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07.12.

2020

Mise en forme par déformation plastique 1

MECA 2

Lecture 03: Materials Characterisation

2020-21

Prof. Dr.-Ing. habil. Sami Chatti

Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

2020-21 L03 – Materials Characterisation 3.1

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Summary of plasticity (1)

True strain Equivalent plastic strain


 
1
d d 2 2
d 

     ln  1 


3
1  22  32 
0  0 
True stress Stress tensor
F   xx  xy  xz    1 0 0 
  
A  ij    yx  yy  yz    0  2 0 
 
   
 zx  zy  zz   0 0  3 

The flow stress is the stress that is necessary to cause


the plastic flow of the material.

Yield criterion (v. Mises)


1
kf    1   2 2   2   3  2   3   1 2 
2
2020-21 L03 – Materials Characterisation 3.2

Summary of plasticity (2)

The flow curve specifies the flow stress as a function of the


equivalent plastic strain. In addition, the flow stress is dependent on
the temperature and the strain rate.

k f ( , , T )

The strain rate can be described by the Levy-Mises flow rule:

     
ij ij

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Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

2020-21 L03 – Materials Characterisation 3.4

Material properties in metal forming


in N/mm²

Stress-strain curve
Elastic region
Yield strength
• Young’s modulus E
Plastic region Necking

• 0.2% proof stress Rp0,2


• Poisson’s ratio ν

Plastic region Elastic region Fracture


Rm

• Flow curve kf (φ) (HOOKE´s line)


R p0,2

• Anisotropy coefficients r , r
(established in the tensile test) E E

ep ee e in %
R p0,2 Yield stress  Stress
Rm Tensile strength e Strain e  et  ee  ep = Au
E Youngs modulus et Total strain
Au Uniform elongation ee Elastic strain A
A Elongation at fracture ep Plastic strain At
At Total elongation

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Tests to determine flow curves

Bulk forming Sheet metal forming

Tensile test

Upsetting test

Torsion test

Hydraulic bulge
test

There are many more tests, which are not discussed here.

Standard test method

Special test method

2020-21 L03 – Materials Characterisation 3.6

Determination of flow curves

Required range: Sheet metal forming:0    1 ; 0    0.1 s


1

Bulk forming: 0    4 ; 0    100 s 1

Range that can be determined


(example: sheet metal forming):

Biaxial tensile test

Tensile test
Flow stress kf

Upsetting test

Shear test
Hydraulic bulge test
Torsion test
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
Equivalent plastic strain 
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Extrapolation approaches

Cold forming: k f  C n (Ludwik/Hollomon)

 K (0   )n (Swift)

...
Flow curves

 k f    k f   k f 0  e c (Voce)

Warm forming: k f  K n m K = K(T)


n = n(T)
m = m(T)

Hot forming: k f  K m


n: Hardening exponent
m: Strain rate sensitivity exponent
2020-21 L03 – Materials Characterisation 3.8

Extrapolation of flow curves

600
Material: DC04
Swift
500 Swift Voce
Flow stress kf in N/mm2

K (MPa) 𝑘 (MPa)
Voce
400 553.5 403.7

300 𝜑0 𝑘 (MPa)
0.0059 179.1
Swift:
n
k = K ( 𝜑 + 𝜑)
200 f 0
Voce: n c
- ( c 𝜑) 0.245 10.19
kf =𝑘 - (𝑘 - 𝑘 ) e
100
0 0.2 0.4 0.6 0.8 1
Equivalent plastic strain 

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Typical flow curves in cold forming

