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Cement and Concrete Composites: Mohammed T. Albahttiti, Ahmad A. Ghadban, Kyle A. Riding, David A. Lange T
Cement and Concrete Composites: Mohammed T. Albahttiti, Ahmad A. Ghadban, Kyle A. Riding, David A. Lange T
Keywords: There are many factors that affect the freeze-thaw durability of concrete elements, including proper air en-
Prestressed concrete trainment system, freeze-thaw durable aggregates, low permeability, and proper curing. While ASTM C666
Concrete saw-cutting allows the excising of small freeze-thaw samples from larger sections it doesn't address the issues that can arise
Freeze-thaw durability when excising samples from prestressed concrete and subsequent testing in freezing and thawing. In order to
investigate the effects of saw-cutting, the existence of reinforcement, and use of prestressing, concrete samples of
different sizes, with and without saw-cutting, with and without reinforcement, and with and without prestres-
sing were tested in freeze-thaw. The freeze-thaw mechanism was adjusted, from that of ASTM C666, for the
larger sample in terms of freezing and thawing rates and the testing method. The results indicate that saw-
cutting through plain concrete had minimal effect on the freeze-thaw durability, whereas sawcuts through re-
inforcement were shown to be very detrimental to the measured durability in the tests.
∗
Corresponding author. 400 W 1st Street, Concrete Industry Management, California State University, Chico, CA, 95929, USA.
E-mail address: malbahttiti@csuchico.edu (M.T. Albahttiti).
https://doi.org/10.1016/j.cemconcomp.2019.103418
Received 1 September 2018; Received in revised form 21 August 2019; Accepted 10 September 2019
Available online 13 September 2019
0958-9465/ © 2019 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license
(http://creativecommons.org/licenses/by-nc-nd/4.0/).
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
prestressed concrete members. This research aims to address the effects of Table 2
saw-cutting and the existence of reinforcement, prestressed or not, in saw- Fresh and hardened air content of all tested samples.
cut samples on freeze-thaw durability of concrete samples during testing. Sample Fresh Air Hardened Air Spacing
Content, % Content, % Factor, in
(mm)
2. Materials
Tie 1 Half Tie 1 (HT1) – 3.6 0.0117
For this study, concrete railroad ties were used as the structural Saw-cut Set 1-M1 (0.2972)
member to be tested, although the results can be generalized to concrete 1 (SHT1) 1-M2
1-B
excised from other structural member types. A total of 10 railroad ties
were examined in this study. Ties 1 through 4 were taken from railroad Tie 2 Half Tie 2 (HT2) – 2.5 0.0131
track during construction, but before being put into service. The pro- Saw-cut Set F-M1 (0.3327)
portions of the mix designs for Ties 1 through 10 were not available to 2 (SHT2) F-M2
F–B
the researchers due to the proprietary nature of these mixes for the ties.
The concrete used to make ties 5 through 10 used granite aggregate Tie 3 Half Tie 3 (HT3) 8.5 4 0.0098
with a nominal maximum size of 0.75 in (19 mm). Type III cement was Saw-cut Set 09-M1 (0.2489)
used in all concrete used in this project. Two different concrete mixtures 3 (SHT3) 09-M2
09-B
where used to make ties 5 through 10: one with air entraining agent and
one without an air entraining agent. Properties of these two types of Tie 4 Half Tie 4 (HT4) – 4 0.0133
concrete are presented in Table 1. The initial fresh air content when Saw-cut Set 06-M1 (0.3378)
available and hardened air void analysis conducted according to ASTM 4 (SHT4) 06-M2
C457 are shown in Table 2. Samples labeled as Cast Prisms and Cast 06-B
Prisms/No Air refer to samples made from the same two mix designs/
Tie 5 Half Tie 5 (HT5) 7 6.1 0.0049
batch used to make ties 5 through 10. These two set of samples, Cast Saw-cut Set PA-1 (0.1245)
Prisms and Cast Prisms/No Air will be the non-half tie samples (non-HT) 5 (SHT5) PA-2
and will act as our benchmarking samples. The half ties were given the PA-W
designation HT#, followed by the tie number. The saw-cut set of samples
Tie 6 Half Tie 6 (HT6) 0.9 2.3 0.0083
were given the designation SHT#, where HT# corresponds to the other Saw-cut Set PNA-1 (0.2108)
half of the same tie used in the half tie testing. Excised samples were also 6 (SHT6) PNA-2
assigned an individual ID in addition to the set ID. The individual ID was
used to help identify the material properties and sample reinforcement. PNA-W
The letter W instead of a number represents samples with embedded Tie 7 Saw-cut Set NPA-1 7 4.9 0.0030
vibrating wire gauge sensors. As for samples that didn't have large scale 7 (NPA) NPA-2 (0.0762)
half ties testing (Ties 7 through 10), they were given IDs that represented
the material and structural properties of the tie. The letter N in these NPA-W
samples refers to No/Non, the letter P refers to prestressed, the letter A
Tie 8 Saw-cut Set NPNA-1 0.9 3.5 0.0090
refers to Air and the letter W refer to Wire/reinforcement. 8 (NPNA) NPNA-2 (0.2286)
NPNA-W
2
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
previous section. Three samples were exerted from the end of each tie,
as shown in Fig. 4. The samples had dimensions of 3 × 4 × 11 in.
