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© Pergamon Press Ltd. 1978. Printed in Great Britain
C O M M I S S I O N ON
S T A N D A R D I Z A T I O N OF LABORATORY AND FIELD TESTS
SUGGESTED M E T H O D S F O R D E T E R M I N I N G
HARDNESS AND ABRASIVENESS O F ROCKS
89
90 International Society for Rock Mechanics
INTRODUCTION
The Commission on Standardization of Laboratory and Field Tests on Rock was appointed in 1967. Subsequent
to its first meeting in Madrid in October 1968, the Commission circulated a questionnaire to all the members
of the International Society for Rock Mechanics, the answers received clearly showing a general desire for
standardized testing procedures. At a further meeting in Oslo in September 1969, tests were categorized and
a priority for their standardization was agreed upon, as given in Table 1.
It was also decided that research tests, including many of the rock physics tests, were beyond the scope
of standardization. Subsequent meetings were held in Belgrade in September 1970, in Nancy in October 1971,
in Lucerne in September 1972, in Katowice in October 1973, in Denver in September 1974, in Minneapolis
in September 1975 and in Salzburg in October 1976. At the Lucerne meeting the Commission was subdivided
into two committees, one on standardization of laboratory tests and the second on the standardization of
field tests.
The present document has been produced by the Committee on Standardization of Laboratory Tests. The
present document covers Category I (4) in Table 1.
It should be emphasized that the purpose of these "Suggested Methods" is to specify rock testing procedures
and to achieve some degree of standardization without inhibiting the development or improvement of techniques.
Any person interested in these recommendations and wishing to suggest additions or modifications should
address his remarks to: The Secretary General, International Society for Rock Mechanics, Laborat6rio Nacional
de Engenharia Civil, Avenida do Brasil, Lisboa, Portugal.
Acknowledgements--The following persons contributed in the drafting of these "Suggested Methods": R. H. Atkinson (U.S.A.), W. E. Bamford
(Australia), E. Broch (Norway), D. U. Deere (U.S.A.), J. A. Franklin (U.K.), C. Nieble (Brazil), F. Rummel (Germany), P. J. Tarkoy (U.S.A.)
and H. van Duyse (Belgium).
* Asterisks indicate that final drafts on these tests have been prepared.
91
508 mm
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=ier Catch pan for specimens
Not less than 1,27m
'measured on
Cover and filler outside of drum
~plate arrangement, ~ '
/R,0e, p,er \
l-ig. 1. Los Angeles abrasion testing machine.
that it may be rotated with the axis in a horizontal cover, in such a way that a plane centred between the
position within a tolerance in slope of 1 in 100. An large faces coincides with an axial plane. The shelf shall
opening in the cylinder shall be provided for the intro- be of such thickness and so mounted, by bolts or other
duction of the test sample. A suitable, dust-tight cover suitable means, as to be firm and rigid. The position
shall be provided for the opening with means for bolt- of the shelf shall be such that the distance from the
ing the cover in place. The cover shall be so designed shelf to the opening, measured along the outside cir-
as to maintain the cylindrical contour of the interior cumference of the cylinder in the direction of rotation
surface unless the shelf is so located that the charge shall be not less than 1,27 m. The shelf shall be made
will not fall on the cover, or come in contact with it of wear resistant steel and shall be rectangular in cross-
during the test. A removable steel shelf extending the section.
full length of the cylinder and projecting inward (b) Balance
89 _ 2 m m shall be mounted on the interior cylindrical A balance or weighing machine accurate within 0,1~
surface of the cylinder, or on the inside surface of the of test load over the range required for this test.
(c) For coarse aggregate smaller than 38 mm the of the original weight of the test sample.1 Report this
sample shall be recombined and the abrasive charge value as the percentage of wear.
selected as described in Table 3. (b) When the procedure described on Procedure Sec-
tion (c) is followed, the uniformity of wear ratio is the
ratio of the loss after 100 or 200 revolutions to the
PROCEDURE
loss after 500 or 1000 revolutions, respectively.
(a) Place the test sample and the abrasive charge in
the Los Angeles abrasion testing machine and rotate
the cylinder at a speed of 30-33 rev/min. The number
REPORTING OF RESULTS
of revolutions shall be 500 for aggregate smaller than
38 mm and 1000 for aggregate larger than 19 mm. The The report should include the following data:
machine shall be so driven and so counterbalanced as (a) Source location and geologic description of the
to maintain a substantially uniform peripheral speed. 4 sample tested.
If an angle-shaped steel member is used as the shelf, (b) Grading of test sample.
the direction of rotation shall be such that the charge (c) Grading of abrasive charge.
is caught on the outside surface of the shelf. (d) The Los Angeles percentage of wear (See Calcula-
(b) After the prescribed number of revolutions, dis- tions section (a) above).
charge the material from the machine and make a pre- (e) The Los Angeles uniformity of wear ratio (see
liminary separation of the sample on a sieve coarser Calculations section (b) above) if applicable.
than 1,7mm (No. 12 US). Sieve the finer portion in
a 1,7-mm sieve. Wash the material coarser than the
1,7-mm sieve, 2 oven dry at 105°-110°C to substantially
IMPORTANT NOTES
constant weight and weigh to the nearest gramm.