Material kf0 (MPa) C (MPa) n Material kf0 (MPa) C(MPa) n

St38* * Pöhlandt 730 0.100 42CrMo4 420 1100 0.149


** Tschätsch
St42* 850 0.230 16MnCr5* 810 0.090
St60* 890 0.150 20MnCr5* 950 0.150
C10* 800 0.240 100Cr6* 1160 0.180
Ck10*,** 260 730 0.216 Al99.5* 110 0.240
Ck15** 280 760 0.165 Al99.5** 60 150 0.222
Ck22** 320 760 0.157 Al99.8** 60 150 0.222
Ck35* 960 0.150 AlMgSi1** 130 260 0.197
Ck35** 340 950 0.178 AlMg3* 390 0.190
Ck45** 390 1000 0.167 CuZn10** 250 600 0.331
Cf53** 430 1140 0.170 CuZn30** 250 880 0.433
15Cr3* 850 0.090 CuZn37** 280 880 0.433
34Cr4** 410 970 0.118 CuZn40* 800 0.330
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Typical flow curves in hot forming

Material m K (MPa) T (oC) Material m K (MPa) T (oC)


C15** 0.154 99/84 1100/1200 CuAl5** 0.163 102 800

C35** 0.144 89/72 1100/1200 Al99.5** 0.159 24 450

C45** 0.163 90/70 1100/1200 AlMn** 0.135 36 480

C60** 0.167 85/68 1100/1200 AlCuMg1** 0.122 72 450

X10Cr13** 0.091 105/88 1100/1250 AlCuMg2** 0.131 77 450

X5CrNi189** 0.094 137/116 1100/1250 AlMgSi1** 0.108 48 450

X5CrNiTi189** 0.176 100/74 1100/1250 AlMgMn** 0.194 70 480

E-Cu** 0.127 56 800 AlMg3** 0.091 80 450

CuZn28** 0.212 51 800 AlMg5** 0.110 102 450

CuZn37** 0.201 44 750 AlZnMgCu1,5** 0.134 81 450

CuZn40Pb2** 0.218 35 650

CuZn20Al** 0.180 70 800


* Pöhlandt
CuZn28Sn** 0.162 68 800 ** Tschätsch

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Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

2020-21 L03 – Materials Characterisation 3.12

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Tensile test

Clamping device
F   Fmax

Length
measuring
system
l  e 

Specimen

kf

 

max 0.2

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Tensile specimen

Flat specimen
Necking

Fracture

Round specimen

Necking

Fracture

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FEM simulation of tensile test

Distribution of strain rate Distribution of equivalent plastic strain


Simple Tension Test Simple Tension Test
Equivalent Plastic Strain Rate Distribution Equivalent Plastic Strain Distribution

Material: Stainless Steel Gage Initial Diameter: 7.54 mm Gage Length: 48 mm Material: Stainless Steel Gage Initial Diameter: 7.54 mm Gage Length: 48 mm
Clamp Diameter: 10 mm Speed: 1 mm/s Clamp Diameter: 10 mm Speed: 1 mm/s

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Tensile test
(ELLI tele-operative testing cell)

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Tensile test: Instability (1)


Extrapolated
True stress-strain
curve

Fracture
Stress

Fracture
Necking starts at the
maximum engineering
Onset of
necking stress and maximum
Engineering stress-strain curve
load, respectively.

Homogeneous forming Necking

Strain

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Tensile test: Instability (2)

Static equilibrium:
d xx dA
F   xx  A  dF  A  d xx   xx  dA 0  (1)


    xx A
Verfestigung
Hardening Querschnittsminderung
Reduction of cross-
section area

Constant volume condition:


dA d
A0   0  A      dA  A  d   0     dxx  d (2)

A 
y A

F F x
Flow curve:

dk f n dk f n
 xx  k f  C n   nC n1  kf   d (3)
d  kf 
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Tensile test: Instability (3)

d xx dk f
(1) and (2) give:  d and accordingly:  d (4)
 xx kf

n
(4) and (3) yield: d  d

Or:  n → Onset of plastic instabilities.

Thus, the tensile test can only be evaluated up to an


equivalent plastic strain of n. This value is in the range of
0.1 < n < 0.4 for most metals.

