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CHAPTER 9
PROPERTIES
Since this method recommends the use of s/n ratio to measure the
quality characteristics deviating from the desired values. There are several S/N
ratios available depending on the type of characteristics: smaller is better,
nominal is best and larger is better.
(I) Smaller the better
N = -10 Log10 [mean of sum of squares of measured data] (9.1)
This is usually the chosen S/N ratio for all undesirable characterstics like
“defects” etc. for which the ideal value is zero. Also, when an ideal value is finite
and is maximum or minimum value is defined, then the difference between
measured data and ideal value is expected to be as small as possible The generic
form of S/N ratio then becomes,
N = - 10 Log 10 [mean of sum of squares of {measured – ideal}] (9.2)
(II) Larger -the -better
N = - Log 10 [mean of sum squares of reciprocal of measured data] (9.3)
This case has been converted to SMALLER –THE-BETTER by taking the
reciprocal of measured data and then taking the S/N ratio as in the smaller the
better case.
(III) Nominal –the –best
(9.4)
This case arises when a specified value is MOST desired, meaning that neither a
smaller nor a larger value is desirable.
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=( (9.8)
For factor A,
= +….+ - (9.9)
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For Error,
= -( + + + + ) (9.10)
Variance, V
(d) F- ratio, F
The confirmation test is used to verify the estimated result with the
experiment results. If the optimal combination of parameters and their levels
coincidently match with one of the experiments in the orthogonal array (OA),
then the confirmatory much with one of the experiments in the OA, then the
confirmatory test is not required.
shown in table 9.2. The interaction between A and C process parameters were
taken to evaluate the effect of PV (product of applied pressure and sliding
velocity) factor (Fazlur Rahman, J. and Mohammed Yunus, 2009).
Table 9.1. Process parameters and levels of the experimental design
Parameters Labels Level 1 Level 2 Level 3
Applied Pressure (MPa) A 0.1 0.2 0.3
Sliding Distance ( m) B 4 6 8
Sliding velocity (m/sec) C 2.5 7.5 12.5
Type of Coating D PSZ AT Alumina
Table 9.3. Experimental layout and results of summary for Wear test
Experiment trials A B C D Weight loss S/N ratio
(Recipes) in mg in dB
1 0.1 4 2.5 PSZ 3.0 9.54
2 0.1 4 7.5 AT 1.8 5.11
3 0.1 4 12.5 A 5.25 14.40
4 0.1 6 2.5 AT 3.8 11.59
5 0.1 6 7.5 A 4.75 13.53
6 0.1 6 12.5 PSZ 8 18.06
7 0.1 8 2.5 A 5.6 14.96
8 0.1 8 7.5 PSZ 8 18.06
9 0.1 8 12.5 AT 8 18.06
10 0.2 4 2.5 AT 3.5 10.88
11 0.2 4 7.5 A 3.6 11.13
12 0.2 4 12.5 PSZ 14 22.9
13 0.2 6 2.5 A 10 20
14 0.2 6 7.5 PSZ 10 20
15 0.2 6 12.5 AT 20 26.02
16 0.2 8 2.5 PSZ 8 18.06
17 0.2 8 7.5 AT 11 20.83
18 0.2 8 12.5 A 25 27.96
19 0.3 4 2.5 A 6.5 16.25
20 0.3 4 7.5 PSZ 12 21.58
21 0.3 4 12.5 AT 16 24.08
22 0.3 6 2.5 PSZ 9 19.08
23 0.3 6 7.5 AT 16 24.08
24 0.3 6 12.5 A 25 27.96
25 0.3 8 2.5 AT 12 21.58
26 0.3 8 7.5 A 16 24.08
27 0.3 8 12.5 PSZ 24 27.6
Table 9.4.Control factors and levels of the experimental design for Hardness
Factors Labels Level 1 Level 2 Level 3
Applied pressure (MPa) A 0.1 0.2 0.3
Sliding Distance ( m) B 4 6 8
Sliding velocity (m/sec) C 2.5 7.5 12.5
Partial Stabilized Alumina-
Type of Coating D Alumina (A)
Zirconia (PSZ) Titania (AT)
Table 9.5. Experimental layout and summary of results for Hardness test
Experiment design using Taguchi method was carried out firstly using
the results of thermal barrier / Thermal drop and secondly using the data of
Thermal cycling test. The experiments were carried out with three control factors
each at three levels are tabulated in table 9.6.