(76.2 × 101.6 × 279.4 mm), as shown in Fig. 5. End pins were then
installed on the saw-cut samples in order to measure length change
resulting from freeze-thaw testing. Finally, the samples were soaked in
lime water for 2 days at 40 ± 3 °F (4 ± 1.7 °C) according to ASTM
C666.
Initial sample measurements were taken on the samples after they
reached 40 ± 3 °F (4 ± 1.7 °C). Initial measurements included change
in weight, change in length, and transverse resonant frequency. In order
to satisfy requirements of ASTM C666 Method A, the samples were
tested at least every 36 freeze-thaw cycles [8]. The samples were tested
according to ASTM C666 with at least 5 cycles per day. A typical saw-
cut sample is presented in Fig. 6.
Fig. 1. Soaked half ties covered with burlap.
3.1.3. Cast samples
cut ends of the ties were epoxied in order to eliminate absorption from In addition to the half ties and saw-cut samples, four cast samples
that end and simulate the presence of a full tie. The half ties were tested were made from the same concrete used to make half ties 5 and 6. Two
at various stages of initial preparation. The tested half ties were 4.25 ft of the samples were made with air-entrained concrete and two without
(1.3 m) long with a trapezoidal cross section (10 in. (254 mm) top, 11 air entrainment. The samples had embedded pins in order to measure
in. (280 mm) bottom, and 10.5 in. (267 mm) height). Fig. 2 shows il- change in length. The cast samples were larger than the saw-cut sam-
lustrations of the shapes of the two types of half ties tested. Half Ties 1 ples, with dimensions of 3 × 4 × 16 in. (76.2 × 101.6 × 406.4 mm) in
through 4 have shapes similar to Shape I, while Half Ties 5 and 6 have order to satisfy ASTM C666 requirements. Cast prism freeze-thaw
shapes similar to Shape II as shown in Fig. 2. Ties 7 through 10 also testing was conducted in accordance with ASTM C666. Initial pre-
share the same shape with Half Ties 5 and 6. paration and testing of these samples was done after the samples were
Initial testing was performed after the samples were soaked in lime moist cured for 14 days. Table 3 summarizes samples used in this part
water. The small sawcut prisms were soaked for 2 days, whereas the of the study and testing done on each sample.