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Evaluation until fracture

After onset of necking:


d
d 
  2  ln  0 
d
with d0 : initial diameter

F 
Siebel: kf  with A  d2
 d  4
A  1  
 8r 
F r
Bridgman: kf 
 4r   d 
A  1    ln1  
 d   4r 
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Tensile test at high temperatures (1000+ C)

YouTube
2020-21 L03 – Materials Characterisation 3.21

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MFDP interactive

Question: How does the stress-strain curve at high temperature (T2) change
qualitatively compared to the test at room temperature (T1)?
a) The stress increases 1
𝑇2
σ0 0,9
𝑇1 0,8

0,7
ε
0,6
b) The stress is reduced A
0,5
B
𝑇1
σ0 0,4 C
𝑇2
0,3

0,2
ε
0,1
c) The curve remains unchanged
0
σ0 A B C
𝑇1 = 𝑇2
ID = sami.chatti@udo.edu
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ε
2020-21 L03 – Materials Characterisation 3.22

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Example 1: Material characterisation by tensile test


F
A specimen with a diameter d0 of 8.5 mm is tested by tensile
F0
loading. The initial measurement length is taken as l0 = 50 mm.
a) The change in length of the specimen is Δl
= 0.06 mm which is subjected to a tensile
load of F = 4.85 kN at the moment when the
l
l0

sample starts to deform plastically. Determine


the elastic modulus and the yield stress.
b) The change in length of the specimen is Δl Spannung
Stress
= 2.51 mm which is subjected to a tensile  in MPa F0 F
load of F = 8.5 kN. Determine the Rm
engineering as well as true stress and strain
values at this point.
R p0,2
c) The sample fractured after a change in

length of Δl = 13.75 mm with the diameter of E= e
5.3 mm. Determine the elongation at fracture
Ag
A (%) and the reduction of area Z (%).
Stress-strain graph in uniaxial Dehnung
Strain
d) What kind of material could it be? e in %
tensile test (schematic)
2020-21 L03 – Materials Characterisation 3.23

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Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

2020-21 L03 – Materials Characterisation 3.24

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Upsetting test (1)


(also: compression test)
F

A0 Attainable true strains


A(F) kf
h0

z
h(F)

 rr 0 0  0 0 0
   
   0 zz 0     0 zz 0    0.8 – 1.0
 0 0 θθ  0 0 0
   

 zz  2 rr  2

2020-21 L03 – Materials Characterisation 3.25

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Upsetting test (2)


10 mm

Aluminium
Steel
20 mm

Specimen before Specimens after


forming forming

Problem: Forming is inhomogeneous due to friction effects


(barrel-shaped bulge of the specimen)

2020-21 L03 – Materials Characterisation 3.26

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Influence of friction

Specimen before
forming Specimens after forming

μ=0 μ = 0.1 μ = 0.5

Finite Element Simulations 0 0.38 0.75 1.13 1.5 

Friction conditions too high ideal (μ=0)


deformation inhomogeneous homogeneous
stress tensor multidimensional one-dimensional
evaluability challenging (under simplifications) relative simple

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Upsetting test according to Rastegaev (1)

Lubricant Advantages:
u0 Good lubrication due to pockets
Homogeneous forming for the most part
Higher true strains possible:  = 1.2 ... 1.5
Drawbacks:
h0

t0

Increase of measuring inaccuracy


d0 End faces do not remain flat

Recommendation: Lubricants:
Room temperature: Paraffin
Up to 300°C: Teflon
u0 = 0.05 d0 (Steel) Up to 400°C: Graphite
Not recommended = 0.03 d0 (Copper) Up to 800°C: Boron nitride
for hot forming t0 = 0.02 d0 800 – 1300°C: Glass

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Upsetting test according to Rastegaev (2)

Edge
Paraffin

Before forming After forming

Conventional Rastegaev Severely deformed

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Determination of flow curve in Rastegaev test (1)

Stress and strain increments:


F
 zz   ,  xx   yy   xy   yz   zx  0
A
dh d
dzz   , dxx  dyy   zz , dxy  dyz  dzx  0
h 2

1
         
 6  xy2   yz2   zx2    zz
2 2 2
k f   v.M .   xx   yy   zz   xx
2 
yy zz

  
d 
2  2
3     
dzz  dxx2  d yy2   2 dxy2  d yz2  dzx2    d
 zz

 0.25dzz2 0.25dzz2  

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Determination of flow curve in Rastegaev test (2)

Thus, the flow stress, the equivalent plastic strain and strain rate are:

F h  v
kf  ;   ln  0  ,   tool
A h h

The reduction of height h is measured during the test. Hence:

4 F  h   1   vtool
kf   1   ;   ln   ,  
 d02  h0   1  h h0  h0  h

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Upsetting test with friction

For the upsetting test, specimens having h < d/2, the following equations
can be approximately used to determine the flow curve:

F  h0  d
d2 /4   ln   or   2ln  
k f    h  d0 
 1 d
1      (Problem: which d ?!)
 3 h

The following must apply for a constant strain rate:

Wz  t   h0 e
vtool   t (Plastometer)

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Ring upsetting test


(also: ring compression test)

10 mm

20 mm

Initial specimen Compressed specimen

2020-21 L03 – Materials Characterisation 3.33

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MFDP interactive

Question: Which statement about the influence of friction on the ring


compression test is correct?
1

Answer options: 0,9

0,8
A) The inside diameter at high friction
0,7
is larger than at low friction
0,6
𝜇 ↑⇒𝐷 ↑
0,5

B) The inside diameter at low friction 0,4


is larger than at high friction 0,3

𝜇 ↓⇒𝐷 ↑ 0,2

0,1
C) The inner diameter is not influenced
0
by the friction A B C

𝐷 = 𝑐𝑜𝑛𝑠𝑡. ID = sami.chatti@udo.edu
0 votes
Reset Vote

2020-21 L03 – Materials Characterisation 3.34

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Simulation of ring compression test

Ring Compression
Equivalent Plastic Strain Distribution
Material: Ck15 Specimen Outer Diameter: 20 mm Specimen Inner Diameter: 10 mm
Specimen Height: 7 mm Fiction Coefficient: 0.1 & 0.5

µ = 0.1

µ = 0.5

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Example 2: Material characterisation by cylinder


compression test
Consider the shown structure of an upsetting test. Assume that there is
no friction between workpiece and tool. The material shall be characterized
until an equivalent plastic strain of 𝜑 = 0.5.
The testing machine can afford a maximum force of 𝐹 = 750 kN.
You know an approximated flow curve for a similar material from the
literature. It is described by 𝑘 = 𝐶 𝜑 with 𝐶 = 195 MPa and 𝑛 = 0.15.
Check, if the planned material characterization can be carried out on this
testing machine. Assume isotropic material behavior.

ℎ = Initial height
𝑑 = Initial diameter
ℎ = Current height
𝑑 = Current diameter
𝐹 = Upsetting force

2020-21 L03 – Materials Characterisation 3.36

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Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

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Torsion test

Stress state:
The only non-zero component
of the stress tensor
(cold forming)
r
1  T 
 z    z   3
3 T  z 
2 R    z 

Strain state:
The only non-zero component
z of the strain tensor
R 1 R
d  z  tan  d   d  d z  d z  d z  d
 2 2
R R
It is:   z   d  z     z  
 2
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Stress and strains at torsion test

Applying v. Mises flow criterion:


  
1
       
2 2
kf   xx   yy   zz   xx
2
 6  xy2   yz2   zx2   3
2   
yy zz z

  2z 


 k f  3 z

  
d 
2
3
2
 2 2
  
dxx  d yy  dzz  2  dxy2  d yz2  dzx2 

  d2z 

2 R
 d  d z consequently:   
3 3 

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Experimental setup of torsion test