Table 9.6. Control factors and levels of experimental design of Thermal Barrier
test
Factors Labels Level 1 Level 2 Level 3
Temperature on coating side (0C) A 700 900 1000
Type of Coating B PSZ Alumina-Titania Alumina
Thickness of Coating (µm) C 150 225 300
Table 9.7. Experimental layout and summary of results for Thermal Barrier test
Trials A B C Thermal Barrier/ S/N ratio in dB
( Recipes) drop 0C
1. 700 PSZ 150 190 45.58
2. 700 AT 225 165 44.35
3. 700 A 300 135 42.61
4. 900 PSZ 225 200 46.02
5. 900 AT 300 170 44.61
6. 900 A 150 125 41.94
7. 1000 PSZ 300 215 46.65
8. 1000 AT 150 160 44.08
9. 1000 A 225 130 42.28
The feasible values for the three control factors of above study were
defined by varying the Temperature on coating side, type of coating and
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Table 9.8. Experimental layout and summary of results for thermal cycling test
There are twenty seven different tests were conducted using the
control factor combinations in the specified orthogonal array table value. Nine
specimens were prepared for each set of parameters to prepare complete response
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table. Taguchi method uses the S/N (signal-to-noise) ratio. S/N ratio is used to
determine the most significant factor. There are three types of S/N ratio criteria
for optimization; smaller the best, larger the better and nominal the best. To get
the better performance of results, smaller the weight loss is desired and hence
smaller the best criteria has been selected and following expression was used for
analysis.
(9.14)
Where y represents the observed data and n number of tests in one trial. The
mean responses of S/N ratio for weight loss are calculated for all factors and are
tabulated. A sample calculation for one of factor (A) is shown below.
9.54+5.11+14.4+11.59 +13.53+18.06+14.96+18.06+18.06
Level1= ----------------------------------------------------------------------------=13.7 dB
9
10.88+11.13+22.9+20+20+26.02+18.06+20.83+27.96
Level2= ----------------------------------------------------------------------- = 19.75 dB
9
6.25+21.58+24.08+19.08+24.08+27.96+21.58+24.08+27.6
Level3= ---------------------------------------------------------------------------=22.92dB
9
Difference, (max-min) = 22.92-13.7
= 9.22 dB
Table 9.9. Mean S/N Ratio Response Table for Wear test
Confirmation Test
levels (since all factors have a confident level more than 90%) of significant
parameters such as A3, C3, B3 and D1. The most optimal set of combination of
parameter is found out. The predicted mean (M) of the response characteristic of
TBC can be expressed as,
M = (A3-T) + (B3-T) + (C3-T) + (D1-T) + T, (9.15)
where T= current grand average of S/N ratio
Table 9.12. The comparison between actual and predicted results of Wear test
Optimum Level
Estimation Experimental Difference
Level A3B3C3D1 A3B3C3D1
Wear in mg 25.7 24 1.7
S/N Ratio in dB 30.22 27.6 0.6
=4.9 (9.17)
run confirmation test. Using ANOVA table ve= 3.923, fe=14 and F (1, 14) =4.6
at 95% confidence level and tabulated.
For the above test, Twenty seven different hardness tests were
conducted using the process parameters combinations in the specified orthogonal
array L16 as shown in table 9.8. To get the better performance, larger the hardness
number is desired and in this case, the larger the best criteria has been selected
for S/N ratio in the analysis.
