 10 the requiremenss of Practices E 4 may be used. Nore 1—For lowsteagth materials (fuch as insulating bricks or castles), a sensitivity of 20 Iht (67 KN) or less i equiced. The wae of @ Ihyéralic testing machine i also prefered over the mechanical type for ‘hese materials, 42 Spherical Bearing Block—The plane surféée of the spherical bearing block (ee Fig. 1) shall have an area which is Seat pe ‘equal to or greater than the cross section 6f 5. Test Specimens ‘cubes or cylinders, 2 in. (5 high. The height shoule: pressing of the brick tn cepa 7 | ] —— ~~ Lats. ily c 133 - 97 (2003) Platen of Testing Machine ‘Spherical Spherical Seat Bearing Block Genter of. Bedding Matericl ‘Spnered Surtooe-F° ‘where required pL Test Specimen _ Pessina Meteril _ FIG, 4 Recommended Design for Crushing Test Assembly, Including Bearing Block only one specimen shall be cut from a single shape and as rmazy of the original surfaces as possible shall be preserved. In preparing specimens fom irregular or large refractory shapes, any method involving the use of abrasives, such 28 a high- speed abrasion wheel, core drill, or rubbing bed, that will produce a specimen with approximately plane and parallel sides without weakening the structure of the specimen may be sed. 52 Insulating Brick or Shapes (typical bulk density of 100 loaf? (1.60 giem*), or greater than 45 % total porosity, or ‘botk}—The test specimens shall be 4% by 41 by 2¥2 or 3 in. {Ud by 11d by 64 or 76 mm), each taken from e different brick. Itis permissible to prepare these specimens from the balf-brick resulting from the modulus of rupture test (see Sections 10-15). The selected compression test section shall be free of cracks, chipped surfaces, and other obvious defects. The test surfaces shall be approximately parallel planes 53 Castable Reftaciores—The test specimens shall be 2- by 2- by Qin, (S1- by 51- by SI-mm)} cubes or cylinders 2 in. (61 mam) in diameter by 2 im. (51 mm) high, prepared by casting or gunning. It is permissible to prepare one specimen ‘oi each S- by 2 by 2in. (230- by 51- by Si-mm) bar after the modulus of rupture test (see Sections 10-15). The selected compression test section shall be free of cracks, chipped surfaces, and other obvious defects. The loaded surfaces shall be epproximately parallel planes. All samples must be dried at 220 to 230° (105 to 110°C) for 18 h (overnight). Upon removal from the oven, allow the sample to cool naturally until oo] to the touch. Complete testing within 2 h of removal from the drying oven. (See Practices C 862 and C 1054.) 6. Procedure 6.1 At least five specimens from an equivalent number of refractory shapes compose a sample, 33 Nore 2—For rltively weak specimens lke insulating cestables or insulating frebeicks, 2 minioum sample size often specimens is pe- ened, 62 Brick and Shapes—Place a cellulose fiber wall board (for example, Masonite‘) 0.25 in, (6.4 mm) in thickness and extending 0.5 in, (12.7 mm) or more beyond the edges of the Joaded faces of the specimen. Apply the load perael to the

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