High strength steel: Mild Steel:


brittle ductile

Experimental setup

Helical Planar
fracture fracture
Specimens

Chen & Ferguson Jeff Thomas, 1997

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Torsion test for sheet metal forming

Inner fixation

Wrinkles

ri
T

Thickness t ro

Outer fixation

Tekkaya & Pöhlandt

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In-plane torsion test (1)

gripped

undeformed
line of
material
ri
T material T
line ro
T formed

ri
rotating
T
ro
T ( )
Stress, differing from zero:  r (r, ) 
2 r 2t
2  T ( )
Strain, differing from zero at the inner gripping:  r (ri , ) 
 dT d 
Tekkaya & Pöhlandt

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In-plane torsion test (2)

With v. Mises yield criterion at r = ri:

  
1
       
2 2
kf   xx   yy   zz   xx
2
 6  xy2   yz2   zx2   3
2   
yy zz r

   r2 

 k f  3 r r ri

  
d 
2
3  
dxx  d yy  dzz  2  dxy2  dyz2  dzx2
2 2 2
    = 2 𝑑𝜑
 3
  dr2 

2 2  T ( )
 d  dr  r r 
3   dT d 
therefore: i
3
Tekkaya & Pöhlandt

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Flow curve in in-plane torsion test

Determination of the flow curve with optical strain measurement:

Optical strain Calculation Point cloud


Attribution
measurement of  or kf 
to kf and 
 and r (x,y) from T and r Flow curve

120

Flow stress kf in MPa


100
80
Point cloud
60
40
20
0
0 0.2 0.4 0.6
Recording GOM Argus, Al99.5; sheet thickness 1mm Equivalent strain 
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Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

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Hydraulic bulge test

Measurement head
Inductive displacement encoder
(height)
Inductive displacement encoder
(vertical)
Inductive displacement encoder
(horizontal)

Die Sheet metal segment

Ring piston
Clamping tool
Pressure transducer
( according to F. Gologranc )

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Stress and strain state in hydraulic bulge test

Pole
Sheet

Clamping
r t

Stress state in pole: Strain increment in pole:

pr 1 dt
    , d  d   dtt  
2t 2 2t
 tt  0

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Flow curve from hydraulic bulge test

 2
 
2
  
2 
kf 
1 
 xx   yy     yy   zz
2  p   
      6 2  2  2
  zz xx xy yz zx  

 r  2 t  p r  2t    pr  2t    pr  2t   

pr
thus: kf 
2t

Similar for the equivalent strain:

2
𝑑𝜑̄ = 𝑑𝜑 + 𝑑𝜑 + 𝑑𝜑 + 2 𝑑𝜑 + 𝑑𝜑 + 𝑑𝜑
3
/ /

dt t
d  dtt     ln 0
t t
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Example 3: Material characterisation by hydraulic


bulge test

The hydraulic bulge test is available to characterize a forming material (see figure).
Pole
Free surface

Sheet

Clamping
Initial sheet position
Look at the pole of the sample on the free surface. Determine the corresponding
three-dimensional stress tensor as a function of the flow stress kf. Assume that the
sample is in a state of homogeneous plastic deformation. The von Mises yield
criterion must be used.

Equivalent stress according to VON MISES:

𝜎 . . = 𝜎 −𝜎 + 𝜎 −𝜎 + 𝜎 −𝜎 + 6(𝜏 +𝜏 +𝜏 )

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Content

L03 – Materials Characterisation


Determination of flow curves
Tensile test
Upsetting test
Torsion test
Hydraulic bulge test
Hardness measurement

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Hardness

Definition:
The resistance of a material against the
penetration of another body

Hardness measurement gives information about


strength
wear resistance of a material

When hardness values are given, the hardness measurement


technique must also be mentioned, since the penetration
capability depends on the shape and the hardness of the other
body as well as on the type and the magnitude of the load.