larger half ties were soaked for 7 days. After the samples were cooled to
40 °F (4 °C) following the 7-day soaking period. After the soaking 3.2. Verification and validation
period, the half ties were removed from the lime water bath and
wrapped with wet burlap. The wet burlap was placed around the ties to In order to verify field samples results, an additional set of samples
ensure that free water was present all around the half ties for the were made in the laboratory. All the additional samples were made
duration of the test. In addition, the samples were wrapped with plastic from a single mixture. This mixture was made with an air content of
wrap to avoid evaporation during the freezing stage. During the testing 5.1% in order to ensure that if failure occurred, it wouldn't be due to the
of the samples excess free water was added to the plastic to ensure poor air system. Also, the mixture was chosen to be very fluid with a
similar conditions to the boxes of small samples. yield stress of 86.2 Pa (0.0125 psi) and a plastic viscosity of 57.1 Pa s
After completing initial testing, the sample was subjected to 300 (38.4 lb/(ft·s)) in order to ensure proper consolidation since it was not
freeze-thaw cycles using a large freeze-thaw chamber. The chamber was subjected to vibration. These parameters correspond to an SCC mix with
designed to hold three whole ties, or six half ties, and cycle the concrete a slump greater than 10 in (250 mm). The mixture utilized ASTM C150
ties between 0 ± 3 °F (−18 ± 1.7 °C) to 40 ± 3 °F (4 ± 1.7 °C). The Type III cement, a natural siliceous sand, a limestone coarse aggregate,
temperatures were maintained at a distance of 4.5 in. (114.3 mm) from a polycarboxylate high range water reducer (HRWR), and a vinsol resin
the top surface of the ties (Center of the samples). The chamber was air entraining agent (AEA). The coarse aggregate had a specific gravity
able to cycle the concrete ties through 3.13 freeze-thaw cycles every of 2.69 and absorption of 0.39% while the fine aggregate had a specific
day with cycle lengths of 460 min. Fig. 3 shows typical temperatures gravity of 2.66, absorption of 0.74% and fineness modulus of 3.02. The
measured by thermocouples from the center of the half tie during water-cement ratio (w/c) used was 0.33. The percentage by volume of
freeze-thaw cycles. Half ties were tested every 36 cycles or less. paste, rock and sand were 30.5%, 31.6% and 31.9%, respectively. The
HRWR and AEA dosages were 7.67 oz/cwt (4.46 ml/kg) and 0.48 oz/
cwt (0.28 ml/kg), respectively. Three set of samples were made for this
3.1.2. Saw-cut samples
verification; plain, reinforced and saw-cut with reinforcement. Both the
In order to understand the effects of saw-cutting, reinforcement
reinforced and the saw-cut reinforced samples had 0.209 in (5.32 mm)
inclusion, and prestressing on freeze-thaw tests, concrete ties were
diameter steel wires. The plain and reinforced prisms were prepared
fabricated with prestressing wires (SHT5 and SHT6) and un-prestressed
using 3 × 4 × 16 in. (76.2 × 101.6 × 406.4 mm) molds while re-
wires (SHT7 and SHT8) and without steel reinforcement (SHT9 and
inforced saw-cut prisms were saw-cut from a 3 × 4 × 85 in.
SHT10). All reinforced ties were made with 0.209 in (5.32 mm) dia-
(76.2 × 101.6 × 2159 mm)-long beam. The saw-cut samples presented
meter steel wires. The prestressed ties were prestressed to 7000 lbs
here were only saw-cut from the ends. Fig. 7 shows the saw-cutting
(31138 N) per wire. In addition to these ties, four additional air-en-
process of the 3 × 4 in. (76.2 × 101.6 mm) beam.
trained prestressed concrete ties were obtained from railroad track
before being placed into service. Three samples were excised from each
3.3. Deterioration measurements
tie and tested in freeze-thaw conditions. The other halves of the pre-
stressed ties were used in the freeze-thaw testing described in the
Measurement of freeze-thaw durability of large-scale prestressed
concrete ties was done using multiple non-destructive testing (NDT)
methods to determine the ability of each method to measure dete-
rioration of prestressed concrete railroad ties undergoing freeze-thaw
testing. These methods included Resonant Frequency (RF), Ultrasonic
Pulse Velocity (UPV), Impact Echo (IE), and mass change measure-
Fig. 2. Sizes and shapes of the half ties tested. ments.
3
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
Fig. 3. Typical freeze-thaw cycle temperatures measured 4.5 in. (114 mm) from the concrete tie surface.
nc2
Pc = x100
n2 (1)
Fig. 4. Saw-cutting samples from the tie end.
where Pc is the RDME after c cycles of freezing and thawing (%), n is the
RF at 0 cycles of freezing and thawing, and nc is the RF after c cycles of
freezing and thawing.
In addition to RF, the UPV and IE were performed on half ties 1
through 6. UPV and IE readings were performed using an Olson
Instruments NDE 360. UPV sensors were placed 38 in. (965 mm) apart
on the top surface, and the IE sensor was placed on the rail seat, as
shown in Fig. 8. From the UPV measurement, the RDME was calculated
by dividing the square of each cycle reading over the square of the
initial reading, and change in thickness was obtained from the IE
method. In addition, all samples were weighed regularly during testing
with a 1,000-lb (454 kg) crane scale with a resolution of 0.1 lb
(0.05 kg).
