ACUMEN LAB

HACH Analysis Worksheet

Sample ID: nFDS0038/0110 (rep 1)

Parameter: Phosphorus
Date of analysis: 21/1/10
Analysis performed by: Yati

Analyte
Abs
standard / ppm
1 0.337
5 0.646
10 0.977
25 1.955

Intercept: 0.2944
Slope: 0.0668

Analyte in
Sample Final volume Dilution
Sample Abs sample
weight (g) (mL) factor
(mg/kg)
A 1.543 2.0076 100 1 742
B 1.002 2.198 100 1 482
C 1.318 2.0987 100 1 731
D 1.033 2.0659 100 1 535
E 2.132 2.1592 100 1 1275
F 1.989 2.0016 100 1 1268
blank 0.254

Calibration Curve Calibration Curve

2.5 12
Peak area
Peak area

10
2
f(x) = 0.0668 x + 0.2944
R²8= 0.9992
1.5
6

1 4

2
0.5
0
0 f(x)5= 0 10 15 20 25 30
0 R²concentration
= 0.00000 of analyte, ppm
0 5 10 15 20 25 30
concentration of analyte, ppm

Checked by
 HACH Analysis Worksheet

Sample ID: Refer Below

Parameter: Phosphorus

Company : ALPHA INDUSTRIES SDN BHD (JB)

Date of analysis: 9-Dec-15
Performed By: Sofea

Analyte
Abs - Blank Abs
standard / ppm

1 0.099 0.155
5 0.492 0.548
10 0.968 1.024
15 1.453 1.453

Intercept c: 0.0049
Slope x: 0.0965

Calibration Curve
1.600
1.400 f(x) = 0.0965 x + 0.0049
1.200 R² = 1.0000
1.000
0.800
0.600
0.400
0.200
0.000
0 2 4 6
Concentration 8 analyte, ppm
of 10 12 14 16

Conc. Analyte in
Sample Final volume Dilution
Sample Abs calculated sample Average
weight (g)/mL (mL) factor
from curve (mg/kg)
nCML0023/1215 0.080 0.5144 100 1 0.198 38.522 39

nCML0024/1215 0.079 0.5034 100 1 0.188 37.306 37

nCML0025/1215-1 0.122 2.0304 100 1 0.633 31.188

32
nCML0025/1215-2 0.124 2.0512 100 1 0.654 31.882

blank 0.056

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 HACH Analysis Worksheet

Sample ID:
Parameter:

Company :
Date of analysis:
Performed By:

Analyte
Abs - Blank Abs
standard / ppm

0.0 0.000 0.015

5 0.214 0.229
10 0.421 0.436
20.0 0.854 0.869
30.0 1.273 1.288
40.0 1.667 1.682
Intercept c: 0.0000
Slope x: 0.0425

Calibration Curve
1.400
1.200 f(x) = 0.0425 x + 0.0000
R² = 1.0000
1.000
0.800
0.600
0.400
0.200
0.000
0.0 5.0 10.0Concentration
15.0 of analyte,
20.0 ppm 25.0 30.0 35.0

Conc. Analyte in
Sample Dilution
Sample Abs calculated sample
weight (g)/mL factor
from curve (mg/kg)
Initial 1 0.132 10.00 25 2.753 68.820

0.5h 0.162 10.00 25 3.459 86.471

1h 0.854 10.00 25 19.745 493.629

3h 0.874 10.00 25 20.216 505.397

Initial 2 0.976 10.00 25 22.616 565.411

3.5h 0.990 10.00 25 22.946 573.649

4.5h 1.057 10.00 25 24.523 613.070

7.5h 1.246 10.00 25 28.971 724.274

Initial 3 1.328 10.00 25 30.901 772.521

8h 1.331 10.00 25 30.971 774.286

9h 1.365 10.00 25 31.772 794.291

12h 1.604 10.00 25 37.397 934.913

Blank 0.015

Checked by: Verified by:

 HACH Analysis Worksheet

Sample ID: Refer Below

Parameter: Phosphorus

Company : TROPICAL CONSOLIDATED CORP. SDN. BHD

Date of analysis: 6-May-15

Analyte
Abs - Blank Abs
standard / ppm

1 0.114 0.180
5 0.491 0.557
10 1.028 1.094
15 1.473 1.473
20 2.009 2.009
30 3.003 3.069

Intercept c: 0.0061
Slope x: 0.0998

Calibration Curve
3.500
3.000
f(x) = 0.0998 x + 0.0061
2.500 R² = 0.9997
2.000
1.500
1.000
0.500
0.000
0 5 10 15
Concentration 20 ppm
of analyte, 25 30 35

Analyte in
Sample Final volume Dilution Conc. calculated
Sample Abs sample Average
weight (g)/mL (mL) factor from curve
(mg/kg)
FDS0224/0415-1 1.039 2.0480 100 1 9.691 473.202
470
FDS0224/0415-2 1.009 2.0074 100 1 9.390 467.794

FDS0225/0415-1 1.062 2.1296 100 1 9.922 465.896

458
FDS0225/0415-2 1.052 2.1858 100 1 9.821 449.332

FDS0226/0415-1 0.849 2.0373 100 1 7.787 382.211

400
FDS0226/0415-2 0.909 2.0086 100 1 8.388 417.613

blank 0.066

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