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Hardness measurement techniques


(static test)
Brinell indentation test Vickers indentation test
F D
22°

Brinell hardness: Vickers hardness:


0.102  F 0.102  2  F  136 
HB   F  2  sin  
A

  D D  D2  d 2  HV  0.102 
F
 0.102 
 2   0.189  F
F=[N], D=[mm], d=[mm] A d2 d2
F=[N], d=[mm], A=[mm²], d d
d 1 2
Advantages of Vickers test A ≡ Surface area of indentation 2
Superior resolution compared to spherical indenters
Indenter is self-similar (hardness is ideally independent of indentation
load and indentation depth)
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Measurement of flow stress by means of


Vickers hardness

Specimen produced by forward rod extrusion (See lecture Cold Forging)

Billet Extrudate  is exactly known in


the axis of the
extrudate

16MnCr5
 = 1.60

240 mm 190 mm

(Tekkaya)

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Relation between Flow stress and Vickers hardness

HV  c  k f ,rep (at*)

where,
HV: Vickers Hardness in kg/mm2
c: Constant with value 2.475
kf,rep: Representative flow stress in kg/mm2
at strain *
FEM simulation of indentation test
*: Offset equivalent plastic strain
(* = 0.112)

(Tekkaya)

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Utilisation of hardness measurement

• Obtain an accurate flow curve of the


material up to high plastic strains Flow stress

• Measure the Vickers hardness (HV) kf,rep


at a given location of the product
kf
• Compute the representative flow
stress (in MPa) from the proposed
formula as
kf,rep (at 𝜑 *) = 9.81  HV / 2.475

• Find from the flow curve the point


with the flow stress kf,rep corres-
ponding to a plastic strain of 𝜑 * Equivalent plastic strain

• The actual flow stress kf at the


respective location is the one
corresponding to 𝜑 = 𝜑 * - 0.112 Vickers indentation test

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Example 4: Material characterisation by hardness test

You want to characterise a material at a


certain location using a machine for
Vickers indentation test. From material
supplier, you got the given flow curve of Flow stress
this material. You applied a force of 16693 600
N on the this location and you measured
an indentation of d1 = d2 = 5 mm. 500
determine the Vickers hardness (HV) of
the material and the value of the flow 400
stress at the corresponding location.
300

200
22°
100

0
0 0.05 0.1 0.15 0.2

Vickers indentation test Equivalent plastic strain

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Further procedures

• Biaxial tensile test • Compression test for sheets • Shear test

• Layer compression test

• High speed tensile test


• Inverse methods

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Appendix: French for Production Engineers

English Français English Français


Biaxial tensile Essai de traction
Hardness Dureté
test biaxiale
Bulging Gonflage Helical fracture Rupture hélicoïdale
Elongation at Allongement à la High speed Essai de traction à
fracture rupture tensile test grande vitesse
Courbe High strength Acier à haute
Flow curve
d'écrouissage steel résistance
Hydraulic bulge Essais d‘emboutissage
Formability Ductilité
test hydraulique
Fracture, Layer Essai d'écrasement en
Rupture
Rupture compression test couches
Hardening Durcissement Mild steel Acier doux
Hardening Coefficient
Necking Rétreint / Striction
exponent d'écrouissage
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Appendix: French for Production Engineers

English Français English Français


Essais de
Planar fracture Rupture plane Torsion test
torsion
Essais de torsion Allongement
Plane Torsion Test Total elongation
planaire total
Uniform Allongement
Ring upsetting test Test de l‘anneau
elongation uniforme
Essai de Essai de
Shear test Upsetting test
cisaillement compression
Vitesse de Critère de
Strain rate Yield criterion
déformation plasticité
Strain rate Coeff. de sensibilité Limite
Yield strength
sensitivity exponent à la vitesse d'élasticité
Résistance en Young’s Module
Tensile strength
traction modulus d'élasticité
Tensile test Essai de traction
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