The resonant frequency, change in length and change in mass were
measured on the small saw-cut and cast prisms according to ASTM
C666. Similar to ASTM C666, samples were considered to be non-dur-
able once the RDME dropped to 60% or less or the sample length in-
creased more than 0.1%.
Out of the six excised sample sets, three sets failed after 70 cycles or
Fig. 5. Three saw-cut samples from the tie end to be 3 × 4 × 11 in. less, one set failed after 121 cycles, and two sets did not fail according
(76.2 × 101.6 × 279.4 mm) in size.
to RDME measurements, as shown in Fig. 9. Failure in the excised
samples began as cracking between the prestressing wires parallel to
RF was performed on both types of half ties with an accelerometer wires on the surfaces of the samples, as shown in Fig. 10. This cracking
that measured the impact wave 38 in. (965 mm) away. The recorded could have developed as a result of three main parameters: thermal
acceleration was analyzed and a Fast Fourier transform (FFT) algorithm diffusivity differences between the concrete and steel, prestress release
4
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
Table 3
Summary of all the samples types and the testing performed on each sample.
Set Sample Air Entrained Type Tests Performed
HT1 ● ● ● ●
HT2 ● ● ● ●
HT3 ● ● ● ●
HT4 ● ● ● ●
HT5 ● ● ● ●
HT6 ● ● ●
SHT1 06-M1 ● ● ● ● ●
06-M2 ● ● ● ● ●
06-B ● ● ● ● ●
SHT2 F-M1 ● ● ● ● ●
F-M2 ● ● ● ● ●
F–B ● ● ● ● ●
SHT3 1-M1 ● ● ● ● ●
1-M2 ● ● ● ● ●
1-B ● ● ● ● ●
SHT4 09-M1 ● ● ● ● ●
09-M2 ● ● ● ● ●
09-B ● ● ● ● ●
SHT5 PA-1 ● ● ● ● ●
PA-2 ● ● ● ● ●
PA-W ● ● ● ● ●
SHT6 PNA-1 ● ● ● ●
PNA-2 ● ● ● ●
PNA-W ● ● ● ●
NPA NPA-1 ● ● ● ● ●
NPA-2 ● ● ● ● ●
NPA-W ● ● ● ● ●
NPNA NPNA-1 ● ● ● ●
NPNA-2 ● ● ● ●
NPNA-W ● ● ● ●
NW A NWA-1 ● ● ● ● ●
NWA-2 ● ● ● ● ●
NWA-W ● ● ● ● ●
NWNA NWNA-1 ● ● ● ●
NWNA-2 ● ● ● ●
NWNA-W ● ● ● ●
due to saw-cutting, and higher absorption rates caused by damage from cracking and deterioration. As a result of deterioration and cracking,
saw-cutting near the reinforcement. Because thermal diffusivity is the some samples lost mass surrounding the prestressing wires, as indicated
rate at which a material conducts thermal energy relative to storing that in Fig. 11 and Fig. 12. This mass loss was accompanied by concrete
energy, the difference between concrete and steel thermal diffusivity expansion as result of cracking and water freezing in the cracks. Fig. 13
rates can lead to deterioration. The difference in thermal diffusivity shows the sample expansion in the excised samples from the six ties. For
between the steel (11.72 mm2/s [0.0182 in2/s]) and concrete samples SHT2 and SHT3, visual inspection revealed cracking in the
(0.76–1.97 mm2/s [0.0012 to 0.0031 in2/s]) typically causes the steel samples, as shown in Fig. 10, that was not detected by the non-de-
to drop in temperature at much faster rates than the concrete [17], structive test methods.
causing the concrete surrounding the steel to be subjected to more se- In order to verify the effects of thermal diffusivity and saw-cutting
vere freeze-thaw cycles, thereby cooling at faster rates and resulting in through the wire, the set of samples excised from ties with non-
5
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
Fig. 11. Change in mass for the six sets of excised samples.
Fig. 12. Sample condition after freeze-thaw cycles for saw-cut samples in
freeze-thaw testing (SHT4).
Fig. 13. Change in length for the six sets of excised samples.
companion cast prisms. The cast prisms and the unreinforced samples
made by saw-cutting had a negligible effect compared to the presence
of steel in the samples. This is significant when comparing air-entrained
plain samples (NWA) to air-entrained non-prestressed samples (NPA) in
terms of length change and RDME, as shown in Fig. 14 and Fig. 15,
respectively.