(c) Valuable information concerning the uniformity 1. This test method combines the essential features
of the sample under test may be obtained by also of ASTM standard test C131-69 and ASTM standard
determining the loss after 100 revolutions in the case test C535-69. Aggregate in the size range of 19 mm to
where 500 revolutions is specified or after 200 revolu- 3 8 m m can be tested by either one of the two pro-
tions in the case where 1000 revolutions is specified. cedures described in this Suggested Method. The
The loss should be determined without washing the specific procedure used for this size aggregate shall be
material coarser than the 1,7-mm sieve. The ratio of reported with the results.
the loss after 100 or 200 revolutions to the loss after 2. If the aggregate is essentially free from adherent
500 or 1000 revolutions, respectively, should not greatly coatings and dust, the requirement for washing before
exceed 0,20 for material of uniform hardness. When and after the test may be waived. Elimination of wash-
this determination is made, care should be taken to ing after testing will seldom reduce the percentage wear
avoid losing any part of the sample; the entire sample, by more than about 0,2 percentage points.
including the dust of abrasion, shall be returned to the 3. Test sieves shall conform to ISO Standard
test machine for the final 400 or 800 revolutions 56501972 (E) "Test sieves-woven metal wire cloth and
required to complete the test. perforated plate--nominal sizes of apertures", Series R
40/3.
4. Back-lash or slip in the driving mechanism is very
CALCULATIONS
likely to furnish test results which are not duplicated
(a) Express the difference between the original weight by other Los Angeles abrasion machines producing
and the final weight of the test sample as a percentage constant peripheral speed.
Hardness and Abrasiveness of Rocks 95
REPORTING O F RESULTS
r
Fig. 2. Core specimen holders.
The following information shall be reported:
(a) Lithologic description of the rock. Source of
sample, including: geographic location, depth and
1As manufactured or licensed by E. Schmidt, Basel, Switzerland. orientations.
96 International Society for Rock Mechanics
Radius (approx)
PART 4. S U G G E S T E D
METHOD FOR
DETERMINATION OF
Fig. 3. Profile of scleroscope diamond showing range of diameters
THE SHORE SCLEROSCOPE 1 of flat tip.
HARDNESS
SCOPE
PROCEDURE
This laboratory method is suggested for the hardness
determination of rock minerals using the Shore sclero- (a) Before each days use, make at least five hardness
scope I and for the verification of other scleroscope hard- readings on the standard test block furnished by the
ness instruments. Rock hardness may be obtained as manufacturer at the hardness level at which the
an average of readings taken at random on individual machine is being used. If the values fall within the range
mineral grains. of the standardized hardness test block the instrument
may be regarded as satisfactory; if not the machine
should be verified using procedures recommended by
APPARATUS
the manufacturer.
The instrument used for determining scleroscope (b) Tests shall be made on fiat surfaces ground
hardness numbers is supplied in two models designated smooth using a No. 1800 grade aluminium oxide abra-
Model C and Model D. Model C-2 is recommended sive powder. An excessively coarse surface will yield
for use with rock. low and erratic readings.
(a) The Scleroscope Model C-2 consists of a vertically- (c) Specimens should have a minimum test surface
disposed barrel containing a precision bore glass tube. of 10cm 2 and a minimum thickness of 1 cm. Small
A scale graduated from 0 to 140, is set behind the barrel specimens should be clamped securely with the fiat test
and is visible through the glass tube. A pneumatic surface perpendicular to the scleroscope axis.
actuating head affixed to the top of the barrel, is (d) To perform a test hold or set the instrument in
manually operated by a rubber bulb and tube. A ham- a vertical position with the bottom of the barrel in
mer drops from a specified height and rebounds within firm contact with the test specimen and normal to the
the glass tube. The hammer for Model C-2 shall have surface of the specimen. Bring the hammer to the ele-
the following dimensions: vated position by squeezing the rubber bulb and then
allow it to fall and strike the test surface and measure
Diameter 5,94 mm
the height of rebound. The height to which the hammer
Mass 2,300 _+ 0,500 g
rebounds on the first bounce indicates the hardness of
Overall length 20,7 to 21,3 mm
the material.
Distance hammer 251,2 + 0,13 - 0,38 mm
(e) To prevent errors resulting from misalignment the
falls
instrument must be set or held in a vertical position,
(b) The diamond must be shaped to produce a cor- using the plumb bob or spirit level on the instrument
rect reading on reference bars of known hardness. In to determine verticality. The most accurate readings of
profile, the diamond is convex, having a radius ter- the scleroscope are obtained with the instrument
minated by a flat striking surface, as shown in Fig. mounted in a clamping stand. Lateral vibrations must
3. The fiat striking surface is approximately circular be avoided since they tend to cause the free fall of
and from 0,1 to 0,4 mm in diameter, depending on the the hammer to be impeded and, hence, cause the instru-
hardness and other physical characteristics of the dia- ment to read low.
mond. (f) An error may result if the indentations are spaced
too closely together. Space indentations at least 5 mm
~Registered trade mark of the Shore Instrument and Mfg. Co., apart and make only one test at the same spot. At
Inc., Jamaica, New York, U.S.A. least 20 hardness determinations should be taken.
Hardness and Abrasiveness of Rocks 97