Confirmation Test
The predicted mean (M) of the optimal set of results and confidence
interval (C.I.) were obtained by using the following equations,
= (40.855-40.602)+(41.41-40.602) + (40.86-40.602) + (40.733-40.602)
+40.602=42.052dB (9.18)
C.I. = [F (1, fe) Ve {1/neff +1/R}]^1/2=0.76 (9.19)
The predicted mean of the response S/N ratio for the hardness (HRC)
lies in the range of 41.294dB < HRC > 42.81dB at the confidence level of 95%
( =0.05).
Figure 9.3. Average Response S/N ratio Graph for Hardness test
There are nine different tests were conducted using the usage
parameter combinations in the specified orthogonal array table to measure the
quality and characteristics of output from desired value. Three specimens were
prepared for each set of parameters to prepare complete response table. Taguchi
method uses the S/N (signal-to-noise) ratio. S/N ratio is used to determine the
most significant parameter. There are three types of S/N ratio criteria for
optimization; smaller the best, larger the best and nominal the best. To get the
better performance, larger the thermal barrier and thermal cycling resistance are
desired. Hence larger the best criteria has been selected and following expression
was used for analysis.
(9.20)
Where yi represents the observed data and n number of tests in one trial. The
average responses of S/N ratio for thermal barrier are calculated for all the
parameters and are tabulated in table3. A sample calculation for one parameter is
shown below.
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Figure 9.4. Average response S/N graph for Thermal Barrier test.
Table 9.16. The average response of S/N ratio for thermal barrier test
Symbols Process Parameters Level Level Level Rank
1 2 3
A Temperature on coating side in 0C 44.18 44.19 44.34 0.16 3
Table 9.17. The optimal set of parameters for thermal barrier test
Symbols Parameter Optimum setting
A. Temperature on coating side (0C) 1000
B. Type of Coating PSZ
C. Thickness of Coating ( microns) 300
From the above table 9.16 and figure 9.4, it is seen that most
significant parameters can be determined by the larger difference of S/N ratio.
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The experimental results have been compared with optimal parameters obtained
by Taguchi technique, it is found that most significant parameter that increases
thermal barrier is type of coating followed by thickness of coating and
temperature on coating side.
run confirmation test. Using ANOVA table, v e= 0.019 and fe=2 and F (1, 2)
=18.51 at 95% confidence level and tabulated.
For the above test, nine different thermal cycling tests were conducted
using the control factor combinations in the specified orthogonal array shown in
table 9.20. To get the better performance, larger the thermal cycling resistance is
desired and in this case also once again the larger the best criteria has been
selected for S/N ratio in the analysis.
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Table 9.20. Experimental layout and summary of results for thermal cycling test
Table shows the L9 array for the thermal cycling test. The
experimental results have been compared with optimal parameters obtained by
Taguchi Technique and it is found that most significant factor is type of coating
followed by thickness of coating and temperature on coating side which is
similar as found in thermal barrier test as shown in table 9.21 and figure 9.5.
From the ANOVA, it is noticed that type of coating (B) indicates the
most significant factor and the highest contribution ratio is thermal cycling
resistance having 85.13%, while Temperature on coating side (A) has the lowest
about 7.744% and Thickness of Coating (C) has moderate value between the
other two 6.122% as shown in table 9.22.
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Table 9.21. The S/N ratio for Number of cycles withstood by Different TBC
Symbols Process Parameters Level1 Level2 Level3 Delta Rank
In order to verify the results once again in the thermal cycling resistance
test, confirmation test has been conducted using predicted average (M) and
Confidence interval (C.I.) at 95% confidence level.
= (50.20-49.9)+(51.17-49.9)+(50.32-49.9)+49.9 = 51.89dB
in the range of 46.26dB < TCT > 46.88dB.
=1.23. (9.18)
Table 9.23. The optimal set of factors for Thermal Cycling test
Optimum Level
Estimation Experimental Difference
Level A3B1C3 A3B1C3
Number of cycles withstood 342 400 58
S/N Ratio in dB 50.66 52.04 1.38