Fig. 9. Average RDME results of the six sets of excised samples. Saw-cut, unreinforced, air-entrained concrete samples (NWA) did not
show deterioration over the 300 cycles of the freeze-thaw testing, ver-
prestressed wires and without wires were compared. Fig. 13 shows the ifying that saw-cutting of plain, unreinforced concrete does not make
average change in mass for the various sets of samples excised from the concrete more vulnerable to freeze-thaw damage (see Fig. 16). The non-
cast-reinforced ties and unreinforced ties, as compared to the air-entrained samples acted as a control group for the air-entrained
6
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
Fig. 14. Change in mass for the saw-cut non-prestressed, saw-cut plain, and cast
prisms samples with and without air entrainment.
Fig. 17. Half ties that developed cracking from the saw-cut (epoxied) end, a.
represents Half Tie 4 (HT4), b. represents Half Tie 3 (HT3) and c. represents
Half Tie 2 (HT2).
Fig. 15. Change in length for the saw-cut non-prestressed, saw-cut plain, and
cast prisms samples with and without air entrainment.
Fig. 18. Average RDME results for half ties as compared to excised samples
from the same ties.
Fig. 16. Average RDME results for the saw-cut non-prestressed, saw-cut plain, soaked in water until weight stabilized for 7 days), damage from saw-
and cast prisms samples with and without air entrainment. cutting wires during manufacturing, and faster freezing rates. The
summary of all initial and final freeze-thaw results is presented in
samples and as expected showed deterioration during testing. Table 4.
Only one-half tie (HT5) passed the freeze-thaw testing without
significant deterioration. In addition, deterioration for half ties HT2, 5. Verification and validation
HT3, and HT4 was determined to be caused by cracking resulting from
the saw-cutting process since propagation of the crack started from the Fig. 20 shows the relative dynamic modulus of elasticity versus the
saw-cut (epoxied) end. This deterioration due to saw-cutting is shown number of cycles of freezing and thawing for all the samples. It can be
in Fig. 17. Fig. 18 shows that excised samples for freeze-thaw testing observed that all of the samples showed little decrease in RDME with no
failed at a much faster rate compared to the ties from which they were issues except for one sample. This sample lost a large piece of concrete
excised. Meanwhile, two half ties showed excessive deterioration: the caused by a big crack after the 70th cycle but that did not show much
tie without air entrainment (HT6), which failed at 215 cycles, and HT1, loss in the relative dynamic modulus of elasticity. Fig. 21 through Fig. 23
which failed at 143 cycles. The excessive deterioration of HT6 is shown show some pictures of the cracked sample. The cause of this crack is
in Fig. 19. Deterioration for sample HT1 began at the tie end, not the believed to be due to the stresses from the steel strands since the crack
middle of the tie where saw-cutting took place. Deterioration of this tie happened at the interface between concrete and steel as shown in Fig. 22
was the result of a poor air void system (3.6% air and 0.0117 in and Fig. 23. These stresses are believed to be due to saw-cutting through
(0.2972 mm) spacing factor), high degree of saturation (samples were the steel. This likely caused micro-cracking that was not apparent until it
was opened during the freeze-thaw cycling by ice.
7
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
Table 4
Summary of all results at failure compared to initial values for each sample.
Sample Failing Initial Results Results at Failure or at 300 Cycles
Cycle
Weight, lb Fundamental Frequency UPV, ft/s (m/s) Weight, lb Length Change Fundamental Frequency UPV, ft/s (m/s) RDME (%)
(kg) (Hz) (kg) (%) (Hz)
6. Conclusions
The goal of this research was to assess the effects of sample excising,
prestress relief by sawcutting, and metal inclusions on the freeze-thaw
durability of concrete. The results obtained from the saw-cut samples
indicate that saw-cutting has a minimal effect on the freeze-thaw dur-
Fig. 20. Freeze-thaw performance of Plain vs Reinforced vs Reinforced Saw-Cut ability, while the presence of prestressed reinforcement in the saw-cut
Concrete. sections can lead to microcracking that opens up during freeze-thaw
testing. Half Tie 3 (HT3) developed cracking parallel to the
8
M.T. Albahttiti, et al. Cement and Concrete Composites 104 (2019) 103418
Acknowledgement
References
Fig. 22. Cracked saw-cut sample ends.
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